High Temperature Grease Performance Lubrication

Technical Topic
Grease High-Temperature Performance

Don't Get Burned by High-Temperature Grease Claims
High-Temperature Claims Can Be Confusing
Grease high-temperature claims based on different standards
can vary widely. The range of approaches commonly used in the
industry to define the maximum temperature at which a grease
will provide adequate lubrication can be confusing for customers
wishing to select the best product for their application. A lubrication
decision based upon a published grease temperature range can lead
to undesired consequences unless the user understands something
about the basis for the high-temperature limit being claimed.
Dropping Point - The Old Way of Doing Things

Historically, high-temperature grease claims were based upon
the grease Dropping Point (Figure A). Primarily intended as a
manufacturing quality control test to confirm proper thickener
formation, rather than a performance indicator, the Dropping Point
indicates the temperature at which the grease thickener loses the
capacity to retain oil under test conditions. At best, this has a
tenuous relationship to real-life high-temperature performance.
It is still quite common to define the grease high-temperature limit
by subtracting a nominal temperature - often 100F (55C) - from
the grease Dropping Point.
Dropping
Point
Test
Figure A
Bearing Tests - A Modern Approach

A better way is to define high-temperature performance capability
in terms of a standardized bearing test. Such tests are conducted
under accelerated operating conditions to promote grease ageing
processes. Factors limiting grease high-temperature performance
include degradation resulting from thickener and base oil oxidation,
and the loss of base oil due to grease bleed and evaporation. In
general, these dynamic grease life determinations better represent
what occurs in the field, providing a measure of grease hightemperature performance limits which is more realistic than claims
based on Dropping Point. In addition, bearing tests can also
provide guidance to required grease re-lubrication intervals at
normal operating temperatures.
There are several bearing tests generally employed to evaluate
grease high-temperature limits. In all of these tests, bearings
mounted in five identical rigs are run in parallel. The hours to
grease failure in each rig can be treated using Weibull statistics
to determine the time at which 50 percent of the bearings are
expected to fail. This defines the "L50" life of the candidate
grease at the chosen test temperature.
The SKF R0F test employs two 6204 test ball bearings in a
continuous operating mode in each of the 5 test rigs. Grease
failure is detected by bearing temperature excursion. The R0F
test has flexibility to vary both speed and load, but a lightly
loaded set-up at 10,000 rpm is typical. The upper continuous
operating temperature limit for a grease is generally determined
by the highest temperature at which the L50 life will exceed
1000 hours.
The DIN 51821 (or FE9) test (Figure B) uses 7206B angular
contact ball bearings which may be run in one of three
standard modes. Method A, in which unshielded bearings are
packed with 2 ml of grease, is typically run at 6000 rpm with
1500 N axial load to classify a grease's high temperature limit.
Grease failure is detected by bearing torque increase, as
indicated by an increase in the power requirement of the rig
motor. Under the DIN 51825 Type K Grease Classification
system, the maximum temperature at which a grease may
be used for continuous lubrication is defined as the highest
temperature at which an L50 of 100 hours is achieved.
ExxonMobil has chosen to base continuous-operation recommendations

upon the results of such bearing tests, at the same time recognizing
that operation at temperatures exceeding this recommendation
can be tolerated for short periods with appropriate adjustments to
relubrication intervals. In assessing the potential of different greases
to satisfy the needs of an application, make sure you're comparing
"apples to apples."
200
390
180
355
160
320
140
285
120
250
Temperature, C
ASTM Method D3336, commonly known as the "Spindle

Life" or "Pope" test, typically operates five 6204 ball bearings
at 10,000 rpm under a 20 hours on / 4 hours off duty cycle.
Grease failure is detected by temperature excursion or
excessive bearing torque.
approaching 400F (200C) on a Dropping Point basis. By sharp

contrast, the limiting temperature for continuous operation arrived
at through DIN 51821 (FE9) bearing tests would be given as 275F
(135C) for Mobilgrease XHP 222, 300F (150C) for Mobilith SHC
220, and 340F (170C) for Mobil Polyrex EM (Figure C). The
difference in temperature limits predicted from dropping point and
bearing test criteria are thus highly significant, translating into as
much as a ten-fold change in expected grease life.
Temperature, F
Industrial High-Temperature Grease Tests
Based on
Dropping
Point
Based on
FE9
Bearing
Test
100
215
Mobilgrease
XHP 222
Mobilith SHC Mobil Polyrex

220
EM
Bearing tests provide more realistic operating temperature

guidelines than can be derived from Dropping Point
Figure C
DIN 51821 (FAG FE9) Bearing Test
Figure B
Assessing Grease Performance

Understanding how the temperature capability of a grease has been
defined can allow a user to make a better informed lubrication
decision. For example, the high-temperature limit of Mobilgrease
XHP 222 based upon a Dropping Point criterion might conservatively
be given as 350F (177C). Mobilith SHC 220, with a similar dropping
point, would typically be accorded a higher upper temperature limit
by virtue of the improved performance of the synthetic base oil.
Mobil Polyrex EM would also be accorded a high-temperature limit
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2007 Exxon Mobil Corporation
The Mobil logotype and the Pegasus design are registered trademarks of Exxon Mobil Corporation.
GR0770TT
Don't Forget the Fundamentals

Finally, always remember that the base oil component of the
grease is primarily responsible for lubrication. The correct base oil
viscosity ensures that an oil film of adequate elastohydrodynamic
(EHL) thickness is formed. The end-user should remember that
viscosity may well be the limiting factor for a given grease at the
equipment operating temperature.
Choosing a grease with the right high-temperature limit, defined by
bearing test results, and the right base oil, is the key to successful
lubrication in challenging high-temperature environments.

High Temperature Grease Performance Lubrication

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Technical Topic

Grease High-Temperature Performance

Dropping Point - The Old Way of Doing Things

Bearing Tests - A Modern Approach

ExxonMobil has chosen to base continuous-operation recommendations

ASTM Method D3336, commonly known as the "Spindle

approaching 400F (200C) on a Dropping Point basis. By sharp

Industrial High-Temperature Grease Tests

Mobilith SHC Mobil Polyrex

Bearing tests provide more realistic operating temperature

Assessing Grease Performance

Don't Forget the Fundamentals

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