This document provides specifications for external coatings to protect steel pipes and components from corrosion. It replaces multiple previous specifications and defines requirements for coating material storage, surface preparation, application, handling, quality management, and documentation. The document includes a general section and 9 appendices that specify requirements for different coating systems and application methods.
This document provides specifications for external coatings to protect steel pipes and components from corrosion. It replaces multiple previous specifications and defines requirements for coating material storage, surface preparation, application, handling, quality management, and documentation. The document includes a general section and 9 appendices that specify requirements for different coating systems and application methods.
This document provides specifications for external coatings to protect steel pipes and components from corrosion. It replaces multiple previous specifications and defines requirements for coating material storage, surface preparation, application, handling, quality management, and documentation. The document includes a general section and 9 appendices that specify requirements for different coating systems and application methods.
This document provides specifications for external coatings to protect steel pipes and components from corrosion. It replaces multiple previous specifications and defines requirements for coating material storage, surface preparation, application, handling, quality management, and documentation. The document includes a general section and 9 appendices that specify requirements for different coating systems and application methods.
EXTERNAL COATINGS FOR CORROSION PROTECTION OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 2 of 20
FOREWORD Rev 0 Issue Pages 20 Appendix A Pages 9 Appendix B Pages 10 Appendix C Pages 14 Appendix D Pages 14 Appendix E Pages 9 Appendix F Pages 10 Appendix G Pages 11 Appendix H Pages 11 Appendix I Pages 12 February 2004 This specification replaces the following Company Functional Specifications:
20001.PIP.PAI.FUN. Rev.0 Spray coating of steel pipes external surface with epoxy or polyurethane paint. 20002.PLI.PAI.FUN. Rev.0 External Polyethylene or Polypropylene Coating, Plant Applied on Steel Pipe. 20003.PLI.PAI.FUN. Rev.0 External Coating with Plastic Tape for Buried Steel Pipe. 20005.PIP.PAI.FUN. Rev.0 External Coal Tar Coating Factory Applied on Steel Pipe. 20006.PLI.PAI.FUN. Rev.0 Repair of Damages Found in The Field n Pipe External Coatings. 20007.SLI.COR.FUN. Rev.0 External Bitumen Coating, Factory Applied on Steel Pipe. 20009.SLI.COR.FUN. Rev.0 External Coating with Epoxy Mastic for Application on Steel Pipes. 20012.PLI.PAI.FUN. Rev.0 Supply and Installation of Plastic Tapes. 20013.PIP.PAI.FUN. Rev.0 Supply and Installation of Heat Shrinkable Sleeves. 20014.SLI.NAV.FUN Rev.0 Coated with anticorrosion filler mass of welded joints areas in concrete weighthed pipelines. 20015.COR.FUN. Rev.0 External coating with epoxy powders factory applied on steel pipes. 20017.SLI.NAV.FUN Rev.0 Insulation of bonded pipe straight lengths by polyurethane foam injection. 20018.PLI.COR.FUN Rev.1 Pipe Assembly of Steel Service Pipes, Polyurethane Thermal Insulation and Outer Casing of High Density Polyethylene. 20022.SLI.COR.FUN. Rev.0 External Tar Polyurethane Coating Factory Applied on Steel Pipes. 20023.VAR.PAI.FUN. Rev.0 Assembly of Fittings and Valves for Steel Service Pipes, Polyurethane Thermal Insulation and Outer Casing of Polyethylene. 20476.VAR.PAI.FUN Rev.0 Application of Protective Coating on Pipe Welded Joints.
0 ISSUE CORM M. CORNAGO CORM M. CORNAGO CORM D. CONDANNI 02.2004 REV. DESCRIPTION PREPARED VERIFIED APPROVED DATE Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 3 of 20
CONTENTS 1 GENERAL........................................................................................................................... 4 1.1 INTRODUCTION................................................................................................................. 4 1.2 SCOPE................................................................................................................................ 4 1.3 REFERENCE STANDARDS............................................................................................... 4 1.3.1 European standard ............................................................................................................. 6 1.3.2 ISO and National Organisations ......................................................................................... 6 1.3.3 Standards of other Organisations ....................................................................................... 7 1.3.4 Laws and decrees............................................................................................................... 8 1.4 DEFINITIONS ..................................................................................................................... 9 1.5 SYMBOLS AND ABBREVIATIONS.................................................................................... 9 1.6 OPERATING ENVIRONMENT......................................................................................... 10 2 FUNCTIONAL REQUIREMENTS..................................................................................... 10 2.1 STORAGE AND HANDLING OF BARE PIPES AND RELATED COMPONENTS .......... 10 2.1.1 Storage areas.................................................................................................................... 10 2.1.2 Handling............................................................................................................................ 10 2.2 COATING MATERIAL STORAGE AND PRESERVATION.............................................. 10 2.3 CRITERIA FOR COATING SYSTEM SELECTION.......................................................... 11 2.4 QUALIFICATION OF THE COATING............................................................................... 11 2.5 SURFACE PREPARATION.............................................................................................. 12 2.5.1 Abrasive materials ............................................................................................................ 14 2.5.2 Steel imperfections ........................................................................................................... 14 2.6 COATING MATERIAL APPLICATION.............................................................................. 14 2.7 ENVIRONMENTAL CONDITIONS ................................................................................... 14 2.8 CUT BACK........................................................................................................................ 15 2.9 MARKING......................................................................................................................... 15 2.10 HANDLING, STORAGE AND DELIVERY OF THE COATED PIPES AND RELATED COMPONENTS ................................................................................................................ 15 2.10.1 Handling............................................................................................................................ 15 2.10.2 Storage.............................................................................................................................. 15 2.10.3 Delivery ............................................................................................................................. 16 3 SAFETY AND ENVIRONMENTAL PROTECTION.......................................................... 16 3.1 GENERAL SAFETY REQUIREMENTS............................................................................ 16 3.2 SPECIFIC SAFETY REQUIREMENTS ............................................................................ 17 4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE ...... 17 4.1 GENERAL......................................................................................................................... 17 4.2 PRE-JOB MEETING......................................................................................................... 17 4.3 RECEPTION OF BARE PIPES......................................................................................... 17 4.4 RECEPTION OF COATING MATERIALS........................................................................ 17 4.5 INSPECTION AND QUALITY CONTROL FUNCTION..................................................... 18 4.5.1 Contractor ......................................................................................................................... 18 4.5.2 Coating Manufacturer ....................................................................................................... 18 4.5.3 Independent Inspection..................................................................................................... 18 4.5.4 Certification of personnel .................................................................................................. 18 4.6 IDENTIFICATION MARKINGS......................................................................................... 18 4.7 INSPECTION OF PRODUCTION PROCESS.................................................................. 19 4.8 PRELIMINARY TESTS..................................................................................................... 19 4.9 TESTS DURING THE WORK PROGRESS..................................................................... 19 4.10 FINAL INSPECTION......................................................................................................... 19 5 DOCUMENTATION AND REPORTING........................................................................... 19 5.1 DOCUMENTS TO PRODUCE AT THE BEGINNING OF WORK.................................... 19 5.2 DOCUMENTS TO PRODUCE DURING WORK PROGRESS......................................... 19 5.3 DOCUMENTS TO PRODUCE AT THE COMPLETION OF WORK................................. 20 Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 4 of 20
1 GENERAL 1.1 INTRODUCTION This Specification is formed by a general part in which the requirements, common to all coatings and systems, are described and by 9 Appendixes, identified with letter A to I. In each Appendix the requirements for a specific coating or coating system, and for a specific method of application, are described. 1.2 SCOPE This Specification defines the minimum functional requirements related to coating works, including supply, characterisation, inspection and testing of protective coatings intended to be applied on the exterior surfaces of steel pipes, including sealines, pipelines, and buried pipes, etc. and related components and fittings as band, valves, etc. According to the requirements of this specification, a Project Technical Specification shall be prepared, which must include consideration of the following factors: The intended service of the pipes (sealine, buried, temperature, etc.); The specific needs of the project; The coating system selected; The application method. Based on the requirements of Project Technical Specification, the Contractor shall prepare a Working Procedure in which methods concerning each work and activity (e.g. abrasive blasting, coating application, cleaning, coating systems selected, inspections, etc.) must be described in detail. Since the performance of the coating can be significantly affected by the quality of work execution (e.g. surface preparation, application of various coats, procedures and inspections) the requirements that must be implemented during intermediate steps of coating operations, should also be described. Before coming into force, the Working Procedure shall be approved by the Company. As a general rule, recommendations and instruction listed in Product Data Sheets published by Coating Manufacturers shall be followed. Possible conflicts and/or discrepancies between Products Data Sheets and this specification shall be submitted to the Company for resolution, and approval for all changes shall be obtained. In Figure 1 the general scheme for the development of the coating project is reported for information only. 1.3 REFERENCE STANDARDS This Specification refers to the most recent issue of the standards listed below, which become an integral part of the specification and all related contractual documents. In the Appendixes of this Specification, reference standards applicable to the specific coating system, application method and testing are listed. It is the Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and make standard available during each inspection step.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 5 of 20
Figure 1 - Scheme for the devolpment of the coating project PROJECT Evaluation of the requirements Operative Service Temperature Environment Coating system selection Project Technical Specification Contractor Working Procedure Company approval PQT QCP Construction Functional Specification 20550 PIP.COR.FUN. Rev.0 Yes No List of Company's qualified systems
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 6 of 20
1.3.1 European standard EN 253 District heating pipes Preinsulated bonded pipe systems for directly buried hot water networks- Pipe assembly of steel service pipe, polyurethane thermal insulation and outer casing of polyethylene. EN 448 District heating pipes Preinsulated bonded pipe systems for directly buried hot water networks- Fitting assemblies of steel service pipe, polyurethane thermal insulation and outer casing of polyethylene. EN 10288 Steel tubes and fittings for onshore and offshore pipelines External two layer extruded polyethylene based coatings. EN 10289 Steel tubes and fittings for onshore and offshore pipelines External liquid applied epoxy and epoxy-modified coatings. EN 10290 Steel tubes and fittings for onshore and offshore pipelines External liquid applied polyurethane and polyurethane-modified coatings. EN 12068 External organic coating for the corrosion protection of buried or immersed steel pipelines used in conjunction with cathodic protection: Tapes and shrinkable materials. 1.3.2 ISO and National Organisations ISO 62 Plastics Determination of water absorption. ISO 527-2 Plastics Determination of tensile properties Part 2: Test conditions for moulding and extrusion plastics. ISO 868 Plastics and Ebonite Determination of indentation by means of durometer (Shore hardness). ISO 1133 Plastics Determination of the melt mass-flow rate (MFR) and the melt volume-flow rate (MVR) of thermoplastic. ISO 1183 Plastics, Methods for determining the density and relative density of non cellular plastics. ISO 1512 Paints and varnishes Sampling of products in liquid or paste forms. ISO 1513 Paints and varnishes Examination and preparation of samples for testing. ISO 1514 Paints and varnishes Standard panels for testing. ISO 1515 Paints and Varnishes Determination of volatile and non volatile matter. ISO 1516 Paints and varnishes Closed cup equilibrium method. ISO 1517 Paints and Varnishes Surface drying test Ballotini method. ISO 1519 Paints and varnishes Bend test (cylindrical mandrel). ISO 1521 Paints and Varnishes Determination of resistance to water Water immersion method. ISO 1524 Paints and varnishes Determination of fineness of grind. ISO 2409 Paints and varnishes Cross-cut test. ISO 2431 Paints and varnishes Determination of flow time by use of flow cups. ISO 2555 Resins in the liquid state or as emulsions or dispersions. Determination of Brookfield RV viscosity. ISO 2811 Paints and varnishes Determination of density. ISO 2815 Paint and Varnishes Buchholz indentation test.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 7 of 20
ISO 3001 Plastics and Ebonite Epoxide compounds Determination of epoxide equivalent. ISO 3231 Paints and varnishes Determination of resistance to humid atmospheres containing sulphur dioxide. ISO 3233 Paints and varnishes Determination of volume of dry coating (non-volatile matter) obtained from a given volume of liquid coating. ISO 3251 Paints and varnishes Determination of non-volatile matter of paints, varnishes and binders for paints and varnishes. ISO 4287 Geometrical Product Specification (GPS) Surface texture: Profile method Terms, definitions and surface texture parameters. ISO 4624 Paints and varnishes Pull-off test. ISO 6270 Paints and varnishes Determination of resistance to humidity. ISO 4892-2 Plastics, Methods of exposure to laboratory light sources Part 2: Xenon-arc sources. ISO 7523 Paints and varnishes Determination of resistance to neutral salt spray. ISO 8501 Parts 1 3 Preparation of steel substrates before application of paints and related products. - Visual assessment of surface cleanliness. ISO 8503 Parts 1 4 Paints and varnishes Preparation of steel substrates before application of paints and related products. Surface roughness characteristics of blast- cleaned steel substrates. ISO 8504 Parts 1 3 Paints and varnishes Preparation of steel substrates before application of paints and related products. Surface preparation methods. ISO 8502 Parts 1 10 Preparation of steel substrates before application of paints and related products. - Test for the assessment of surface cleanliness. ISO 9227 Corrosion tests in artificial atmospheres Salt Spray tests. ISO 11124 Part 1 4 Paints and varnishes Preparation of steel substrates before application of paints and related products. Specifications for metallic blast-cleaning abrasives. ISO 11125 Parts 1 7 Paints and varnishes Preparation of steel substrates before application of paints and related products. Test methods for metallic blast-cleaning abrasives. ISO 11126 Parts 1 8 Paints and varnishes Preparation of steel substrates before application of paints and related products. Specifications for non-metallic blast-cleaning abrasives. ISO 11127 Parts 1 7 Paints and varnishes Preparation of steel substrates before application of paints and related products. Test methods for non-metallic blast-cleaning abrasives. ISO 11420 Methods for the assessment of the degree of carbon black dispersion in polyolefin pipes, fittings and compounds. ISO 12944 Parts 1 8 Paint and varnishes. Corrosion protection of steel structures by protective paint systems. 1.3.3 Standards of other Organisations ASTM D 570 Standard test method for water absorption of plastics. ASTM D 638 Standard test method for tensile properties of plastics. ASTM 746 Standard test method for brittleness temperature of plastics and elastomers by impact. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 8 of 20
ASTM A 780 Specification for repair of damaged hot-dip galvanized coatings. ASTM D 823 Method of producing films of uniform thickness of paint, varnish, lacquer and related products on test panels. ASTM D 1000 Method of testing pressure sensitive adhesive coated tapes used for electrical insulation. ASTM D 1141 Specification for substitute ocean water. ASTM D 1200 Test method for viscosity of paints, varnishes and lacquers by Ford viscosity cup. ASTM D 1525 Standard Test Method for Vicat Softening Temperature of Plastics. ASTM D 1640 Drying, Curing or film formation of organic coatings at room temperature. ASTM D 2240 Standard Test Method for Rubber Property - Durometer Hardness. ASTM D 2369 Test method for volatile content of coatings. ASTM D 2371 Test method for pigment content of solvent-reducible paints. ASTM D 3359 Method for measuring adhesion by tape test. ASTM 3418 Standard test method for transition temperatures of polymers by differential scanning calorimetry. ASTM D 4060 Standard test method for abrasion resistance of organic coatings by the Taber abraser. ASTM D 4285 Test method for indicating oil or water in compressor air. ASTM D 4541 Test method for pull-off strength of coatings using portable adhesion testers. ASTM D 4940 Test method for conductimetric analysis of water-soluble ionic contamination of blasting abrasives. ASTM G 8 Test method for cathodic disbonding of pipeline coatings. ASTM G 53 Recommended practice for operating light and water exposure apparatus (fluorescent UV-condensation type) for exposure of non-metallic materials. NACE RP0188 Discontinuity (holiday) testing of protective coatings. NACE RP0287 Field measurement of surface profile of abrasive blast cleaned steel surfaces using replica tape. NACE RP0394 Application, performance, and quality control of plant-applied, fusion- bonded epoxy external pipe coating. NACE RP0490 Holiday detection of fusion-bonded epoxy external pipeline coatings of (0,25 mm to 0,76 mm). SSPC-PA 2 Measurement of dry coating thickness with magnetic gauges. SSPC-SP 1 Solvent cleaning. 1.3.4 Laws and decrees Italian Health Minister (Ministero della Sanit) Decree No. 50 dated 16th February 1993. Italian Internal Minister (Ministero degli Interni) Circular No. 2838/4112 dated 20th May 1996. Any other local law, decree and regulation where the coating work is performed. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 9 of 20
1.4 DEFINITIONS Coating Manufacturer: The manufacturer or supplier of the coating material intended to be applied on the pipes or components. Coating material: The liquid, liquefiable, mastic, powder or any other composition and material intended to be applied on the pipes or components. Coating system: The complete number and type of coats applied to a substrate in a predetermined order. Coating: The liquid, liquefiable, mastic, powder or any other composition and material that after application to a substrate, is converted into a solid protective adherent film. Cut-back: The pipe surface (dimension) to be left bare (uncoated) at both ends of each pipe. Dry-spray: Phenomenon that may occur during paint application by spray. Dry particles (dusting) of atomised paint fall over areas already coated or to be coated, but not yet dried, making surface rough and matt. If overcoated can cause possible adhesion problem. Material Safety Data Sheet: Document published by Coating Manufacturer. Product Data Sheet: Document published by Coating Manufacturer describing product characteristics, use, application and storage instructions. Stripecoat: Additional coat of paint applied usually by brush on difficult-to- reach areas and on weld seams, edges, bolts, nuts, etc, to provide specified film thickness. Substrate: Solid surface intended to be coated or lined with the specified coating system. Thermo-Hygrometric Condition: Environmental conditions detected during coating work. 1.5 SYMBOLS AND ABBREVIATIONS DFT (Dry Film Thickness) Dry thickness of a coating present on surface after the complete drying of the product. WFT (Wet Film Thickness) Wet thickness of the coating present on surface at the time of its application. N.A. Not Applicable. ISO International Organization for Standardization. ASTM American Society for Testing and Materials. SSPC The Society for Protective Coatings. NACE NACE International, formerly the National Association of Corrosion Engineers. DIN Deutsches Institute fur Normung. EN European Norms. UNI Ente Nazionale Italiano di Unificazione. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 10 of 20
1.6 OPERATING ENVIRONMENT Pipes, components and fittings coated according to the requirements of this Specification and Appendixes, during the service may be located in various geographic locations and in a variety of environmental and service conditions. In each Appendix, suitable operating environments and service conditions for the specific coating or coating system and for the specific method of application are described in detail. 2 FUNCTIONAL REQUIREMENTS 2.1 STORAGE AND HANDLING OF BARE PIPES AND RELATED COMPONENTS 2.1.1 Storage areas Area(s) intended for the storage of pipes, components and fittings shall meet the following requirements: a) They shall be at least 30 m away from any type of electric power cable. The distance shall be measured along the ground from the vertical projection to the ground of the nearest cable; b) Shall be free from any kind of vegetation (e.g. grass, weed, shrubs, etc). A surrounding area of sufficient width to prevent fire spreading to the pipe stacks shall also be free of vegetation; c) Shall be free of prominent stones and other foreign matter that may damage the pipe or components; d) Shall be levelled, in order to allow uniform loading of the supports and ensure stack stability; e) Shall have sufficient load bearing capacity to prevent pipe sinking into contact with the ground; f) Shall never be directly exposed to salt water spray. 2.1.2 Handling All stacking operations shall be performed using suitable lifting equipment (such as cranes, overhead or other lift trucks) with adequate slings and hooks. Hooks for lifting pipes from their ends shall be equipped with a rubber or copper sheathing in order to avoid damages to pipe and end bevels. Suspended pipes shall be provided with appropriate side guide ropes to the lifting equipment, to prevent the traverse of the pipes. During handling operation the pipes shall not knock or bump against other obstacles or pipes. The positioning of the pipes on those already stacked shall be performed with greatest care. Slings and hooks shall also neither strike nor scrape the pipes. Suitable flat wooden supports shall be positioned on the ground. The first and last wooden supports shall be positioned at least at 0,5 m from the pipe end. 2.2 COATING MATERIAL STORAGE AND PRESERVATION All coating materials must be properly stored in the Contractors facility. The following minimum requirements must be satisfied: a) The store shall be appropriately ventilated and comply with provisions law in force concerning safety and fire prevention; b) Coating materials (liquid, solid or packaged) shall be kept in their original sealed and labelled containers or package; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 11 of 20
c) Coating materials shall be protected from direct sun, frost and rain, stored in a thermally controlled store with constant temperature in the range of +15 to +25C; d) The coating materials store shall be located at a proper distance from any significant heat source and from any area where free flames, welding works, and tools causing sparks are used; e) Containers and packages shall not be placed nor stored on wet or damp surfaces, nor in areas where flood can occur; f) All products that become altered for any reason or show the container and/or package partially or totally destroyed and/or damaged shall be removed from the store, not used for the coating work and properly disposed of; g) Coating materials shall be stored and used in a manner that assures that products are used within their storage limits (shelf-life), and those stored first are the first used. 2.3 CRITERIA FOR COATING SYSTEM SELECTION Performance criteria for specific coating systems are defined in the appropriate Appendix. To select the most suitable system for a project the following basic criteria have to be considered: a) Project needs and requirements; b) Environmental service exposure (seawater, soil, other); c) Service temperature. 2.4 QUALIFICATION OF THE COATING Only coating materials qualified and approved by the Company shall be selected and applied. The coating materials shall be purchased directly from a Coating Manufacturer qualified by the Company. Qualification requirements shall apply to all coating materials and systems described in the Appendixes of this Specification, as well as to the repair products. In each Appendix the requirements for the qualification of the specific coating material and system are described. As a general rules, two test levels are requested, divided as follows: a) Tests for the characterisation of the coating material; b) Tests for the characterisation of the coating system to verify its suitability and performance in the intended environment and service. All tests and analysis required by this Specification and by related Appendixes shall be performed and suitably reported by independent laboratories qualified and approved by the Company. The qualification of a coating material or coating system is not binding for the Company, which shall select, at its sole discretion, coatings that are added to the qualified coatings list. The Companys qualification is given for an open-ended term. However the Company reserve the right to require at any time the repetition of one or more of the qualification tests in order to verify the quality of the coating or as consequence of possible coating failure. If the result of one or more tests is negative, the qualification will be cancelled. Any modification to the formulation or components of a coating material or system, even if considered minor, made by the producer after the qualification, shall be notified in writing to the Company. The Company reserves the right to require the performance of part or all of the test procedure, or to accept or reject the modified product, without further tests. The modified coating material or system - when qualified - may be used in place of the previous one or as an alternative. The Contractor is obliged to select the specific coating material(s) from the list of products qualified by the Company for the specific use. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 12 of 20
Under no circumstance the Company approval of a coating system shall be considered a guarantee from the Company related to the coating materials and repair products and they performance, but just an approval to use it. The process steps for the pre-qualification and qualification of coating materials and coating systems are shown in Figure 2, which is provided for information and clarification only. 2.5 SURFACE PREPARATION Surface preparation method shall be selected in accordance with standard ISO 8504-1 and in conformance with the recommendations of standard ISO 12944-4. As general rule, all surfaces to be coated shall be cleaned to the specified preparation grade to obtain a surface that meets the requirements defined the appropriate Appendix. Before any surface preparation (abrasive blasting, power tooling, etc.) oil, grease and other visible contaminants, shall be removed with suitable detergents according to SSPC-SP1 standard. Petroleum, kerosene, naphtha or other greasy solvent shall not be used. At completion of surface preparation, and in any case before application of coating materials, the amount of water-soluble salts (chlorides) on surfaces shall not be more than 5 g/cm (micrograms per square centimetre). Extraction of contaminants from surface shall be done according to standard ISO 8502-6. Quantitative determination of water-soluble salts shall be performed according to standard ISO 8502-9. No surface preparation shall be performed on surfaces that are moist or may become moist before application of the coating. Blast cleaned surfaces may not be washed with acids, detergents or solvent solutions, nor treated with rust inhibitors, unless otherwise specified. Surface preparation, shall be always carried out by abrasive blasting according to the recommendation of standard ISO 8504-2. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 13 of 20
Figure 2 Schematic process for the pre-qualification and qualification of coating materials and coating system
Document for pre - qualification of each coating material and system
ENI Data evaluation
Comments
(Positive or Negative )
Data, information and sample for testing
Independent Laboratory Steel samples preparation
Lab test execution
Report of the tests
Data evaluation
Comments
(Positive or Negative)
Coating materials and coating systems qualified
Positive
Coating Manufacturer Negative Inspection
Testing schedule ENI Positive Negative
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Preparation grade will conform to the specified requirements of specific coating materials listed in the Appendixes and in any case according to standard ISO 8501-1. Profile of abrasive blasted surface shall conform to the specified requirement listed in the Appendix for the specific coating system and measured according to standard ISO 8503 or to NACE RP 0287. 2.5.1 Abrasive materials All abrasive material used for blasting shall be dry and clean and shall be tested for soluble salts content. Conductivity measured according to standard ASTM D-4940, shall not exceed 150 S/cm (microSiemens per centimetres) and chloride content, shall be less than 25 ppm. Non-metallic abrasives shall meet the requirements of standard ISO 11126 Parts 18. Tests and controls shall be done according to standard ISO 11127 Part 17. Metallic abrasives shall meet the requirements of standard ISO 11124 Parts 14. Tests and controls shall be done according to standard ISO 11125 Part 17. Abrasive type and size shall be selected in order to assure the required profile and roughness of substrate. In no circumstance will use of silica abrasive be allowed. 2.5.2 Steel imperfections All surface imperfections of substrate detected before or during surface preparation shall be removed with suitable power tools according to the requirement of standard ISO 8501-3 as follows: Grade P3 for all pipes, components and fitting projected for immersion service (permanent or intermittent) or buried; Grade P2 for all pipes, components and fitting that will be used in marine and industrial environments. Welding shots, drops and spatters, pores in welding seams, lamination defects, edges, flame cuts, fragments and dents or any other foreign material not removed during construction are considered to be imperfections, and shall be removed. Spot and discontinuous welds are not permitted on these surfaces. 2.6 COATING MATERIAL APPLICATION In general before the application of any coating material, all surfaces shall be dry and free of rust, grease, oil, dust and dirtiness, soluble salts and any other foreign material. Coating materials must be applied to the blast cleaned pipes before any oxidation appears. Surfaces that show visible oxidation or deterioration shall be re-prepared. In particular all coating materials application shall be performed according to Coating Manufacturers recommendations reported in the product data sheet of each material and according to the specified requirements listed in the appropriate Appendix. Any conflict between product data sheets and Company requirements listed in the Appendixes shall be submitted to the Company for approval. 2.7 ENVIRONMENTAL CONDITIONS Surface preparation shall not be carried out when the steel temperature is less than 3C above dew point or when the relative humidity of the air is greater than 85%. No coatings shall be applied when the steel temperature is less than 3C above dew point, when the relative humidity of the air is greater than 85%, or when the air temperature is less than 10C, excluding those products which are suitable for application at low temperature. Environmental conditions shall be measured according to standard ISO 8502-4. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 15 of 20
In outdoor application, no coating materials shall be applied when there is a likelihood of a detrimental weather change within two hours after application. The contractor shall supply all necessary weather protection and any other equipment to ensure that the coating works are carried out according to this specification and agreed production programme. Where preheating is required the specific requirements defined in the appropriate Appendix must be carefully followed. 2.8 CUT BACK Cut back dimension are specific to each coating. The requirements related to the cut back are detailed in the relevant Appendix. As general rule, before coating application the Contractor shall properly protect the end areas and the pipe bevel that must remain perfectly clean and free from any traces of coating. Once the coating operations are completed these bare ends shall be temporarily protected from corrosion, using only products that are easily removable by brushing. If not specified in the order or other contractual documents, the Company shall approve the materials used for temporary protection. 2.9 MARKING All pipes shall be identified with specific and unique markings. The Contractor shall restore any original markings that may have been removed by the coating process, according to Company instructions. Markings shall be applied using indelible paint. 2.10 HANDLING, STORAGE AND DELIVERY OF THE COATED PIPES AND RELATED COMPONENTS 2.10.1 Handling Handling shall be carried out using suitable equipment, provided with the proper protective sheathing, in order to avoid damages to the pipes and/or to the coating. Use of steel ropes or slings or any equipment, which could damage the coating and the ends, shall be prohibited. All personnel involved in the handling operations shall be of proven experience and adequately trained. Handling operations and equipment shall strictly comply with the applicable safety rules and laws. At completion of coating work the minimum time before handling, storage and loading of coated pipes shall be fully in accordance with the instructions reported in Product Data Sheet published by the Coating Manufacturer, to the specific requirements mentioned in the relevant Appendix and any particular instruction provided by the Company. 2.10.2 Storage Area(s) intended for the storage of the pipes and components shall meet the following requirements: a) They shall be at least 30 m away from any type of electric power cable. The distance shall be measured along the ground from the vertical projection to the ground of the nearest cable; b) Shall be free from any kind of vegetation (e.g. grass, weed, shrubs, etc). A surrounding area of sufficient width to prevent fire spreading to the pipe stacks shall also be free of vegetation; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 16 of 20
c) Shall be free of prominent stones and other foreign matter that may damage the coatings; d) Shall be levelled, in order to allow uniform loading of the supports and ensure stack stability; e) Shall have sufficient load bearing capacity to prevent pipe sinking into contact with the ground; f) Shall never be directly exposed to salt water spray. Stacks of coated pipes and components intended to be stored for a long period shall be protected from the action of ultraviolet radiation and direct heat. Stacks shall have a maximum height of 3 m, excluded the dimensions of bottom and intermediate supports. In consideration of the type of the ground (cement slab, compressed rock, soil, etc) the support shall provide sufficient distance from the ground and shall be sufficient in size and number to avoid permanent deformation and to provide proper load distribution. As a general rule, the maximum allowable number of rows is as follows: For pipes of diameter up to 12" (323 mm): No. 6; For pipes with diameter between 14" (355 mm.) and 20" (508 mm.): No. 4; For pipes with diameter between 22" (558 mm.) and 28" (711 mm.): No. 3; For pipes with diameter between 30" (762 mm.) and 36" (915 mm.): No. 2; For pipes with diameter over 36" (915 mm.): No. 1. 2.10.3 Delivery Coated pipes and components shall be visually inspected before delivery, and any damage shall be repaired according to the requirements reported in the Appendix for the specific coating. Handling of coated pipes for loading shall be done fully in accordance with the requirement of previous item 2.9.1. Loading of pipes and components in the factory or in the field shall be done with particular care to avoid damages to the pipes, components and to the coating during transportation. Pipes having a diameter under 80 mm (3 in) shall be shipped in bundles strapped in at least 4 or 5 points using strong, possibly non metallic, straps at least 25 mm wide. Careful visual inspections shall be performed after transportation, and all pipes and components showing damages and/or surface defects shall be properly repaired according to the requirements of the Appendix for the specific coating. Coating flattened due to stacking on wooden bearing pieces shall retain at least 67% of their former thickness, or repairs shall be made. 3 SAFETY AND ENVIRONMENTAL PROTECTION 3.1 GENERAL SAFETY REQUIREMENTS The Company, in consideration of its policy for Safety and Environmental protection, forbids the use of any coating material containing tar and any abrasive material considered hazardous to health for the operators. The Contractor shall observe the rules, laws and regulations on health, safety and environmental protection applicable to his premises, or in the country where the works are performed. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 17 of 20
All coating materials, solvents, curing agents, etc. shall report on their containers, data required by local laws and rules, and shall be accompanied by the related Material Safety Data Sheets. 3.2 SPECIFIC SAFETY REQUIREMENTS Safety requirements must be carefully observed during handling and application of each coating according to Material Safety Data Sheets and Product Data Sheets published by Coating Manufacturers. Special attention is to be given to the following items: Mixing and handling of coating material shall be performed in areas that are not judged to be dangerous and where air can circulate freely; Blast cleaning abrasives shall not be harmful to operators' health; Storage of coating material shall be done as reported in item 2.2 of this Specification; Disposal of residual materials (spent abrasives, coating materials, solvent, etc.) shall be performed fully in accordance with rules, regulations and laws in force in the country where the coating work is performed. 4 REQUIREMENTS FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 4.1 GENERAL Contractor must comply with all Requirements for Quality Management and/or Quality Assurance that are defined in the applicable Quality and Execution Requirements Specification attached to the invitation to bid. Before starting any coating work the Contractor shall submit for approval to the Company the procedures relevant to the qualification tests and to the proposed methods of execution of the works, applicable for the specific coating process. 4.2 PRE-JOB MEETING Before the beginning of the works a pre-job meeting shall be held with attendance of the representatives of all involved parties (Company, Contractor, Coating Manufacturer, Subcontractors and Third-Party Inspector) The purpose of the meeting is to clarify and agree the production procedures, qualification tests, checks and inspections program, report forms and any other necessary requirements to achieve the correct job execution. 4.3 RECEPTION OF BARE PIPES Upon receiving the pipes to be coated, the Contractor shall first verify that the pipes are not damaged and are free of any visible defect. Damages and defects, including but not limited to, dents, cuts or scratches on the bevel, shall be immediately recorded on the shipping documents, reporting the serial number of the pipe(s) concerned. Damaged or non-conforming pipes and components shall be set aside. A detailed report of the damage must be prepared and submitted to the Company, which shall provide instructions for repair or disposal of the damaged pipes and components. 4.4 RECEPTION OF COATING MATERIALS The Contractor shall ensure that coating materials purchased and supplied comply with the specified requirements. The Contractor shall file and retain for at least 3 years all the technical and administrative documents related to the purchase, both those issued by himself and by the Coating Manufacturer. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 18 of 20
All coating materials shall be delivered to the job site in their original containers with intact labels and seals. The containers shall be provided with identifying documents clearly stating their content and shelf life. 4.5 INSPECTION AND QUALITY CONTROL FUNCTION 4.5.1 Contractor The Contractor shall nominate the inspector responsible for performing quality control functions according to the Quality Control Plan (QCP). The inspector shall have adequate experience of the specific coating process. A statement of the inspectors name and a listing of appropriate experience shall be included with the QCP when submitted for approval, and shall be subject to the approval of the Company. The Contractors inspector shall perform all necessary QC checks and tests to ensure that work complies with the requirements of the approved QCP and with the Companys specification. 4.5.2 Coating Manufacturer The Coating Manufacturer shall provide technical support whenever work is performed. The Coating Manufacturer shall verify that the coating process meets written technical requirements, and shall, through visits and inspections as necessary, confirm that completed work complies with the specified requirements. 4.5.3 Independent Inspection In addition to the in-house inspector defined in item 4.5.1 above, the Contractor shall appoint an independent, third-party inspector, who shall verify and confirm that the execution of every working step, from storage of bare pipes to the final inspection and delivery, complies with the requirements of this specification and the appropriate Appendix(s). The appointment of the third-party inspector shall be subject to approval by the Company. The independent inspector shall verify the Contractors QC testing, and provide written reports that are submitted to both the Contractor and the Company, and to the Coating Manufacturer when requested. 4.5.4 Certification of personnel All personnel involved in the inspection process and defined in items 4.5.1, 4.5.2 and 4.5.3 shall be NACE International or FROSIO Certified, and shall have adequate experience of the specific coating process. 4.6 IDENTIFICATION MARKINGS Before starting any work, the Contractor shall have the Packing List of the pipes and components to be coated. If the Packing List is not yet available, the Contractor shall request and obtain it before starting the work. The serial numbers shall be compared and reconciled with those reported in the Packing List, identifying any inconsistencies and discrepancies. In case the anomaly noticed cannot be resolved (e.g. lack of serial number) a report shall be submitted to the Company in writing. Before starting the work the serial numbers shall be marked in such way that the identification can be maintained thorough the coating process (e.g. with indelible paint on the inside surface of pipe). This serial number shall follow the pipe or components in all production steps and is an integral part of the final marking procedure. It shall be recorded on all production documents and on the quality control certificates. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 19 of 20
If no original serial number can be found or traced for any pipe or component, the Contractor shall assign a special serial number or sequence of serial numbers to such items. 4.7 INSPECTION OF PRODUCTION PROCESS Contractor shall provide a suitable organisation, able to perform the following tasks: Prepare a work procedure describing in detail the various activities to be performed, including the proper equipment to be used, an adequate work environment, compliance with reference standard and rules and with specific Company requirements; Monitor and check specific characteristics of any production process. 4.8 PRELIMINARY TESTS The following tests/inspections shall be performed before start the coating work. Verify: Storage of the pipes; Storage of coating material; Containers and packaging integrity; Shelf life validity of coating materials; Compliance of all documents (shipping, packing list identification, marking etc.). 4.9 TESTS DURING THE WORK PROGRESS During the works progress, Contractor shall perform all inspections and tests detailed in each Appendix related to the coating and application method. All data concerning each inspection step shall be permanently recorded in reports or a logbook. 4.10 FINAL INSPECTION When coating work is finished, the Contractor shall perform all final inspections and tests detailed in each Appendix related to the coating and application method. All data concerning each inspection step shall be permanently recorded in reports or a logbook. 5 DOCUMENTATION AND REPORTING 5.1 DOCUMENTS TO PRODUCE AT THE BEGINNING OF WORK Prior to start the activity the Contractor shall submit to the Company documents that describe the following: Working method(s); Plan and schedule of operations for surface preparation and coating; Characteristics of storage area and location where the coating materials will be stored; Plan of inspection and administrative controls to be performed before, during and after operations; Type of coating materials that will be used. 5.2 DOCUMENTS TO PRODUCE DURING WORK PROGRESS During work progress, the Contractor must keep a working Data Log, which shall be available any time to the Company, as well as reports and information required by item 4. of this specification and by the specific requirements of the relevant Appendix. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Page 20 of 20
Furthermore, the product and material safety data sheets for each product used shall be available. 5.3 DOCUMENTS TO PRODUCE AT THE COMPLETION OF WORK When work is completed the Contractor shall prepare a final report including following data: Surface preparation characteristics; Trade name and characteristics of the coating used; Test certificates of the coating materials, divided by batch numbers; Sequence of coating application; Atmospheric and thermo-hygrometric conditions; Inspections and tests performed and the relevant results, including final acceptance reports; Repairs (if any).
Eni S.p.A. Exploration & Production Division FUNCTIONAL SPECIFICATION APPENDIX A FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF LIQUID EPOXY AND EPOXY-MODIFIED COATINGS ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 2 of 9
CONTENTS APPENDIX A....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 3 3.1 GENERAL CRITERIA......................................................................................................... 3 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING......................... 4 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 4 3.3.1 Labelling.............................................................................................................................. 4 3.3.2 Required product information.............................................................................................. 4 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 5 3.4.1 Preparation of steel samples .............................................................................................. 5 3.4.2 Qualification tests................................................................................................................ 6 3.5 FINAL REPORTING OF LAB.............................................................................................. 7 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 7 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 8 5.1 PREHEAT........................................................................................................................... 8 5.2 SURFACE PREPARATION................................................................................................ 8 5.3 COATING APPLICATION................................................................................................... 8 5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) ................................................ 8 5.4 CUT BACK.......................................................................................................................... 8 5.5 REPAIR OF DEFECTS....................................................................................................... 9 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE........... 9 6.1 GENERAL........................................................................................................................... 9 6.2 QUALITY CONTROL PLAN................................................................................................ 9 6.3 TESTS DURING THE WORKS PROGRESS AND FINAL INSPECTION.......................... 9 7 DOCUMENTATION AND REPORTING............................................................................. 9
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 3 of 9
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to European Standard EN 10289 (Steel tubes and fittings for onshore and offshore pipelines External liquid applied epoxy and epoxy-modified coatings), the content of which must be considered an integral part of this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coating are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, supply and application of liquid epoxy and epoxy-modified tar-free coating to external surfaces of steel pipes and components for onshore and offshore services as defined in Item 1 of standard EN 10289. The coating system assumed by this Appendix is the Type 3: -20C to +80C, thickness class C (1.500 m) of standard EN 10289. 1.3 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered in this Appendix are two-pack liquid products, solvent free, and composed of a base (epoxy resin) and curing agent that can be applied by brush or spatula, airless spray or plural-components spray equipment in high thickness and that harden rapidly in air. The coating materials can be applied at ambient temperature over + 5C with a Dry Film Thickness (DFT) of 1.500 m when applied by brush or spray showing a continuous and uniform film free of sags, runs or any other visible defect. 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided in Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, including those provided for repair, subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 4 of 9
qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The application documentation shall include all data listed in Table 1 of standard EN 10289. In addition the following data must be provided: a) Material Safety Data Sheet of each component; b) Application method, i.e. brush, spatula, airless spray, plural-component (bi-mixer) spray; c) Coating system description; d) Finger printing Infrared scans of each component of a coating material with and without pigment. Coating Manufacturers Product Quality Manager shall certify the finger printing; e) Name and address of the laboratory where the tests will be performed; f) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original containers bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coating material (Part A); b) Name of the curing agent (Part B); c) Coating Manufacturer name; d) Colour of the coating material; e) Batch number of each component (Part A, Part B); f) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide to the selected laboratory the information listed in the Table 1 of standard EN 10289. In addition, the following data shall be provided: a) Material Safety Data Sheet of each component; b) Viscosity of the base and curing agent according to standard ISO 2555 at temperature of 5, 15, 25, 35 and 40C; c) Finger printing Infrared scans of each component of a coating material with and without pigment and of coating fully cured. Coating Manufacturers Product Quality Manager shall certify the finger printing, reporting the method and resolution used; d) Thermal analysis, reporting the method used: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 5 of 9
Curve of curing reaction with temperature scan from ambient temperature to the end of reaction; Glass Transition (T g ) temperature; Scan speed (C/min); Temperature at the beginning of the reaction, max temperature at the end of the reaction and heat content; e) Shore D according to standard ISO 868 in consideration of the time in isothermal condition at 5, 15, 25, 35 and 40C. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. For two-pack products, the tests shall be performed both for the base and the curing agents. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer, including, but not limited to: Viscosity; Density; Solids by Volume; Solids by Weight; Infra-Red Scans (Finger printing). 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe and steel panels) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples As general rule the tests shall be performed on carbon steel samples having following dimension: a) Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum; b) Panels: 300 x 300 mm, Thickness 5 mm. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 6 of 9
Where dimensions of steel samples reported in this item differ from those reported in the standard EN 10289, the requirements laid in the standard EN 10289 shall apply. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5 and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0 including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method (brush, spatula, airless spray, etc.) for which the qualification is required and to the same application parameters (e.g. DFT). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.4.2 Qualification tests Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 1. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 7 of 9
TABLE 1 Test to be performed on coated steel samples Test Type Standard/Method Acceptance criteria Dry Film Thickness EN 10289 Annex A Min 1.500 m (Class C) Max 1.800 m Appearance and continuity EN 10289 Item 7.4 Free of defects as per standard EN 10289 Impact test EN 10289 Annex C At 5C, 4,5 J At +23C, 10 J Hardness Shore D ISO 868 As per Coating Manufacturer data Holiday detection EN 10289 Annex B NACE RP0188 Free from holidays Adhesion test Resistance to removal EN 10289 Annex D Rating 2 at (23 2)C Rating 4 at max service temp. 2C Adhesion test Pull-off method EN 24624 ISO 4624 Not less than 10 MPa at (23 2)C, using pneumatic instrument Cathodic Disbonding EN 10289 Annex E 8 mm max at (23 2)C per 28 days 8 mm max at (60 2)C per 2 days Specific electrical insulation resistance EN 10289 Item 7.11 and Annex F R s = 10 7 at (23 2)C per 100 days R s = 10 4 at T max service 2C per 30 days Adhesion test after immersion in tap water EN 10289 Annex G Rating 2 at (23 2)C per 100 hours Indentation resistance EN 10289 Annex H 0,2 mm at (23 2)C 30% of initial measured thickness at max service temp 2C Thermal ageing EN 10289 Annex J 10 MPa after cooling using pneumatic instrument Infrared scan No variations of the values demonstrated by the Coating Manufacturer. Water absorption ISO 62 ASTM D 570 1% max Abrasion resistance ASTM D4060 Taber Test 195 mg weight loss after 1000 cycles with abrasive wheels CS-17 and 1000 g applied load as average of at least 3 test specimens. 3.5 FINAL REPORTING OF LAB At completion of all tests a detailed report shall be provided to the Company, describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical application test shall be performed in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 8 of 9
c) The need, where applicable, for special application equipment. The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. At completion of the application test the following checks shall be performed: Dry Film Thickness according to standard EN 10289 Annex A; Appearance and continuity according to standard EN 10289 Item 7.4; Hardness Shore D According to standard ISO 868; Holiday detection according to standard EN 10289 Annex B or NACE RP0188; Adhesion test Resistance to removal according to standard EN 10289 Annex D. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The preheat temperature shall be kept between 35C and 50C; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. The preheat temperature can be checked using either temperature indicating crayons or contact thermometers. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with item 6.1 of standard EN 10289 and to the specific requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN Rev.0. 5.3 COATING APPLICATION Coatings shall be mixed and applied fully in accordance with item 6.2 of standard EN 10289 and to the specific requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN Rev. 0. 5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) Wet film thickness shall be measured in accordance with standard ISO 2808. Calibration of DFT gauges and measurement method shall be carried out according to standard SSPC-PA2. 5.4 CUT BACK The pipe surface shall be left bare (uncoated) at both ends of the pipe for (150 20) mm distance from the ends. For fittings and components cut back shall be specified and approved by the Companys Representative. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 February 2004 Appendix A - Page 9 of 9
The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of paint. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contract documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping. Coating used for repair of defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to item 9 of standard EN 10289. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN Rev. 0 must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity, b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. 6.3 TESTS DURING THE WORKS PROGRESS AND FINAL INSPECTION Contractor shall perform during the works progress and at completion of the work all inspections and tests reported in the Table 5 of standard EN 10289. 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN Rev. 0. Eni S.p.A. Exploration & Production Division FUNCTIONAL SPECIFICATION APPENDIX B FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF LIQUID POLYURETHANE AND POLYURETHANE MODIFIED COATINGS ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 2 of 10
CONTENTS APPENDIX B....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 3 3.1 GENERAL CRITERIA......................................................................................................... 3 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING......................... 4 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 4 3.3.1 Labelling.............................................................................................................................. 4 3.3.2 Required product information.............................................................................................. 4 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 5 3.4.1 Preparation of steel samples .............................................................................................. 5 3.4.2 Qualification tests................................................................................................................ 6 3.5 FINAL REPORTING OF LAB.............................................................................................. 7 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 8 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 8 5.1 PREHEAT........................................................................................................................... 8 5.2 SURFACE PREPARATION................................................................................................ 8 5.3 COATING APPLICATION................................................................................................... 8 5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) ................................................ 8 5.4 CUT BACK.......................................................................................................................... 9 5.5 REPAIR OF DEFECTS....................................................................................................... 9 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE........... 9 6.1 GENERAL........................................................................................................................... 9 6.2 QUALITY CONTROL PLAN................................................................................................ 9 6.2.1 Tests during the works progress and final inspection......................................................... 9 7 DOCUMENTATION AND REPORTING........................................................................... 10
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 3 of 10
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to the European Standard EN 10290 (Steel tubes and fittings for onshore and offshore pipelines External liquid applied polyurethane and polyurethane-modified coatings), the content of which must be considered an integral part of this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coating are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, supply and application of liquid polyurethane and polyurethane-modified tar-free coating to external surface of steel pipes and components for onshore and offshore services as defined in Item 1 of standard EN 10290. The coating system assumed by this Appendix is the Type 3: -20C to +80C, thickness class B (1.500 m) of standard EN 10290. 1.3 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered in this Appendix are multi-component liquid products and composed of a polyol and an isocyanate that can be applied by brush or spatula, or airless spray or plural-components spray equipment in high thickness and that harden rapidly in air. The coating materials can be applied at ambient temperature over + 5C with a Dry Film Thickness (DFT) of 1.500 m when applied by brush or spray showing a continuous and uniform film free of sags, runs or any other visible defect. 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided in the Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, including those provided for repair, subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 4 of 10
If the formulation of one or all coating materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests b) Coating system characterisation tests 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The application documentation shall include all data listed in Table 1 of standard EN 10290. In addition the following data must be provided: a) Material Safety Data Sheet of each component; b) Application method, i.e. brush, spatula, airless spray, plural-component (bi-mixer) spray; c) Coating system description; d) Finger printing Infrared scans of each component of a coating material with and without pigment. Coating Manufacturers Product Quality Manager shall certify the finger printing; e) Name and address of the laboratory where the tests will be performed; f) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated; 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original containers bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coating material (Part A); b) Name of the curing agent (Part B); c) Coating Manufacturer name; d) Colour of the coating material; e) Batch number of each component (Part A, Part B); f) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide the selected laboratory whit the information listed in the Table 1 of standard EN 10290. In addition, the following data shall be provided: a) Material Safety Data Sheet of each component; b) Viscosity of the base and curing agent according to standard ISO 2555 at temperature of 5, 15, 25, 35 and 40C; c) Finger printing Infrared scans of each component of a coating material with and without pigment and of coating fully cured. Coating Manufacturers Product Quality Manager shall certify the finger printing, reporting the method and resolution used; d) Thermal analysis, reporting the method used: Curve of curing reaction with temperature scan from ambient temperature to the end of reaction; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 5 of 10
Glass Transition (T g ) temperature; Scan speed (C/min); Temperature at the beginning of the reaction, max temperature at the end of the reaction and heat content. e) Shore D according to standard ISO 868 in consideration of the time in isothermal condition at 5, 15, 25, 35 and 40C. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. For two-pack products, the tests shall be performed both for the base and the curing agents. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer, including, but not limited to: Viscosity; Density; Solids by Volume; Solids by Weight; Infra-Red Scans (Finger printing). 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe and steel panels) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples As general rule the tests shall be performed on carbon steel samples having following dimension: a) Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum; b) Panels: 300 x 300 mm, Thickness 5 mm. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 6 of 10
Where dimensions of steel samples reported in this item differ from those reported in the standard EN 10290, the requirements laid in the standard EN 10290 shall apply. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5, and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0 including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method (brush, spatula, airless spray, etc.) for which the qualification is required and to the same application parameters (e.g. DFT). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.4.2 Qualification tests Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 1. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 7 of 10
TABLE 1 Test to be performed on coated steel samples Test Type Standard/Method Acceptance criteria Dry Film Thickness EN 10290 Annex A Min. 1.500 (Class B) Max. 1.800 m Appearance and continuity EN 10290 Item 7.4 Free of defects as per standard EN 10290 Impact test EN 10290 Annex C At 5C, 4,5 J At +23C, 10 J Hardness Shore D ISO 868 As per Coating Manufacturer data Holiday detection EN 10290 Annex B NACE RP0188 Free from holiday Adhesion test Resistance to removal EN 10290 Annex D Rating 3 at (23 2)C Rating 4 at max service temp. 2C Adhesion test: Pull-off EN 24624-ISO 4624 Not less than 10 MPa at (23 2)C, using pneumatic instrument. Cathodic Disbonding EN 10290 Annex E 8 mm max at (23 2)C per 28 days 10 mm max at (60 2)C per 2 days Specific electrical insulation resistance EN 10290 Item 7.11 and Annex F R s = 10 7 at (23 2)C per 100 days R s = 10 4 at max service temp 2C per 30 days Adhesion test after immersion in tap water EN 10290 Annex G Rating 2 at (23 2)C per 100 hours Indentation resistance EN 10290 Annex H 0,2 mm at (23 2)C 30% of initial measured thickness at max service temp 2C Thermal ageing EN 10290 Annex J 10 MPa after cooling using pneumatic instrument Infrared scan No variations of the values demonstrated by the Coating Manufacturer. Water absorption ISO 62 ASTM D 570 1% max Flexibility EN 10290 Item 7.15 and Annex K 1. Pipes: S = 0,020 at 0 2C S = 0.030 at 23 2C 2. Fitting: S = 0,005 at 0 2C S = 0.010 at 23 2C Elongation EN 10290 Item 7.17 10% Abrasion resistance ASTM D4060 Taber Test 195 mg weight loss after 1000 cycles with abrasive wheels CS-17 and 1000 g applied load as average of at least 3 test specimens.
3.5 FINAL REPORTING OF LAB At completion of all tests a detailed report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 8 of 10
4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be perform in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; c) The need, where applicable, for special application equipment; The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. At completion of the application test the following checks shall be performed: Dry film Thickness according to standard EN 10290 Annex A; Appearance and continuity according to standard EN 10290 Item 7.4; Hardness Shore D according to standard ISO 868; Holiday detection according to standard EN 10290 Annex B or NACE RP0188; Adhesion test Resistance to removal according to standard EN 10290 Annex D. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The preheat temperature shall be kept between 35C and 50C; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. The preheat temperature can be checked using either temperature indicating crayons or contact thermometers. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with item 6.1 of standard EN 10290 and to the specific requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN Rev.0. 5.3 COATING APPLICATION Coatings shall be mixed and applied fully in accordance with item 6.2 of standard EN 10290 and to the specific requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) Wet film thickness shall be measured in accordance with standard ISO 2808. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 9 of 10
Calibration of DFT gauges and measurement method shall be carried out according to standard SSPC-PA2. 5.4 CUT BACK The pipe surface shall be left bare (uncoated) at both ends of the pipe for (150 20) mm distance from the ends. For fittings and components cut back shall be specified and approved by the Companys Representative. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of paint. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contract documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping. Coating used for repair of defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to item 9 of standard EN 10290. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. 6.2.1 Tests during the works progress and final inspection Contractor shall perform during the works progress and at completion of the work all inspections and tests reported in the Table 5 of standard EN 10290. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix B - Page 10 of 10
7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division FUNCTIONAL SPECIFICATION APPENDIX C FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF THREE LAYERS EXTRUDED POLYETHYLENE COATINGS ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 2 of 14
CONTENTS APPENDIX C....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 OPERATIVE ENVIRONMENT............................................................................................ 3 1.4 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 2.1 CHARACTERISTICS OF THE PRIMER............................................................................. 3 2.2 CHARACTERISTICS OF THE ADHESIVE ........................................................................ 4 2.3 EXTRUDED POLYETHYLENE........................................................................................... 4 2.4 COATING THICKNESS...................................................................................................... 5 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 6 3.1 GENERAL CRITERIA......................................................................................................... 6 3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING................................. 6 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 6 3.3.1 Labelling.............................................................................................................................. 6 3.3.2 Product information............................................................................................................. 6 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 8 3.4.1 Preparation of steel samples .............................................................................................. 8 3.5 QUALIFICATION TESTS.................................................................................................... 8 3.6 FINAL REPORTING OF LAB.............................................................................................. 9 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 9 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................. 10 5.1 PREHEAT......................................................................................................................... 10 5.2 SURFACE PREPARATION.............................................................................................. 10 5.3 COATING APPLICATION................................................................................................. 10 5.3.1 Application of Powder Epoxy Primer ................................................................................ 10 5.3.2 Application of the Adhesive............................................................................................... 10 5.3.3 Application of Extruded Polyethylene ............................................................................... 10 5.3.4 Cooling.............................................................................................................................. 10 5.3.5 Thickness of the coating system....................................................................................... 11 5.4 CUT BACK........................................................................................................................ 11 5.5 REPAIR OF DEFECTS..................................................................................................... 11 5.5.1 Max number of repair........................................................................................................ 11 5.5.2 Inspection.......................................................................................................................... 11 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE......... 11 6.1 GENERAL......................................................................................................................... 11 6.2 QUALITY CONTROL PLAN.............................................................................................. 11 7 DOCUMENTATION AND REPORTING........................................................................... 12
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 3 of 14
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to the European Standard EN 10288 (Steel tubes and fittings for onshore and offshore pipelines - External two layers extruded polyethylene based coatings), the content of which must be considered an integral part of this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coating are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for the qualification, supply and application of factory applied external three layers extruded polyethylene based coatings for the external surfaces of steel pipes and components for onshore and offshore services as defined in Item 1 of standard EN 10288. 1.3 OPERATIVE ENVIRONMENT External extruded polyethylene coating can be used for the protection of buried or submerged tubes service and suitable for the following maximum service temperature: From 20 to +80C for offshore application; From 20 to +70C for onshore buried pipelines. 1.4 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provisions of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered in this Appendix consist of three layers as follows: 1st layer - Powder Epoxy Primer (DFT 80 150 m); 2nd layer - Extruded Adhesive (DFT 150 250 m); 3rd layer - Extruded Polyethylene outer sheath. 2.1 CHARACTERISTICS OF THE PRIMER The 1 st layer (Primer) shall be formed by a powder epoxy primer completely compatible with the adhesive that shall maintain perfect adhesion to the substrate and to the adhesive and shall meet the characteristics specified in the Table 1: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 4 of 14
Table 1 Characteristic Method Acceptance Criteria Gel time @ 180C Heating plate (DIN 55990 T8) 80 + 10 s Max Specific gravity Standard method 1,20 1,60 Moisture content Powder: 20 g Temperature: 105C Time: 30 minutes 0,5% (max.) Glass Transition (T g ) temperature Differential heat analysis T g < -5C Bend test DIN 53452 2,5 per diameter No holiday
2.2 CHARACTERISTICS OF THE ADHESIVE The 2 nd layer (Adhesive) shall be formed by a polymer intended to provide adhesion between the primer and 3 rd layer (extruded polyethylene) The extruded adhesive shall meet the requirements listed in the Table 2:
Table 2 Characteristic Standard Acceptance Criteria Melt flow rate ISO 1133 1 to 6 g/10 min Density ISO 1183 0,93 to 0,95 Breaking strength 12 MPa Elongation at break ASTM D 638 600 % Shore D hardness ASTM 2240 35 Brittle point ASTM 746 - 60C VICAT Softening point (9,8 N) ASTM 1525 > 90C Melting point ASTM 3418 > 120C
2.3 EXTRUDED POLYETHYLENE The 3 rd layer (Extruded Polyethylene) shall be formed by the polyethylene outer sheath. The extruded polyethylene shall meet the requirements of Table 3: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 5 of 14
Table 3 Characteristic Standard Acceptance Criteria Melt flow rate ISO 1133 0,25 to 3 g/10 min Density ISO 1183 0,94 to 0,96 Carbon Black content ASTM D 1603 2.0% Tensile strength at yield at 23C ASTM D 638 17 MPa Elongation at break at 23C ASTM D 638 > 600% Shore D hardness ASTM D 2240 50 Water Absorption ASTM D 570 0,05% 24 h VICAT Softening point (9,8 N) ASTM D 1525 > 110C Melting point ASTM D 3418 > 110C Brittle point MA 17238 < -20C Specific resistance DIN 30670 10 8 at (232)C per 100 days
2.4 COATING THICKNESS The minimum thickness of the coating system at any point shall correspond to the value given in Table 2 of the standard EN 10288 depending on the specified Class (1, 2, 3). Coating thickness shall be measured in accordance with the method defined in Annex A of the standard EN 10288. The coating thickness is also given in the following Table 4 where for Classes 1, 2 and 3 the following definition shall be assumed: Class 1 Normal Thickness: buried condition with low mechanical aggressiveness or on lines with extra anti-rock protection; Class 2 Reinforced Thickness: buried condition with mechanical aggressiveness (rock or clay) and for submerged pipeline with service temperature below 80C; Class 3 Extra-reinforced Thickness: submerged pipeline for deep sea or with concrete coating and/or when the temperature is higher than 80C.
Table 4 Minimum thickness (mm) Line pipe diameter (mm) Class 1 Class 2 Class 3 D 114,3 1,5 1,8 2,5 114,3 < D 273 1,8 2 2,7 273 < D 508 2 2,2 2,9 508 < D 762 2,2 2,5 3,2 762 < D 2,5 3 3,7 Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 6 of 14
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by the Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, including those provided for repair, subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The documentation forwarded to the Company shall include all data listed in Table 1 of standard EN 10288. In addition the following data must be provided: a) Material Safety Data Sheet of each component; b) Application method; c) Coating system description; d) Name and address of the laboratory where the tests will be performed; e) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original containers bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coatings material (primer, adhesive and extruded polyethylene); b) Coating Manufacturer name; c) Colour of the coating material; d) Batch number of each component (primer, adhesive and extruded polyethylene); e) Manufacturing date. 3.3.2 Product information For each coating material submitted to qualification testing, the Coating Manufacturer shall provide the selected laboratory whit the information listed in the following Table 5. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 7 of 14
Table 5 - Information and data to be provided by Coating Manufacturer Item Primer Adhesive Polyethylene Product Data Sheet (PDS) Yes Yes Yes Material Safety Data Sheet (MSDS) Yes Yes Yes Date of issue of PDS Yes Yes Yes Date of issue of MSDS Yes Yes Yes Name of Manufacturer Yes Yes Yes Name and type of the product Yes Yes Yes Factory of origin Yes Yes Yes Batch number Yes Yes Yes Shelf life Yes Yes Yes Physical state of delivered product Yes Yes Yes Packaging Yes Yes Yes Storage condition Yes Yes Yes Sieve analysis Yes No No Gel time Yes No No Specific gravity Yes No No Moisture content Yes No No Glass Transition (T g ) temperature Yes No No Bend test Yes No No Density No Yes Yes Melting point No Yes Yes Melt flow rate No Yes Yes Braking strength No Yes Yes Elongation at break @ 23C No Yes Yes Shore D hardness No Yes Yes Brittle point No Yes Yes VICAT Softening point (9,8N) No Yes Yes Carbon black content No No Yes Tensile strength at yield at 23C No No Yes Water absorption No No Yes Thermal ageing No No Yes UV ageing No No Yes Stress cracking resistance No No Yes Specific resistance No No Yes Content of pigment No No Yes Dispersion of pigment No No Yes Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 8 of 14
For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer. 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instruction. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully followed. The selected laboratory shall supervise, record and report all the steps of the coating work. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples As general rule the tests shall be performed on carbon steel samples having following dimension: Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Where dimensions of steel samples reported in this item differ from those reported in the standard EN 10288, the requirements laid in the standard EN 10288 shall apply. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5, and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and according to the same application parameters (e.g. thickness). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.5 QUALIFICATION TESTS Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 6. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 9 of 14
3.6 FINAL REPORTING OF LAB At completion of all tests a complete report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples.
Table 6 Test to be performed on coated steel samples Test Type Standard/Method Acceptance criteria Dry Film Thickness EN 10288 Annex A As per standard EN 10288 Table 2. Appearance and continuity EN 10288 Item 8.2 Free of defects as per standard EN 10288 Impact resistance EN 10288 Annex C 5 J per mm coating thickness Holiday detection EN 10288 Annex B NACE RP0274 Free from holiday Cathodic Disbonding EN 10288 Annex J 30 mm max at (23 2)C per 28 days 30 mm max at (60 2)C per 2 days 30 mm max at (402)C per 7 days Specific electrical insulation resistance EN 10288 Annex F R s = 10 8 at (23 2)C per 100 days Indentation resistance EN 10288 Annex E 0,3 mm at (23 2)C 0,5 mm at (60 2)C Peel Force (N/10 mm) EN 10288 Annex D At (23 2)C Min Average 60, Average 80 At (80 2)C Min Average 15, Average 20 Elongation at break EN 10288 Annex G 350 % at (23 2)C Resistance to ultraviolet irradiation EN 10288 Annex H.1 A 50% 0,65 MFR 1,35 Thermal stability EN 10288 Annex H.2 0,65 MFR 1,35 at (100 2)C per 2400 hours Flexibility EN 10288 Item 8.14 3% at (23 2)C Hardness Shore D ASTM D 2240 50 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory, a practical test shall be performed in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; c) The need, where applicable, for special application equipment. The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. At completion of the application test the following checks shall be performed: Dry Film Thickness according to standard EN 10288 Annex A; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 10 of 14
Appearance and continuity according to standard EN 10288 Item 8.2; Holiday detection according to standard EN 10288 Annex B or NACE RP0274. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The preheat temperature shall be kept between 35C and 50C; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with item 7.1 of standard EN 10288 and to the specific requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN Rev.0. 5.3 COATING APPLICATION Coatings shall be mixed and applied, in a continuous coating line, fully in accordance with item 7.2 of standard EN 10288 and to the specific functional requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3.1 Application of Powder Epoxy Primer The pipes shall be heated in an induction oven in accordance with the temperature recommended by the Coating Manufacturer. Application shall be made by electrostatic spray equipment at DFT of 80 150 m in consideration of the powder and intended service operation. 5.3.2 Application of the Adhesive The adhesive shall be applied by extrusion prior the complete polymerisation of the Powder Epoxy Primer. The temperature shall be fully in accordance with Coating Manufacturer recommendations. 5.3.3 Application of Extruded Polyethylene The application of Extruded Polyethylene outer sheath shall be performed by lateral or axial extrusion and than the coating shall be smoothed by pressure rollers. During the production the temperature shall be always in accordance with Coating Manufacturer recommendations. 5.3.4 Cooling When the coating process is completed, the pipe shall be sprayed with fresh water in order to cool it to a temperature of 60C (10C). Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 11 of 14
5.3.5 Thickness of the coating system Coating thickness shall be measured in accordance with the method defined in Annex A of the standard EN 10288. The minimum thickness of the coating system at any point shall correspond to the value given in Table 4 of this Appendix depending on the specified class (1, 2 or 3). 5.4 CUT BACK The pipe surface shall be left bare (uncoated) at both ends of the pipe for 150 ( 20) mm distance from the ends and the coating shall be beveled at the cut back forming a bevel angle of 30 unless otherwise specified. For fittings and components cut back shall be specified and approved by the Companys Representative. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of paint. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contractual documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping. Coating used to repair the defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to item 10 of standard EN 10288 and method submitted to the Company for approval before the beginning of the production. 5.5.1 Max number of repair Contractor shall repair all defects detected by holiday detection and/or any kind of damaged area less than 50 cm 2 . In case any individual damaged area is greater than 50 cm 2 , the pipe shall be completely re- coated. A maximum of 3 (three) repairs per pipe is allowed, but in no case the total repaired areas shall exceed 150 cm 2 . 5.5.2 Inspection The repaired area shall be 100% inspected with a holiday detector set to 10 kV per mm of coating thickness according to the methods defined in Appendix B of standard EN 10288. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 12 of 14
the Production Quality Tests (PQT) necessary to fully meet the provisions of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. According to Table 8 of standard EN 10288 and the requirements of this Appendix, the Contractor shall perform during the works progress and at completion of the coating works all inspections and tests reported in the following Table 7. 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 13 of 14
Table 7 - Nature and frequency of testing and control Properties Test method Acceptance Criteria Frequency Surface condition before blasting - Every pipe Steel imperfection ISO 8501-3 Grade P3 Every pipe Dimensions, shape and properties of abrasive blasting material ASTM D-4940 Conductivity 150 S/cm Chloride content < 25 ppm Twice per shift Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every pipe Degree of abrasive blasting ISO 8501-1 Sa 2,5 Every pipe Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 pipes and 4 time per shift Roughness of the blast cleaned surface - 60 R z 80 m Once per shift Relative Humidity and Dew Point ISO 8502-4 RH < 85% 4 time per shift Steel temperature 3C above dew point 4 time per shift Temperature of heating before coating IR camera recording As per Coating Manufacturer Every pipe Appearance and continuity Visual Free of defects Every pipe Thickness of the primer EN 10288 Annex A As per requirement First 10 pipes and 1 per hour Thickness of the coating system EN 10288 Annex A As per requirement First 10 pipes and 1 per hour Cut back Visual As per requirement Every pipe Holiday detection EN 10288 Annex B As per requirement Every pipe Impact resistance EN 10288 Annex C As per requirement Once per week Peel force EN 10288 Annex D As per requirement 2 Tests once per shift at 23C 2 Tests once per week at 60C Indentation resistance EN 10288 Annex E As per requirement Once per week Electrical insulation resistance EN 10288 Annex F As per requirement To be agreed at pre-job meeting Elongation at break EN 10288 Annex G As per requirement To be agreed at pre-job meeting
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix C - Page 14 of 14
Table 7 - Nature and frequency of testing and control Properties Test method Acceptance Criteria Frequency Resistance to ultraviolet irradiation EN 10288 Annex H.1 As per requirement To be agreed at pre-job meeting Thermal stability EN 10288 Annex H2 As per requirement To be agreed at pre-job meeting Cathodic disbonding EN 10288 Annex J As per requirement To be agreed at pre-job meeting
Eni S.p.A. Exploration & Production Division FUNCTIONAL SPECIFICATION APPENDIX D FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF THREE LAYERS EXTRUDED POLYPROPYLENE COATINGS ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 2 of 14
CONTENTS APPENDIX D....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 OPERATIVE ENVIRONMENT............................................................................................ 3 1.4 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 2.1 CHARACTERISTIC OF THE PRIMER............................................................................... 3 2.2 ADHESIVE.......................................................................................................................... 4 2.3 EXTRUDED POLYPROPYLENE........................................................................................ 4 2.4 COATING THICKNESS...................................................................................................... 5 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 5 3.1 GENERAL CRITERIA......................................................................................................... 5 3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING................................. 6 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 6 3.3.1 Labelling.............................................................................................................................. 6 3.3.2 Product information............................................................................................................. 6 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 8 3.4.1 Preparation of steel samples .............................................................................................. 8 3.5 QUALIFICATION TESTS.................................................................................................... 8 3.6 FINAL REPORTING OF LAB.............................................................................................. 9 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 9 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................. 10 5.1 PREHEAT......................................................................................................................... 10 5.2 SURFACE PREPARATION.............................................................................................. 10 5.3 COATING APPLICATION................................................................................................. 10 5.3.1 Application of Powder Epoxy Primer ................................................................................ 10 5.3.2 Application of the Adhesive............................................................................................... 10 5.3.3 Application of Extruded Polypropylene............................................................................. 10 5.3.4 Cooling.............................................................................................................................. 10 5.3.5 Thickness of the coating system....................................................................................... 11 5.4 CUT BACK........................................................................................................................ 11 5.5 REPAIR OF DEFECTS..................................................................................................... 11 5.5.1 Max number of repair........................................................................................................ 11 5.5.2 Inspection.......................................................................................................................... 11 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE......... 11 6.1 GENERAL......................................................................................................................... 11 6.2 QUALITY CONTROL PLAN.............................................................................................. 12 7 DOCUMENTATION AND REPORTING........................................................................... 12
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 3 of 14
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. For testing and acceptance criteria only, this Appendix refers to the European Standard EN 10288 (Steel tubes and fittings for onshore and offshore pipelines External two layers extruded polyethylene based coatings). 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, supply and application of factory applied external three layers extruded polypropylene based coatings for the external surface of steel pipes and components for onshore and offshore pipelines transporting oil, gas or water. 1.3 OPERATIVE ENVIRONMENT External extruded polypropylene coating can be used for the protection of buried or submerged tubes service and suitable for the following maximum service temperature: From 20 to +80C for applications at ambient temperature or medium temperatures (standard coating); From 20 to +120C for high temperatures offshore application (thermal stabilised coating); From 20 to +110C for high temperatures onshore buried pipelines (thermal stabilised coating). 1.4 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered in this Appendix consist of three layers as follows:. 1st layer - Powder Epoxy Primer (DFT 80 150 m); 2nd layer - Extruded Adhesive (DFT 250 300 m); 3rd layer - Extruded Polypropylene outer sheath. 2.1 CHARACTERISTIC OF THE PRIMER The 1 st layer (Primer) shall be formed by a powder epoxy primer completely compatible with the adhesive that shall maintain perfect adhesion to the substrate and to the adhesive. The thickness of The Company requirements of the primer are given in the Table 1: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 4 of 14
Table 1 Characteristic Method Acceptance Criteria Gel time @ 180C Heating plate (DIN 55990 T8) 80 + 10 s Max Specific gravity Standard method 1.20 1.60 Moisture content Powder: 20 g Temperature: 105C Time: 30 minutes 0.5% (max.) Glass Transition (T g ) temperature Differential heat analysis T g < -5C Bend test DIN 53452 2,5 per diameter No holiday 2.2 ADHESIVE The 2 nd layer (Adhesive) shall be formed by a polymer intended to provide adhesion between the primer and 3 rd layer (extruded polypropylene) The extruded adhesive shall meet the requirements listed in the Table 2:
Table 2 Characteristic Standard Acceptance Criteria Melt flow rate ISO 1133 1 to 12 g/10 min Density ISO 1183 0,90 to 0,92 Breaking strength 20 MPa Elongation at break ASTM D 638 400% Shore D hardness ASTM 2240 57 Brittle point ASTM 746 - 20C VICAT Softening point (9,8 N) ASTM 1525 > 120C Melting point ASTM 3418 > 130C
2.3 EXTRUDED POLYPROPYLENE The 3 rd layer (extruded polypropylene) shall be formed by the polypropylene outer sheath. The extruded polypropylene shall meet the requirements of Table 3: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 5 of 14
Table 3 Characteristic Standard Acceptance Criteria Melt flow rate ISO 1133 0,6 to 4 g/10 min. Density ISO 1183 0,9 to 0,92 Carbon Black content ASTM D 1603 0% Tensile strength at yield at 23C ASTM D 638 20 MPa Elongation at break at 23C ASTM D 638 > 400% Shore D hardness ASTM D 2240 60 Water Absorption ASTM D 570 0,05% 24 h VICAT Softening point (9,8 N) ASTM D 1525 > 135C Melting point ASTM D 3418 > 150C Brittle point MA 17238 < -20C Specific resistance DIN 30670 10 8 at (232)C per 100 days 2.4 COATING THICKNESS The minimum thickness of the coating system at any point shall correspond to the value given in the Table 4 where for Classes 1, 2 and 3 the following definition shall be assumed: Class 1 Normal Thickness: buried condition with low mechanical aggressiveness or on lines with extra anti-rock protection; Class 2 Reinforced Thickness: buried condition with mechanical aggressiveness (rock or clay) and for submerged pipeline with service temperature below 80C; Class 3 Extra-reinforced Thickness: submerged pipeline for deep sea or with concrete coating and/or when the temperature is higher than 80C.
Table 4 Minimum thickness (mm) Line pipe diameter (mm) Class 1 Class 2 Class 3 D 114,3 1,5 1,8 2,5 114,3 < D 273 1,8 2 2,7 273 < D 508 2 2,2 2,9 508 < D 762 2,2 2,5 3,2 762 < D 2,5 3 3,7 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided item 2.4 of Functional Specification. 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, including those provided for repair, subject of this Appendix. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 6 of 14
The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 REQUIREMENTS FOR PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The documentation forwarded to the Company shall include all data listed in Table 1 of standard EN 10288. In addition the following data must be provided: a) Material Safety Data Sheet of each component, b) Application method; c) Coating system description; d) Name and address of the laboratory where the tests will be performed; e) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original containers bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coatings material (primer, adhesive and extruded polypropylene); b) Coating manufacturer name; c) Colour of the coating material; d) Batch number of each component (primer, adhesive and extruded polypropylene); e) Manufacturing date. 3.3.2 Product information For each coating material submitted to qualification testing, the Coating Manufacturer shall provide the selected laboratory with the information listed in the following Table 5. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 7 of 14
Table 5 - Information and data to be provided by Coating Manufacturer Item Primer Adhesive Polyethylene Product Data Sheet (PDS) Yes Yes Yes Material Safety Data Sheet (MSDS) Yes Yes Yes Date of issue of PDS Yes Yes Yes Date of issue of MSDS Yes Yes Yes Name of Manufacturer Yes Yes Yes Name and type of the product Yes Yes Yes Factory of origin Yes Yes Yes Batch number Yes Yes Yes Shelf life Yes Yes Yes Physical state of delivered product Yes Yes Yes Packaging Yes Yes Yes Storage condition Yes Yes Yes Sieve analysis Yes No No Gel time Yes No No Specific gravity Yes No No Moisture content Yes No No Glass Transition (T g ) temperature Yes No No Bend test Yes No No Density No Yes Yes Melting point No Yes Yes Melt flow rate No Yes Yes Braking strength No Yes Yes Elongation at break @ 23C No Yes Yes Shore D hardness No Yes Yes Brittle point No Yes Yes VICAT Softening point (9,8N) No Yes Yes Carbon black content No No Yes Tensile strength at yield at 23C No No Yes Water absorption No No Yes Thermal ageing No No Yes UV ageing No No Yes Stress cracking resistance No No Yes Specific resistance No No Yes Content of pigment No No Yes Dispersion of pigment No No Yes Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 8 of 14
For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer. 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturer s duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix are carefully followed. The selected laboratory shall supervise, record and report all steps of the coating work. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples As general rule the tests shall be performed on carbon steel samples having following dimension: Pipe sections: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum. For each test, 2 series of 3 samples shall be prepared. One series shall be used for the test, while one shall be identified and kept for possible checks and controls. Where dimensions of steel samples reported in this item differ from those reported in the standard EN 10288, the requirements laid in the standard EN 10288 shall apply. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5 and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and to the same application parameters (e.g. thickness). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.5 QUALIFICATION TESTS Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 6. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 9 of 14
3.6 FINAL REPORTING OF LAB At completion of all tests a complete report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples.
TABLE 6 Test to be performed on coated steel samples Test Type Standard/Method Acceptance criteria Dry Film Thickness EN 10288 Annex A As per value of Table 4 of this Appendix Appearance and continuity EN 10288 Item 8.2 Free of defects Impact resistance EN 10288 Annex C 7 J per mm coating thickness Holiday detection EN 10288 Annex B NACE RP0274 Free from holiday Cathodic Disbonding EN 10288 Annex J 30 mm max at 23 (2)C per 28 days 30 mm max at 60 (2)C per 2 days 40 mm max at max service temperature per 28 days Specific electrical insulation resistance EN 10288 Annex F R s = 10 8 at (23 2)C per 100 days Indentation resistance EN 10288 Annex E 0,2 mm at (23 2)C 0,4 mm at (60 2)C Peel Force (N/10 mm) EN 10288 Annex D At (23 2)C Min Average 80, Average 100 At (100 2)C Min Average 30, Average 40 At (120 2)C Min Average 15, Average 20 Elongation at break EN 10288 Annex G 400% at (23 2)C Resistance to ultraviolet irradiation EN 10288 Annex H.1 A 50% 0,65 MFR 1,35 Thermal stability EN 10288 Annex H.2 0,65 MFR 1,35 at (100 2)C per 2400 hours Flexibility EN 10288 Item 8.14 3% at (23 2)C Hardness Shore D ASTM D 2240 60 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be perform in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; c) The need, where applicable, for special application equipment. The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. At completion of the application test the following checks shall be performed: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 10 of 14
Dry film Thickness according to standard EN 10288 Annex A Appearance and continuity according to standard EN 10288 Item 8.2. Holiday detection according to standard NACE RP0274. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The preheat temperature shall be kept between 35C and 50C; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with the specific requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3 COATING APPLICATION Coatings shall be mixed and applied, in a continuous coating line, fully in accordance to the specific functional requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3.1 Application of Powder Epoxy Primer The pipes shall be heated in an induction oven in accordance with the temperature recommended by the Coating Manufacturer. Application shall be made by electrostatic spray equipment at DFT of 80 150 m in consideration of the powder and intended service operation. 5.3.2 Application of the Adhesive The adhesive shall be applied by extrusion prior the complete polymerisation of the Powder Epoxy Primer. The temperature shall be fully in accordance with Coating Manufacturer recommendations. 5.3.3 Application of Extruded Polypropylene The application of Extruded Polypropylene outer sheath shall be performed by lateral or axial extrusion and than the coating shall be smoothed by pressure rollers. During the production the temperature shall be always in accordance with Coating Manufacturer recommendations. 5.3.4 Cooling When the coating process is completed, the pipe shall be sprayed with fresh water in order to cool it to a temperature of 60C (10C). Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 11 of 14
5.3.5 Thickness of the coating system Coating thickness shall be measured in accordance with the method defined in Annex A of the standard EN 10288. The minimum thickness of the coating system at any point shall correspond to the value given in Table 4 of this Appendix depending on the specified class (1, 2 or 3). 5.4 CUT BACK The pipe surface shall be left bare (uncoated) at both ends of the pipe for 150 (20) mm distance from the ends and the coating shall be beveled at the cut back forming a bevel angle of 30 unless otherwise specified. For fittings and components cut back shall be specified and approved by the Companys Representative. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of paint. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contractual documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping. Coating used to repair the defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to item 10 of standard EN 10288 and method submitted to the Company for approval before the beginning of the production. 5.5.1 Max number of repair Contractor shall repair all defects detected by holiday detection and/or any kind of damaged area less than 50 cm 2 . In case any individual damaged area is greater than 50 cm 2 , the pipe shall be completely re- coated. A maximum of 3 (three) repairs per pipe is allowed, but in no case the total repaired areas shall exceed 150 cm 2 . 5.5.2 Inspection The repaired area shall be 100% inspected with a holiday detector set to 10 kV per mm of coating thickness according to the methods defined in Appendix B of standard EN 10288. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 12 of 14
6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the provisions of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity, b) Description of the test, c) Applicable reference documents, d) Applicable check procedures and methods, e) Acceptability criteria f) Frequency of the checks g) Persons required to be present at the inspections. According to the requirements of this Appendix, the Contractor shall perform during the works progress and at completion of the coating works all inspections and tests reported in the the following Table 7 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 13 of 14
Table 7 Nature and frequency of testing and control Properties Test method Acceptance Criteria Frequency Surface condition before blasting - Every pipe Steel imperfection ISO 8501-3 Grade P3 Every pipe Dimensions, shape and properties of abrasive blasting material ASTM D-4940- 150 S/cm Chloride content < 25 ppm Twice per shift Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every pipe Degree of abrasive blasting ISO 8501-1 Sa 2,5 Every pipe Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 pipes and 4 time per shift Roughness of the blast cleaned surface - 60 R z 80 m Once per shift Relative Humidity and Dew Point ISO 8502-4 RH < 85% 4 time per shift Steel temperature 3C above dew point 4 time per shift Temperature of heating before coating IR camera recording As per Coating Manufacturer Every pipe Appearance and continuity Visual Free of defects Every pipe Thickness of the primer EN 10288 Annex A As per requirement First 10 pipes and 1 per hour Thickness of the coating system EN 10288 Annex A As per requirement First 10 pipes and 1 per hour Cut back Visual As per requirement Every pipe Holiday detection EN 10288 Annex B As per requirement Every pipe Impact resistance EN 10288 Annex C As per requirement Once per week Peel force EN 10288 Annex D As per requirement 2 Tests once per shift at 23C 2 Tests once per week at 60C Indentation resistance EN 10288 Annex E As per requirement Once per week Electrical insulation resistance EN 10288 Annex F As per requirement To be agreed at pre-job meeting
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix D - Page 14 of 14
Table 7 Nature and frequency of testing and control Properties Test method Acceptance Criteria Frequency Elongation at break EN 10288 Annex G As per requirement To be agreed at pre-job meeting Resistance to ultraviolet irradiation EN 10288 Annex H.1 As per requirement To be agreed at pre-job meeting Thermal stability EN 10288 Annex H2 As per requirement To be agreed at pre-job meeting Cathodic disbonding EN 10288 Annex J As per requirement To be agreed at pre-job meeting
Eni S.p.A. Exploration & Production Division
FUNCTIONAL SPECIFICATION APPENDIX E FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF PLASTIC TAPE OR SHRINKABLE SLEEVES COATINGS ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 2 of 9
CONTENTS APPENDIX E ............................................................................................................................................ 1 1 GENERAL................................................................................................................................ 3 1.1 INTRODUCTION...................................................................................................................... 3 1.2 SCOPE..................................................................................................................................... 3 1.3 OPERATIVE ENVIRONMENT................................................................................................. 3 1.4 REFERENCE STANDARDS.................................................................................................... 3 2 GENERAL COATING CHARACTERISTICS.......................................................................... 3 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM............................... 3 3.1 GENERAL CRITERIA.............................................................................................................. 3 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING.............................. 4 3.3 COATING MATERIALS CHARACTERISATION TEST........................................................... 4 3.3.1 Labelling................................................................................................................................... 4 3.3.2 Product information.................................................................................................................. 4 3.4 COATING SYSTEM CHARACTERISATION TESTS.............................................................. 4 3.4.1 Preparation of steel samples ................................................................................................... 5 3.5 QUALIFICATION TESTS......................................................................................................... 5 3.6 FINAL REPORTING OF LAB................................................................................................... 5 4 PRACTICAL APPLICATION TEST IN THE SHOP ................................................................ 7 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION........................................ 7 5.1 PREHEAT................................................................................................................................ 7 5.2 SURFACE PREPARATION..................................................................................................... 7 5.3 COATING APPLICATION........................................................................................................ 8 5.3.1 Thickness of the coating system.............................................................................................. 8 5.4 CUT BACK............................................................................................................................... 8 5.5 REPAIR OF DEFECTS............................................................................................................ 8 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE................ 8 6.1 GENERAL................................................................................................................................ 8 6.2 QUALITY CONTROL PLAN..................................................................................................... 8 6.2.1 Tests during the works progress and final inspection.............................................................. 9 7 DOCUMENTATION AND REPORTING.................................................................................. 9
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 3 of 9
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to the European Standard EN 12068 (External organic coating for the corrosion protection of buried or immersed steel pipelines used in conjunction with cathodic protection: Tapes and Shrinkable materials) the content of which must be considered an integral part of this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coatings are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, supply and application of Plastic Tape or Shrinkable sleeves coating to external surfaces of steel pipes and components for buried or immersed services as defined in Item 1 of standard EN 12068. 1.3 OPERATIVE ENVIRONMENT Item 4 of standard EN 12068 defines the classification of Plastic Tape or Shrinkable coating on the basis of their mechanical loss resistance, maximum service temperature and of special condition of use. For the mechanical resistance the coating combination considered by this Appendix shall be Class C of standard EN 12068, High mechanical resistance coating. For the maximum service temperature and special condition of use, the Classes considered by this Appendix are all those defined in the Items 4.1.3 and 4.1.4 of standard EN 12068. 1.4 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The different type of coatings that are considered by this Appendix are listed in Item 3.2 of standard EN 12068 Qualification of coating material and coating system. 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by Item 2.4 of Functional Specification. 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 4 of 9
approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The application documentation shall include all data listed in Tables 3 to 7 of standard EN 12068. In addition the following data must be provided: a) Material Safety Data Sheet of each component; b) Application method; c) Coating system description; d) Name and address of the laboratory where the tests will be performed; e) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original containers bearing the coating manufacturers label, clearly showing following information: a) Name of the coatings material; b) Coating manufacturer name; c) Colour of the coating material; d) Batch number of each component; e) Manufacturing date. 3.3.2 Product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide the selected laboratory with the information listed in the Tables 3 to 7 of standard EN 12068. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer. 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 5 of 9
The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples Test sample shall be representative for the production and shall be prepared according to the provisions of standard EN 12068. If not otherwise specified as general rule the pipe sections shall have the following dimension: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5, and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and to the same application parameters (e.g. thickness). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.5 QUALIFICATION TESTS Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Tables 1 and 2. 3.6 FINAL REPORTING OF LAB At completion of all tests a complete report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 6 of 9
TABLE 1 Test to be performed on coated steel samples Acceptance criteria Test Type Max Temp Standard Method EN 12068 Cathodic Disbonding Peeling tape on tape Peeling from pipe Impact Resistance, At 23C 30/50/HT Appendix H 15 J 15 J 15 J Indentation Resistance At 23C 30 10,0 N/mm 2 10,0 N/mm 2 10,0 N/mm 2
At operating T max 50/HT 10,0 N/mm 2 10,0 N/mm 2 10,0 N/mm 2
residual thickness Appendix G 0,6 mm 0,6 mm 0,6 mm Specific electrical insulation resistance R s 100 10 8 m 2 10 8 m 2 10 8 m 2
R s 100 / R s 70 30/50/HT Appendix J 0,8 m 2 0,8 m 2 0,8 m 2
Cathodic Disbonding At 23C 30/50/HT 10 mm 10 mm 10 mm At operating T max 50/HT Appendix K 25 mm 25 mm 25 mm Peel resistance tape on tape Internal tape on internal tape and external tape on internal tape
At 23C 30/50/HT 1,0 N/mm 1,5 N/mm 1,5 N/mm At operating T max 50/HT 0,2 N/mm 0,2 N/mm 0,2 N/mm External tape on external tape At 23C 30/50/H 0,2 N/mm 0,2 N/mm 0,2 N/mm At operating T max 50/HT Appendix B 0,2 N/mm 0,2 N/mm 0,2 N/mm Peeling resistance of the tape From steel pipe At 23C 30/50/HT 0,5 N/mm 0,75 N/mm 1,0 N/mm At operating T max 50/HT 0,05 N/mm 0,075 N/mm 0,1 N/mm From coating applied on shop At 23C 30/50/HT 0,4 N/mm 0,4 N/mm 0,4 N/mm At operating Tmax 50/HT Appendix C 0,04 N/mm 0,04 N/mm 0,04 N/mm Lap shear strength At 23C 30/50/HT 0,05 N/mm 2 0,05 N/mm 2 0,05 N/mm 2
At operating Tmax 50/HT Appendix D 0,05 N/mm 2 0,05 N/mm 2 0,05 N/mm 2
. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 7 of 9
TABLE 2 Test to be performed on coated steel samples Test Type Classes Standard Method EN 12068 Acceptance criteria Thermal ageing, relation between Resistance to scratch 125 B 100 /B 0 0,75 B 100 /B 70 0,8 Elongation to break 125 E 100 /E 70 0,75 E 100 /E 70 0,8 Resistance to peeling tape on tape P 100 /P T 0,75 P 100 /P 70 0,8 Resistance to peeling on steel pipe All classes Appendix E A 100 /A T 0,75 A 100 /A 70 0,8 UV radiation resistance, relation between Elongation to break 125 E X /E 0 0,75 Resistance to scratch Class UV only Appendix F 125 B X /B 0 0,75 Low- temperature flexibility At 20C Below 20C Class L Class VL Appendix N No delamination No cracking or scratch Microbiologic resistance All classes Appendix M No variation compared to the not buried samples 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be perform in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by coating manufacturer; c) The need, where applicable, for special application equipment; The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The pipe or component shall be preheated to at least 5C above the dew point to remove the presence of moisture prior to surface cleaning. 5.2 SURFACE PREPARATION Surface preparation shall be performed according to the recommendations of the Coating Manufacturer reported in the product data sheet of each material, as required in Table 7 of standard EN 12068 and to the specific functional requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 8 of 9
5.3 COATING APPLICATION Coatings material application shall be performed in accordance with Coating Manufacturers recommendation reported in the product data sheet of each material, as required in Table 7 of standard EN 12068 and to the specific functional requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3.1 Thickness of the coating system The minimum thickness of the coating system at any point shall correspond to the value reported in the product data sheet of each material, as required in Table 7 of standard EN 12068 depending on the type and class of the coating specified. 5.4 CUT BACK Where applicable the pipe surface shall be left bare (uncoated) at both ends of the pipe for (150 20) mm distance from the ends and the coating shall be beveled at the cut back forming a bevel angle of 30 unless otherwise specified. For fittings and components cut back shall be specified and approved by the Companys Representative. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of coating. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contractual documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after the construction or shipping. Coating and any other material used for the repair of defects and damages shall be supplied by the same Coating Manufacturer of the original Coating system. Any repair shall be performed according to specific Coating Manufactures recommendation as required in Table 7 of standard EN 12068. The acceptability of coating repair and the repair procedure is subject to agreement between the Company and Contractor. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test;
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix E - Page 9 of 9
c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. 6.2.1 Tests during the works progress and final inspection Contractor shall perform during the works progress and at completion of the work all inspections and tests required by Functional Specification 20550 PIP.COR.FUN. Rev. 0 and by this Appendix, including, but not limited to: Surface condition of the pipes or component; Steel imperfection; Dimension and properties of the abrasive material, if applicable; Degree of surface preparation; Degree of cleanliness; Relative humidity, dew point, steel temperature; Appearance and continuity of the coating; Coating thickness; Cut back, if applicable; Holyday detection; Peel force; Etc. 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division
FUNCTIONAL SPECIFICATION APPENDIX F FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF EPOXY POWDER COATING ON EXTERNAL SURFACES OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 2 of 10
CONTENTS APPENDIX F ....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 3 3.1 GENERAL CRITERIA......................................................................................................... 3 3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING...................... 4 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 4 3.3.1 Labelling.............................................................................................................................. 4 3.3.2 Required product information.............................................................................................. 4 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 6 3.4.1 Preparation of steel samples .............................................................................................. 6 3.4.2 Qualification tests................................................................................................................ 6 3.5 FINAL REPORTING OF LAB.............................................................................................. 6 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 7 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 8 5.1 PREHEAT........................................................................................................................... 8 5.2 SURFACE PREPARATION................................................................................................ 8 5.3 COATING APPLICATION................................................................................................... 8 5.3.1 Coating Thickness .............................................................................................................. 9 5.4 CUT BACK.......................................................................................................................... 9 5.5 REPAIR OF DEFECTS....................................................................................................... 9 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE........... 9 6.1 GENERAL........................................................................................................................... 9 6.2 QUALITY CONTROL PLAN................................................................................................ 9 6.2.1 Tests during the works progress and final inspection....................................................... 10 7 DOCUMENTATION AND REPORTING........................................................................... 10
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 3 of 10
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to the NACE Standard RP 0394 Application, Performance, and Quality Control of Plant-Applied, Fusion-Bonded Epoxy External Pipe Coating, the content of which must be considered an integral part of this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coating are defined. 1.2 SCOPE This Appendix defines the minimum requirements for qualification, supply and application of fusion-bonded epoxy (FBE) coatings to the external surfaces of steel pipes and components for onshore and offshore service as defined in Section 1 of NACE standard RP0394. 1.3 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating system considered by this Appendix is the epoxy resin powders applied by fusion. To meet the minimum requirements listed in Table 2 of this appendix the coating thickness shall be 360 50 microns (m). The Company, taking in consideration the specific requirements of the Project Technical Specification, shall specify the minimum and maximum thickness. However the differential between minimum and maximum thickness shall not be less than 100 m. 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by the Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 4 of 10
If the formulation of one or all coatings materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The documentation forwarded to the Company shall include all data listed in Table 1 of this Appendix. In addition the following data must be provided: a) Material Safety Data Sheet of each product; b) Application method; c) Coating system description; d) Finger printing Infrared scans of each component of a coating material with and without pigment. Coating Manufacturers Product Quality Manager shall certify the finger printing; e) Name and address of the laboratory where the tests will be performed; f) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, to be tested shall be delivered and stored in original containers bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coating material; b) Coating Manufacturer name; c) Colour of the coating material; d) Batch number of each product; e) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide the selected laboratory with the following information: Product Data Sheet (PDS); Material Safety Data Sheet (MSDS); Date of issue of PDS; Date of issue of MSDS; Name of Coating Manufacturer; Name and type of the product; Factory of origin; Batch number; Shelf life; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 5 of 10
Physical state of delivered product; Packaging; Storage condition; Sieve analysis; Gel time; Specific gravity; Moisture content; Glass Transition (T g ) temperature; Bend test; Finger printing Infrared scans of each component of a coating material with and without pigment and of coating fully cured. Coating Manufacturers Product Quality Manager shall certify the finger printing, reporting the method and resolution used. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer, including and listed in Table 1. The epoxy powder shall meet the value limits for the properties listed in following table:
Table 1 Epoxy Powder Properties Property Test Method Acceptance criteria Density NACE RP0394 Appendix B As per Coating Manufacturers specification 3,5% Particle Size 2% max retained on 150 m (100 mesh) sieve; 0,1 % max retained on 250 m (60 mesh) sieve; Shelf life NACE RP0394 Appendix C As per Coating Manufacturers recommendation Gel Time NACE RP0394 Appendix D As per Coating Manufacturers specification 20% Cure Cycle As per Coating Manufacturer Capable of cure at temperatures below 275C; time: as per Coating Manufacturer recommendation. Glass Transition (T g ) Temperatures NACE RP0394 Appendix E As per Coating Manufacturers recommendation Heat of reaction NACE RP0394 Appendix E As per Coating Manufacturers s recommendation Moisture content NACE RP0394 Appendix F 0,5 % max Total volatile Content NACE RP0394 Appendix G 0,6 % max Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 6 of 10
3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe and steel panels) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples As general rule the tests shall be performed on carbon steel samples having following dimension: a) Pipe section: Length 700 mm, Diameter 150-300 mm (6-12), Wall Thickness 4 mm minimum; b) Panels: 300 x 300 mm, Thickness 5 mm. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Where dimensions of steel samples reported in this item differ from those reported in the standard NACE RP0394, the requirements laid in the standard NACE RP0394 shall apply. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5, and 6 of this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0 including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and to the same application parameters (e.g. DFT). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.4.2 Qualification tests Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 2. 3.5 FINAL REPORTING OF LAB At completion of all tests a detailed report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 7 of 10
Table 2 Test to be performed on coated steel samples Test Type Standard/Method NACE RP0394 Acceptance criteria Cathodic Disbonding (24 h) Appendix H Max. radius: 8 mm Cathodic Disbonding (28 d) Appendix H Max. radius: 10 mm Chemical Resistance Appendix I No blistering Cross-Section Porosity Appendix J Rating of 1 to 3 Interface Porosity Appendix K Rating of 1 to 4 Flexibility Appendix K No cracks, tears or delamination Impact Resistance Appendix L 1,5 J min Strain Polarization Appendix M No cracking Thermal Analysis (Differential Scanning Calorimetry) Appendix E As per Coating Manufacturers recommendations Hot Water Soak Appendix N A rating of 1 to 3, inclusive Abrasion Appendix O Max. 300 mg Penetration ASTM G 17 at 93C Less than 10% 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be performed in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; c) The need, where applicable, for special application equipment. The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application; At completion of the application test, all the checks listed in Table 4 shall be performed; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 8 of 10
Table 3 Production test Requirements Test Test Method NACERP0394 Acceptance Criteria Cathodic Disbonding (24 h) Appendix H Max radius: 12mm (1)
Flexibility Appendix K No cracks, tears, or delamination (1)
Hot water Soak Appendix N Rating of 1 to 3, inclusive (1)
Interface Contamination Appendix P Max 30% (2)
Cross-Section Porosity Appendix J Rating of 1 to 3, inclusive (2)
Thermal Characteristics Appendix E T g of 5C, max or 95% conversion H minimum (3)
Impact Resistance Appendix L 1,5 J minimum (3)
(1) The failure of this tests shall be grounds for rejection of all pipe coated after the previous acceptable test and prior to the next acceptable test result. (2) The failure of this test shall be grounds for requiring changes to the application process parameters. (3) This test is required only when specified by the Company. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The preheat temperature shall be kept between 35C and 50C; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with the specific functional requirements reported in Item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3 COATING APPLICATION Coatings shall be applied in accordance with the functional requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and with the Coating Manufacturers recommendations as defined in Section 7 of standard NACE RP0394. Powder recycling shall be allowed up to a proportion of 10%, suitable mixed with fresh powder. The recycled powder shall be clean and passed through a magnetic filter to remove metallic particles and through a 120 mm sieve to remove all aggregates. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 9 of 10
5.3.1 Coating Thickness The Dry film thickness (DFT) shall be 360 (50) m and the absolute minimum thickness shall not be less 310 m. Coating thickness shall be measured fully in accordance with the requirements of Item 5.3.3.2 of standard NACE RP0394. 5.4 CUT BACK The pipe surface shall be left bare (uncoated) at both ends of the pipe for (150 20) mm distance from the ends. For fittings and components cut back shall be specified and approved by the Companys Representative. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of coating. Once the coating operations are completed, cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contract documents, must be approved by the Companys Representative. 5.5 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping. Coating used to repair the defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to Section 9 of standard NACE RP0394 and method submitted to the Company for approval beginning of the production. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix F - Page 10 of 10
6.2.1 Tests during the works progress and final inspection Contractor shall perform during the works progress and at completion of the work all inspections and tests reported in Table 4:
Table 4 Inspection during work progress Test Test method Frequency Surface Preparation ISO 8501-1 Continuously Surface Profile ISO 8503-1 Once per four hour Surface Inspection - Each pipe Application Temperature - Each pipe Application criteria - Systematically during any application Coating Thickness - 3 location on each pipe (The acceptance criteria of the test shall be in accordance with the provisions of item 8.3.3.7 of standard NACE RP0394) Holiday inspection NACE RP0490 Each pipe (The acceptance criteria of the test shall be in accordance with the provisions of item 8.3.3.8 of standard NACE RP0394) Production Test Rings - At minimum one sample for each of the lots defined in paragraph 8.3.4 of standard NACE RP0394 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. Eni S.p.A. Exploration & Production Division FUNCTIONAL SPECIFICATION APPENDIX G FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF ANTICORROSIVE FILLER MASS ON WELDED JOINTS AREAS OF STEEL PIPES AND COMPONENTS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 2 of 11
CONTENTS APPENDIX G....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 OPERATIVE ENVIRONMENT............................................................................................ 3 1.4 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 4 3.1 GENERAL CRITERIA......................................................................................................... 4 3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING...................... 4 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 4 3.3.1 Labelling.............................................................................................................................. 4 3.3.2 Required product information.............................................................................................. 4 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 6 3.4.1 Preparation of steel samples .............................................................................................. 6 3.4.2 Qualification tests................................................................................................................ 7 3.5 FINAL REPORTING OF LAB.............................................................................................. 8 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 8 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 8 5.1 PREHEAT........................................................................................................................... 8 5.2 SURFACE PREPARATION................................................................................................ 8 5.3 COATING APPLICATION................................................................................................... 8 5.3.1 General ............................................................................................................................... 8 5.3.2 Application method ............................................................................................................. 8 5.3.3 Coating thickness................................................................................................................ 9 5.4 REPAIR OF DEFECTS....................................................................................................... 9 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE........... 9 6.1 GENERAL........................................................................................................................... 9 6.2 QUALITY CONTROL PLAN................................................................................................ 9 6.2.1 Tests during the works progress and final inspection......................................................... 9 7 DOCUMENTATION AND REPORTING........................................................................... 10
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 3 of 11
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. Moreover, the Companys additional functional requirements for qualification and application of the coating are defined reported. 1.2 SCOPE This Appendix defines the minimum functional requirements for pre-qualification, supply and application of anticorrosion filling mass of polyurethane base, that shall be applied immediately before pipe laying for refilling and protection of the weld of the steel pipes and component. 1.3 OPERATIVE ENVIRONMENT External polyurethane mass coating can be used for the protection of buried or submerged tubes service and suitable for the following maximum service temperature: From 20 to +80C for applications at ambient temperature or medium temperatures (standard coating); From 20 to +120C for high temperatures offshore application (thermal stabilised coating); From 20 to +110C for high temperatures onshore buried pipelines (thermal stabilised coating). 1.4 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered by this Appendix are based on polyurethane resins and special fillers with regulating density. The product may be formed by a base component, a hardening agent, filler and an accelerator (if applicable). As general guide, the coating shall be applied with a Dry Film Thickness (DFT) in the range of 10 to 500 mm. Application can be made by extrusion or by gravity casting, into a metal mould positioned around the welded joint pneumatically or by hand. The final coating shall have a continuous and uniform film free of sags, runs or any other visible defect. The Dry Film Thickness shall be selected in consideration of the product and intended service operation. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 4 of 11
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by the Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coatings materials forming a coating system is changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 DOCUMENTATION FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The documentation forwarded to the Company shall include all data listed in Table 1 In addition the following data must be provided: a) Material Safety Data Sheet of each component; b) Application method; c) Coating system description; d) Finger printing Infrared scans of each component of a coating material with and without pigment. Coating Manufacturers Product Quality Manager shall certify the finger printing; e) Name and address full style of the laboratory where the tests will be performed; f) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent or thinner to be tested shall be delivered and stored in original container bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coating material (Base, Hardener, Filler, Accelerator); b) Coating Manufacturer name; c) Colour of the coating material; d) Batch number of each component (Base, Hardener, Accelerator); e) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide the selected laboratory with the following information: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 5 of 11
Product Data Sheet (PDS); Material Safety Data Sheet (MSDS); Date of issue of PDS; Date of issue of MSDS; Name of Coating Manufacturer; Name and type of the products; Date of manufacture; Factory of origin; Batch number; Shelf life; Colour of the mixed product; Method of application; Physical state of delivered product; Method of application; Solids content; Specific gravity; Packaging; Storage condition; Pot life; Shelf life; Surface preparation; Mixing ratio (by weight); Mixing instructions; Recommended cleaning solvent(s); Recommended instruction for application; Range of application temperature (ambient, pipe and product) and humidity; Range of service temperature; Recommended minimum and maximum DFT; Specific curing requirements; Time to complete curing; De-moulding time; Specific gravity; Viscosity of the base and curing agent according to standard ISO 2555 at temperature of 5, 15, 25, 35 and 40C; Finger printing Infrared scans of each component of a coating material with and without pigment and of coating fully cured. Coating Manufacturers Product Quality Manager shall certify the finger printing, reporting the method and resolution used; Thermal analysis, reporting the method used: Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 6 of 11
Curve of curing reaction with temperature scan from ambient temperature to the end of reaction; Glass Transition (T g ) temperature; Scan speed (C/min); Temperature at the beginning of the reaction, max temperature at the end of the reaction and heat content. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The tests shall be performed both for the base and the curing agents. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer. 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in other suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples The tests shall be performed on carbon steel samples as described in the following items. 3.4.1.1 Steel pipes samples Since one of the main scope of the qualification tests of weld field joint coating is to ascertain its compatibility with shop applied coating, steel pipes samples must be coated with one or more system listed in Table 1 and for which the Coating Manufacturer of weld field joint coating requires the qualification. The length of the coated steel pipe shall be such as to assure that the length of the test zones is equivalent to the field joint coating plus the overlap areas. The minimum acceptable dimension of coated steel pipe sections is: Length 1000 mm, Diameter 150 mm (6), and Wall thickness 5 mm. The test zone shall be free of any coating and a girth cap weld shall be added at the centre of it in order to mimic the field weld. The time for coating application on a test zone shall not exceed the estimated field joint coating time on shop, yard, on the barge, etc. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 7 of 11
3.4.1.2 Steel panels Where applicable, the dimension of steel panels sample shall be: 300 x 300 mm, Thickness 5 mm. 3.4.1.3 General For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5, and 6 of this Appendix and the Functional Specification 20550 PIP.COR.FUN. Rev. 0 including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and to the same application parameters (e.g. DFT). The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.4.2 Qualification tests Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are reported in Table 1.
TABLE 1 Test to be performed on coated steel samples Test Type Standard/Method Acceptance criteria Compression strength ASTM D 695 45 Mpa Sea water resistance 25 cm 3 specimen immerged in sea water for 1000 hours at temperatures varying from 18C to 40C No loss in properties. No significant water absorption Impact resistance Cylindrical specimen, 60 mm. diameter 60 mm. high, under a 5 kg sphere falling from 1,5 m No breaks No cracks Resistance to temperature changes Cubic specimen, 60 mm side, exposed to 10 cycles as follows 1 hour in 90C 1 hour in 0 C refrigerator No variation in any one dimension, no loss in properties Thermal resistance dimensional stability Cubic specimen, 60 mm side, exposed 4 hours at 135C No variation in any one dimension Apparent density ASTM D 1622 1500 Kg/m 3 1,5 % Cathodic disbonding ASTM G8 Max 9 mm Tensile strength ASTM D 638 Average 11 MPa Resistance to bacterial attack
No variation compared to the not buried samples De-moulding time 5 min.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 8 of 11
3.5 FINAL REPORTING OF LAB At completion of all tests a detailed report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems, a practical test shall be performed in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instruction provided by Coating Manufacturer; c) The need, where applicable, for special application equipment. The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. Company can required additional specific tests if consider necessary for a particular project. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PREHEAT The equipment used for preheating the pipes shall be approved by the Company. If the Contractor uses for preheating purposes free open flames in direct contact with the pipe surface, the surface shall be kept in motion in respect to the flame at a minimum rate of 10 mm/s, along a helically winding path. The flame shall also be adjusted in its combustion ratio so that soot or other combustion products are not deposited on the metal. All measures shall be taken and developed by the Contractor in order to avoid possible stoppages of the line resulting in the steel being brought to uselessly or damagingly high temperatures. The pipe shall be preheated to at least 5 C above the dew point to remove the presence of moisture prior to surface cleaning; it shall be checked at least three times for every work shift (at start, middle, and end) and whenever stoppages occur in the production line. All temperature measurements shall be recorded on the production certificate. 5.2 SURFACE PREPARATION Surface preparation shall be performed fully in accordance with specific functional requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3 COATING APPLICATION 5.3.1 General Coatings shall be applied fully in accordance with the Coating Manufactures recommendations and to the specific functional requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.3.2 Application method As general requirements the coating mass shall be applied either by extrusion or by gravity casting, into a metal mould positioned around the weld joint pneumatically or by hand. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 9 of 11
The filling mass shall be introduced in the mould by extrusion equipment that automatically doses and mixes the components, or by direct casting from a container of the previously dosed and thoroughly stirred component mix. The extrusion equipment shall include all the component suitable to perform a correct application according to the Coating Manufacturer recommendation 5.3.3 Coating thickness The minimum and maximum coating thickness shall be in accordance with the characteristic of the product and intended service operation. The minimum and maximum coating thickness shall be in accordance with Coating Manufacturers recommendation. 5.4 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that may occur during or after the application. Coating used to repair of defects and damages shall be supplied by the same Coating Manufacturer of the original Coating system. Any repair shall be performed according to Coating Manufacturer recommendations and the method submitted to the Company for approval before the beginning of the production. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections. 6.2.1 Tests during the works progress and final inspection Contractor shall perform during the works progress and at completion of the work all inspections and tests reported in the Table 2. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 10 of 11
7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix G - Page 11 of 11
Table 2 Nature and frequency of testing and control Properties Test method Acceptance Criteria Frequency Surface condition before blasting - Every weld joint Steel imperfection ISO 8501-3 Grade P3 Every weld joint Dimensions, shape and properties of abrasive blasting material ASTM D-4940- 150 S/cm Chloride content < 25 ppm Twice per shift Cleaning before abrasive blasting SSPC-SP1 Free of oil, grease, etc. Every weld joint Degree of abrasive blasting ISO 8501-1 Sa 2,5 Every pipe Degree of cleanliness (dust level) ISO 8502-3 < Class 2 First 10 weld joint and 4 time per shift Roughness of the blast cleaned surface - 60 R z 80 m Once per shift Relative Humidity and Dew Point ISO 8502-4 RH < 85% 4 time per shift Steel temperature 3C above dew point 4 time per shift Temperature of heating before coating IR camera recording As per Coating Manufacturer Every weld joint Appearance and continuity Visual Free of defects Every weld joint Thickness of the coating system - As per requirement First 10 pipes and 1 per hour
Eni S.p.A. Exploration & Production Division
FUNCTIONAL SPECIFICATION APPENDIX H FUNCTIONAL REQUIREMENTS FOR THE QUALIFICATION AND APPLICATION OF PROTECTIVE COATING ON EXTERNAL WELD JOINTS OF ONSHORE AND OFFSHORE PIPELINES 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 2 of 11
CONTENTS APPENDIX H....................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 2.1 TYPES OF FIELD JOINT COATINGS................................................................................ 3 2.2 CRITERIA FOR COATING SELECTION............................................................................ 4 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 4 3.1 GENERAL CRITERIA......................................................................................................... 4 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING......................... 4 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 5 3.3.1 Labelling.............................................................................................................................. 5 3.3.2 Required product information.............................................................................................. 5 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 6 3.4.1 Preparation of steel samples .............................................................................................. 6 3.4.2 Qualification tests................................................................................................................ 7 3.5 FINAL REPORTING OF LAB.............................................................................................. 7 3.6 PRACTICAL APPLICATION TEST IN THE SHOP............................................................. 7 4 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 7 4.1 SURFACE PREPARATION................................................................................................ 7 4.1.1 General ............................................................................................................................... 7 4.1.2 Power tool cleaning............................................................................................................. 7 4.1.3 Abrasive blasting tool cleaning ........................................................................................... 7 4.1.4 Overlapping areas............................................................................................................... 8 4.2 COATING APPLICATION................................................................................................... 8 4.2.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) ................................................ 8 4.3 REPAIR OF DEFECTS....................................................................................................... 8 5 SPECIFIC REQUIREMENTS FOR COATING APPLICATION ......................................... 9 5.1 HEAT-SHRINKABLE MATERIALS APPLICATION............................................................ 9 5.2 POLYMERIC PLASTIC TAPES.......................................................................................... 9 5.3 FUSION-BONDED EPOXY POWDER............................................................................... 9 5.4 INJECTION APPLIED POLYPROPYLENE........................................................................ 9 5.5 INJECTION APPLIED POLYURETHANE ........................................................................ 10 5.6 LIQUID EPOXY RESIN (TAR FREE) ............................................................................... 10 5.7 LIQUID POLYURETHANE (TAR FREE) .......................................................................... 10 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE......... 10 6.1 GENERAL......................................................................................................................... 10 6.2 CHECKS INSPECTION AND TESTING........................................................................... 10 6.2.1 Tests during the works progress and final inspection....................................................... 10 7 DOCUMENTATION AND REPORTING........................................................................... 11
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 3 of 11
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. Moreover, the Companys additional functional requirements for pre-qualification and application of the coatings are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, selection, supply and application of the external weld field joint coatings. The coatings for weld field joint coatings shall ensure the suitable corrosion protection and coating continuity to the steel pipes surface left bare (uncoated) during coating application on shop. They are applied when pipes are joined by welding to form pipelines used for onshore or offshore oil, gas or water transportation. 1.3 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS Weld field joints shall be protected with a coating system compatible with the coating already applied on the pipes and allow suitable application under the conditions expected to be faced on the field. 2.1 TYPES OF FIELD JOINT COATINGS The coatings for weld joints considered in this Appendix are listed in Table 1.
TABLE 1 TYPE OF FIELD JOINT COATINGS Heat-shrinkable materials Polymeric plastic tapes Fusion-bonded epoxy powder Injection applied polypropylene Injection applied polyurethane Liquid epoxy resin (tar free) Liquid polyurethane (tar free) Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 4 of 11
2.2 CRITERIA FOR COATING SELECTION The external coatings for the corrosion protection of steel pipes and components provided by Functional Specification 20550.PIP.COR.FUN. Rev.0 are defined in the various appendixes as follows: Appendix A: Liquid epoxy and epoxy-modified coating; Appendix B: Liquid polyurethane and polyurethane-modified coating; Appendix C: Three layers extruded polyethylene (PE) coating; Appendix D: Three layers extruded polypropylene (PP) coating; Appendix F: Epoxy Powder (FBE) coating. The field joint coatings has to satisfied the following requirements: a) It must be compatible with one or more coating provided by the above Appendixes; b) It must be resistant to the service temperature of the pipeline; c) It must be suitable for the application condition and process provided on the various fields. 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by the Item 2.4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, included those provided for repair, subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system shall be changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests; b) Coating system characterisation tests. 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The application documentation shall include all data concerning each weld field joint coating for which the pre-qualification is required, including, but not limited to: a) Name of the coating system; b) Product Data Sheet; c) Code of the coating as listed in Table 1 of this Appendix; d) Compatibility of the proposed coating with the coating system provided in the Appendixes of Functional Specification 20550 PIP.COR.FUN. Rev.0; e) Finger printing (where applicable) Infrared scans of each component of a coating material with and without pigment. Coating Manufacturers Product Quality Manager shall certify the finger printing; Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 5 of 11
f) Application procedures; g) Material Safety Data Sheet of each component; h) Name and address of the laboratory where the tests will be performed; i) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated, coating type applied on the pipeline. 3.3 COATING MATERIALS CHARACTERISATION TEST The characterisation test of the coating materials and coating systems for weld joint have to satisfy the requirements reported in Table 2.
TABLE 2 Characterisation tests TYPE OF COATING CHARACTERISATION Heat-shrinkable materials As per Appendix E requirements Polymeric plastic tapes As per Appendix E requirements Fusion-bonded epoxy powder As per Appendix F requirements Injection applied polypropylene As per Appendix D requirements Injection applied polyurethane As per Appendix G requirements Liquid epoxy resin (tar free) As per Appendix A requirements Liquid polyurethane (tar free)
As per Appendix B requirements 3.3.1 Labelling Each coating material, solvents and thinners to be tested shall be delivered and stored in original container bearing the Coating Manufacturers label, clearly showing following information: a) Coating manufacturer name; b) Name and complete identification of product including factory origin; c) Reference to applicable coating standards; d) Colour of the coating material; e) Batch number of each component; f) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, Coating Manufacturer shall provide the selected laboratory with the information detailed in each relevant Appendix and related to the different field joint coating system. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 6 of 11
For two-pack products, the tests shall be performed both for the base and the curing agents. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer for each coating as required in Table 2. 3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing, where applicable, and application instruction. The Coating Manufacturer shall also supply a sufficient number of test samples (e.g. pipe and/or steel panels) as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and relevant Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and relevant Appendix are carefully followed. The selected laboratory shall supervise, record and report all coating work steps. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples The tests shall be performed on carbon steel samples as described in the following items. 3.4.1.1 Steel pipes samples Since one of the main scope of the qualification tests of weld field joint coating is to ascertain its compatibility with shop applied coating, steel pipes samples must be coated with one or more system listed in Table 1 and for which the Coating Manufacturer of weld field joint coating requires the qualification. The length of the coated steel pipe shall be such as to assure that the length of the test zones is equivalent to the field joint coating plus the overlap areas. The minimum acceptable dimension of coated steel pipe sections is: Length 1000 mm, Diameter 150 mm (6), and Wall thickness 5 mm. The test zone shall be free of any coating and a girth cap weld shall be added at the centre of it in order to mimic the field weld. The time for coating application on a test zone shall not exceed the estimated field joint coating time on shop, yard, on the barge, etc. 3.4.1.2 Steel panels Where applicable, the dimension of steel panels sample shall be: 300 x 300 mm, Thickness 5 mm. 3.4.1.3 General For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Samples shall be cleaned and coated with the complete weld field joint coating, according to all requirements provided by this Appendix and Functional Specification 20550 PIP.COR.FUN. Rev. 0 including, but not limited, to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method (brush, spatula, airless spray, etc.) for which the qualification is required and to the same application parameters. The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 7 of 11
3.4.2 Qualification tests Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The tests to be performed and the acceptance criteria are detailed in the items related to the different field joint coating system. 3.5 FINAL REPORTING OF LAB At completion of all tests a detailed report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. 3.6 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be perform in the shop in order to ascertain: a) The applicability of the coating material; b) The correctness and suitability of the instructions provided by Coating Manufacturer; c) The need, where applicable, for special application equipment; The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problem, if any, faced during the application. 4 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION The requirements listed in the following items are common to all field joint coatings. 4.1 SURFACE PREPARATION 4.1.1 General Surface preparation shall be performed in accordance with Coating Manufacturer recommendations and with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev.0 and related applicable Appendix. At the time of coating application, the surface to be coated shall be dry, clean and free of any foreign material and contaminants. Any steel and welding imperfection shall be removed to comply with the grade P2 of standard ISO 8501-3. After removal of the steel imperfections, the thickness of the steel pipe shall comply with the minimum tolerance requirements of the pipe standard. 4.1.2 Power tool cleaning Power tool cleaning shall be performed according to standard ISO 8504-2 in order to comply with grade Sa 2,5 of standard ISO 8501-1. The roughness of the cleaned surface shall be in accordance with Coating Manufacturer recommendations. 4.1.3 Abrasive blasting tool cleaning Abrasive blasting shall be performed according to standard ISO 8504-3 in order to comply with grade St3 of standard ISO 8501-1. The roughness of the cleaned surface shall be in accordance with Coating Manufacturer recommendations. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 8 of 11
4.1.4 Overlapping areas The shop-applied coating close to the field joint to be coated shall be prepared and abraded to assure the suitable adhesion of the field joint coating. The method shall be in accordance with Coating Manufacturer recommendations. In consideration of the type of shop-applied coating and the field joint coating the dimension overlap area shall be according to the figure listed in Table 3.
TABLE 3 Overlapping FIELD JOINT COATING OVERLAP DIMENSION Heat-shrinkable materials 100 mm Polymeric plastic tapes 70 mm Fusion-bonded epoxy powder 50 mm Injection applied polypropylene 70 mm Injection applied polyurethane 70 mm Liquid epoxy resin (tar free) 50 mm Liquid polyurethane (tar free)
50 mm 4.2 COATING APPLICATION The steel temperature of field joint shall be 3C above the dew point and within the range of Coating Manufacturer recommendations. Field joint temperature must be checked with suitable instrument in order to meet the application conditions (steel temperature and shop-applied coating) recommended by Coating Manufacturer. As general rule coating application shall be done according to the general requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and related Appendixes. In particular Coating Manufacturers recommendation reported in the product data sheet shall be followed. In case an additional mechanical resistance is required, the provisions of Appendix I of Functional Specification 20550 PIP.COR.FUN Rev. 0 shall apply. 4.2.1 Wet Film Thickness (WFT) and Dry Film Thickness (DFT) Where applicable, Wet Film Thickness and Dry Film Thickness for each type of coating provided by this appendix shall be in accordance with Coating Manufacturer recommendations. 4.3 REPAIR OF DEFECTS The Contractor shall repair all coating defects and damages that will occur during the coating application or at its completion. Coating used for repair of defects and damages shall be supplied by the same Coating Manufacturer of the original Coating system. Any repair shall be performed according to Coating Manufacturers recommendation reported in the product data sheet. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 9 of 11
5 SPECIFIC REQUIREMENTS FOR COATING APPLICATION 5.1 HEAT-SHRINKABLE MATERIALS APPLICATION Heat-shrinkable materials may be applied without or with a liquid epoxy primer, depending on the nature of adhesive. If required the application of epoxy primer shall be made according to the requirement of Table 7 of standard EN 12068 (ref. Appendix E of Functional Specification 20550 PIP.COR.FUN. Rev.0). For the application of heat-shrinkable materials, in addition to the provision of Appendix E of Functional Specification 20550 PIP.COR.FUN. Rev.0, as general guide the following procedure shall be implemented: When the welding joint has been completed the area shall be cleaned as specified; Area to be coated shall be heated to 70C; The shrinkable sleeve must be positioned so as to provide a 100 mm overlap on both sides of the shop-applied coating suitably abraded to assure the good adhesion when shrinking is completed; By external side heat sleeve to a surface temperature adapted to the specific product to be applied (from 90 to 240C) with a hot air ring unit or a gas torch. Heat progressively and regularly, starting from the middle of the sleeve and going towards the ends to avoid forming air pockets. 5.2 POLYMERIC PLASTIC TAPES Polymeric plastic tape may be applied without or with a liquid epoxy primer, depending on the nature of adhesive. If required the application of epoxy primer shall be made according to the requirement of Table 7 of standard EN 12068 (ref. Appendix E of Functional Specification 20550 PIP.COR.FUN. Rev.0). For the application of polymeric plastic tape, in addition to the provision of Appendix E of Functional Specification 20550 PIP.COR.FUN. Rev.0, as general guide the following procedure shall be implemented: When the welding joint has been completed the area shall be cleaned as specified; Apply a thin coat of compatible primer, if any, and allow the primer to dry. Spirally wrap the area with tapes of a sufficient width, using the right overlap (no less than 50%) and sufficient tension to ensure a complete adhesion of the coating. Suitable hand tools shall be used to achieve a suitable coating application (e.g. cigarette wrapping may be used in certain circumstances). In any case overlapping shall be made according to Coating Manufacturer recommendations. 5.3 FUSION-BONDED EPOXY POWDER The application of fusion bonded epoxy powder (FBE) on field joints shall be made fully in accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix F. 5.4 INJECTION APPLIED POLYPROPYLENE Injection applied polypropylene coating system consists of: An epoxy primer coat, which if in form of powder can be applied by dusting or by electrostatic spray, if liquid it can be applied by spraying. No primer must be applied to shop-applied coating. One coat of modified polypropylene powder applied by spraying. The coating thickness is obtained injecting polypropylene in a suitable mould. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 10 of 11
Suitable heating system and process shall be used to obtain the proper adhesion of the field joint coating on the shop-applied coating. 5.5 INJECTION APPLIED POLYURETHANE The application of injection applied polyurethane on field joints shall be made fully in accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix G. 5.6 LIQUID EPOXY RESIN (TAR FREE) The application of liquid epoxy resin on field joints shall be made fully in accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix A. 5.7 LIQUID POLYURETHANE (TAR FREE) The application of liquid polyurethane resin on field joints shall be made fully in accordance with the provisions of Functional Specification 20550 PIP.COR.FUN Rev.0, Appendix B. 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL The additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. 6.2 CHECKS INSPECTION AND TESTING Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity; b) Description of the test; c) Applicable reference documents; d) Applicable check procedures and methods; e) Acceptability criteria; f) Frequency of the checks; g) Persons required to be present at the inspections; 6.2.1 Tests during the works progress and final inspection Contractor shall perform during the works progress and at completion of the work all inspections and tests reported in the items related to the different field joint coating system. The specific requirements provided in the Appendixes listed in Table 2 and item 4 of Functional Specification 20550.PIP.COR.FUN Rev. 0 shall be fully followed unless otherwise specified by the Company. As general rule, the Contractor shall perform during the work progress and at completion of it at least the inspection and test reported in Table 4. The feasibility of the test listed in Table 4 is related to the specific site condition of the project such as production rate, location etc. In any Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix H - Page 11 of 11
case all data concerning each inspection step, or the reasons for that it has not been performed, shall be permanently recorded in report or logbook. 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.
Table 4 Inspection during the work progress Test Method of test Frequency Surface preparation ISO 8501-1 Each weld joint Roughness of the blast cleaned surface of the weld joint ISO 8503-1 Checks number to be agreed with the Company Temperature of the surface to be coated - Each weld joint Thermo-hygrometric condition - Three times per shift and any time the condition changed Application criteria - Systematically during any application Visual inspection of the coating - Each weld joint Inspection of the thickness - Once per shift Holiday detection test NACE RP 0274 Each weld joint Adhesion test DIN 30671 Checks number to be agreed with the Company Cathodic disbonding DIN 30671 Checks number to be agreed with the Company
Eni S.p.A. Exploration & Production Division
FUNCTIONAL SPECIFICATION APPENDIX I FUNCTIONAL REQUIREMENTS FOR QUALIFICATION AND APPLICATION OF POLYURETHANE THERMAL INSULATION SYSTEMS TO PIPE AND ASSEMBLY OF INSULATED PIPES, VALVES AND FITTINGS 20550 PIP.COR.FUN
Rev. 0 - February 2004
ENGINEERING COMPANY STANDARD Documento riservato di propriet di Eni S.p.A. Divisione Agip. Esso non sar mostrato a Terzi n utilizzato per scopi diversi da quelli per i quali stato inviato. This document is property of Eni S.p.A. Divisione Agip. It shall neither be shown to Third Parties not used for purposes other than those for which it has been sent. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 2 of 12
CONTENTS APPENDIX I......................................................................................................................................... 1 1 GENERAL........................................................................................................................... 3 1.1 INTRODUCTION................................................................................................................. 3 1.2 SCOPE................................................................................................................................ 3 1.3 OPERATIVE ENVIRONMENT............................................................................................ 3 1.4 REFERENCE STANDARDS............................................................................................... 3 2 GENERAL COATING CHARACTERISTICS..................................................................... 3 2.1 CHARACTERISTIC OF THE PRIMER............................................................................... 4 2.2 CHARACTERISTIC OF THE POLYURETHANE RIGID FOAM (PUR) .............................. 4 2.3 CHARACTERISTIC OF THE CASING............................................................................... 4 3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM.......................... 5 3.1 GENERAL CRITERIA......................................................................................................... 5 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING......................... 5 3.3 COATING MATERIALS CHARACTERISATION TEST...................................................... 6 3.3.1 Labelling.............................................................................................................................. 6 3.3.2 Required product information.............................................................................................. 6 3.4 COATING SYSTEM CHARACTERISATION TESTS......................................................... 7 3.4.1 Preparation of steel samples .............................................................................................. 8 3.5 QUALIFICATION TESTS.................................................................................................... 8 3.6 FINAL REPORTING OF LAB.............................................................................................. 8 4 PRACTICAL APPLICATION TEST IN THE SHOP ........................................................... 9 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION................................... 9 5.1 PIPE ASSEMBLY ............................................................................................................... 9 5.1.1 Surface preparation ............................................................................................................ 9 5.1.2 Coating Application............................................................................................................. 9 5.1.3 Thickness of the coating system......................................................................................... 9 5.1.4 Centre line deviation ........................................................................................................... 9 5.1.5 Cut back............................................................................................................................ 10 5.1.6 Repair of defects............................................................................................................... 10 5.2 FITTINGS ASSEMBLIES.................................................................................................. 10 5.2.1 Surface preparation .......................................................................................................... 10 5.2.2 Thickness of the coating system....................................................................................... 10 5.2.3 Centre line deviation ......................................................................................................... 10 5.2.4 Cut back............................................................................................................................ 10 5.2.5 Angular between casing segments of bend and minimum length .................................... 10 5.2.6 Polyethylene welding ........................................................................................................ 11 5.2.7 Increase of the diameter of the casing pipe...................................................................... 11 5.2.8 Minimum insulation thickness in bends ............................................................................ 11 5.2.9 Tolerance of the main fitting dimensions .......................................................................... 11 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE......... 11 6.1 GENERAL......................................................................................................................... 11 6.2 QUALITY CONTROL PLAN.............................................................................................. 11 7 DOCUMENTATION AND REPORTING........................................................................... 12
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 3 of 12
1 GENERAL 1.1 INTRODUCTION This Appendix is an integral part of the Functional Specification 20550 PIP.COR.FUN. Rev. 0 and for no reason can be used separately. All requirements, standards and articles reported in the Functional Specification 20550 PIP.COR.FUN. Rev. 0 are fully applicable to this Appendix. It refers to the following European Standards: EN 253 (District heating pipes Preinsulated bonded pipe system for directly buried hot water networks Pipe assembly of steel service pipe, polyurethane thermal insulation and outer casing of polyethylene) EN 448 (District heating pipes Preinsulated bonded pipe system for directly buried hot water networks Fitting assemblies of steel service pipe, polyurethane thermal insulation and outer casing of polyethylene) Moreover, the Companys additional functional requirements for pre-qualification and application of the coating are defined. 1.2 SCOPE This Appendix defines the minimum functional requirements for qualification, supply and application for straight lengths and fittings assemblies (e.g. bends, T-pieces, reducers and anchor) of prefabricated thermal insulated pipe-in-pipe assemblies, comprising as steel service pipe from DN 20 to DN 1200, rigid polyurethane foam insulation and an outer casing of polyethylene as defined in item 1 of standard EN 253 and item 1 of standard EN 448. 1.3 OPERATIVE ENVIRONMENT Polyurethane thermal insulation and outer casing of polyethylene coating can be used for the protection of buried or submerged pipes and fittings for continuous service at various temperatures up to 120C and occasionally with a peak temperature up to 140C as defined in item 1 of standard EN 253. 1.4 REFERENCE STANDARDS This Appendix refers to the most recent version of the standards listed in the Functional Specification 20550 PIP.COR.FUN. Rev. 0. All listed standards become an integral part of this Appendix and all related contractual documents. It is Contractors duty to have copies of the standards applicable to each project and provide copies of each relevant standard whenever work takes place. Contractor shall provide evidence of provision of standards to the Company before work begins and during each inspections step. 2 GENERAL COATING CHARACTERISTICS The coating systems considered in this Appendix consist of three layers as follows: 1 st layer Liquid Epoxy Primer (DFT not less 250 m) 2 nd layer - Polyurethane rigid foam (PUR) 3 rd layer - Polyethylene outer casing The characteristics of the coatings materials are applicable to pipe assembly and to fitting assemblies and shall meet the requirements of standard EN 253. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 4 of 12
2.1 CHARACTERISTIC OF THE PRIMER The 1 st layer (Primer) shall be formed by a liquid epoxy or powder epoxy primer completely compatible with the polyurethane rigid foam and shall meet the characteristics specified in the Table 1.
Table 1 Requirements of liquid Primer Characteristic Acceptable Criteria Dry film Thickness Not less than 150 m Solid by weight (for liquid epoxy primer) 90 Minimum operating temperature 120C
2.2 CHARACTERISTIC OF THE POLYURETHANE RIGID FOAM (PUR) The 2 nd layer (polyurethane rigid foam) shall be formed by a polymer and shall meet the requirements listed in Table 2:
Table 2 Requirements of Polyurethane Rigid Foam for pipe assembly and fittings Characteristic Standard Units Acceptable Criteria Cells structure EN 253 item 4.4.2 % Closed cells content 88 Foam density EN 253 item 4.4.3 Kg/m 3 60 Compressive strength EN 253 item 4.4.4 MPa 0,3 Water absorption at elevated temperature EN 253 item 4.4.5 % Volume 10
2.3 CHARACTERISTIC OF THE CASING The 3 rd layer (polyethylene outer casing) shall provide complete protection from water moisture and the suitable strength necessary for handling and laying the insulated pipe. The polyethylene outer casing shall meet the requirements listed in the Table 3.
Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 5 of 12
Table 3 Requirements of Polyethylene Outer Casing for pipe assembly and fittings MATERIAL PROPERTIES Characteristic Standard Acceptable Criteria Density EN 253 item 4.3.1.1 944 Kg/m 3
Black content EN 253 item 4.3.1.1 2,5 % 0,5 Melt flow rate EN 253 item 4.3.1.2 0,58 g/10 min (when tested according to EN 1133) Thermal stability EN 253 item 4.3.1.3 20 min (when tested according to EN 278) CASING PROPERTIES Characteristic Standard Acceptable Criteria Thickness EN 253 item 4.3.2.2 In accordance with Table 5 of standard EN 253 but never less than 3 mm Appearance EN 253 item 4.3.2.4 Free of defects Elongation at break EN 253 item 4.3.2.5 350% Heat reversion EN 253 item 4.3.2.6 3% Long- term mechanical properties EN 253 item 4.3.2.7 2000 h with tensile stress of 4,0 MPa at 80C Stress crack resistance EN 253 item 4.3.2.8 300 h
3 QUALIFICATION OF COATING MATERIAL AND COATING SYSTEM 3.1 GENERAL CRITERIA All requirements provided by the item 2.4 of Functional Specification. 20550 PIP.COR.FUN. Rev. 0 must be fully followed. Qualification requirements shall apply to all coating materials and coating systems, including those provided for repair, subject of this Appendix. The Coating Manufacturer shall arrange, at its own expenses, all tests required by this Appendix. The tests shall be performed and suitably reported by independent laboratory, qualified and approved by the Company. The Company reserve the right to attend and inspect the tests execution. If the formulation of one or all coating materials forming a coating system shall be changed after the qualification test, the new coating material and coating system shall be re-qualified. Two levels of tests are requested: a) Coating materials characterisation tests b) Coating system characterisation tests 3.2 REQUIREMENTS FOR THE PRE-QUALIFICATION OF THE COATING Any Coating Manufacturer that intends to qualify one or more of its coating systems shall inform the Company in writing. The documentation forwarded to the Company shall include all data listed in following table 4. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 6 of 12
In addition the following data must be provided: a) Material Safety Data Sheet of each component b) Application method. c) Coating system description d) Name and address of the laboratory where the tests will be performed. e) Reference list of the major projects reporting at least the following information: name of the project, name of the customer, name of the applicator, year in which the work was performed, length and dimension of the pipeline coated. 3.3 COATING MATERIALS CHARACTERISATION TEST 3.3.1 Labelling Each coating material, solvent and thinner to be tested shall be delivered and stored in original container bearing the Coating Manufacturers label, clearly showing following information: a) Name of the coatings material (primer, polyurethane rigid foam, and polyethylene outer casing); b) Coating Manufacturer name; c) Batch number of each component (primer, polyurethane rigid foam, and polyethylene outer casing); d) Manufacturing date. 3.3.2 Required product information For each coating material submitted to qualification testing, the Coating Manufacturer shall provide the selected laboratory with the information listed in the following Table 4. For all data provided, the Coating Manufacturer must report the method and standard used, the figure assured and related acceptable deviations. All data and documentation provided by Coating Manufacturer shall be included as part of the final test report prepared by the laboratory. For each Batch Number three samples shall be drawn: one will be used for the analysis, while the other two will be kept, for a time not exceeding the shelf life reported on the product data sheet, for possible further checks. The selected laboratory must test the coating material in order to verify the accuracy and consistency of the data for physical properties provided by the Coating Manufacturer. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 7 of 12
Table 4 Information and data to be provided by Coating Manufacturer Item Primer Polyurethane Rigid Foam Polyethylene Outer Casing Product Data Sheet (PDS) Yes Yes Yes Material Safety Data Sheet (MSDS) Yes Yes Yes Date of issue of PDS Yes Yes Yes Date of issue of MSDS Yes Yes Yes Name of Manufacturer Yes Yes Yes Name and type of the product Yes Yes Yes Factory of origin Yes Yes Yes Batch number Yes Yes Yes Shelf life Yes Yes Yes Physical state of delivered product Yes Yes Yes Packaging Yes Yes Yes Storage condition Yes Yes Yes Viscosity Yes No No Density Yes No Yes Solid by volume Yes No No Finger printing Yes No No Viscosity Yes No No Cells structure No Yes No Foam density No Yes No Compressive strength No Yes No Water absorption at elevated temperature No Yes No Black content No No Yes Melt flow rate No No Yes Thermal stability No No Yes Long- term mechanical properties No Yes Yes Appearance No No Yes Elongation at break No No Yes Heat reversion No No Yes Stress crack resistance No No Yes
3.4 COATING SYSTEM CHARACTERISATION TESTS The Coating Manufacturer shall supply to the chosen laboratory a sufficient quantity of coating material forming the coating systems, together with detailed mixing and application instructions. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 8 of 12
The Coating Manufacturer shall also supply a sufficient number of pipe sections and as defined in the next paragraph. The laboratory shall perform the necessary coating work on the samples (surface preparation, application, inspection and reporting) fully in accordance with the requirements of Functional Specification 20550 PIP.COR.FUN. Rev. 0 and this Appendix. If the laboratory is unable to perform the coating work, it shall be the Coating Manufacturers duty to perform the work in another suitable location provided that the Company is informed and the requirements of Functional Specification and Appendix are carefully followed. The selected laboratory shall supervise, record and report all the steps of the coating work. The Company reserve the right to attend during preparation of samples. 3.4.1 Preparation of steel samples Test sample shall be representative for the production and shall be prepared as follows: For pipe assembly: according to Item 5.1.1 of standard EN 253; For fitting assemblies: according to Item 5.2 of standard EN 448. Where test requirements specified in the standards EN 253 and EN 448 differ from those in other standards referred to, the requirements laid in the standards EN 253 and EN 448 shall apply. For each test, 2 sets of 3 samples shall be prepared. One set shall be used for the test, while one shall be identified and kept for possible checks and controls. Samples shall be cleaned and coated with the complete coating system listed in this Appendix, according to all requirements provided by items 5 and 6 of this Appendix and by the Functional Specification 20550 PIP.COR.FUN. Rev. 0, including but not limited to inspections, controls and testing reports of each working step. The coating application shall be performed using the same method for which the qualification is required and to same application parameters. The coated samples may be tested immediately after complete curing or suitably stored. However the tests must be executed within 3 months from the preparation of the samples. 3.5 QUALIFICATION TESTS The method for testing shall comply with the provisions of Item 5 of standard EN 253 for pipe assembly and Item 5 of standard EN 448 for fitting assemblies. Two coated samples shall be used for the execution of each required test. The result of the test performed on the two samples shall not be in conflict or different. The results will be considered acceptable if all results conform to the requirements and acceptance criteria of this Appendix. The acceptance criteria are reported in Tables 2, 3 and 5. 3.6 FINAL REPORTING OF LAB At completion of all tests a complete report shall be provided to the Company describing the preparation of the samples, the description and the results of the tests performed on coating materials, the description and the results of the tests performed on the steel samples. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 9 of 12
TABLE 5 Requirements of Pipe Assembly and Fitting Assemblies Characteristic Standard Acceptance Criteria Increase in diameter of the casing pipe EN 253 item 5.4.1 2% Centre line deviation As per Table 7 of EN 253 Shear strength EN 253 item 5.4.4 As per Table 8 of EN 253 Thermal conductivity EN 253 item 5.4.5 0,033 W/(m x K) Impact resistance EN 253 item 5.4.6 No visible cracks Creep behavior EN 253 item 5.4.7 Radial displacement 2,5 mm 4 PRACTICAL APPLICATION TEST IN THE SHOP At completion of qualification tests of coating materials and coating systems in the laboratory a practical test shall be perform in the shop in order to ascertain: a) The applicability of the coating material b) The correctness and suitability of the instruction provided by Coating Manufacturer. c) The need, where applicable, for special application equipment The test shall be performed on a significant length and number of pipes and/or components, which has to be agreed with the Coating Manufacturer, to enable the evaluation of problems, if any, faced during the application. 5 FUNCTIONAL REQUIREMENTS FOR COATING APPLICATION 5.1 PIPE ASSEMBLY 5.1.1 Surface preparation Surface preparation shall be performed fully in accordance with item 4.2.4 of standard EN 253 and to the specific functional requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev.0. 5.1.2 Coating Application Coatings shall be applied fully in accordance with the Coating Manufactures recommendations and to the specific requirements reported in item 2.6 of Functional Specification 20550 PIP.COR.FUN. Rev. 0. 5.1.3 Thickness of the coating system The minimum thickness of the coating system at any point shall correspond to the recommended value given in Tables 1 and 5 of standard EN 253. The tolerance on the outside diameter of the pipe ends shall be in accordance with Table 2 of EN 253. 5.1.4 Centre line deviation The distance between the centre line of the service pipe and fittings ends shall correspond to the values given in Table 7 of standard EN 253. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 10 of 12
5.1.5 Cut back Both ends of the service pipe shall be free from insulation for a minimum of 150 mm. The tolerance on the declared value shall be 10mm as defined in item 4.5.1 of standard EN 253. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of coating. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contract documents, must be approved by the Companys Representative. 5.1.6 Repair of defects The Contractor shall repair all coating defects and damages that may occur during or after construction or shipping Coating used for repair of defects and damages shall be supplied by the same Coating Manufacturer of the original coating system. Any repair shall be performed according to the requirements specified in the standard EN 253. 5.2 FITTINGS ASSEMBLIES 5.2.1 Surface preparation Surface preparation shall be performed fully in accordance with item 4.1.8 of standard EN 448 and to the specific requirements reported in item 2.5 of Functional Specification 20550 PIP.COR.FUN. Rev.0. 5.2.2 Thickness of the coating system The minimum thickness of the coating system at any point shall comply with the requirements of item 4.1.2 of standard EN 448. The tolerance on the outside diameter of the pipe ends shall be in accordance with Table 2 of EN 253. 5.2.3 Centre line deviation The distance between the centre line of the service pipe and the casing at fittings ends shall correspond to the values given in Table 2 of standard EN 448. 5.2.4 Cut back Both ends of the service pipe shall be free from insulation for a minimum of 150 mm. The tolerance on the declared value shall be 10mm as defined in item 4.4.4.1 of standard EN 448. The Contractor shall properly protect these end areas and the pipe bevel, that must remain perfectly clean and free from any traces of coating. Once the coating operations are completed cut-back areas shall be protected from corrosion by applying a temporary protection, easily removable by brushing. The type of this temporary protection, if not specified in the order or other contract documents, must be approved by the Companys Representative. 5.2.5 Angular between casing segments of bend and minimum length The maximum angle (alpha), between two adjacent segments of the casing of a bend shall not exceed 45 as defined in item 4.4.2 of standard EN 448. Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 11 of 12
The length, of the casing pipe at the ends of the fittings and valves shall not be less than 200 mm. 5.2.6 Polyethylene welding The welding process shall be performed in accordance with procedure reported in Annex B of standard EN 448. The melt flow rate of the pipes to be welded shall not differ more than 0,5 g/10 min. The related test shall be performed in accordance with item 4.3.1.2 of EN 253. The visual appearance of all welds shall be examined in accordance with item 5.6.2 of standard EN 448 and with the requirements provided in item 4.4.3 of standard EN 448. 5.2.7 Increase of the diameter of the casing pipe After foaming, the mean outside diameter of the casing pipe shall not have increased by more than 2%. The measurement shall be performed in accordance with item 5.6.4 of standard EN 448. 5.2.8 Minimum insulation thickness in bends The insulation thickness of the bends, shall not at any point be less than 50% of the nominal insulation thickness and nowhere less than 15 mm. The measurement shall be performed in accordance with item 5.6.5 of standard EN 448. 5.2.9 Tolerance of the main fitting dimensions The tolerance of the main fitting dimension shall be in accordance with Table 6.
TABLE 6 Tolerances of the main fitting dimensions DN H L 300 10 mm 20 mm > 300 25 mm 50 mm 6 REQUIREMENT FOR QUALITY MANAGEMENT AND QUALITY ASSURANCE 6.1 GENERAL Additional requirements for Quality Management and/or Quality Assurance are contained in the applicable Quality and Execution Requirements Specification attached to the Invitation to Bid. The provisions reported in item 4 of Functional Specification 20550 PIP.COR.FUN. Rev. 0 must be carefully followed. 6.2 QUALITY CONTROL PLAN Before the pre-job meeting and the beginning of the work the Contractor shall prepare and submit to the Company approval a detailed Quality Control Plan (QCP) reporting in detail all the Production Quality Tests (PQT) necessary to fully meet the requirements of Functional Specification 20550.PIP.COR.FUN. Rev. 0 and of this Appendix. The following activities, but not limited to, must be listed: a) Description of the activity, b) Description of the test, c) Applicable reference documents, Eni S.p.A. Exploration & Production Division 20550 PIP.COR.FUN Rev. 0 - February 2004 Appendix I - Page 12 of 12
d) Applicable check procedures and methods, e) Acceptability criteria, f) Frequency of the checks, g) Persons required to be present at the inspections. The Contractor shall perform during the works progress and at completion of the work all inspections listed in the Tables D.1, D.2, D.3 and D.4 of Annex D of standard EN 253 and Table A.2 of standard EN 448. 7 DOCUMENTATION AND REPORTING At completion of the work the Contractor shall produce all documentation and reporting required in item 5 of Functional Specification 20550 PIP.COR.FUN. Rev. 0.