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release 09/ /1998

Injection Moulding mini guide

contents

update

GE Plastics

Injection Moulding
mini guide
EN a

release 09/ /1998

Injection Moulding mini guide 1 contents

C o n t e n t s
Guidelines for production start-up . . . . . . . inlay
4.1.3 Purging compounds

. . . . . . . . . . . . . . . . . . . . . . 20 . . . . . . . . . . . . . . . . . . . . . . 21 . . . . . . . . . . . . . . . . . . 25 . . . . . . . . . . . . . . . . . 26 . . . . . . . . . . . . . . . 27 . . . . . . 27

1 Product overview . . . . . . . . . . . . . . .

4.1.4 Details per product

1.1 Amorphous injection moulding resins . . . . . . . . . . 7 1.2 Semi-crystalline injection moulding resins . . . . . . 7 1.3 Other products . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

4.1.5 Preparation before setting 4.1.6 Setting mould and machine

4.1.7 Starting the injection process

4.1.8 Setting temperature, speeds and pressures

2 Materials

....................... 9

4.1.9 Mould temperature control

. . . . . . . . . . . . . . . . . 30

2.1 Storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 2.2 When can resin pick up moisture? . . . . . . . . . . . . 9 2.3 When can moisture be a problem? . . . . . . . . . . . . 9 2.4 Importance of drying . . . . . . . . . . . . . . . . . . . . . . . 9 2.5 Pre-drying times . . . . . . . . . . . . . . . . . . . . . . . . . . 11 2.6 TVI test for checking moisture content . . . . . . . . . 12

4.2 Optimizing production . . . . . . . . . . . . . . . . . . . . . . 32


4.2.1 How to improve venting

. . . . . . . . . . . . . . . . . . . 32 . . . . . . . . . . . . . . . 32 . . . . . . . . . . . . . 33 . . . . . . . . . 33

4.2.2 How to improve mould release

4.2.3 How to influence mould shrinkage

4.2.4 How to use hot runner tooling systems 4.2.5 How to save energy

. . . . . . . . . . . . . . . . . . . . . . 34

3 Injection moulding machine

. . . . 15

5 Quality assurance

. . . . . . . . . . . . . . 35

3.1 Choosing a machine . . . . . . . . . . . . . . . . . . . . . . . 15 3.2 Screw geometry and design . . . . . . . . . . . . . . . . . 16 3.3 Vented barrels . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

5.1 Quality control . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 5.2 Visual control . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 5.3 Mechanical control . . . . . . . . . . . . . . . . . . . . . . . . 35 5.4 Weight control . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

4 Production

. . . . . . . . . . . . . . . . . . . . . . 19

5.5 Dimensional stability . . . . . . . . . . . . . . . . . . . . . . 36 5.6 Stress control . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 5.7 Viscosity control . . . . . . . . . . . . . . . . . . . . . . . . . . 37 5.8 Other methods . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

4.1 Setting up production . . . . . . . . . . . . . . . . . . . . . . 19


4.1.1 Safety

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 . . . . . . . . . . . . . . . . . . . . 19

4.1.2 Purging; change-overs

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Injection Moulding mini guide 1 Contents

Injection Moulding mini guide 1 contents

6 Part defects and


c o r r e c t i v e a c t i o n s . . . . . . . . . . . . . . 39
6.1 Fault diagnosis . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 6.2 Fault descriptions, causes and actions . . . . . . . . . 40
6.2.1 Black specks

6.2.14 Sink marks

. . . . . . . . . . . . . . . . . . . . . . . . . . . . 56 . . . . . . . . . . . . . . . . . . . . . . . . . 58

6.2.15 Splay / streaks 6.2.15.1 Splay

. . . . . . . . . . . . . . . . . . . . . . . . . . . 58 . . . . . . . . . . . . . . . . . . . . . . . . 59 . . . . . . . . . . . . . . . . . . . . . . . . 60

6.2.15.2 Gate splay 6.2.15.3 Streaking 6.2.16 Stringing 6.2.17 Voids

. . . . . . . . . . . . . . . . . . . . . . . . . . . 40 . . . . . . . . . . . . . . . . . . . . . . . . 41 . . . . . . . . . . . . . . . . . . . . . . . 42 . . . . . . . . . . . . . . . . . . 43

6.2.2 Blisters, bubbles

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62

6.2.3 Blush / flow marks

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63 . . . . . . . . . . . . . . . . . . . 64

6.2.4 Burn marks / diesel effect 6.2.5 Delamination

6.2.18 Warpage, part distortion 6.2.19 Weldlines / knit lines

. . . . . . . . . . . . . . . . . . . . . . . . . . 44 . . . . . . . . . . . . . . . . . . . . . . . 45

. . . . . . . . . . . . . . . . . . . . . 65

6.2.6 Dimensions of part 6.2.7 Discolouration 6.2.8 Flash

. . . . . . . . . . . . . . . . . . . . . . . . . . 46

7 Reusing materials 8 References

. . . . . . . . . . . . . . 67

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49 . . . . . . . . . . . . . . . . . . . . . . . . . 50 . . . . . . . . . . . . . . . . . . . . . . . 51 . . . . . . . . . . . . . . . . . . . 51 . . . . . . . . . . . . . . . . . . . . 52 . . . . . . . . . . . . . . . . . . . 53

. . . . . . . . . . . . . . . . . . . . . 71

6.2.9 Jetting 6.2.10 Pitting

Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

6.2.11 Record grooves

6.2.12 Release problems

6.2.12.1 Sticking in cavity 6.2.12.2 Sticking on core 6.2.12.3 Sticking of sprue 6.2.13 Short shots

. . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

Injection Moulding mini guide 1 inlay

Injection Moulding mini guide 1 inlay

Profile Cycolac
ABS

CRT3370 EP GPM5500 GPM5500M GPM5500S GPM5500T GSM G121 G320 G360 G361 G365 G366(M) G368 SEA2 S157 S570 S700(S)(T) S701(S) S702(S) S703 S704(S) S705 S706(S) VW300 VW55(M) XS158M X37 Cycoloy
PC/ABS

2 3 1 1 1 1 7 1 7 9 9 9 9 7 5 5 1 1 1 1 3 1 3 1 6 5 5 9

C1000(A) C1000HF C1100(A) C1100HF C1200(HF) C1200HFM C2100HF C2800 C2950 C6200 C6400 LG9000 Enduran
PBT

11 11 12 12 13 13 14 15 14 15 15 12

7062(X) Gelon
PA6.6/PA6

78

ACF6 AFG6 AFR200B AFR200Y

61 61 62 63

AFR450B AFR450X1 AFR450X2 AFR460B AFR470X1 AFR470X2 AFR560B AFR682A1 AG3(K) AG4(K) AG5(K) AG6(K) AG6ST01 AG6ST43 AG7(K) AG10(K) AK6 AK8 ALM ALY540A ALY640A1 AST02 AST03 AST04 AST41 AST43 AST44 AS6 A28(K)(N) A28UL BFR200A BFR200Y BFR450A BFR450B BFR460A BFR552Y3 BGS6H1 BG3(H) BG4(H) BG5(H) BG6(H)(U) BG6ST02 BG6ST41 BG6ST43 BG10(H) BG7(H) BG8 BK8 BLM BPP01 BST01 BST02 BST03 BST04 BST42 BST43

62 64 64 62 64 64 62 65 61 61 61 61 61 61 61 61 66 66 67 67 68 67 67 67 67 67 67 61 67 67 69 69 70 70 70 70 70 71 71 71 71 69 69 69 71 71 71 72 73 73 73 73 73 73 73 73

BST44 BS6 BS10 BT6 B28(H)(N) B28(U)(UL) B40 CFR200Y Lexan


PC

73 70 70 69 74 74 74 75

FL900P GR1210 HF1110R HF1130R HF1140R HF500R LS1 LS2 LS3 ML3019 ML3041 ML3042 ML3260 ML3286 ML3400 ML3513 ML3562 ML3729 OQ1020LN OQ1030LN OQ3620 OQ2830 OQ4320 OQ4820 101(R) 103(R) 104R 121(R) 123R 124R 1278R 134R 141(R) 143(R) 144R 161R 163R 164(R) 201R 2014R 2034 221R 223R 241(R) 243R

23 23 18 18 18 18 18 19 17 17 18 17 19 17 19 17 19 18 25 25 17 17 19 17 17 17 17 18 18 18 19 17 19 19 19 19 19 19 17 19 19 18 18 19 19

261R 263R 2814R 3412R 3413R 3431R 500R 503R 920(A) 923(A) 940(A) 943(A) 950(A) 953A Noryl
PPE/PS

19 19 17 17 17 17 17 17 18 18 18 18 19 19

V180HF V190 725A 731(S)

33 40 29 29

Noryl GTX
PPE/PA

CTI2550 FN150 GFN1(V) GFN1720 GFN2(V) GFN3(V) HB1525 HB3525 HF180 HF185 HIN120P IN120 N110(S) N110HG N190 PX1112(A) PX1115 PX1134 PX1180 PX1181 PX1185 PX1786G PX2245 PX9406N SE0 SE1 SE90 SE100 SE1GFN1 SE1GFN2 SE1GFN3 V0150B V01505 V01525 V01550 V02570 V03505 V03550 V090

29 33 29 30 29 31 32 29 33 33 29 29 34 34 33 29 29 29 36 36 36 37 33 29 29 29 33 29 29 29 37 37 36 29 37 30 29 38 39

GTX810 GTX820 GTX830 GTX914 GTX918W GTX924 GTX934 GTX944 GTX954 GTX964 GTX974 Ultem
PEI

41 41 41 42 42 43 43 43 43 43 43

AR9300 ATX100F ATX200F CRS5001 CRS5201 CRS5311 1000 1010 1010F 1110(F) 2100 2110 2200 2210 2300 2310 2312 2400 2410 4000 4001 6000 7801 9075 Valox
PBT - PET

53 83 84 54 50 50 47 47 48 49 47 47 48 48 48 48 49 50 50 51 47 50 50 52

310SE0 312C 315 325(C)(F) 325M 357X 359 3607U 362 4012 4022 4031 4032 412 420(SE0) 430 451E 4521 457 4631 467 5021 5031 508 5510 553 735 7523 771 8032(U) 815 830 855 865 Xenoy
PC/PBT

76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 57 76 79 57 57 57 57 57

Mould Melt temp. Nozzle

Zone 3

Zone 2

Zone 1

Hopper Moisture content C 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 80-100 80-100 60-80 60-80 60-80 60-80 60-80 80-120 80-120 80-100 80-100 80-120 80-120 80-120 80-120 % max. 0.1 0.1 0.05 0.1 0.1 0.1 0.1 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02

Predrying Profile

C 1 40-80 2 40-80 3 65-80 5 40-80 6 40-80 7 40-80 9 40-80 11 60-90 12 60-90 13 60-90 14 60-90 15 50-70 1780-120 1880-100 1980-110 23 65-95 2580-100 2980-120 3080-120 3180-120 3280-100 33 60-80 3460-100 3660-100 100-130 37 100-130 38 39 60-80 40 60-80 4180-100 4280-120 4380-120 140-180 47 140-180 48 140-180 49 140-180 50 140-180 51 140-160 52 135-140 53 120-170 54

C 220-260 230-260 250-270 200-230 180-210 240-270 250-280 240-270 250-280 260-290 250-280 230-270 290-320 280-300 280-310 290-320 300-330 280-300 290-330 280-300 280-300 260-280 280-300 280-300 300-320 280-310 270-290 260-280 280-300 280-310 290-320 370-410 370-410 360-400 370-410 370-415 360-380 350-400 360-410

C 210-250 220-250 240-260 190-220 180-200 220-260 245-275 220-260 230-270 240-280 230-270 220-260 280-310 270-290 270-290 290-320 280-320 260-280 290-310 280-300 270-290 240-260 260-280 260-280 280-300 280-300 250-270 240-260 270-290 270-300 280-310 350-405 360-410 360-400 370-410 360-405 360-380 350-410 360-400

C 220-260 230-260 245-265 195-225 185-205 230-270 250-280 230-270 240-280 250-290 240-280 230-270 290-320 280-300 280-310 290-320 300-340 280-300 310-330 290-310 280-300 260-280 280-300 280-300 300-320 300-320 270-290 260-280 280-300 280-300 290-320 360-415 370-420 370-410 380-420 370-415 360-380 350-410 370-410

C 220-260 230-260 240-260 195-225 185-205 210-250 250-280 230-270 240-280 250-290 230-270 220-260 280-310 270-290 270-290 280-310 280-320 260-280 290-310 270-290 260-280 240-260 260-280 260-280 280-300 280-300 250-270 240-260 270-290 270-290 280-300 350-405 360-410 360-400 370-410 360-405 345-365 350-400 350-390

C 200-240 220-250 230-250 180-210 170-190 210-250 230-260 210-240 220-250 230-260 210-240 200-230 270-300 260-280 260-280 265-295 240-280 240-260 270-290 250-270 240-260 220-240 240-260 240-260 260-280 260-280 230-250 220-240 260-280 260-280 260-280 340-395 350-400 240-380 350-390 350-395 320-340 350-370 325-365

Hours 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 2-4 4-6 2-3 2-4 2-4 2-3 2-3 2-4 2-3 2-3 2-4 2-3 2-4 2-3 2-3 2-3 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6

C 85-95 85-95 85-95 80-85 80-85 85-95 90-100 90-100 95-105 100-110 90-100 80-90 120 120 120 120 120 100-120 110-120 100-120 100-110 80-100 80-100 80-100 110-120 110-120 70-80 80-100 100-110 100-120 100-120 150 150 150 150 150 160 150 150 1 2 3 5 6 7 9 11 12 13 14 15 17 18 19 23 25 29 30 31 32 33 34 36 37 38 39 40 41 42 43 47 48 49 50 51 52 53 54

CL100B CL101 CL200 CL300 CL500U XL1339 XL1562 1760T 5730 6370 6380U

79 79 79 79 79 81 79 80 79 80 82

DR48 DR51 VAC3001N VX5005 VX5011 VX5022 260HPR 3007

76 76 76 76 76 76 76 76

October 1998

Temperature Profiles are only guidelines, to be used for start-up. Drying times as mentioned are hot residence times (pellets are at drying temperature) resulting in low moisture levels as indicated. Excessive drying times should be avoided. Please check with your local GE Plastics representative to ensure you have the most up-to-date information.

Injection Moulding mini guide 1 inlay

Injection Moulding mini guide 1 inlay

Profile Cycolac
ABS

CRT3370 EP GPM5500 GPM5500M GPM5500S GPM5500T GSM G121 G320 G360 G361 G365 G366(M) G368 SEA2 S157 S570 S700(S)(T) S701(S) S702(S) S703 S704(S) S705 S706(S) VW300 VW55(M) XS158M X37 Cycoloy
PC/ABS

2 3 1 1 1 1 7 1 7 9 9 9 9 7 5 5 1 1 1 1 3 1 3 1 6 5 5 9

C1000(A) C1000HF C1100(A) C1100HF C1200(HF) C1200HFM C2100HF C2800 C2950 C6200 C6400 LG9000 Enduran
PBT

11 11 12 12 13 13 14 15 14 15 15 12

7062(X) Gelon
PA6.6/PA6

78

ACF6 AFG6 AFR200B AFR200Y

61 61 62 63

AFR450B AFR450X1 AFR450X2 AFR460B AFR470X1 AFR470X2 AFR560B AFR682A1 AG3(K) AG4(K) AG5(K) AG6(K) AG6ST01 AG6ST43 AG7(K) AG10(K) AK6 AK8 ALM ALY540A ALY640A1 AST02 AST03 AST04 AST41 AST43 AST44 AS6 A28(K)(N) A28UL BFR200A BFR200Y BFR450A BFR450B BFR460A BFR552Y3 BGS6H1 BG3(H) BG4(H) BG5(H) BG6(H)(U) BG6ST02 BG6ST41 BG6ST43 BG10(H) BG7(H) BG8 BK8 BLM BPP01 BST01 BST02 BST03 BST04 BST42 BST43

62 64 64 62 64 64 62 65 61 61 61 61 61 61 61 61 66 66 67 67 68 67 67 67 67 67 67 61 67 67 69 69 70 70 70 70 70 71 71 71 71 69 69 69 71 71 71 72 73 73 73 73 73 73 73 73

BST44 BS6 BS10 BT6 B28(H)(N) B28(U)(UL) B40 CFR200Y Lexan


PC

73 70 70 69 74 74 74 75

FL900P GR1210 HF1110R HF1130R HF1140R HF500R LS1 LS2 LS3 ML3019 ML3041 ML3042 ML3260 ML3286 ML3400 ML3513 ML3562 ML3729 OQ1020LN OQ1030LN OQ3620 OQ2830 OQ4320 OQ4820 101(R) 103(R) 104R 121(R) 123R 124R 1278R 134R 141(R) 143(R) 144R 161R 163R 164(R) 201R 2014R 2034 221R 223R 241(R) 243R

23 23 18 18 18 18 18 19 17 17 18 17 19 17 19 17 19 18 25 25 17 17 19 17 17 17 17 18 18 18 19 17 19 19 19 19 19 19 17 19 19 18 18 19 19

261R 263R 2814R 3412R 3413R 3431R 500R 503R 920(A) 923(A) 940(A) 943(A) 950(A) 953A Noryl
PPE/PS

19 19 17 17 17 17 17 17 18 18 18 18 19 19

V180HF V190 725A 731(S)

33 40 29 29

Noryl GTX
PPE/PA

CTI2550 FN150 GFN1(V) GFN1720 GFN2(V) GFN3(V) HB1525 HB3525 HF180 HF185 HIN120P IN120 N110(S) N110HG N190 PX1112(A) PX1115 PX1134 PX1180 PX1181 PX1185 PX1786G PX2245 PX9406N SE0 SE1 SE90 SE100 SE1GFN1 SE1GFN2 SE1GFN3 V0150B V01505 V01525 V01550 V02570 V03505 V03550 V090

29 33 29 30 29 31 32 29 33 33 29 29 34 34 33 29 29 29 36 36 36 37 33 29 29 29 33 29 29 29 37 37 36 29 37 30 29 38 39

GTX810 GTX820 GTX830 GTX914 GTX918W GTX924 GTX934 GTX944 GTX954 GTX964 GTX974 Ultem
PEI

41 41 41 42 42 43 43 43 43 43 43

AR9300 ATX100F ATX200F CRS5001 CRS5201 CRS5311 1000 1010 1010F 1110(F) 2100 2110 2200 2210 2300 2310 2312 2400 2410 4000 4001 6000 7801 9075 Valox
PBT - PET

53 83 84 54 50 50 47 47 48 49 47 47 48 48 48 48 49 50 50 51 47 50 50 52

310SE0 312C 315 325(C)(F) 325M 357X 359 3607U 362 4012 4022 4031 4032 412 420(SE0) 430 451E 4521 457 4631 467 5021 5031 508 5510 553 735 7523 771 8032(U) 815 830 855 865 Xenoy
PC/PBT

76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 76 57 76 79 57 57 57 57 57

Mould Melt temp. Nozzle

Zone 3

Zone 2

Zone 1

Hopper Moisture content C 40-60 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 60-80 40-60 40-60 40-60 40-60 60-80 60-80 60-80 80-100 % max. 0.02 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02

Predrying Profile

C 5760-110 6170-120 6270-100 63 40-80 6490-120 6580-100 6690-110 67 70-90 68 70-90 69 60-80 70 70-90 7170-120 7270-100 73 60-90 74 60-80 75 70-90 7640-100 7860-100 79 60-80 8060-100 8160-100 8260-110 100-125 83 125-140 84

C 260-285 260-290 260-280 260-280 260-290 260-280 270-290 260-280 260-290 240-260 250-270 250-280 260-280 220-250 220-240 240-260 250-270 255-280 255-270 255-270 265-275 265-285 325-360 340-380

C 265-275 250-270 250-270 250-270 260-280 250-270 260-280 250-270 260-280 230-250 240-260 240-270 250-270 210-240 210-230 230-250 240-260 245-270 250-265 250-265 260-275 260-275 320-340 340-360

C 260-280 260-280 260-280 260-280 270-290 260-280 270-290 260-280 270-290 240-260 250-270 250-280 260-280 220-250 220-240 240-260 245-265 250-270 250-270 250-270 260-280 260-280 320-340 340-360

C 255-280 260-280 260-280 260-280 270-290 260-280 270-290 260-280 270-290 240-260 250-270 250-280 260-280 220-250 220-240 240-260 240-255 240-260 240-265 240-265 250-275 250-275 310-330 330-350

C 240-260 270-290 270-290 260-280 270-290 260-280 270-290 260-280 270-290 240-260 250-270 250-280 260-280 220-250 220-240 240-260 230-245 230-250 230-250 230-250 240-270 240-270 300-320 320-340

Hours 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 4-6 2-4 2-4 2-4 2-4 4-6 4-6 3-4 3-4

C 110-120 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 75-85 110-120 110-120 90-100 100-110 110-120 110-120 125-135 130-140 57 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 78 79 80 81 82 83 84

CL100B CL101 CL200 CL300 CL500U XL1339 XL1562 1760T 5730 6370 6380U

79 79 79 79 79 81 79 80 79 80 82

DR48 DR51 VAC3001N VX5005 VX5011 VX5022 260HPR 3007

76 76 76 76 76 76 76 76

October 1998

Temperature Profiles are only guidelines, to be used for start-up. Drying times as mentioned are hot residence times (pellets are at drying temperature) resulting in low moisture levels as indicated. Excessive drying times should be avoided. Please check with your local GE Plastics representative to ensure you have the most up-to-date information.

Product overview
This Injection Moulding mini guide supplementary to the Injection Moulding brochure that shows detailed information is specially designed as a handy pocket guide and quick reference for use on the shop floor. The inlaid pages show details on pre-drying and temperature settings of machine, mould and material for all standard GE Plastics resins.

1.1 Amorphous injection moulding resins


Cycolac Cycoloy Lexan Noryl Noryl Xtra Ultem
ABS Resins PC + ABS Thermoplastic Alloys PC Polycarbonate Resins PPE + PS Modified PPO Resins PPE + PS Modified PPO Resins PEI Polyetherimide Resins

1.2 Semi-crystalline injection moulding resins


Enduran Lomod Noryl GTX Supec Valox Xenoy
PBT Thermoplastic Polyester Resins Flexible Engineering Thermoplastic Resins PPE Modified PA Alloys PPS Polyphenylenesulphide Resins PBT + PET Thermoplastic Polyester Resins PC + PBT Thermoplastic Alloys

1.3 Other products


Azdel - Azloy Azmet Technopolymer Structures Remex Engineering Plastics Kapronet Purging Compound

Materials
2.1 Storage
GE Plastics resins are supplied in the form of ready-to-process pellets in sealed bags or containers. No special storage conditions are necessary, however, all containers must be kept dry and away from sunlight since UV radiation could affect both packaging and contents. Special care must be taken to keep Lexan and Noryl GTX resins as dry as possible during storage.

2.2 When can resin pick up moisture?


during transport and storage during prolonged exposure to atmosphere, even after initial drying on its way to the machine hopper, when no hot (dry) air is used in case of high relative humidity

2.3 When can moisture be a problem?


pellets packed too deeply in the trays of drying ovens: lack of air circulation will prevent drying inefficient drying equipment machine hopper lid not sealed

2.4 Importance of pre-drying


Most thermoplastics absorb atmospheric moisture, which under normal processing conditions can cause degradation of the polymer. Specially Lexan, Ultem and Valox as hygroscopic resins demand proper pre-drying before moulding: these polymers do react with moisture at high (processing) temperatures. When this reaction occurs, polymer chains break, resulting in loss of properties. Excessive moisture can manifest itself in splay, silver streaking, blisters or degradation, which reduce the cosmetic and physical properties of moulded components. The removal of moisture is therefore essential to ensure optimal performance of the final part. Although Noryl resin has one of the lowest moisture

Injection Moulding mini guide 2 Materials

Injection Moulding mini guide 2 Materials

2.5 Pre-drying times


absorption levels of engineering plastics, it is advised to dry before moulding - particularly where surface appearance is critical. For filled materials the drying time might be slightly longer; the allowed moisture level is the same. Due to a larger surface area of the pellets, recycled resins have a faster pick-up rate of moisture: drying time should in general be increased from 4 to 6 hours. It is recommended to dry regrind materials separately.
Effect of drying time on impact strength of Effect of drying time on moisture content of

Lexan resin
800
Izod Notched Impact J/m

Lexan resin, at 120C


0,25
Moisture %

700 600 500

0,20

Although exceeding recommended drying times will not affect the properties of resins such as Lexan, Valox, Ultem and Xenoy, it is recommended not to dry for longer periods of time as indicated in the enclosed inlay. With Noryl resin, exceeding drying times may result in surface defects due to oxidization. 90% of Noryl resins moisture is removed anyway during the first hour of drying. Excessive drying time with Cycolac resin may give a slight surface oxidation of the pellets resulting in colour shift of light colours. This is caused by the fact that too long or too high air temperature may drive out required additives: resin will process poorly, parts get brittle, colours change. It is important that the typical drying times assume that the pellets are up to drying temperature before the clock starts. Drying time taken to get the pellets up to drying temperature does not practically contribute to the effective overall drying.
For details per grade, see enclosed inlay.

400 300 200 100 0 0 30 60 90 120


Drying time, minutes

0,10 0,08 0,06 0,04 0,02 0 0 30 60 90 120


Drying time, minutes

Gardner Falling Dart Impact Nm

Effect of moisture content on impact strength of

Valox 310 resin


45 40 30
50 secs moulding cycle

wet 0,5% moisture dried 0,05% moisture

11

0 240
Melt temperature, C

270

Injection Moulding mini guide 2 Materials

Injection Moulding mini guide 2 Materials

2.6 TVI test for checking moisture content


PICTURE 1

Measuring moisture content can be done by laboratory equipment such as the Carl Fischer titration method or others. Since these long, unwieldy lab techniques are impractical in most moulding shops, GE Plastics has developed a simple, fast and low-cost method to determine whether moisture-sensitive thermoplastic pellets are dry and ready for processing. In brief, this method means heating a few pellets to their melting point and observing whether bubbles are present (indicating moisture in the resin) or absent (indicating a dry material). Called TVI (Tomasettis Volatile Indicator), the test requires little in the way of equipment and calls for just four simple steps. See pictures. The TVI test can be used for Lexan, Ultem, Noryl, Noryl GTX, Cycolac, Cycoloy, Valox and Xenoy resins, but not for glass reinforced grades. Not to be used for Supec and Lomod resins. The necessary equipment is a hot plate capable of maintaining various temperatures from 200 to 350C, two glass microscope slides, a straight edge or tongue depressor, a pair of tweezers and ideally a surface pyrometer to check the plate temperature if no hot plate is available, a quick check can be done by using a heater band of the moulding machine. Moisture is denoted by bubbles in the flattened granules: the number and size increase with the amount of moisture present. A few small bubbles mean moisture contents of 0.02 to 0.03%, numerous bubbles indicate 0.05 to 0.1%, and many large bubbles moisture above 0.1%. To avoid misleading conclusions, it is advisable to always test at least four granules, as bubbles that appear in only some granules might be trapped air, rather than moisture.

Heat two microscope glass slides on hot plate for about two minutes (be sure surface is clean) - Valox and Xenoy resins: 250C, Noryl and Noryl GTX resins: 280C, Lexan resin: 290C, Ultem resin: 350C, Cycolac resin: 250C, Cycoloy resin: 275C.
PICTURE 2

Use tweezers to place three or four pellets from the drier on one of the slides. Place the other slide immediately on top of the granules.

PICTURE 3

Press the two slides together with a straight edge until the granules are flattened out to about 12 mm diameter.

PICTURE 4

12

Remove the sandwiched slides and allow to cool. Amount and size of bubbles indicate percentage of moisture. If only one or two bubbles are present, they may be only trapped air and no moisture: to be sure, use at least three or four pellets.

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Injection moulding machine


3.1 Choosing a machine
Shot size %

shot size %

- in general 30 to 90%, depending on resin type and in relation to residence time and melt temperature shot size < 20 % - can cause material degradation, part defects shot size > 90% - no melt homogeneity, inconsistent part quality, packing problems
Residence time

residence time residence time

- always related to melt temperature - maximum 6 to 12 min. depending on resin type too long - material degradation too short - insufficient plastification and homogeneity of plasticized material colour pigments - high residence times may change colours

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Injection Moulding mini guide 3 Injection Moulding Machine

Injection Moulding mini guide 3 Injection Moulding Machine

3.2 Screw geometry and design


L/D ratio and compression ratio

L/D 22:1 to 25:1 L/D 18:1 to 24:1 CR 2:1 to 2.5:1 CRs higher than 2.5:1

for Valox, Xenoy resins for all other resins for all resins not recommended

too high r.p.m. too high r.p.m. too high r.p.m. too high r.p.m.

- material degradation - breakage of glass fibres in glass filled products - increased wear of screw and barrel - inability to control melt temperature

Non-return valves / back flow valves

3.3 Vented barrels


Dos

sliding ring valves ball check valves


Nozzles

- for all resins - not recommended

open nozzles - for all resins reversed taper nozzles - for Cycolac resin, not for Valox resin shut-off nozzles - for Supec resin, not advised for other resins nozzle orifices - as large as possible, 1 mm smaller than sprue top nozzle temperature - heater band plus adequate control drooling - check nozzle radius
Screw cushion

do monitor carefully the temperature profile of the barrel do keep residence times below 8 min. do contact your local GE Plastics representative for any advice on vented barrel processing
Donts

screw cushions

- 3 to 10 mm of plasticizing stroke, dependent on screw diameter/ material compression

dont process Ultem, Supec, Xenoy or Lomod resins using vented barrel equipment dont process FR grades using vented barrel equipment dont use vented barrel equipment for critical appearance applications dont change material frequently dont use filters in nozzles dont use if possible a vented barrel machine

Screw speeds

16

r.p.m. - always in relation to screw diameter circumferential speed - most important circumferential speed - unfilled and filled grades preferred 0.10 - 0.25 m/s. circumferential speed - grades with special fillers preferred 0.10 - 0.20 m/s. r.p.m. - adjust moulding cycle: screw rotation must fall in cooling time r.p.m. - as low as practicable, but beware of insufficient plastification

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Production
4.1 Setting up production
4.1.1 Safety

General recommendations for safety in injection moulding are: appropriate protective clothing should always be worn when handling hot materials and during cleaning operations; continuous and direct removal of processing fumes and dust with a local exhaust system and a re-supply of fresh air will promote good workplace ventilation; avoid eye or skin contact with smoke, fumes, dust and vapours by installing an exhaust hood over the injection moulding machine nozzle. Similar ventilation precautions should be taken for all cleaning operations.
4.1.2 Purging; change-overs

When changing materials during moulding, purging of the cylinder is required. Contamination with foreign or degraded resins can cause problems, such as delamination or black specks. Actual degradation of the to-be moulded material may result in parts which neither look nor perform satisfactorily.

Start-up from an empty and clean barrel is straightforward: barrel heaters are set according to the advised temperature profiles, and individual adjustments are made as production starts.
During breaks in production the following steps are advised: 1. close off hopper feed 2. empty plasticizing cylinder 3. move screw as far forward as possible 4. reduce barrel temperatures to recommended levels When starting up again, set the barrel heaters to normal processing temperatures, extrude until residual material is completely purged and begin moulding. The initial shots should be checked for contaminants in the moulded parts.

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Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

4.1.4 Details per product

When a material change is necessary, or a production run ends , thorough purging of the cylinder is essential to remove all traces of previous polymers. Otherwise results may be unsatisfactory. Problems that may occur include material degradation, resulting in black specks, or, if materials are not compatible, delamination in the moulded parts. In some cases special procedures are necessary. Purging can be done with nozzles either in place or removed, but removal allows cleaning and inspection for foreign matter. Be sure to avoid danger of splatter when purging. Add purging material with the screw rotating slowly. The purging material should be pressed out immediately and submerged in cold water before being disposed off. Purging should always be done with adequate ventilation.
Colours and FR

FR Cycolac resin

Production stagnation longer than 10 minutes or with normal shut down: purge with standard ABS. When changing to another ABS or another thermoplastic, all FR ABS must be removed before increasing heat settings. Since ABS is not particularly compatible with other polymers, standard ABS is the best purge material. When changing from a high viscosity thermoplastic to FR ABS, decrease temperatures and purge with FR ABS, then make temperature adjustment and continue moulding.
Cycoloy resin

Never switch off the heating when PC/ABS is in the barrel: reduce barrel temperatures to 160C. Always purge FR Cycoloy.
Lexan resin

Extended interruption of production may result in melt discolouration: purging is necessary. Switching colours involves purging until the original colour is completely displaced. When using pigmented or flame-retardant materials, clean the screw and barrel mechanically. During reassembly of threaded components of the injection unit, care must be taken that no grease is in contact with the cylinder, screw surface or nozzle area.
4.1.3 Purging compounds

As with all PC containing thermoplastics resins, (Cycoloy PC/ABS resin, Xenoy PC/PBT resin), never switch off the heating when the resin is still in the barrel. Reduce to 170C or clean screw with other material, otherwise black specks will occur or even the screw could be damaged; for transparent parts, it is strongly recommended to clean the screw thoroughly before starting moulding. Ideally a machine should only be used for moulding PC.
CHANGING FROM OTHER POLYMERS TO LEXAN RESIN

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Cycolac resin Cycoloy resin Lexan resin Lomod resin Noryl resin Noryl GTX resin Noryl Xtra resin Supec resin Ultem resin Valox resin Xenoy resin

ABS, PMMA, SAN ABS, PMMA, PC, SAN PC, PP, PS PE, PP, PS PS, PMMA PE, PP, PMMA Noryl, PS HDPE, PP, GF PC GF PC, PC, PMMA, HDPE PS, HDPE PS, HDPE

Thorough purging is especially essential before moulding Lexan resin in transparent, translucent or bright colours. Since the melt temperature required for Lexan resin is often higher than the degradation level of other thermoplastics, it is imperative that all traces of other polymers are purged out before starting moulding Lexan material. Extra care must be taken with POM. Its accelerated degradation at even the lowest melt temperatures, as advised for some Lexan grades, will produce unacceptable quantities of formaldehyde.

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Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

Contamination with nitrogen-containing polymers such as ABS and PA or FR polymers can cause chemical reactions that may severely degrade the polycarbonate, showing as dark spots in moulded parts. Should this occur after thorough purging of the machine, remove the screw and clean both cylinder and screw. A thorough inspection should be made of cylinder, screw and check rings for cracks and proper fit. Best purging material is polycarbonate or some proprietary compounds.
CHANGING FROM LEXAN RESIN TO OTHER POLYMERS

Noryl resin

Where other materials are used after Lexan polymer, thorough purging to remove all traces of Lexan material must be done before the barrel has cooled. Purge with a PMMA and drop the cylinder temperatures if the resins to be moulded afterwards are POM, ABS or PA. Do NOT purge directly with PA or ABS after Lexan resin.
INTERRUPTION OF PRODUCTION

PS and PMMA are effective purging materials for all Noryl resins. Purging should be done within the melt temperature range of the particular Noryl grade. When moulding has to be stopped, the following steps are recommended: maintain cylinder temperature for interruptions of up to 15 minutes lower cylinder temperature by 40C for periods from 15 minutes to 2 hours reduce further to 170C for interruptions from 2 to 12 hours purge out barrel and shut off heat for periods longer than 12 hours
Noryl Xtra resin

Purge always with PS after process interruption.


Supec resin

Keeping Lexan resin overnight or over a weekend in the cylinder is generally not recommended but can be done in the following way: reduce cylinder temperature to 170 to 180C leave heaters on ensure that the temperature never drops below 160C, otherwise Lexan resin will adhere to the cylinder walls and may pull off metal particles and degraded resin as it cools and contracts. This contamination will show as black specks in the mouldings when production is restarted. during production delays, empty the screw to prevent overheating.

HDPE, PP or glass-filled PC are suitable materials for purging the barrel after moulding Supec resin.
Ultem resin
CHANGING FROM OTHER POLYMERS TO ULTEM RESIN

22

Lomod resin

Lomod resin requires no special purging procedures: normal purging with HDPE, LDPE, PP or PS will do. Because the processing temperatures of these materials are within the same range as used for Lomod resins, there is no need to reduce cylinder temperatures.

Thorough purging is essential when changing to Ultem resins. Since the processing temperature of Ultem resins (350 to 410C) is well above the degradation level of most other thermoplastics, it is essential to remove all traces of other polymers to avoid contamination resulting in black specks. Best purging material for Ultem resin is glass-filled Lexan regrind; drying is not recommended. Purge at the processing temperature of Ultem resin, continue to purge until the actual barrel temperature has reached 350C, followed by the standard start-up procedure. Chemical purging compounds are not recommended. As with Lexan resin, take extra care with POM even at the lowest temperatures used for moulding Ultem resin. Its accelerated degradation produces unacceptable quantities of formaldehyde. FR polymers which contain nitrogen must be purged completely, otherwise contamination can cause chemical reactions that degrade Ultem resin.

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Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

4.1.5 Preparation before setting

CHANGING FROM ULTEM RESIN TO OTHER POLYMERS

Purging the cylinder after moulding of Ultem resin parts can be done by using Lexan polycarbonate. Put Lexan resin in the hopper when temperature settings are still at the high level as used for Ultem resin. The settings should be reduced to 300C, however, the moment Lexan material is fed in. Purging can be completed by high viscosity PE or GE Plastics Kapronet purging compound. For stubborn cases purging can be done by using glass fibre-filled Lexan resin.
INTERRUPTION OF PRODUCTION

Part

Was the part produced before? On what machine? Has the previous experience been recorded? How many mouldings are needed? By when? Any special measuring equipment needed? Weight and size of moulding: cylinder and clamping force?
Material

Short breaks: empty barrel and shut off hopper. Stopping production for more than 30 minutes: purge barrel empty and drop temperature settings down to 200C. When stopping production for overnight, empty the barrel and drop temperature settings to around 200C. If stopping for the weekend, switch off temperature settings after purging the barrel. When shutting down the machine, the hopper must be shut off at the throat and the machine should continue running until all residual resin is run out of the barrel. The screw must be left in its forward-most position with the barrel heaters set at 200C for long periods of time. This reduces black speck contamination during start-up. If temperatures are dropped too low, Ultem resin will stick on metal parts and pull off particles, that result in black specks. Similar to Lexan resin.
Valox resin

Where is the material stored? Is the material pigmented? In what colour? Does the material contain recycle? And in what percentage? Does the material need pre-drying? Temperature and time of pre-drying? And with what equipment?
Mould

Where is the mould stored? How can it be transported? What clamping equipment is needed? Does it fit in with the specified machine data, tiebars, core pulling devices, etc.? Are the mould and clamping devices ready to use? What temperature control is needed and what equipment does this require?
Machine

24

When changing over to Valox resins from higher melt temperatures or heat sensitive materials, either PS or HDPE may be used as purging material. Due to the scrubbing action of glass fibres, purging for glass-reinforced Valox resin may not be necessary.
Xenoy resin

When is the specified machine available? Is the machine in good working order, free from problems, lubricated, with clean mould platens etc.? What cylinder is needed? And what nozzle? Should the cylinder be purged? Has the additional equipment been planned: core pulling devices, air ejectors, robots etc.? Any trimming equipment, shrink fixtures needed?

25

Never switch off the heating when PC/PBT is in the barrel: reduce barrel temperatures to 160C.

Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

4.1.6 Setting mould and machine

4.1.7 Starting the injection process

Mounting the mould and setting the clamping unit

set mould height on the machine with the clamping unit closed check clamping devices fix mould securely to the lifting tackle, ensuring that the two mould halves remain together, if necessary by bolting lock mould and thoroughly tighten up clamping bolts set clamping force at desired level set mould safety device: low pressure and high pressure set mould opening stroke, with damping. set ejectors set speed of the clamping unit set up the mould safety protection heat up mould to the required temperature
Setting the injection unit

26

bring injection unit into rear position check nozzle radius and diameter check penetration depth of nozzle check the centring of the nozzle to the sprue bushing heat up cylinder set cylinder temperatures (not too high) and screw speed after having heated up the cylinder, set nozzle contact force make sure the mould is closed initially set material feed somewhat lower than the required shot weight set the position for change-over to hold-on pressure based on safety side plasticize stepwise under manual control, while observing how the material feeds: this should be consistent and not in jerky movements after a short pause, purge out manually and check the melt temperature set injection speed and injection pressure to average values
Setting the machine controls

When all settings have been checked, switch over from manual to semi-automatic mode. In general the settings must be optimized after several shots. Take following steps: increase or reduce metering optimize injection speed observe the material cushion in front of the screw check pressure build-up during injection check cooling time and if possible shorten it set screw r.p.m. to a low value: plastification time should be slightly shorter than cooling time check mould locking force harmonize machine movements to obtain a better balance of speeds, sequence and damping if visually acceptable mouldings are being produced, check quality where necessary, optimize and store the various functions record machine setting data ensure that mouldings are correctly taken out and transported away ensure quality control aim for a fully-automatic machine cycle to ensure uniform moulding quality
4.1.8 Setting temperatures, speeds and pressures

Temperatures

Cylinder-, mould- and melt temperature settings as advised are guidelines, to be used for starting up the production. They are typical for most applications. However, where part geometry and mould design demand for it, higher melt temperatures can be used: the residence times at those temperatures should be kept as short as possible. Too high melt temperatures may result in colour changes when pigmented resins are used.
Injection speed

27

set the operational selector switch to manual set injection time, after-pressure time and pause time initially somewhat longer than necessary, then optimize them after a few shots

Injection speed is largely governed by the complexity of the part, the mould quality and the gating system. Slow injection speeds should be used during start-up.

Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

However, fast injection speeds in general are desirable; they - avoid premature freezing of the melt - reduce visibility of weld lines - give better welding of weld lines - increase surface gloss - keep melt temperature in the mould at a higher level - improve transfer of pressure in the mould - reduce overall orientation Several effects can be created by changing the screw advance speed during injection. A slower speed at the start of injection - reduces mould deformation - reduces tendency for jetting - reduces matt spots in the gate area A slower speed at the end of injection - can reduce variation of properties of the moulding - enables reduction of clamping force - improves venting due to reduction of air compression Profiled injection speed can control shear in some areas of the moulding, e.g. through grille areas etc.
Injection pressure

After pressure (hold pressure)

After pressure compensates for volume shrinkage of the melt during cooling in the mould. It should be maintained until the gate is frozen: the corresponding duration of after pressure should result in a constant part weight during moulding. Insufficient holding pressure may lead to: - sink marks - voids - variations in part dimensions - increased shrinkage Too high holding pressure may lead to: - problems with ejection of the moulding - stress in the gate area - warpage A decrease of the holding pressure at the end of the holding pressure time : - reduces internal stresses - reduces warpage because differences in shrinkage in the moulding far and close to the gate are reduced Since after pressure is mould-related, depending on surface quality, part thickness, shape of gating, etc, it is difficult to recommend exact levels of after pressure. For GE Plasticsresins, after pressure may vary from 30 to 80% of the injection pressure.
Back pressure

28

The injection pressure should be established to mould full parts consistently with a satisfactory finish free of sink marks, weld lines or similar defects. The level of injection pressure, which should always be started at the minimum level, depends on many things: - type and grade of material - complexity of the part - quality and polish of the mould - type of gating - material viscosity Generally, the lowest pressures which still provide the desired properties, appearance and moulding cycle are preferred.

Back Pressure has two functions: 1. it consolidates the melt by excluding air, thereby ensuring consistency of shot volume and removing splay caused by entrapped air. 2. it increases shear on the material: high shear may be necessary for masterbatching, dry colouring, mixing additives and sometimes to obtain a homogeneous melt with low-compression screws. High back pressure is also used in structural foam moulding to prevent pre-blowing of the blowing agent. It can be used in a similar way for solid mouldings as a trick to reduce splay caused by (too high) moisture content.

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Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

The main function of back pressure is to improve mixing of the material: in most cases a low back pressure of 4 to 5 bar is sufficient to get a homogeneous melt without overheating the material. The maximum level of back pressure is related to screw diameter and screw r.p.m. Attention must be paid when moulding flame retardant, glass fibre-filled, pigmented resins and polymer blends. In general, levels of back pressure should not exceed 10 bar.
4.1.9 Mould temperature control

Semi-crystalline materials
hot moulds

- higher level of in-mould crystallization - high shrinkage values


cold moulds

- crystallization after moulding - danger of warpage during use of part


Water-based or oil-based units

needs to

heat up the mould to operating temperature - before production remove heat from mould cavity and control tool temperature during production keep mould at uniform temperature - during production
results in

mould temperature below 100C: water-based mould temperature above 100C: oil-based or pressurized water-based heat transmission of oil is about half that of water: heat transmission surface area with oil is twice as big as for water pipes and couplings must take the heat requirements
Mould cooling system

optimization of cycle time insurance of high and uniform quality of mouldings


Mould temperature

very important parameter controls cycle time controls product properties


surface appearance dimensions shrinkage warpage crystallization rate moulded-in stress levels thermal behaviour of the moulded parts

periodically clean entire temperature control circuit by flushing with a special solution: removes dirt and lime use insulating plates to insulate mould from machine - reduces the time to heat the mould up to the required temperature - extremely important when using hot-manifold and hot-runner moulds

Amorphous materials

30

hot moulds

- improve properties - no dramatic change of shrinkage values


cold moulds

31

- filling difficulties - high injection pressures needed - high melt temperature needed

Injection Moulding mini guide 4 Production

Injection Moulding mini guide 4 Production

4.2 Optimizing production


4.2.1 How to improve venting

Whenever a given mould creates problems with venting, such as burn marks or short shots, the first thing to do is to lower the injection speed. This does not increase venting, but it lowers the amount of air that has to leave the mould within a certain period of time. No burn marks on the part due to the diesel effect: as air cannot escape quickly enough, it will be compressed, its heat content will be concentrated in a small volume, resulting in a large temperature increase causing the incoming plastic to burn, (pressure x volume = constant). However, it could be necessary to increase the injection pressure in order to fill the part. If lowering the injection speed does not help, the venting should be increased. The amount of venting that is possible or required can be tested by taping very thin copper foil on the closing surfaces of the mould. Starting with 0.01 mm thick foil and gradually going thicker, it can be found by trial and error how much the venting can be increased before the part will show flash. Attention when soft moulds are used: the copper foil may damage the mould surface.
4.2.2 How to improve mould release

Too high mould temperature can lead to part warpage; too low mould temperature can result in insufficient flow, leading to overpacking. Increase of cooling time often has a positive effect. Although mould release is different for each GE Plastics resin, mostly high injection pressures and overfilling are the major causes of problems. A good way of checking is weight control of the parts during production.
4.2.3 How to influence mould shrinkage

32

Apart using well-known silicones-free release agents not to be used when mouldings are painted or decorated afterwards changing processing conditions can influence mould release. With beaker-shaped mouldings, it is important to keep the core lower in temperature than the cavity the part will shrink on the core and not stick in the cavity, where no ejector pins are available. This requires cooling the mould with separate fluid circuits. In general it is important to closely control the mould temperature. The temperature should not fluctuate too much, or increase in an uncontrolled way. A well-designed cooling layout, together with a correct way of connecting the various cooling channels a parallel layout rather than a serial one can help to keep the mould temperature as even as possible over the total mould surface. Overpacking too high injection pressure, for too long can create release problems: lowering injection pressure obviously is needed.

Factors that influence shrinkage are cavity pressure and aftershrinkage. Cavity pressure is dependent upon mould temperature, melt temperature, injection speed, injection pressure, level of afterpressure and afterpressure time and, most importantly, the dimensions of gate- and runner systems (loss of pressure). Main parameters are injection pressure, afterpressure and afterpressure time. Parameters like back pressure, melt- and mould temperature have less influence on mould shrinkage. Aftershrinkage depends on the temperature of the part when it leaves the mould. This temperature again relates to the melt temperature, mould temperature and cooling time. Parts moulded out of materials such as Noryl GTX resin can show increased dimensions resulting from pick-up of moisture in the air, due to the hygroscopic behaviour of the polyamide present in Noryl GTX resin. The level of this moisture pick-up and the speed with which it occurs depend on relative humidity, (RH), temperature and wall thickness of the moulding. At 23C and 50% RH saturation can take months.
4.2.4 How to use hot runner tooling systems

Hot runners tend to make the whole process of moulding in general more susceptible to material degradation; not only due to longer residence times at higher temperatures, but also through the often not completely balanced flow/temperature control in a hot runner system. This may result in big differences in temperature in the various zones of hot runner blocks or nozzles.

33

Injection Moulding mini guide 4 Production

5
Also very important is the lowering of the temperature of the hot runner when the moulding process is interrupted, (in case of problems for example), otherwise too much degradation of the material might occur. Purging the cylinder is rather easy, whilst purging the hot runner system is much more difficult. Sometimes however it may be necessary, otherwise the mould would be filled with degraded material. This might be difficult to remove from the mould surface and it could lead to staining. Also very important with hot runner systems is the option of an electrical circuit that allows gradual heating up. Eventual moisture present in the heater cartridges can evaporate: it avoids the chance of short circuiting. This is especially important in case a hot runner system has not been used for a long period of time. Also important is the possibility to heat the zones separately by using different control units. The power can be varied and thus uniform temperatures created.
4.2.5 How to save energy

Quality assurance
5.1 Quality control
Effective quality control enables simple yet accurate testing of materials and parts for behaviour and defects under processing conditions. Accepting the quality of the material, the main points are material degradation and unsatisfactory part performance. Where materials have a narrow processing window, deviations in mechanical, thermal and physical properties can occur. The narrower this window, the harder it becomes to maintain part consistency, and thus rejection rates increase. Material that can be processed using a wide range of processing conditions provide an almost negligible rejection rate. This processing flexibility, however, makes the discovery of deviations from the optimum on moulded parts more difficult. Successful quality control is based on the comparison of production parts with samples of a good quality and known properties. Quality control systems based on statistical process models, such as SPC, are recommended. For all parts, however, control methods should be related to the desired performance of the application, and, not least, the cost of it. The effects of costly engineering to attain certain unnecessarily high standards should always be borne in mind.

Tips that not only save money, but also material: do not keep the machine nozzle always against the mould: after the gate is frozen, pull the cylinder back from the mould directly after plasticizing in case of a shut-off nozzle use insulated plates between mould and machine aim for optimal control of the mould temperature; the allowed temperature difference between temp-in and temp-out of the coolant is a balance between quality of moulding (1 to 2C) and economics (3 to 5C) keep screw r.p.m. at a low level: the plastification time should be slightly shorter than the cooling time do not use a cylinder with a too high capacity for the actual shot weight

5.2 Visual control


This is the most important control method, as there is mostly a direct correlation between appearance and properties of the moulding. Extensive descriptions of deviations are discussed in Chapter 6 Part Defects and Corrective Actions.

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5.3 Mechanical control


Due to the varying shapes and sizes of moulded parts, mechanical testing can be difficult. It is therefore advisable to prescribe procedure, conditions and equipment carefully, and to experiment with testing. Mechanical testing demonstrates whether material quality and processing conditions affect the

35

Injection Moulding mini guide 5 Quality Assurance

Injection Moulding mini guide 5 Quality Assurance

mechanical properties of the part, and can also be related to practical requirements. A common procedure is the falling dart test, which assesses the components ductility. The prime objective is to check for material degradation during processing. This affects impact properties, as do other deviations from optimal processing such as bubbles, sink marks, weak knitlines, etc.

5.4 Weight control


An economical, fast and easy method that can be carried out at the production location. Often preferred over dimensional methods, since weight variations will be more readily noticeable than those of dimensions. It can also assist in checking bubbles and voids, or other deviations from the filling rate of the cavity in the tool. Wide variations in weights of parts can indicate insufficient production and/or machine tolerances. Stabilizing part weight in general indicates stabilized processing conditions.

mouldings: a light source with a linear polarized filter can then be used to detect internal stress concentrations. Stress levels can also be checked using stress corrosive fluids such as TnBP for Noryl resin and toluol N propanol for Lexan resin. (GE Plastics representatives can supply more information.) A simple but effective way to check stress in parts moulded out of Lexan resin is to observe them after 24 hours immersion in a 80C solution of 100 g dishwashing powder with 10 g gloss agent in 1 liter water.

5.7 Viscosity control


Measuring viscosity of plastics materials can be used to check possible degradation of the resin resulting from injection moulding, UV ageing/weathering or heat ageing. Differences in flow before and after indicate material degradation: any deviation from original granulate flow could be related to either abusive moulding or non-controlled part ageing. For Lexan PC and PC blends such as Cycoloy and Xenoy resins, the intrinsic viscosity or IV method is used. It demonstrates whether the material has been properly pre-dried and/or degraded during moulding. The percentage loss in IV of the material due to moulding of the part is an indication of material degradation. Information on exact figures can be obtained via GE Plastics representatives. For all materials the MVR (melt volume rate) or MFR (melt flow rate) can be used same test, just a different way of measuring the result: MVR in cm3 /10 min., MFR in g/10 min. The delta flow data of MVR and MFR show the change of the material during and after processing. During processing, phenomena such as thermal degradation, crosslinking and other desired or undesired processes can occur. These are very dependent upon moulding conditions, part design and tool design.

5.5 Dimensional stability


Factors such as orientation of polymer chains, internal stresses and filling rate of the cavity have an influence on performance characteristics of a part. Dimensional stability is thus dependent upon the control of all setting parameters on the moulding machine. Thermal stability tests can be carried out for shrinkage and/or deformation of parts following preconditioning at just above the resins heat distortion temperature. Complete mouldings should be used and a detailed study of each application is required to set correct parameters, using mouldings produced under optimal conditions.

36

37

5.6 Stress control


Due to tool or part design it is not always possible to produce really stress-free parts. For transparent materials such as Lexan resin it is often advisable to produce pre-production test

Injection Moulding mini guide 5 Quality Assurance

6
5.8 Other methods
Very reliable methods of quality control are tests according to government and agency standards such as VDE, KEMA, SEMKO, NEMKO, etc. For these standards, test methods for both application and material are provided. This avoids possible confusion between moulder and end-user. More and more computer-based control systems are used nowadays. Many new software and hardware tools enhances the quality of moulds, machines and mouldings produced with them. They give possibilities to optimize, visualize and monitor basic settings of the injection moulding machine. Using pressure sensors in moulds, filling phases can be analyzed to get information about orientation, appearance and crystallinity of moulded parts. Deviations of several shots following each other can be calculated statistically and monitored afterwards. Differences in quality can be signalled immediately.

Part defects and corrective actions


6.1 Fault diagnosis
If a part has been produced satisfactorily and it goes wrong, something has changed. The principle is not to change conditions immediately. The cause should be identified and rectified . Never adjust one condition to compensate for a failure or change in another condition. For example, if melt temperature has increased, dont reduce speeds or pressures or mould temperature to compensate. Identify problem , that is to say reduce melt temperature to what it was before, by checking and replacing thermocouples, etc.
Ask questions

what has changed ? what is fault? when did it start? how often does it occur? where is fault? is the fault randomly situated or always in same place? etc.
Identify causes of defects

38

test, observe, conclude and study history of faults injection speed: test screw speed: test back pressure: test melt temperature: test etc. machine: check
heating of cylinder mould temperature control material cushion locking of mould etc.

39

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2 Fault descriptions, causes and actions


6.2.1 Black specks 6.2.2 Blisters, bubbles

Dark spots due to thermal damage

Blisters can cause bulges on the surface

DESCRIPTION

DESCRIPTION

Small black areas (spots) inside the material, mostly present in transparent resins.
CAUSES

Small air-or gas-filled hollows in the moulding, cooling voids.


CAUSES

machine

mould

machine

down time too long barrel switched off over a long period of time poor purging of barrel dirty plasticizing unit inadequate nozzle

dead edges in gate/ runner system


material

granule impurities degradation by other resins pick-up of degraded material from cylinder wall during cooling

injection pressure too low inadequate functioning of back flow valve suck-back too long plasticizing too fast air trap in the hopper feed improper feed
mould

ACTIONS

IN ORDER AS SHOWN

volatiles and trapped gas mould temperature too low thin to thick transition
material

40

1. purge with an appropriate material in general: Kapronet for Lexan PC: ground acrylic or regrind Lexan resin for Ultem resin: regrind Ultem resin or glass-filled Lexan resin dont drop temp. settings while purging; (for details on purging, see pages 19 to 24) 2. check for impurities: use uncontaminated material, do proper housekeeping 3. check and adjust melt temperature 4. check for dead edges: nozzle, back flow valve, gates/runners 5. check for screw wear

melt overheating
ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7.

control holding / injection pressure increase back pressure increase mould temperature check back flow valve allow for adequate venting enlarge gate shorten land length

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Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.3 Blush / flow marks

6.2.4 Burn marks / diesel effect

Dull spot (corona) near the sprue

Diesel effect (burns) due to entrapped air at the end of the flow path

DESCRIPTION

DESCRIPTION

Blush and flow marks are the result of variations in material temperature, caused by the temperature gradient between machine nozzle and mould sprue bushing. A halo around the direct sprue is the result of cold material in the nozzle tip section. Eliminating the temperature gradient will minimize the blush and halo effects.
CAUSES

Burn marks are (often) brown streaks. They are usually caused by overheating the material due to entrapped air (diesel effect): this causes the darkening in colour.
CAUSES

machine

mould

machine

mould

injection speed too slow or too fast injection pressure too low hold pressure too long

inadequate mould cooling mould too hot around gate mould too cold gate too small wrong gate location gate land length too long wrong hot runner system
material

problems with back flow valve injection speed too fast back pressure too high

inadequate venting: entrapped air frictional burning check sprue diameter


material

melt too hot or too cold: may create shear


ACTIONS

IN ORDER AS SHOWN

melt temperature too low


ACTIONS

IN ORDER AS SHOWN

42

1. 2. 3. 4.

adapt injection speed add a large cold slug area add cold wells at the end of runner systems control nozzle heat better: if necessary add beryllium copper tip (not recommended for FR resins) 5. shorten or eliminate standard sprue bushing: use a hot sprue bushing 6. clean flow must exist from the cylinder, adaptor, nozzle and tip: avoid and eliminate any dead pockets or sections

check venting channels for dirt decrease injection speed decrease injection pressure use programmed injection check for heater malfunctioning reduce screw r.p.m. decrease nozzle temperature reduce melt temperature improve mould cavity venting - add vents to ejector pins - add vents to parting line of part 10. enlarge gate to reduce frictional burning 11. alter position and/or increase gate size

1. 2. 3. 4. 5. 6. 7. 8. 9.

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Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.5 Delamination

6.2.6 Dimensions of part

DESCRIPTION

Cosmetics article with flaked off skin

Excessive shrinkage means part dimensions differing from expected ones; amorphous resins behave differently to semi-crystalline materials.
CAUSES

machine

DESCRIPTION

Separation of layers in the moulded part that can be peeled off: flaking of surface layers. It results from insufficient layer bonding due to inhomogeneities and high shear stresses.
CAUSES

injection pressure too low injection hold pressure time too short overall cycle too short back flow valve cracked excessive cylinder clearance heater bands burned out
mould

machine

injection speed too high


mould

too hot gates too small (related to inadequate pressures) gating in the wrong place mould too small
IN ORDER AS SHOWN

mould too cold sharp corners in gate area shear heat caused at sharp corners
material

ACTIONS

melt too hot poorly melted incompatible colour dyes cross contamination with other polymers too much use of recycled material
IN ORDER AS SHOWN

ACTIONS

44

1. 2. 3. 4. 5. 6. 7. 8. 9.

increase melt temperature increase mould temperature decrease injection speed eliminate contamination check percentage regrind dry material purge equipment change material radius all sharp corners at gate

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11.

increase injection pressure increase cooling time increase mould temperature maintain uniform cycle time operation check machine for erratic operation check the percentage regrind to virgin material increase gate size reduce gate land length relocate gate if glass-filled compounds balance runner and/or gate system reduce number of cavities to balanced system

45

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.7 Discolouration

6.2.8 Flash

Colour streaks due to poor blending in the plasticizing unit

Large area overspraying

DESCRIPTION

DESCRIPTION

The appearance of areas in the moulding with a deviating colour.


CAUSES

A film of material attached to the moulding at the mould parting line.


CAUSES

machine

material

machine

contamination
mould

check sprue diameter pin-point too small poor venting

melt too hot or too low: may create shear long residence time instability of polymer/ pigments

clamping pressure too low injection pressure too high injection speed too fast
mould

ACTIONS

IN ORDER AS SHOWN

inadequate mould supports clamping force too low damaged mould surface: parting line excessive projected area
material

46

1. purge heating cylinder 2. lower material temperature by - reducing cylinder temperature - decreasing screw speed - reducing back pressure 3. lower nozzle temperature 4. check residence time 5. check machinery purging 6. shorten overall cycle 7. check hopper and feed zone for contaminants 8. check for proper cooling of ram and feed zone 9. provide additional vents in mould 10. move mould to smaller shot size press to reduce residence time

melt too hot viscosity too low


ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7. 8.

reduce injection speed reduce injection pressure and/or booster time increase clamping force check mould for proper mould support and/or parallelism reduce melt temperature reduce mould temperature check excessive vent depths change to higher clamping machine

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Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.9 Jetting

6.2.10 Pitting

DESCRIPTION

Jetting starting at the gate, spreading over the entire moulded part

Pitting is the presence of unmelted particles due to difficult dispersion of additives, wrong mixing or crosslinking during processing.
CAUSES

machine

wrong or worn out screw, giving hang-ups melt temperature too low injection pressure too low
DESCRIPTION

mould

A turbulent flow in the resin melt: the melt strand enters the cavity in an uncontrolled way. Due to cooling down, the strand is not fused homogeneously with the melt that follows. It shows as a serpentine line on the part surface. Too little restriction when filling the cavity: material is injected in empty space (wrong gate angle).
CAUSES

shear in gating sharp corners


material

inhomogeneous material contamination


ACTIONS

IN ORDER AS SHOWN

machine

injection speed too fast


mould

mould too cold gates too small gate land length wrong wrong gate location
material

1. 2. 3. 4. 5. 6. 7.

get shear down lower back pressure decrease injection speed change temperature profile check regrind percentage check shot size vs part check hot-runner: torpedoes

melt too cold


ACTIONS

IN ORDER AS SHOWN

48

1. 2. 3. 4. 5. 6. 7. 8.

decrease injection speed check nozzle heating increase mould temperature increase melt temperature increase gate size avoid gating at thick section modify gate location or angle: directly into wall or pin use tab gate or submarine plus pin

49

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.11 Record grooves

6.2.12

Release problems

6.2.12.1 Sticking in cavity

Concentric record grooves

DESCRIPTION

At end of cycle, the moulding does not release from the mould but sticks in the cavity (female mould side).
CAUSES

machine

DESCRIPTION

Resembles the grooves of gramophone records. At slow speed - as material nears cold tool - it loses its flow (below HDT) before actual contact. The melt that follows flows over cooled melt, to repeat the cycle.
CAUSES

injection pressure too high injection speed too high holding time too long too much material feed
mould

cavity too hot release is better from hot mould (20C below HDT) mould too cold poor mould finish
material

machine

injection speed too low injection pressure too low


mould

melt too hot


ACTIONS

IN ORDER AS SHOWN

mould too cold different texture of mould halves: polished vs coarse grain
material

melt too cold


ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13.

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1. 2. 3. 4. 5.

increase injection speed increase injection pressure increase melt temperature increase mould temperature check mould textures

check cycle time: cooling decrease injection pressure decrease injection hold time decrease injection speed decrease booster time reduce and adjust feed for constant cushion check for poor mould finish or corrosion on mould surface increase mould opening time decrease material temperature by lowering cylinder temperatures and/or nozzle lower mould temperature adjust the cavity temperature to a 20C differential between mould halves check mould for undercuts and/or insufficient draft and taper use proper mould release

51

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.12.2 Sticking on core

6.2.12.3 Sticking of sprue

DESCRIPTION

DESCRIPTION

At end of cycle, the moulding does not release from the mould but sticks on the core (male mould side).
CAUSES

At end of cycle, the sprue does not release from the mould but sticks in the sprue bushing.
CAUSES

machine

machine

injection pressure too high


mould

core too hot core bending creation of vacuum especially on thin-walled parts
ACTIONS

injection pressure too high too much material feed nozzle frozen nozzle diameter too large for sprue bush inadequate draft angle drool from nozzle
mould

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7. 8. 9. 10.

check cycle time: cooling decrease injection pressure decrease injection hold time decrease booster time adjust feed for constant cushion decrease mould-closed time increase core temperature decrease cylinder and nozzle temperature check mould for undercuts and/or insufficient draft check mould for bending: rule of thumb is 1:5 for core diameter to core length

too hot ineffective sprue pullers


ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13.

52

decrease injection pressure decrease injection hold time decrease booster time increase die-closed time decrease mould temperature at sprue bushing leave nozzle against mould: no pull back raise nozzle temperature check incorrect seat between nozzle and sprue: sizes and alignment of holes in nozzle and sprue bushing sprue bushing hole must be larger: reduce nozzle diameter for sprue bushing being used check polishing of sprue check proper design of sprue puller pin check cone of sprue: usually 1:20, for difficult jobs 1:15 provide more effective sprue puller: - increase sprue puller by increasing taper of sprue puller - polish worn or rough sprue bushing

53

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.13 Short shots

ACTIONS

IN ORDER AS SHOWN

Solidified flow front on a glass fibre reinforced housing

1. 2. 3. 4. 5. 6. 7. 8. 9.

DESCRIPTION

increase dosage increase injection pressure increase booster time forward increase material temperature by increasing cylinder temperatures increase mould temperature, if glass-filled check material flow length vs wall section thickness increase nozzle diameter check restrictions of nozzle, runners and actual gating increase gate size of sprue and runner system

Resulting from incomplete filling of the mould: parts of the moulding are not formed.
CAUSES

machine

improper feed injection pressure too low injection speed too low injection time too short faulty back flow valve ring
mould

poor mould venting mould too cold


material

melt temperature too low viscosity too high

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55

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.14 Sink marks

ACTIONS

IN ORDER AS SHOWN

Sink marks due to wall thickness variations

1. 2. 3. 4. 5. 6. 7.

DESCRIPTION

Visible defects resulting from insufficient cooling before removal from the mould. A heavy rib intersecting a thin wall may show up sink marks: these are very difficult to eliminate by varying processing conditions. Too high holding pressure useless when gating is too small creates very high stresses in gate areas.
CAUSES

8. 9. 10. 11. 12. 13.

increase injection speed to maximum range sometimes lower injection speed: crystalline materials increase injection hold time increase injection pressure reduce melt temperature reduce mould temperature check for hot spots: separate water channels in cooling system / add heat pipes such as thermal pins or beryllium copper slugs for spot cooling enlarge and/or add vents to mould parting line increase size of sprue and/or runners increase gate size and reduce gate land length relocate gate next to heavy or thicker areas core out heavy wall sections where possible incorporate textured surfaces

machine

injection pressure too low injection pressure time too short short of shot capacity
mould

mould temperature too high: too high shrinkage gate too small: leads to early cooling/freezing at the gate, holding pressure cannot help anymore to compensate for the shrinkage land length too long wrong dimensions rib vs wall
material

56

melt too hot

57

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.15

Splay / streaks

6.2.15.1 Splay

DESCRIPTION

Splay marks, silver streaks, splash marks are the result of (a) moisture on the pellets which should be removed under recommended drying times and temperatures (b) products of degradation due to overheating (c) residual non-aqueous volatiles in material (a) and (c) will produce fine lines emanating from the gate all over the part whereas (b) will show up as coarse lines, lumps in sections of the moulded parts.
CAUSES

6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16.

decrease injection speed raise mould temperature shorten or eliminate screw decompression shorten overall cycle increase back pressure; in case of drooling, reduce back pressure check for drooling check for contamination (e.g. water or oil leaking into mould cavity) barrel purging (hang-ups) allow for adequate venting open gates move mould to smaller shot-size press

machine

degraded material
hot spot in cylinder material hang-up area at nozzle tips or adaptors

6.2.15.2 Gate splay

DESCRIPTION

injection pressure too low or too high injection speed too low or too high back pressure too low
mould

frictional burning at gate, in machine nozzle or hot runner trapped volatiles


material

Gate splay is the appearance of dull spots around the gate, resulting from temperature differences in the material, (too high shear forces tearing the surface layer). Often moisture streaking resulting from improper pre-drying.
CAUSES

melt too hot contamination in resin excessive moisture Noryl resin: degradation of material due to too long pre-drying at high temperatures
IN ORDER AS SHOWN

machine

injection too fast


mould

mould too cold gate too small improper gate location or too sharp angle gate to part
material

ACTIONS

58

1. check pre-drying: dry material before use 2. check moisture content after pre-drying 3. check effectiveness of drying equipment: temperature and time 4. lower nozzle temperature 5. lower material temperature by: - lowering cylinder temperature - decreasing screw speed - lowering back pressure

melt too cold


ACTIONS

59

IN ORDER AS SHOWN

1. 2. 3. 4. 5.

decrease injection speed increase mould temperature increase melt temperature increase gate size change gate location

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.15.3 Streaking

DESCRIPTION

The appearance of large, dull and lamellar areas on the surface of a moulding.
CAUSES

Burnt streaks due to excessive residence time in the plasticizing cylinder

machine

damaged back flow valve ring


mould

areas of hang-up hot spots


material

contamination caused by stock or machine


if steady pattern: machine if erratic pattern: material pigmentation / instability of material
ACTIONS

Streaks due to excessive moisture content of the granules

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7.

check for material contamination by other resins check barrel purging check for cracked or worn back flow valve ring check for worn feed screw check for excessive clearance on screw/barrel dimensions check for overheated cylinder heater bands check for overheated nozzle heater bands

Air streak (near the sprue) due to sucked in air during decompression

60

Glass fibre streaks (clearly visible weld line)

61

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.16 Stringing

6.2.17 Voids

DESCRIPTION

DESCRIPTION

Stringing is the appearance of a thin plastic string coming from the sprue.
CAUSES

Vacuole hollows (empty bubbles) in the moulding, due to thermal shrinkage that draws material away from the fluid core of a part.
CAUSES

machine

back pressure too high nozzle temperature too high


mould

machine

wrong sprue
material

injection pressure too low injection pressure time too short injection speed too high back pressure too low
mould

insufficient melt strength


CORRECTIONS

TRY IN ORDER AS SHOWN

1. 2. 3. 4. 5.

use suck back: only for crystalline materials lower back pressure lower or increase nozzle temperature use different temperature profile do not use sprue breaks

mould temperature too low incorrect material flow part wall too thick
material

melt too hot wrong material grade: some Lexan resin types more sensitive
ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5.

decrease injection speed to medium range increase holding time reduce melt temperature increase mould temperature check gate size: too small results in freezing at gate with voids and sinks in other areas of the part 6. increase gate size and reduce gate land length 7. increase nozzle size and/or runner system 8. redesign part to obtain equal wall sections

62

63

Injection Moulding mini guide 6 Part Defects and Corrective Actions

Injection Moulding mini guide 6 Part Defects and Corrective Actions

6.2.18 Warpage, part distortion

6.2.19 Weld lines / knit lines

DESCRIPTION

A dimensional deformation of the moulding resulting from frozen-in stress, or because the part was taken too hot from the mould. Basically it is due to pressure differences between areas.
CAUSES

Colour differences at a weld line

part

mould

wrong part design part too heavy


machine

insufficient cooling time too high injection pressure

wrong gate location: different shrinkage in different flow directions too big undercuts inadequate ejector pins cavity too hot
material

DESCRIPTION

orientation of fillers wrong material choice


ACTIONS

These lines occur where two plastics flow fronts in the mould meet. The streams of plastic should be hot enough to fuse adequately. Weld lines are not just surface marks, but can be points of weakness: notches, stress raisers.
CAUSES

IN ORDER AS SHOWN

part

mould

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16.

64

equalize temperature of both mould halves observe mould for uniform part ejection check handling of parts after ejection from mould check part weight: take care with Valox resin increase injection hold time increase cooling time increase or reduce injection pressure increase mould close time increase or reduce mould temperature set differential mould temperatures to counteract warpage due to part geometry use shrink fixtures and jigs for uniform cooling of the part check gate locations and total number of gates to reduce orientation additional gates may be required to overcome overpacking or underpacking on large parts increase gate dimensions change gate location if glass-filled, notice fibre orientation redesign part to equalize wall variation in moulded part heavy and thin walls in same part create differential shrinkage stresses

wrong part design


machine

injection speed too slow injection pressure too low injection time forward too short

mould too cold insufficient venting inaccurate functioning of back flow valve distance from gate excessive
material

melt too cold


ACTIONS

IN ORDER AS SHOWN

1. 2. 3. 4. 5. 6. 7. 8. 9.

increase injection pressure increase injection hold time increase injection speed raise melt temperature by increasing cylinder temperatures raise mould temperature check for proper venting of the part vent the cavity in the weld area provide an overflow well next to the weld area change gate location to alter flow pattern

65

>>>

Injection Moulding mini guide 6 Part Defects and Corrective Actions

7
10. increase gate and/or main runner system 11. reduce gate land length 12. spot heat particular area with thermal pins or cartridge heaters 13. use textured surfaces

Reusing materials
Thermoplastics resins in general can be recycled into similar applications: this means that a company can grind, clean and eventually upgrade the material. GE Plastics product range of selected post-consumer recycle materials is called Remex Engineering Plastics. This activity of reusing materials is called recycling . During production, such as with injection moulding, sprues, faulty mouldings, short shots, and so on, can be reground directly in the production facility and reused. This can be done by using reground resin on its own, or by mixing regrind with virgin material. This activity of reusing materials is called regrinding . To avoid misunderstanding, only regrinding will be discussed here. Sprues, runners and faulty mouldings produced from GE Plastics resins can all be reground. Care should be taken to ensure that reground material is not degraded and is clean and free from impurities. Parts that show traces of over heating or burning, and also parts with humidity related defects such as splash, should never be reground. Obviously reground materials should be of the same composition and not be mixed with other plastic grades. If there is the slightest doubt whether degradation or contamination has occurred, the material should not be reused. It is also very important that reground materials are properly pre-dried, as with virgin materials. Although many resins show minimal reduction in properties after regrinding, special attention is required to ensure that reground materials in principle are not used for impact critical applications. Care must also be taken when reusing flame retardant or heavily pigmented materials.

66

67

Injection Moulding mini guide 7 Reusing Materials

Injection Moulding mini guide 7 Reusing Materials

In general, it is very difficult to quantify what mixing percentages of reground : virgin material are possible. These differ from case to case, being related to customerdefined part quality requirements and applicable standards and regulations. The following factors should be borne in mind when using reground materials: - moulding conditions of first moulding process - impact behaviour of final parts - flame retardancy, UL requirements - UV resistance - colour stability - chemical resistance - physical properties - preparation of material prior to use - disposal of dirty parts - proper pre-drying - moulding conditions of second moulding process GE Plastics understands that the plastics processing community wants to take advantage of this important feature of thermoplastics materials. Therefore, while the company can only be held liable for the quality of delivered of virgin material, it is committed to supplying the information which will allow processors to achieve the levels of quality and performance expected by customers. GE Plastics recommends the use of a specific methodology wherever plastics are to be reground for reuse. The recommended methodology to determine whether, and to what extent, reground materials can be used for the production of industrial products is as follows: - define the critical characteristics and the acceptable level of performance in agreement with the final end-user - conduct trials with different mixing levels of regrind, for example in steps of 10, 20, 30%, etc. - measure the characteristics of the parts produced with these levels

- compare the obtained values with the acceptable level of performance and select accordingly - agree with the end-user the maximum acceptable proportion of regrind

68

69

References
Spuitgieten Kort en Bondig, Werkmetaal, 1990 * Handbuch der Temperierung mittels flssiger Medien, Regloplas, 1992 * Guide to surface defects on thermoplastic injection molded parts, K.I.M.W., 1992 ** Total Quality Process Control for Injection Molding, M.J. Gordon, 1993 Understanding Injection Molding Technology, Herbert Rees, 1994 How to Make Injection Molds, Menges/Mohren, 1993 Plastic Part Design for Injection Molding, Robert A. Malloy, 1994 Spritzgiewerkzeuge, Menges/Mohren, 1991 Injection Molds, Gastrow, 1993 Injection moulding of thermoplastics, Christof Kempf, Michael Renger, 1992 Schnelles betriebssicheres Einstellen der Spritzgiemaschine, Bhler Einfhrung in die Kunststoffverarbeitung, Walter Michaeli, 1992 Injection Molding of Engineering Thermoplastics, Tony Whelan, John Goff, 1990 Maschineneinstellstrategie fr Spritzgiemaschinen, Klaus Niemann, 1992 several internal and external GE Plastics publications numerous suggestions given by GE Plastics specialists * A word of thanks for the permission to quote
some phrases ** A word of thanks for the permission to use pictures of mouldings with defects

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GE Plastics
European Headquarters General Electric Plastics B.V. 1 Plasticslaan, PO Box 117 NL - 4600 AC Bergen op Zoom The Netherlands Tel. (31) (164) 29 29 11 Fax (31) (164) 29 29 40 Headquarters Sales Region General Electric Plastics B.V. Gagelboslaan 4 NL - 4623 AD Bergen op Zoom The Netherlands Tel. (31) (164) 29 23 91 Fax (31) (164) 29 17 25 United Kingdom GE Plastics Limited Old Hall Road Sale Cheshire M33 2HG United Kingdom Tel. (44) (161) 905 50 00 Fax (44) (161) 905 51 19 Germany General Electric Plastics GmbH Eisenstrae 5 D - 65428 Rsselsheim Germany Tel. (49) (6142) 6010 Fax (49) (6142) 65746 France General Electric Plastics France S..R.L. Z.I. St. Gunault B.P. 67 F - 91002 Evry-Cedex France Tel. (33) (1) 60 79 69 00 Fax (33) (1) 60 77 56 53 Italy General Electric Plastics Italia S.p.A. Viale Brianza, 181 I - 20092 Cinisello Balsamo (Milano) Italy Tel. (39) (02) 61 83 41 Fax (39) (02) 61 83 42 11 Spain General Electric Plastics Ibrica S.A Avenida Diagonal, 652-656 Edificio D. Planta 3 08034 Barcelona Spain Tel. (34) (93) 252 16 00 Fax (34) (93) 280 26 19 DISCLAIMER: THE MATERIALS AND PRODUCTS OF THE BUSINESSES MAKING UP THE GE PLASTICS UNIT OF GENERAL ELECTRIC COMPANY, USA, ITS SUBSIDIARIES AND AFFILIATES (GEP), ARE SOLD SUBJECT TO GEPS STANDARD CONDITIONS OF SALE, WHICH ARE INCLUDED IN THE APPLICABLE DISTRIBUTOR OR OTHER SALES AGREEMENT, PRINTED ON THE BACK OF ORDER ACKNOWLEDGMENTS AND INVOICES, AND AVAILABLE UPON REQUEST. ALTHOUGH ANY INFORMATION, RECOMMENDATIONS, OR ADVICE CONTAINED HEREIN IS GIVEN IN GOOD FAITH, GEP MAKES NO WARRANTY OR GUARANTEE, EXPRESS OR IMPLIED, (I) THAT THE RESULTS DESCRIBED HEREIN WILL BE OBTAINED UNDER END-USE CONDITIONS, OR (II) AS TO THE EFFECTIVENESS OR SAFETY OF ANY DESIGN INCORPORATING GEP MATERIALS, PRODUCTS, RECOMMENDATIONS OR ADVICE. EXCEPT AS PROVIDED IN GEPS STANDARD CONDITIONS OF SALE, GEP AND ITS REPRESENTATIVES SHALL IN NO EVENT BE RESPONSIBLE FOR ANY LOSS RESULTING FROM ANY USE OF ITS MATERIALS OR PRODUCTS DESCRIBED HEREIN. Each user bears full responsibility for making its own determination as to the suitability of GEPs materials, products, recommendations, or advice for its own particular use. Each user must identify and perform all tests and analyses necessary to assure that its finished parts incorporating GEP materials or products will be safe and suitable for use under end-use conditions. Nothing in this or any other document, nor any oral recommendation or advice, shall be deemed to alter, vary, supersede, or waive any provision of GEPs Standard Conditions of Sale or this Disclaimer, unless any such modification is specifically agreed to in a writing signed by GEP. No statement contained herein concerning a possible or suggested use of any material, product or design is intended, or should be construed, to grant any license under any patent or other intellectual property right of General Electric Company or any of its subsidiaries or affiliates covering such use or design, or as a recommendation for the use of such material, product or design in the infringement of any patent or other intellectual property right. * Company not connected with the English company of a similar name. Lexan, Noryl, Noryl GTX, Noryl Xtra, Valox, Ultem, Xenoy, Cycolac, Cycoloy and Enduran are Registered Trademarks of General Electric Co., USA. Gelon is a Trademark of General Electric Co., USA.

Injection Moulding mini guide

IMG Eng/3M/0998

For your convenience, the preference for Max Fit Visible Magnification should be changed from 800% to 150%.
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