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SURFACE VEHICLE J1 703 AUG201 4

STANDARD I ssu ed 1 9 46 - 1 2

R e vi s e d 2 0 1 4- 0 8

S u p e rs e d i n g J 1 7 0 3 AU G 2 0 1 2

M o to r Ve h i cl e Brake Fl u i d

R ATI O N ALE

S AE J 1 7 0 3 h as be en e d i te d to co rre l ate Tabl e 1 , Te s t Pro ce d u re n u m beri n g wi th th e Tes t P ro ce d u re S e cti o n s .

1 . SCOP E

Th i s S AE S tan d ard co vers m o to r ve h i cl e brake fl u i d s of th e n o n pe tro l e u m type , bas e d u po n g l yco l s , g l yc o l eth e rs an d

appro pri ate i n h i b i to rs , fo r u s e in th e braki n g s ys te m o f an y m o to r ve h i cl e s u ch as a pas s en g e r car, tru ck, bu s , o r trai l er.

Th e s e fl u i d s are n o t i n te n d e d fo r u s e u n d e r arcti c co n d i ti o n s . Th e s e fl u i d s are desi g n ed fo r u s e i n braki n g s ys te m s fi tte d

wi th ru bb er cu ps an d s eal s m ad e from s tyren e - b u tad i e n e ru bbe r ( S B R ) , o r a te rpo l ym er o f e th yl en e , pro p yl en e , an d a d i e n e

(EPD M ) .

2. R E FE R E N C E S

2. 1 App l i cabl e D o cu m e n ts

Th e fo l l o wi n g pu b l i cati o n s fo rm a part o f th i s s pec i fi cati o n to th e e xten t s pe ci fi e d h e rei n . U n l ess o th erwi s e i n d i cate d , th e

l ates t i s s u e o f S AE pu bl i cati o n s s h al l ap pl y.

2. 1 . 1 S AE P u b l i cati o n s

Avai l ab l e from S AE I n te rn ati o n al , 40 0 C o m m o n weal th D ri ve , W arre n d al e , P A 1 5 0 9 6- 0 0 0 1 , Te l : 87 7- 6 0 6 - 73 2 3 ( i n s i d e U S A

an d C an ad a) o r 72 4- 7 76- 4 9 70 ( o u ts i d e U S A) , www. s ae. o rg .

S AE J 5 2 7 Braze d D o u b l e W al l Lo w- C arbo n S te e l Tu b i n g

S AE J 1 7 0 4 M o to r Ve h i cl e Brake Fl u i d bas e d u po n g l yco l s , g l yco l e th e rs an d th e co rres po n d i n g b o rate s

__________________________________________________________________________________________________________________________________________

S AE Tech n i cal S t an d ard s B o ard R u l e s pro vi d e th at: “Th i s rep o rt i s pu bl i s h ed b y S AE to ad van c e th e s tate o f tec h n i c al an d en g i n e eri n g s ci en c e s . Th e u s e o f th i s rep o rt i s e n ti rel y

vo l u n ta ry, an d i ts ap pl i cabi l i ty an d s u i ta bi l i ty fo r an y parti c u l ar u s e , i n cl u d i n g an y pate n t i n fri n g em e n t a ri s i n g t h e re fro m , i s th e s o l e re s po n s i bi l i t y o f th e u s er. ”

S AE revi e ws each tech n i cal re po rt at l eas t eve ry fi ve ye ars at wh i ch ti m e it m ay be revi s e d , re affi rm e d , s tabi l i ze d , or c an c el l e d . S AE i n vi te s yo u r wri tte n co m m e n ts an d

s u g g e s ti o n s .

C o p yri g h t © 2 0 1 4 S AE I n te rn ati o n al

Al l ri g h ts res e rved . N o part o f th i s pu bl i c ati o n m ay be re pro d u ce d , s to red i n a ret ri eval s ys te m o r tran s m i tted , i n an y fo rm o r b y an y m ea n s , el ect ro n i c, m e ch a n i c al , p h o to co p yi n g ,

reco rd i n g , o r o th e rwi s e , wi th o u t th e pri o r wri tten p erm i s s i o n o f S AE .

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2. 1 . 2 AS TM P u bl i cati o n s

Avai l ab l e from AS TM I n tern ati o n al , 1 0 0 B arr H arbo r D ri ve, P . O . B o x C 7 0 0 , W es t C o n s h o h o cken , P A 1 9 42 8- 2 9 5 9 , Te l : 6 1 0 -

83 2 - 9 58 5 , www. as tm . o rg

AS TM D 3 4- 0 8 S tan d ard G u i d e fo r C h em i cal An al ys i s o f W h i te P i g m e n ts

AS TM D 9 1 Te s t M eth o d fo r P rec i pi tati o n N u m be r o f Lu bri cati n g O i l s

AS TM D 3 44 M e th o d o f Te s t fo r R e l ati ve D ry H i d i n g P o wer o f P ai n ts

AS TM D 3 9 5 Te s t M e th o d s fo r R u b be r P ro pe rty - C o m pre s s i o n S e t

AS TM D 4 1 2 Te s t M e th o d s fo r R u b be r P ro pe rti es i n Ten s i o n

AS TM D 4 45 Te s t M e th o d fo r Ki n e m ati c Vi s co s i t y o f Tran s pare n t an d O paq u e Li q u i d s ( an d th e C al cu l ati o n o f D yn am i c

Vi s co s i t y)

AS TM D 6 6 4 Te s t M eth o d fo r N e u tral i zati o n N u m be r o f P o ten ti o m e tri c Ti trati o n

AS TM D 2 1 3 7 S tan d ard Te s t M e th o d s fo r R u bb e r P ro pe rty- Bri ttl e n e s s P o i n t o f Fl e x i bl e P o l ym e rs an d C o ate d Fabri cs

AS TM D 8 6 5 Te s t M eth o d fo r R u bbe r - D ete ri o rati o n b y h e at i n g i n Ai r ( Tes t Tu be E n cl o s u re )

AS TM D 1 1 2 0 M e th o d o f Te s t fo r B o i l i n g P o i n t o f E n g i n e C o o l an ts

AS TM D 1 2 0 9 Te s t M e th o d fo r C o l o r o f C l e ar Li q u i d s ( P l ati n u m - C o bal t P i g m e n ts )

AS TM D 1 3 64 Te s t M e th o d fo r W ater i n Vo l ati l e S o l ve n ts ( Fi s ch e r R e ag e n t Ti trati o n M e th o d )

AS TM D 1 41 5 M e th o d o f Te s t fo r I n tern ati o n al H ard n e s s o f Vu l can i ze d N atu ral R u b be r an d S yn th eti c R u bb e rs

AS TM D 1 6 1 3 Te s t M e th o d fo r Aci d i t y i n Vo l ati l e S o l ve n ts an d C h e m i cal I n te rm ed i ate s U s e d i n P ai n t, Varn i s h , Lacq u er,

an d R e l ate d P ro d u cts

AS TM D 2 2 40 M e th o d o f Te s t fo r I n d en tati o n H ard n e s s o f R u b be r an d P l as ti cs b y M ean s o f a D u ro m ete r

AS TM D 3 1 82 R eco m m e n d e d P racti ce fo r R u bbe r- M ate ri al s , E q u i pm e n t, an d P ro ce d u res fo r M i xi n g S tan d ard

C o m po u n d s an d P re pari n g S tan d ard Vu l can i zed S h e e ts

AS TM D 3 1 85 M e th o d s fo r R u bb er- E val u ati o n o f S B R ( S t yre n e - Bu tad i en e R u bbe r) i n cl u d i n g M i xtu re s wi th O i l

AS TM E 1 S pe ci fi cati o n fo r AS TM Th e rm om e ters

AS TM E 1 45 S pe ci fi cati o n fo r G ravi t y- C o n vecti o n an d Fo rce d - Ven ti l ati o n O ve n s

2. 2 R e l ate d P u bl i cati o n s

Th e fo l l o wi n g pu b l i cati o n s are pro vi d e d fo r i n fo rm ati o n pu rpo s e s o n l y an d are n ot a re q u i re d p art of th i s S AE Te ch n i cal

Re po rt.

2. 2 . 1 AS TM P u bl i cati o n s

Avai l ab l e from AS TM I n te rn ati o n al , 1 0 0 B arr H arbo r D ri ve , P . O . B o x C 7 0 0 , W es t C o n s h o h o cke n , P A 1 9 42 8 - 2 9 5 9 , Tel : 61 0 -

83 2 - 9 5 85 , www. as tm . o rg

AS TM E 2 60 S tan d ard R eco m m e n d e d P racti ce fo r G e n eral G as C h ro m ato g raph y P ro ce d u re

AS TM E 2 9 8 E val u ati o n o f Be n zo yl P e ro xi d e s
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3. M ATE R I ALS

Th e q u al i t y o f th e m ate ri al s u s e d s h al l b e s u ch th at th e re s u l ti n g pro d u ct wi l l co n fo rm to th e req u i rem e n ts o f th i s s tan d ard

an d i n s u re u n i fo rm i ty o f pe rfo rm an ce .

4. R E Q U I R E M E N TS

R eq u i rem e n ts are g i ve n i n Tabl e 1 , u s i n g th e tes t pro ced u res acco rd i n g to S e cti o n 5 .

TABLE 1 - S AE J 1 70 3 TE S T P R O C E D U R E S AN D R E Q U I R E M E N TS

Test
Procedure Test Description Unit Requirements
Section
5.1 Equilibrium Reflux Boiling Point (ERBP)
5.2 Wet Equilibium Reflux Boiling Point (WERBP) °C ≥ 205
°C ≥ 1 40

5.3 Viscosity
5. 3. 1 at - 40 ° C m m ²/s ≤ 1 500
5. 3. 2 at 1 0 0 ° C m m ²/s ≥ 1 .5

5.4 pH Value - 7. 0 to 1 1 . 5

5.5 Fluid Stability °C ± 5

5. 5. 1 H i g h te m pe ratu re S tabi l i t y
°C ± 5
5. 5. 2 C h e m i cal S tabi l i t y

5.6 Metal Corrosion

5. 6. 1 W et C o rro s i o n

M e tal S tri p C h aracte ri s ti cs , afte r tes t

W e i g h t C h an g e o f M e tal S tri ps M axi m u m

Ti n n e d I ro n m g /cm ² ± 0. 2

S te e l m g /cm ² ± 0. 2

Al u m i n i u m m g /cm ² ± 0. 1

C as t I ro n m g /cm ² ± 0. 2

Bras s m g /cm ² ± 0. 4

C o p pe r m g /cm ² ± 0. 4

Ap pe aran ce - N o P i tti n g o r ro u g h n es s o u ts i d e

co n tact are a

S tai n i n g an d d i s co l o rati o n - P e rm i tte d

Li q u i d ch aracte ri s ti cs after te s t

Ap pe aran ce - N o g e l l i n g o r crys tal l i n e d e po s i t

pH Val u e - 7. 0 to 1 1 . 5

Se d i m en t % ≤ 0.1

R u bb er C h aracte ri s ti cs , afte r tes t

S B R ( R M - 0 3 a)

B l i s te rs o r s l o u g h i n g - N on e

H ard n e s s d e cre as e, m axi m u m I RH D 1 5

B as e d i am e te r i n creas e , m axi m u m mm 1 .4

E P D M ( R M - 69 )

B l i s te rs o r s l o u g h i n g - N on e

H ard n e s s d e cre as e, m axi m u m I RH D 1 0

Vo l u m e i n cre as e % 0 to 1 0
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TABLE 1 - S AE J 1 70 3 TE S T P R O C E D U R E S AN D R E Q U I R E M E N TS ( C O N TI N U E D )

Test
Procedure Test Description Unit Requirements
Section
5. 6 . 2 D ry Fl u i d ( as rece i ve d ) –

M e tal S tri p C h aracte ri s ti cs , after tes t

W e i g h t C h an g e o f M e tal S tri ps M axi m u m

2
Ti n n e d I ro n m g /cm ± 0. 2

2
S te el m g /cm ± 0. 2

2
Al u m i n u m m g /cm ± 0. 1

2
C as t I ro n m g /cm ± 0. 2

2
Bras s m g /cm ± 0. 4

2
C o p pe r m g /cm ± 0. 4

Ap pearan ce - N o p i tti n g o r ro u g h n e s s o u ts i d e

co n tact are a

S tai n i n g an d d i s co l o rati o n - P erm i tte d

Li q u i d C h aracate ri s ti cs , afte r te s t

Ap pearan ce N o g e l l i n g o r crys tal l i n e d e po s i ts

pH Val u e - 7. 0 to 1 1 . 5

S e d i m en t % ≤ 0.1
R u bbe r C h aracte ri s ti cs , afte r te s t

S B R ( R M - 0 3 a)

B l i s te r N on e

Sl ou g h i n g N on e

EP DM (RM -69)

B l i s te r N on e

Sl ou g h i n g N on e

5.7 Fluidity and Appearance at Low Temperatures

5 . 7. 1 At - 40 ° C

S trati fi cati o n - N on e

S e d i m en tati o n / cr ys tal i zati o n - N on e

Bu bbl e I n ve rs i o n Ti m e s ≤ 10
Ap pearan ce at R o o m Tem pe ratu re - As o ri g i n al

5 . 7. 2 At - 50 ° C

S trati fi cati o n - N on e

S e d i m en tati o n / cr ys tal i zati o n - N on e

Bu bbl e I n ve rs i o n Ti m e s ≤ 35
Ap pearan ce at R o o m Tem pe ratu re - As o ri g i n al

5.8 Water Tolerance

5. 8. 1 At - 40 ° C

S trati fi cati o n - N on e

S e d i m en tati o n / cr ys tal i zati o n - N on e

C o n tras t l i n e s o n h i d i n g p o we r

ch art to be d i s ce rn i b l e wh e n

Ap pearan ce - vi e we d th ro u g h fl u i d .

Bu bbl e I n ve rs i o n Ti m e s ≤ 10
5 . 8. 2 At 6 0 ° C

S trati fi cati o n - N on e

S e d i m en tati o n % vo l ≤ 0.05
S e d i m en t i n C o m m e rci al P ackag e d fl u i d % vo l ≤ 0.1 5
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TABLE 1 - S AE J 1 70 3 TE S T P R O C E D U R E S AN D R E Q U I R E M E N TS ( C O N TI N U E D )

Test
Procedure Test Description Unit Requirements
Section
5.9 Compatibility
5. 9 . 1 At - 40 ° C

S trati fi cati o n - N on e

S e d i m e n tati o n / cr ys tal i zati o n - N on e

C o n tras t l i n e s o n h i d i n g p o wer

ch art to be d i s ce rn i bl e wh e n

Ap pe aran ce - vi e wed th ro u g h fl u i d .

5. 9 . 2 60°C

S trati fi cati o n - N on e

S e d i m e n tati o n % vo l ≤ 0.05
5.1 0 Resistance to Oxidation
N o P i tti n g o r ro u g h n es s o u ts i d e

co n tact are a. N o m o re th an a
M e tal App earan ce -
trace o f g u m .

S tai n i n g / D i s co l o rati o n - P e rm i tte d

W ei g h t l o s s o f Al u m i n i u m m g /cm ² ≤ 0.05
W ei g h t l o s s o f C as t I ro n m g /cm ² ≤ 0.3
5.1 1 Effect on Rubber
5. 1 1 . 1 S tyre n e bu tad i en e R u bbe r ( S BR ) R M - 0 3 a

At 7 0 ° C

H ard n e s s d e cre as e I RH D 0 to 1 0

Bas e D i am e te r i n creas e mm 0 . 1 5 to 1 . 4

Bl i s ters - N on e

Sl ou g h i n g - N on e

5. 1 1 . 2 At 1 2 0 ° C

H ard n e s s d e cre as e I RH D 0 to 1 5

Bas e D i am e te r i n creas e mm 0 . 1 5 to 1 . 4

Bl i s ters - N on e

Sl ou g h i n g - N on e

5. 1 1 . 3 E th yl e n e P ro p yl en e D i e n e M o n o m e r ( E P D M ) R M - 6 9

At 7 0 ° C

H ard n e s s d ecre as e I RH D 0 to 1 0

Vo l u m e i n cre as e % 0 to 1 0

Bl i s ters - N on e

Sl ou g h i n g - N on e

5. 1 1 . 4 At 1 2 0 ° C

H ard n e s s d ecre as e I RH D 0 to 1 5

Vo l u m e i n cre as e % 0 to 1 0

Bl i s ters - N on e

Sl ou g h i n g - N on e
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5. TE S T P R O C E D U R E S

5. 1 E q u i l i bri u m R e fl u x Bo i l i n g P o i n t

D ete rm i n e th e e q u i l i bri u m re fl u x bo i l i n g po i n t o f th e brake fl u i d b y AS TM D 1 1 2 0 wi th th e fo l l o wi n g e xce pti o n s :

5. 1 . 1 App aratu s

5. 1 . 1 . 1 Th e rm om ete r

AS TM E 1 , 7 6 m m i m m ers i o n , cal i brate d . U s e AS TM 3 C o r 3 F th erm om ete r. Fo r fl u i d s b o i l i n g b e l o w 3 0 0 ° C ( 5 72 ° F) , AS TM

2 C o r 2 F th e rm om e ter o r o th e r s u i tab l e n o n - m ercu ry co n tai n i n g te m pe ratu re m eas u ri n g d e vi ce , s u ch as a th e rm o co u pl e,

capab l e o f o p e rati n g i n th e s am e te m pe ratu re ran g e an d h avi n g eq u al o r b e tter accu rac y m ay b e u s e d .

5. 1 . 1 . 2 H eat S o u rce

H e at s o u rce , vari ab l e au to tran s fo rm e r- co n tro l l e d h e ati n g m an tl e d e s i g n e d to fi t th e fl ask, o r an e l e ctri c h eate r wi th rh e o s tat

h e at co n tro l .

5. 1 . 1 . 3 Bo i l i n g P o i n t S to n es R M - 75

S i l i co n C arb i d e B o i l i n g S to n es #8 .

5. 1 . 1 . 4 P re parati o n o f Apparatu s

Th o ro u g h l y cl e an an d d ry al l g l as s ware be fo re u s e. Attach th e fl as k to th e co n d e n s e r. P l ace th e m an tl e u n d e r th e fl as k an d

s u ppo rt i t wi th a s u i tab l e ri n g cl am p an d l ab o rato r y t yp e s tan d , h o l d i n g th e wh o l e as s em bl y i n pl ace b y a cl am p.

N O TE : P l ace th e wh o l e as s e m bl y i n an are a fre e fro m d rafts o r o th e r t yp e s o f s u d d en te m peratu re ch an g e s .

5. 1 . 2 P ro ce d u re

W h en e ve ryth i n g is in re ad i n es s , tu rn on th e co n d en s e r water an d app l y h e at to th e fl as k at s u ch a rate th at th e fl u i d is

re fl u xi n g i n 1 0 m i n ± 2 m i n at a rate i n e xce s s o f 1 d ro p/s .

I m m e d i ate l y ad j u s t h e at i n p u t to o btai n a s p e ci fi e d e q u i l i bri u m refl u x rate o f 1 to 2 d ro p/s o ver th e n e xt 5 m i n ± 2 m i n pe ri o d .

M ai n tai n a ti m e d an d co n s tan t e q u i l i bri u m refl u x rate o f 1 to 2 d ro p/s fo r an ad d i ti o n al 2 m in; re co rd th e averag e val u e o f

fo u r te m peratu re re ad i n g s take n at 3 0 s i n te rval s as th e e q u i l i bri u m re fl u x bo i l i n g po i n t.

5. 1 . 3 R e pe atab i l i t y ( S i n g l e An al ys t)

Th e s tan d ard d e vi ati o n of re s u l ts ( e ach th e ave rag e of d u pl i cate s ) , o b tai n e d b y th e s am e an al ys t on d i ffere n t d a ys , h as

be en es ti m ate d to be 0. 4 °C ( 0 . 88 ° F) at 72 d e g re e s of fre ed o m . Two s u ch val u e s sh ou l d be co n s i d ere d s u s pect (95%

co n fi d en ce l e ve l ) i f th e y d i ffe r b y m o re th an 1 . 5 ° C ( 2 . 5 ° F) .

5. 1 . 4 R e pro d u ci b i l i t y ( M u l ti l abo rato ry)

Th e s tan d ard d e vi ati o n o f res u l ts ( e ach th e ave rag e o f d u pl i cate s ) , o btai n e d b y an al ys ts i n d i ffere n t l abo rato ri e s , h as be e n

es ti m ate d to be 1 . 8 ° C ( 3 . 0 2 ° F) at 1 7 d e g ree s o f fre e d o m . Two s u ch val u e s s h o u l d be co n s i d e re d s u s p e ct ( 9 5 % co n fi d e n ce

l e vel ) i f th e y d i ffe r b y m o re th an 5 ° C ( 9 ° F) .
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5. 2 W et E q u i l i bri u m R e fl u x Bo i l i n g P o i n t

5. 2 . 1 H u m i d i fi cati o n P ro ce d u re

Lu bri cate th e g ro u n d - g l as s j o i n t o f a 2 5 0 m m ( 9 . 89 i n ) I . D . bo wl - fo rm d es i ccato r h avi n g m atch e d tu bu l at ed g l as s co ve r an d

fi tted wi th a N o . 8 ru bbe r s to ppe r. P o u r 450 m L ± 1 0 m L ( 1 5 . 2 2 o z ± 0 . 3 4 o z) o f d i s ti l l e d wate r i n to th e d e s i ccato r an d i n s e rt

a perfo rate d p o rce l ai n pl ate ( C o o rs N o. 6 0 4 56 or e q u i val en t) . I m m e d i ate l y pl ace on e o pe n R M - 49 co rro s i o n te s t j ar

co n tai n i n g 3 5 0 m L ± 5 m L of th e te s t brake fl u i d i n to th e d e s i ccato r. P l ace a s e co n d o pe n R M - 49 co rro s i o n te s t j ar co n tai n i n g

350 mL ± 5 mL of TE G M E ( tri e th yl e n e g l yc o l m o n o m e th yl e th er, brake fl u i d g rad e- Ap pe n d i x E) ( R M - 71 ) i n to th e s am e

d e s i ccato r. Th e wate r co n te n t of th e TE G M E co n tro l fl u i d at th e s tart of expo s u re s h al l h ave be e n ad j u s te d to 0. 50% ±

0 . 0 5 % b y wei g h t ( Karl Fi s c h e r an al ys i s o r e q u i val e n t) . R e p l ace d e s i ccato r co ver an d i n s ert at o n ce i n to an AS TM E 1 45,

T ype I I A, fo rce d ve n ti l ati o n o ve n s et at 5 0 ° C ± 1 ° C ( 1 2 2 ° F ± 1 . 8 ° F) .

P e ri o d i cal l y, d u ri n g o ve n h u m i d i fi cati o n d e term i n e wat er co n ten t o f th e co n tro l fl u i d . W h e n th e wate r co n te n t o f th e co n tro l

fl u i d h as re ach ed 3 . 70 % ± 0 . 0 5 % b y we i g h t, re m o ve t h e d e s i ccat o r fro m th e o ve n an d s e al th e tes t s am pl e . Al l o w th e s e al ed

j ar to co o l fo r 6 0 to 9 0 m i n at 2 3 ° C ± 5 ° C ( 7 3 . 4 ° F ± 9 ° F) .

5. 2. 2 W et E q u i l i bri u m R e fl u x B o i l i n g P o i n t

H u m i d i f y th e brake fl u i d as d es cri be d i n 5 . 2 . 1 an d d e te rm i n e th e bo i l i n g p o i n t o f th e h u m i d i fi e d brake fl u i d as d e s cri be d i n

5. 1 .

5. 3 Vi s co s i t y

D e te rm i n e th e ki n em ati c vi s co s i ty o f th e fl u i d b y AS TM D 4 45.

2
5. 3 . 1 R epo rt th e vi s co s i ty to th e n e are s t mm /s ( ce n ti s to kes ) . D u pl i cate ru n s wh i ch ag ree wi th i n 1 . 2% re l ati ve to te s t

res u l t are acce ptabl e fo r ave rag i n g ( 9 5 % co n fi d en ce l e ve l ) .

5. 3. 2 R e pe atab i l i t y ( S i n g l e An al ys t)

Th e co e ffi ci e n t o f vari ati o n o f re s u l ts ( each th e averag e o f d u pl i cates ) , o btai n e d b y th e s am e an al ys t o n d i ffe ren t d ays h as

be e n e s ti m ate d to be 0 . 4% at 47 d eg re es o f fre ed o m . Two s u ch val u e s sh ou l d be co n s i d e re d s u s pect ( 9 5 % co n fi d en ce

l e ve l ) i f th e y d i ffe r b y m o re th an 1 . 2 %.

5. 3. 3 R e pro d u ci b i l i t y ( M u l ti l abo rato ry)

Th e co e ffi ci e n t o f vari ati o n o f re s u l ts ( e ach th e ave rag e o f d u pl i cate s ) , o btai n ed b y an al ys ts in d i ffere n t l abo rato ri es , h as

be e n e s ti m ate d t o b e 1 % at 1 5 d e g re e s o f free d o m . Two s u ch val u e s s h o u l d b e co n s i d e re d s u s pe ct ( 9 5 % co n fi d e n ce l e ve l )

i f th e y d i ffer b y m o re th an 3 %.

5. 4 pH Val u e

M i x th e fl u i d wi th an e q u al vo l u m e o f a m i xtu re o f 50 % e th an o l an d 5 0 % d i s ti l l e d wate r n eu tral i ze d to a pH o f 7 . 0 . D e te rm i n e

th e p H o f th e res u l ti n g s o l u ti o n e l e ctro m e tri cal l y at 2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F) , u s i n g a p H m e ter e q u i pp e d wi th a cal i brate d

fu l l ran g e ( 0 to 1 4) g l as s e l ectro d e an d a cal o m e l re fe re n ce e l ectro d e, as s p eci fi e d i n AS TM D 6 6 4.

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 8 o f 2 4

5. 5 Fl u i d S tab i l i t y

5. 5 . 1 H i g h Tem pe ratu re S tab i l i t y

H e at a n e w s am pl e o f th e o ri g i n al te s t brake fl u i d to a te m pe ratu re of 1 85 °C ± 2 °C (365 °F ± 3 . 6 ° F) b y th e pro ced u re

s pe ci fi e d i n 5 . 1 an d m ai n tai n at th at te m pe ratu re fo r 2 h . Th en d e term i n e th e bo i l i n g po i n t o f th i s brake fl u i d as s pe ci fi e d i n

5. 1 . Th e d i ffere n ce be twee n th i s o bs e rved boi l i n g po i n t an d th at pre vi o u s l y d et e rm i n ed in 5. 1 s h al l be co n s i d e re d as th e

ch an g e i n bo i l i n g po i n t o f th e brake fl u i d .

5. 5 . 2 C h e m i cal S tabi l i ty

M i x 3 0 m L o f te s t brake fl u i d wi th 3 0 m L o f S AE C o m pati bi l i t y Fl u i d d e s cri be d i n App e n d i x B ( R M - 6 6 0 6 /I S O 4 9 2 6 ) . D e term i n e

th e e q u i l i bri u m refl u x bo i l i n g po i n t o f th i s fl u i d m i xtu re b y u s e o f th e tes t app aratu s s peci fi e d i n S e cti o n 5 . 1 . 1 , app l yi n g h e at

to th e fl as k at s u ch a rate th at th e fl u i d i s re fl u x i n g i n 1 0 m i n ± 2 m i n at a rate i n exce s s o f 1 d ro p/s . Th e re fl u x rate s h al l n o t

exce e d 5 d ro ps /s . R eco rd th e m axi m u m fl u i d tem pe ratu re o bs e rve d d u ri n g th e fi rs t m i n u te afte r th e fl u i d b e g i n s re fl u xi n g at

a rate i n e xce s s o f 1 d ro p /s . O ver th e n e xt 1 5 m i n ± 1 m i n , ad j u s t an d m ai n tai n th e rate o f re fl u x to 1 to 2 d ro ps /s . M ai n tai n

a ti m ed an d co n s tan t e q u i l i bri u m refl u x rate of 1 to 2 d ro ps /s fo r an ad d i ti o n al 2 m in; re co rd th e ave rag e val u e of fo u r

te m pe ratu re re ad i n g s taken at 3 0 s i n te rval s as th e fi n al e q u i l i bri u m refl u x bo i l i n g p o i n t. C h e m i cal re ve rs i o n i s e vi d e n ced b y

th e d e creas e i n te m peratu re b e twe e n th e m axi m u m fl u i d te m peratu re re co rd e d an d th e fi n al e q u i l i bri u m re fl u x bo i l i n g p o i n t.

5. 6 C o rro s i o n

5. 6 . 1 W et C o rro s i o n Te s t

2 2
P repare two s e ts o f s tri ps fro m e ach o f th e m e tal s l i s te d i n Appe n d i x A, e ach s tri p h avi n g a s u rface are a o f 2 5 cm ± 5 cm

( appro xi m ate l y 8 cm l o n g , 1 . 3 cm wi d e , an d n o t m o re th an 0 . 6 cm th i ck) . D ri l l a h o l e betwee n 4 an d 5 m m i n d i am e te r an d

abo u t 6 m m from o n e en d o f e ach s tri p. W i th th e e xce pti o n o f th e ti n n e d i ro n s tri ps , cl ean th e s tri ps b y abrad i n g th e m o n al l

s u rface are as wi th 320 A (RM - 29) or P 40 0 wat erpro o f carbo ru n d u m pape r an d i s o pro p an o l or e th an o l u n ti l al l s u rface

s cratch es , cu ts , an d pi ts are re m o ve d fro m th e s tri ps , u si n g a n e w p i e ce o f carbo ru n d u m pape r fo r e ach d i ffe ren t type o f

m e tal . W as h th e s tri ps , i n cl u d i n g t h e ti n n e d i ro n , wi th i s o pro p an o l o r e th an o l an d d ry th e s tri ps wi th a cl e an l i n t- fre e cl o th

an d pl ace s tri ps i n a d es i cc ato r co n tai n i n g d e s i ccan t m ai n tai n e d at 2 3 ° C ± 5 ° C ( 7 3 . 4 ° F ± 9 ° F) fo r at l eas t 1 h.

H an d l e t h e s tri ps wi th g l o ve s , o r cl e an fo rce ps o r co tto n cl o th s afte r po l i s h i n g to avo i d fi n g e rpri n t co n t am i n ati o n .

Wei g h e ach s tri p to th e n e are s t 0 . 1 mg an d as s e m bl e e ach set of s tri ps on an u n co ated s te e l bo l t ( R M - 6 1 ) in th e o rd e r

ti n n ed i ro n , s te el , al u m i n u m , cas t i ro n , bras s , an d co ppe r, s o th at th e s tri ps are i n e l ectri cal co n tact. B e n d th e s tri ps , o t h e r

th an cas t i ro n , s o th at th ere i s a s e parati o n o f at l e as t 3 m m be twe e n ad j ace n t s tri ps fo r a d i s tan ce o f abo u t 6 cm from th e

fre e e n d o f th e s tri ps .

U s e two S B R cu ps ( R M - 0 3 a) an d two 2 5 . 4 m m x 2 5 . 4 m m ( 1 in x 1 i n ) E P D M ru b be r s l ab s to ck ( R M - 6 9 ) te s t s peci m e n s .

M e as u re th e b as e d i am ete r o f th e two s tan d ard S BR cu ps ( R M - 0 3 a) d e s cri be d i n App en d i x C , u s i n g an o pti c al co m parato r

o r m i crom e ter to th e n e are s t 0 . 0 2 m m ( 0 . 0 0 1 i n ) al o n g th e cen te rl i n e o f th e S AE an d ru bbe r t yp e i d en ti fi cati o n s an d at ri g h t

an g l e s to th i s ce n te rl i n e . Take th e m e as u re m en ts wi th i n 0. 4 m m (0. 01 5 i n ) o f th e bo tto m e d g e an d p aral l e l to th e bas e o f

th e cu p. D i s card an y cu p i f th e two m e as u re d d i am e ters d i ffe r b y m o re th an 0 . 0 8 m m ( 0 . 0 0 3 i n ) . Ave rag e th e two re ad i n g s

of e ach cu p. S u ppo rt th e ru bbe r cu p on a ru bber an vi l o r c yl i n d e r h avi n g a fl at ci rcu l ar to p s u rface of at l e as t 1 9 mm in

d i am e te r, a th i ckn e s s of at l e as t 9 mm, a h ard n e s s wi th i n 5 I RH D o f th e h ard n e s s o f th e ru bbe r te s t cu p. D ete rm i n e th e

h ard n e s s o f each cu p th u s s u ppo rte d b y th e pro ce d u re s pe ci fi ed i n AS TM D 1 41 5 u s i n g th e S tan d ard Te s te r.

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N O TE : AS TM D 2 2 40 m ay be u s e d fo r q u al i t y co n tro l an d ro u ti n e te s ts wh e n a t yp e A d u ro m e te r i s e q u i p pe d wi th a fi xtu re

fo r kee pi n g th e pl an e o f th e pre s s u re fo o t o n th e d u ro m e ter paral l el to th e pl an e o f th e cu p face d u ri n g m e as u re m en t.

D e te rm i n e th e s l ab h ard n e s s . D e term i n e th e we i g h t o f th e E P D M ru bb er s l ab s to ck i n ai r ( m 1 ) to th e n eare s t 1 mg th e n

d ete rm i n e th e app aren t we i g h t of th e s l ab s to ck i m m ers e d in d i s ti l l e d wate r at ro o m tem peratu re ( m 2) . Q u i ckl y d i p e ach

s pe ci m en i n al co h o l an d th e n b l o t d ry wi th fi l te r pap e r fre e o f l i n t an d fo rei g n m atte r.

O btai n two s trai g h t- s i d e d ro u n d g l as s j ars , h avi n g a cap aci ty o f ap pro xi m ate l y 4 75 m l an d i n n er d i m e n s i o n s o f appro xi m atel y

1 0 0 m m i n h ei g h t an d 75 m m i n d i am e ter ( R M - 49 ) . To th e R M - 4 9 co rro s i o n te s t j ar, app l y fo u r wrap pi n g s o f 1 9 m m ( 3 /4 i n )

Tefl o n tape aro u n d th e j ar th re ad s al l o wi n g a 3 m m ( 1 /8 i n ) h e i g h t abo ve th e to p o f th e j ar. P l ace o n e S BR c u p ( R M - 0 3 a)

wi th lip ed g e faci n g u p, in e ach of th e two g l as s j ars . U se o n l y ti n n ed s te e l lids ve n ted wi th a h ol e 0. 8 mm ± 0. 1 mm in

d i am e te r ( R M - 64) .

I n s ert a m e tal s tri p as s e m bl y i n s i d e e ach cu p wi th th e bo l te d e n d i n co n tact wi th th e co n cavi t y o f th e cu p an d th e fre e e n d

e xten d i n g u p ward in th e j ar. P l ace o n e EPDM ru bbe r s l ab s to ck ( R M - 69 ) te s t s peci m en fl at o n th e b o tto m o f th e tes t j ar.

M i x 760 m L o f tes t fl u i d wi th 4 0 m L o f d i s ti l l ed wate r. Ad d 4 0 0 m l o f th e th e te s t fl u i d /water m i xtu re to co ve r th e m e tal s tri p

as s em bl y i n e ach j ar. Ti g h ten th e l i d an d pl ace th e j ars i n an o ven m ai n tai n e d at 1 0 0 ° C ± 2 ° C ( 2 1 2 ° F ± 3 . 6 ° F) fo r 1 2 0 h

± 2 h.

Al l o w th e j ars to co o l at 2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F) fo r 6 0 to 9 0 m i n .

I m m ed i ate l y fo l l o wi n g th e c o o l i n g pe ri o d , re m o ve th e m etal s tri ps from th e j ars b y u s e o f a fo rceps , rem o vi n g l o o s e ad h eri n g

s e d i m en t b y ag i tati o n o f th e m etal s tri p as s e m bl y i n th e fl u i d i n th e j ar, an d rem o ve th e ru bb e r cu ps from th e j ars b y u s e o f

a fo rce ps , rem o vi n g l o o s e ad h e ri n g s e d i m en t b y ag i tati o n o f th e cu p i n th e fl u i d i n j ar. R i n s e cu ps i n i s o pro p an o l o r e th an o l

an d ai r d ry c u ps . E xam i n e tes t s tri ps an d te s t j ars fo r ad h e ri n g crys tal l i n e d e po s i t, d i s as s e m bl e th e m etal s tri ps , re m o vi n g

ad h e ri n g fl u i d b y fl u s h i n g wi th wate r, an d cl e an i n d i vi d u al s tri ps b y wi pi n g wi th a cl o th wette d wi th i s o pro pan o l o r e th an o l .

E xam i n e th e s tri ps fo r e vi d en ce o f co rro s i o n an d pi tti n g . P l ace s tri ps i n a d e s i ccato r co n tai n i n g a d es i ccan t m ai n tai n e d at

2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F ) fo r at l eas t 1 h o u r.

W i th i n 1 5 m i n u te s afte r re m o vi n g th e s l abs from th e fl u i d , wei g h e ach E P D M ru bbe r s l ab s to ck ( R M - 69 ) i n ai r ( m 3 ) , ag ai n

to th e n e are s t m i l l i g ram , th e n re we i g h i m m e rs e d i n ro o m tem peratu re d i s ti l l e d water ( m 4) to d ete rm i n e th e vo l u m e ch an g e

afte r h o t fl u i d i m m e rs i o n . D e te rm i n e th e s l ab h ard n es s .

W i th i n 1 5 m in afte r re m o vi n g th e cu ps fro m th e fl u i d , vi s u al l y e xam i n e e ach cu p fo r evi d e n ce of sl o u g h i n g , bl i s te rs , an d

o th e r fo rm s o f d i s i n te g rati o n . M e as u re th e bas e d i am ete r an d h ard n es s o f e ach cu p.

Afte r o n e h o u r i n th e d e s s i cato r, m e tal s tri ps are we i g h e d to th e n e are s t 0 . 1 m g . D e term i n e th e d i ffe re n ce i n we i g h t o f e ach

m etal s tri p an d d i vi d e th e d i ffe ren ce b y th e to tal s u rface are a o f th e m etal s tri p m e as u red i n s q u are ce n ti m e ters . Averag e

th e m eas u re d q u an ti ti es o f th e d u pl i cate s . In th e e ve n t o f a m arg i n al pas s o n i n s p e cti o n , o r o f a fai l u re i n o n l y o n e o f th e

d u p l i cate s , an o th e r s et of d u p l i cate tes t s am pl es s h al l be ru n . B o th re pe at s am pl e s m u st m ee t al l th e req u i rem e n ts of

pro ce d u re 5. 6 .

E xam i n e th e fl u i d i n th e j ars fo r g e l l i n g . Ag i tate th e fl u i d i n th e j ars to s u s pe n d an d u n i fo rm l y d i s pe rs e s e d i m e n t an d tran s fe r

a 1 0 0 m l po rt i o n o f th i s fl u i d to an AS TM co n e- s h ape d ce n tri fu g e tu be an d d ete rm i n e perce n t s e d i m e n t as d e s cri be d i n 8 . 2

o f AS TM D 9 1 . M e as u re th e pH val u e o f th e co rro s i o n te s t fl u i d b y th e pro ce d u re s pe ci fi ed i n S e cti o n 5. 4.

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M e as u re th e h ard n es s of each s pec i m en . Vo l u m e ch an g e s s h al l be repo rted as a p e rcen tag e of th e o ri g i n al vo l u m e ,

cal cu l ate d as fo l l o ws :

(m 3 – m
4
) –( m
1
– m
2
)
% chan g e i n v o l u m e = × 1 00
(m1 – m
2
)
(Eq. 1 )

wh e re:

m1 = th e i n i ti al m as s i n g ram s i n ai r

m 2 = th e i n i ti al m as s i n g ram s i n wate r

m 3 = th e m as s i n g ram s i n ai r afte r i m m e rs i o n i n tes t fl u i d

m 4 = th e apparen t m as s i n g ram s i n wate r afte r te s t.

5. 6 . 2 D ry C o rro s i o n Te s t

P repare an d we i g h two s e ts o f m e tal te s t s tri ps as d e tai l ed i n pro ce d u re 5 . 6 . 1 .

U s e two S B R cu ps ( R M - 0 3 a) , an d two 2 5 . 4 m m x 2 5. 4 m m ( 1 in x 1 in) E P D M ru b ber s l ab s to ck ( R M - 6 9 ) te s t s peci m en s,

as d e s cri be d i n Appe n d i x C an d Ap pen d i x D , re s pe cti ve l y.

O btai n two s trai g h t- s i d e d ro u n d g l as s j ars , h avi n g a cap aci ty o f ap pro xi m ate l y 4 75 m l an d i n n er d i m e n s i o n s o f appro xi m ate l y

1 0 0 m m i n h e i g h t an d 75 m m i n d i am e ter ( R M - 49 ) . To th e R M - 4 9 co rro s i o n te s t j ar, app l y fo u r wrap pi n g s o f 1 9 m m ( 3 /4 i n )

Tefl o n tap e aro u n d th e j ar t h re ad s al l o wi n g a 3 mm ( 1 /8 i n ) h e i g h t ab o ve th e to p o f th e j ar. P l ace o n e S B R cu p ( R M - 3 a)

wi th l i p ed g e faci n g u p, in e ach o f th e two g l as s j ars . U se o n l y ti n n e d s te e l lids ve n te d wi th a hole 0. 8 mm ± 0. 1 mm in

d i am e ter ( R M - 64) .

I n s ert a m e tal s tri p as s e m bl y i n s i d e e ach cu p wi th th e bo l te d en d i n co n tact wi th th e co n cavi t y o f th e cu p an d th e fre e en d

e xten d i n g u p ward in th e j ar. P l ace o n e E P D M ru bb e r s l ab s to ck ( R M - 69 ) te s t s p e ci m e n fl at o n th e b o tto m o f th e te s t j ar.

Ad d 40 0 ml of d ry te s t fl u i d to co ve r th e m e tal s tri p as s em bl y i n e ach j ar. Ti g h ten th e lid an d pl ace th e j ars in an o ve n

m ai n tai n e d at 1 0 0 ° C ± 2 ° C ( 2 1 2 ° F ± 3 . 6 ° F) fo r 1 2 0 h ± 2 h .

Al l o w th e j ars to co o l at 2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F) fo r 6 0 to 9 0 m i n .

I m m e d i ate l y fo l l o wi n g th e c o o l i n g pe ri o d , re m o ve th e m e tal s tri ps from th e j ars b y u s e o f a fo rce ps , rem o vi n g l o o s e ad h e ri n g

s ed i m en t b y ag i tati o n o f th e m e tal s tri p as s e m bl y i n th e fl u i d in th e j ar. R i n s e c u ps i n i s o pro pan o l o r e th an o l an d ai r d r y

cu ps . E xam i n e tes t s tri ps an d te s t j ars fo r ad h eri n g c rys tal l i n e d epo s i t, d i s as s e m bl e th e m etal s tri ps , re m o vi n g ad h eri n g

fl u i d b y fl u s h i n g wi th water, an d c l e an i n d i vi d u al s tri ps b y wi p i n g wi th a cl o th we tte d wi th i s o pro pan o l o r e th an o l . E xam i n e

th e s tri ps fo r e vi d en ce o f co rro s i o n an d p i tti n g . P l ace s tri ps i n a d es i ccato r co n tai n i n g a d e s i ccan t m ai n tai n ed at 2 3 ° C ± 5 ° C

( 73 . 4 ° F ± 9 ° F) fo r at l eas t 1 h o u r.

After o n e h o u r i n th e d e s s i cato r, m e tal s tri ps are we i g h e d to th e n e are s t 0 . 1 m g . D e term i n e th e d i ffe ren ce i n we i g h t o f e ach

m e tal s tri p an d d i vi d e th e d i ffere n ce b y th e to tal s u rface are a o f th e m e tal s tri p m eas u red i n s q u are ce n ti m e te rs . Ave rag e

th e m eas u re d q u an t i ti es o f th e d u pl i cates . In th e e ve n t o f a m arg i n al pas s o n i n s p e cti o n , o r o f a fai l u re i n o n l y o n e o f th e

d u p l i cate s , an o th e r s e t o f d u pl i cate te s t s am pl e s s h al l be ru n . B o th re pe at s am pl e s m u s t m ee t al l th e re q u i re m e n ts o f 5 . 6 .

I m m e d i ate l y fo l l o wi n g th e c o o l i n g p e ri o d , rem o ve th e ru bbe r s peci m en s from th e j ars b y u s e o f a fo rce ps , re m o vi n g l o o s e

ad h eri n g s e d i m en t b y ag i tati o n o f th e cu p i n th e fl u i d i n j ar. Vi s u al l y exam i n e each cu p fo r e vi d en ce o f s l o u g h i n g , b l i s te rs ,

an d o th e r fo rm s of d i s i n te g rati o n .

E xam i n e th e fl u i d in th e j ars fo r g el l i n g . M e as u re th e pH val u e of th e co rro s i o n te s t fl u i d by th e pro ce d u re s pe ci fi e d in

pro ced u re 5 . 4 Ag i tate th e fl u i d i n j ars to s u s pe n d an d u n i fo rm l y d i s p e rs e s ed i m e n t an d tran s fe r a 1 0 0 m L po rti o n o f th i s fl u i d

to an AS TM co n e - s h ap e d c en tri fu g e tu b e an d d e te rm i n e pe rce n t s e d i m e n t as d es cri be d i n S ecti o n 8 . 2 o f AS TM D 9 1 .

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5. 7 Fl u i d i t y an d Ap pe aran ce at Lo w Te m pe ratu re

5. 7. 1 At –40 ° C ( –4 0 ° F)

P l ace 1 00 m L o f th e te s t fl u i d in a g l as s s am pl e bo ttl e ( R M - 59 a) h avi n g a capaci ty o f ap pro xi m ate l y 1 2 5 m L, an o u ts i d e

d i am e ter o f 3 7 m m ± 0 . 5 m m , an d an o veral l h e i g h t o f 1 6 5 m m ± 3 m m . S to ppe r o r cap th e bo ttl e ti g h tl y an d p l ace i n a co l d

bath m ai n tai n ed at –40 ° C ± 2 ° C ( –40 ° F ± 3 . 6 ° F) fo r 1 44 h ± 4 h . R em o ve th e bo ttl e from th e bath , q u i ckl y wi pe th e b o ttl e

wi th a cl e an l i n t- fre e cl o th s atu rate d wi th i s o pro p an o l or e th an o l , an d e xam i n e th e fl u i d fo r e vi d en ce of s trati fi cati o n ,

s ed i m e n t, o r crys tal s . I n ve rt th e b o ttl e an d d ete rm i n e th e n u m be r o f s e co n d s re q u i re d fo r th e ai r b u bb l e to tra ve l to th e to p

o f th e fl u i d . Al l o w th e fl u i d to warm to ro om tem pe ratu re 2 3 ° C ± 5 ° C ( 73 ° F ± 9 ° F) ; i f n eces s ary, al l o w to s tan d fo r as l o n g

as 4 h . E xam i n e th e fl u i d fo r cl ari t y an d app e aran ce b y c o m pari n g i t to an o ri g i n al s am pl e o f th e tes t fl u i d in an i d en ti cal

co n tai n er.

5. 7. 2 At –5 0 ° C ( –5 8 ° F)

P l ace 1 0 0 m L o f fl u i d i n a g l as s s am pl e bo t tl e ( s am e as i n –40 ° C tes t abo ve) . S to p pe r o r cap th e bo ttl e ti g h tl y an d p l ace i n

a co l d bath m ai n tai n ed at –5 0 ° C ± 2 ° C ( –5 8 ° F ± 3 . 6 ° F) fo r 6 h ± 0 . 2 h . R em o ve th e bo ttl e fro m th e bath , q u i ckl y wi p e th e

bo ttl e wi th a cl e an l i n t- fre e cl o th s atu rate d wi th i s o pro p an o l o r e th an o l , an d e xam i n e th e fl u i d fo r e vi d e n ce o f s trati fi cati o n ,

s ed i m e n t, o r crys tal s . I n ve rt th e b o ttl e an d d ete rm i n e th e n u m be r o f s e co n d s re q u i re d fo r th e ai r b u bbl e to travel t o th e to p

o f th e fl u i d . Al l o w th e fl u i d to warm to ro om tem pe ratu re 2 3 ° C ± 5 ° C ( 73 ° F ± 9 ° F) ; i f n ece s s ary, al l o w to s tan d fo r as l o n g

as 4 h. E xam i n e th e fl u i d fo r cl ari ty an d app earan ce by c o m pari n g i t to a s am pl e of th e o ri g i n al te s t fl u i d in an i d e n ti cal

co n tai n er.

5. 8 W ate r To l eran ce

5. 8 . 1 At –40 ° C ( –4 0 ° F)

M i x 9 6 . 5m L o f te s t fl u i d an d 3 . 5m L o f d i s ti l l e d wate r i n to an AS TM co n e s h ape d c en tri fu g e tu be d e s cri be d i n S e cti o n 5 . 1 in

AS TM D 9 1 . S to p pe r th e tu be wi th a co rk an d p l ace i n a co l d bath m ai n tai n e d at –40 ° C ± 2 ° C ( –40 ° F ± 3 . 6 ° F) fo r 2 2 h ±

2 h . R e m o ve th e cen tri fu g e tu be from th e bath , q u i ckl y wi p e th e tu be wi th a cl e an l i n t- free cl o th s atu rate d wi th i s o pro pan o l

1
or e th an o l , d ete rm i n e th e tran s pare n c y of th e fl u i d by pl ac i n g th e tu b e ag ai n s t a hiding po we r te s t ch art ( R M - 2 8) an d

o bs ervi n g th e c l ari t y of th e co n tras t l i n es on th e ch art wh e n vi e we d th ro u g h th e fl u i d . E xam i n e th e fl u i d fo r e vi d en ce of

s trati fi cati o n an d s e d i m en tati o n . I n ve rt th e tu b e an d d e term i n e th e n u m ber o f s e co n d s re q u i re d fo r th e ai r bu bbl e to trave l

to th e to p o f t h e fl u i d . Th e ai r b u bbl e s h al l be co n s i d e red to h ave re ach e d th e to p o f th e fl u i d wh e n th e to p o f th e bu bbl e

re ach e s th e 2 m L g rad u ati o n o f th e ce n tri fu g e tu b e.

5. 8. 2 At 6 0 ° C ( 1 40 ° F)

P l ace th e ce n tri fu g e tu be fro m 4. 8 . 1 in an o ve n m ai n tai n e d at 6 0 ° C ± 2 ° C ( 1 40 ° F ± 3 . 6 ° F) fo r 2 2 h ± 2 h. R em o ve th e

tu be from th e o ve n an d i m m e d i ate l y e xam i n e th e co n te n ts fo r e vi d e n ce of s trati fi cati o n . D e te rm i n e perce n t sedi m en t by

vo l u m e as d es cri be d i n S ec ti o n 8 o f AS TM D 9 1 .

5. 9 C o m pati bi l i t y

5. 9. 1 At –40 ° C ( –4 0 ° F)

Mix 50 m L of fl u i d wi th 50 m L of S AE C o m pati b i l i t y Fl u i d d e s cri be d in Appe n d i x B (RM -6606/ I SO 4926) an d po u r t h i s

m i xtu re i n to an AS TM co n e - s h ape d cen tri fu g e tu be d e s cri bed i n S ecti o n 5 . 1 i n AS TM D 9 1 an d s to pp e r wi th a co rk. P l ace

cen tri fu g e tu be fo r 2 2 h ± 2 h i n a bath m ai n tai n e d at –40 ° C ± 2 ° C ( –4 0 ° F ± 3 . 6 ° F) . R e m o ve th e ce n tri fu g e tu be fro m th e

bath , q u i ckl y wi pe th e tu b e wi th a cl ean l i n t- fre e cl o th s atu rate d wi th i s o pro pan o l o r eth an o l , d e term i n e th e tran s paren c y o f

1
th e fl u i d b y pl aci n g th e tu b e ag ai n s t a hiding po wer te s t ch art ( AS TM D 3 4- 0 8 , RM - 28) an d o bs e rvi n g th e cl ari t y o f th e

co n tras t l i n e s o n th e ch art wh en vi e we d th ro u g h th e fl u i d . E xam i n e th e fl u i d fo r s trati fi cati o n an d s e d i m e n tati o n .

5. 9. 2 At 6 0 ° C ( 1 40 ° F)

1
A s u i tabl e h i d i n g po wer ch art i s d es cri be d i n AS TM D 3 4, M eth o d o f Te s t fo r R el ati ve D ry H i d i n g P o wer o f P ai n ts, pu bl i s h ed by th e Am e ri can S o ci ety

fo r Tes ti n g an d M ateri al s, o r i n M eth o d 41 1 2 o f Fe d eral Tes t M eth o d S tan d ard N o . 1 41 .

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P l ace th e c e n tri fu g e tu b e fro m S ecti o n 4. 9 . 1 i n an o ve n at 6 0 ° C ± 2 ° C ( 1 40 ° F ± 3 . 6 ° F) fo r 2 2 h ± 2 h . R e m o ve th e tu be

from th e o ve n an d i m m e d i atel y exam i n e th e co n ten ts fo r evi d e n ce o f s trati fi cati o n . D e te rm i n e perce n t s ed i m e n t by vo l u m e

as d e s cri be d i n S e cti o n 8 . 2 o f AS TM D 9 1 .

5. 1 0 R e s i s tan ce to O xi d ati o n

P re pare two s e ts o f al u m i n u m an d cas t i ro n te s t s tri ps ( R M - 0 8 an d R M - 0 9 ) b y th e pro ce d u re s pe ci fi e d i n 5 . 6 . W ei g h e ach

s tri p to th e n eares t 0 . 1 m g an d as s e m bl e a s tri p o f each m e tal o n an u n co ate d s te e l bo l t ( R M - 6 2 ) , s e parati n g th e s tri ps at

each e n d wi th a p i ece o f ti n fo i l ( R M - 2 7) ( m i n . 9 9 . 5 % ti n , m ax. 0 . 5% l e ad ) appro xi m ate l y 1 2 m m s q u are an d be twe en 0 . 0 2

an d 0 . 0 6 m m i n th i ckn e s s .

P l ace 3 0 m L ± 1 m L o f fl u i d i n a s m al l g l as s bo t tl e ap pro xi m ate l y 1 2 0 m L i n cap aci ty. Ad d 6 0 m g ± 2 m g o f reag en t g rad e

be n zo yl p e ro xi d e as per AS TM E 29 8, an d 1 .5 m L ± 0. 05 m L d i s ti l l e d wate r to bo ttl e . S to pp er th e bo ttl e an d s h ake th e

co n te n ts , avo i d i n g g e tti n g th e s o l u ti o n o n th e s to ppe r. P l ace bo ttl e i n an o ve n at 7 0 ° C ± 2 ° C ( 1 5 8 ° F ± 3 . 6 ° F) fo r 1 2 0 m i n

± 1 0 m i n , s h aki n g e ve r y 1 5 m i n u te s to e ffe ct s o l u ti o n o f th e pe ro xi d e. R em o ve th e bo ttl e fro m th e o ven , d o n o t d i s tu rb th e

s to pper, an d c o o l i n ai r at ro o m tem pe ratu re , 2 3 ° C ± 5 ° C ( 73 ° F ± 9 ° F) .

P l ace appro xi m ate l y 1 /8 s e cti o n o f a s tan d ard S B R cu p d es cri be d i n Ap pe n d i x C ( R M - 0 3 a) i n th e bo tto m of e ach o f P l ace

appro xi m ate l y 1 /8 s e cti o n o f a s tan d ard S BR cu p d e s cri be d i n App e n d i x C ( R M - 0 3 a) i n th e bo tto m o f e ach o f two te s t tu b e s

abo u t 2 2 mm in d i am e ter an d 1 75 mm in l e n g th . Ad d 1 0 m L o f prep are d te s t fl u i d to e ach tes t tu be . P l ace a m e tal - s tri p

as s em bl y i n e ach tu be wi th th e en d o f th e s tri ps re s ti n g o n th e ru bbe r, th e s o l u ti o n co ve ri n g ab o u t o n e - h al f th e l e n g th o f th e

s tri ps , an d th e bo l te d en d re m ai n i n g o u t o f th e s o l u ti o n . S to pp e r th e tu b e s wi th co rks an d s to re u pri g h t fo r 2 2 h ± 2 h at

2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F) . Lo o s e n t h e s to ppers an d p l ace th e tu b e s fo r 1 6 8 h ± 2 h in an o ven m ai n tai n e d at 70 ° C ±

2 °C ( 1 58 ° F ± 3 . 6 ° F) . Aft er th e h e ati n g pe ri o d , re m o ve fro m th e o ve n an d al l o w to co o l to ro o m te m pe ratu re fo r 6 0 - 9 0

m i n u te s . R em o ve an d d i s as s em bl e th e m e tal s tri ps . E xam i n e th e s tri ps fo r g u m d e po s i ts . W i pe th e s tri ps wi th a cl o th we t

wi th i s o pro pan o l or e th an o l an d exam i n e fo r pi tti n g or ro u g h e n i n g of s u rface . P l ace s tri ps in d e s i ccato r co n tai n i n g a

d e s i ccan t m ai n tai n ed at 2 3 ° C ± 5 ° C ( 73 . 4 ° F ± 9 ° F) fo r at l eas t 1 h o u r. W e i g h e ach s tri p to th e n e are s t 0 . 1 mg.

D ete rm i n e co rro s i o n l o s s b y d i vi d i n g th e d i ffe re n ce i n wei g h t o f e ach m etal s tri p b y th e to tal s u rface are a o f each m e tal s tri p

m e as u re d in s q u are ce n ti m ete rs . Ave rag e th e m e as u re d q u an ti ti e s o f th e d u pl i cates . In th e e ve n t o f a m arg i n al pas s on

i n s pe cti o n , or of a fai l u re in on l y on e of th e d u p l i cate s , an o th e r set of d u p l i cate tes t s am pl es s h al l be ru n . Bo th rep e at

s am pl e s m u s t m e et al l th e re q u i re m e n ts o f pro ce d u re 5 . 6 .

5. 1 1 E ffe ct o n R u bbe r

Fo r te s t pro ce d u res 5. 1 1 . 1 an d 5. 1 1 . 2, u se s tan d ard S BR cu ps d e s cri b e d in Ap pe n d i x C ( R M - 0 3 a) . M e as u re th e bas e

d i am ete r o f al l cu ps an d h ard n e s s o f al l s p e ci m en s as d e s cri bed i n 4 . 6, d i s card i n g an y cu ps wh o s e d i am e te rs d i ffe r b y m o re

th an 0 . 0 8 m m ( 0 . 0 0 3 i n ) .

Fo r th e te s t pro ced u re 5 . 1 1 . 3 an d 5 . 1 1 . 4 cu t 25. 4 m m x 25. 4 m m (1 i n ch x1 i n ch ) te s t s pe ci m e n s from s tan d ard E P D M s l ab

s to ck as d es cri be d i n Ap pe n d i x D ( R M - 6 9 ) . D e te rm i n e vo l u m e o f each i n th e fo l l o wi n g m an n er:

Wei g h th e s pe ci m e n in ai r (m 1 ) to th e n e ares t m i l l i g ram an d th e n we i g h th e s p e ci m e n s i m m e rs e d in ro o m tem pe ratu re

d i s ti l l ed wate r ( m 2 ) co n tai n i n g n o m o re th an 0 . 2 % o f a s u i tab l e wetti n g ag e n t. P l u ro n i c L- 6 1 ( BAS F) o r eq u i val e n t h as b ee n

fo u n d to be acce ptab l e .

D e te rm i n e h ard n es s o f e ac h s pe ci m e n as d es cri b e d i n pro ced u re 5 . 6 .

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5. 1 1 . 1 Te s t at 70 ° C ( 1 58 ° F)

P l ace two s tan d ard S BR cu ps i n a s trai g h t- s i d e d ro u n d g l as s j ar ( R M - 5 1 ) , h avi n g a capaci t y o f appro xi m atel y 2 50 m L an d

i n n e r d i m en s i o n s o f appro xi m ate l y 1 2 5 m m i n h e i g h t an d 5 0 m m i n d i am ete r, an d a ti n n e d s tee l l i d ( R M - 5 2 a) . Ad d 7 5 m L o f

fl u i d to th e j ar an d h e at fo r 70 h ± 2 h at 7 0 ° C ± 2 ° C ( 1 5 8 ° F ± 3 . 6 ° F) . Al l o w th e j ar to co o l at 2 3 ° C ± 5 ° C ( 7 3 . 4 ° F ± 9 ° F)

fo r 6 0 to 9 0 m i n . R e m o ve th e cu ps from th e j ar, was h q u i ckl y wi th i s o pro pan o l o r e th an o l , an d ai r d r y cu ps . E xam i n e th e

cu ps fo r d i s i n te g rati o n as e vi d e n ce d b y b l i s te rs o r s l o u g h i n g . M e as u re th e bas e d i am e te r an d h ard n e s s o f e ach cu p wi th i n

1 5 m i n after rem o val from th e fl u i d .

5. 1 1 . 2 Te s t at 1 2 0 ° C ( 2 4 8 ° F)

P l ace two s t an d ard S BR c u ps ( R M - 0 3 a) in a s trai g h t- s i d e d ro u n d g l as s j ar ( R M - 5 1 ) , h avi n g a cap aci t y o f appro xi m ate l y

2 5 0 m L an d i n n e r d i m e n s i o n s o f appro x i m atel y 1 2 5 m m i n h e i g h t an d 5 0 m m i n d i am e te r, an d a ti n n e d s te el l i d ( R M - 5 2 a) .

Ad d 75 m L o f fl u i d to th e j ar an d h e at fo r 70 h ± 2 h at 1 2 0 ° C ± 2 ° C ( 2 48 ° F ± 3 . 6 ° F) . Al l o w th e j ar to co o l at 2 3 ° C ± 5 ° C

( 73 . 4 ° F ± 9 ° F) fo r 6 0 to 9 0 m i n . R e m o ve th e cu ps fro m th e j ar, was h q u i ckl y wi th i s o pro pan o l o r e th an o l , an d ai r d ry c u ps .

E xam i n e th e cu ps fo r d i s i n te g rati o n as e vi d en ce d by bl i s te rs or s l ou g h i n g . M e as u re th e bas e d i am e te r an d h ard n e s s of

each cu p wi th i n 1 5 m i n afte r rem o val fro m th e fl u i d .

5. 1 1 . 3 Te s t at 70 ° C ( 1 58 ° F)

P l ace two 25. 4 mm x 25. 4 mm (1 in x 1 in) s tan d ard EPD M te s t s p e ci m e n s (RM - 69) in a s trai g h t- s i d e d ro u n d g l as s j ar

h avi n g a capaci t y o f ap pro xi m atel y 2 5 0 m L an d i n n e r d i m e n s i o n s o f appro xi m ate l y 1 2 5 m m i n h e i g h t an d 5 0 m m i n d i am e te r,

an d a ti n n e d s te el l i d ( R M - 5 2 a) . Ad d 75 m L o f fl u i d to th e j ar an d h e at fo r 70 h ± 2 h at 7 0 ° C ± 2 ° C ( 1 5 8 ° F ± 3 . 6 ° F) . Al l o w

th e j ar to co o l to 23 °C ± 5 °C (73. 4 °F ± 9 ° F) fo r 6 0 to 90 m in. R em o ve th e s p e ci m e n s from th e j ar, was h q u i ckl y wi th

i s o pro p an o l o r e th an o l , an d ai r d ry. E xam i n e th e s pe c i m e n s fo r d i s i n teg rati o n as e vi d e n ce d b y bl i s te rs o r s l o u g h i n g . W ei g h

each s p e ci m e n i n ai r ( m 3 ) , ag ai n to th e n e ares t m i l l i g ram , an d th e n re we i g h i m m e rs ed i n ro o m te m pe ratu re d i s ti l l e d wate r

(m 4 ) , to d e term i n e th e vo l u m e afte r h o t fl u i d i m m ers i on . M e as u re th e h ard n es s o f e ach s peci m e n . Al l we i g h i n g s m u s t be

com pl ete d wi th i n 6 0 m i n afte r rem o val fro m th e te s t fl u i d .

Vo l u m e ch an g es s h al l be re po rte d as a perce n tag e o f th e o ri g i n al vo l u m e, cal cu l ate d as pe r E q u ati o n 1 .

5. 1 1 . 4 Te s t at 1 2 0 ° C ( 2 4 8 ° F)

P l ace two 25. 4 mm x 25. 4 mm (1 in x 1 in) s tan d ard EPD M tes t s p eci m e n s ( R M - 69 ) in a s trai g h t- s i d e d ro u n d g l as s j ar

h avi n g a capaci t y o f ap pro xi m ate l y 2 5 0 m L an d i n n e r d i m en s i o n s o f appro xi m ate l y 1 2 5 m m i n h e i g h t an d 5 0 m m i n d i am e te r,

an d ti n n ed s te e l l i d ( R M - 5 2 a) . Ad d 75 m L o f fl u i d to th e j ar an d h eat fo r 70 h ± 2 h at 1 2 0 ° C ± 2 ° C ( 2 4 8 ° F ± 3 . 6 ° F) . Al l o w

th e j ar to co o l to 23 °C ± 5 °C (73. 4 °F ± 9 ° F) fo r 60 to 90 m in. R e m o ve th e s p e ci m e n s from th e j ar, was h q u i ckl y wi th

i s o pro p an o l or e th an o l , an d ai r d r y. E xam i n e th e s p e ci m e n s fo r d i s i n te g rati o n as e vi d e n ce d by b l i s te rs or sl ou g h i n g .

D e te rm i n e th e vo l u m e ch an g e as i n 4 . 1 1 . 3 . M e as u re th e h ard n e s s o f e ach s pe c i m e n .

R e po rt th e ru b be r s we l l to th e n e are s t 0. 03 mm (0. 001 in). D u pl i cate re s u l ts wh i ch ag re e wi th i n 0. 1 0 mm (0 . 0 0 4 in) are

acce ptab l e fo r ave rag i n g ( 9 5 % co n fi d e n ce l e ve l ) .

5. 1 1 . 5 R e pe atabi l i t y o f th e B as e D i am ete r I n cre as e M e as u re m en t ( S i n g l e An al ys t)

Th e s tan d ard d e vi ati o n o f re s u l ts ( e ach th e averag e o f d u p l i cate d e te rm i n ati o n s ) o btai n e d b y th e s am e an al ys t o n d i ffe re n t

d ays h as be e n es ti m ate d to be 0 . 0 5 m m ( 0 . 0 0 2 i n ) at 46 d e g re e s o f free d o m . Two s u ch val u e s s h o u l d b e co n s i d e re d s u s pect

( 9 5 % co n fi d e n ce l e ve l ) i f th e y d i ffe r b y m o re th an 0 . 1 3 m m ( 0 . 0 0 5 i n ) .

5. 1 1 . 6 R epro d u ci b i l i t y o f th e B as e D i am e te r I n creas e M eas u rem e n t ( M u l ti l abo rato ry)

Th e s tan d ard d e vi ati o n o f re s u l ts ( e ach th e ave rag e o f d u pl i cate s ) o btai n e d b y an al ys ts i n d i ffe re n t l abo rato ri e s h as be e n

e s ti m ate d to be 0. 08 mm (0. 003 i n) at 7 d e g re e s of fre e d o m . Two s u ch val u e s sh ou l d be co n s i d e re d s u s pe ct (95%

co n fi d e n ce l e ve l ) i f th e y d i ffe r by m o re th an 0 . 2 0 m m (0 . 0 0 8 i n ) .
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6. N O TE S

6. 1 M arg i n al I n d i ci a

A ch an g e bar ( l ) l o cate d i n th e l e ft m arg i n i s fo r th e co n ve n i e n ce o f th e u s e r i n l o cati n g areas wh e re te ch n i cal re vi s i o n s , n o t

ed i to ri al ch an g e s , h ave b e e n m ad e to th e pre vi o u s i s s u e o f th i s d o cu m e n t. An ( R ) s ym bo l to th e l e ft o f th e d o cu m en t ti tl e

i n d i cate s a co m pl ete re vi s i o n o f th e d o cu m e n t, i n c l u d i n g tech n i cal re vi s i o n s . C h an g e bars an d ( R ) are n o t u s e d i n o ri g i n al

pu b l i cati o n s , n e i th e r i n d o c u m en ts th at co n tai n e d i to ri al ch an g e s o n l y.

P R E P AR E D B Y TH E S AE BR AKE FLU I D S S TAN D AR D S C O M M I TTE E

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AP P E N D I X A - S TAN D AR D C O R R O S I O N TE S T S TR I P S

A. 1

TABLE A1 - S TAN D AR D C O R R O S I O N TE S T S TR I P S

C o rro s i o n M ate ri al
S u rface R e q u i rem e n ts
Te s t S tri p S pe ci fi cati on G e n e ral M ate ri al D ata D i m en s i on s

Ti n n e d i ron AS TM A 6 2 4 , Fe d e ral S R ti n pl ate e l ectrol yti c, bri g h t: Appro x. 8 cm l o n g ; 1 . 3 cm wi d e As s h e ared . C l e an an d

RM-06a S pe ci fi cati on QQ- T- N o . 2 5 , type M R Th i ckn es s: As pu rch ase d u n i fo rm ti n n i n g .

2 2
42 5 A Te m pe r 3 , base we i g h t 85 l b S u rface area: 2 5 cm ± 5 cm

Fe rro s tan d an d D OS o i l

S te e l S AE 1 0 1 8 Lo w carbo n s h ee t Appro x. 8 cm l o n g ; 1 . 3 cm wi d e E d g e s m ach i n e d to

RM-07 C o l d rol l e d Th i ckn es s: Appro x. 0 . 2 cm re m o ve s h e ari n g

2 2
H ard n e ss : 40 to 7 2 R B S u rface area: 2 5 cm ± 5 cm m arks . C l e an u n i fo rm

s u rfaces .

Al u m i n u m S AE AA2 0 2 4 W ro u g h t al u m i n u m al l o y Appro x. 8 cm l o n g ; 1 . 3 cm wi d e E d g e s m ach i n e d to

RM-08 Te m pe r T3 Th i ckn es s: Appro x. 0 . 2 cm re m o ve s h e ari n g

2 2
H ard n e ss : 75 RB typi cal S u rface area: 2 5 cm ± 5 cm m arks . C l e an u n i fo rm

s u rfaces .

C as t i ro n S AE G 3 0 0 0 S o ft au to m o ti ve cas t i ron . Mu st Appro x. 8 cm l o n g ; 1 . 3 cm wi d e S u rface g ri n d 4 s i d e s to

RM-09 be fre e from sh ri n kag e cavi ti es, Th i ckn es s: Appro x. 0 . 4 cm d i m en si o n u s i n g a we l l -

2 2
po ro si ty, o r an y o th e r d e fe cts S u rface area: 2 5 cm ± 5 cm d re ss e d N o . 8 0

d e tri m e n tal to spe ci fi cati o n u se o f Al u n d u m wh e e l . C l e an

th e m ate ri al . u n i fo rm s u rfaces .

H ard n e ss : 8 6 to 9 8 R B

B ras s S AE C A2 6 0 W ro u g h t al l o y—ye l l o w brass Appro x. 8 cm l o n g ; 1 . 3 cm wi d e E d g e s m ach i n e d to

RM-1 0 R o l l e d s h e e t o r s tri p; h al f h ard Th i ckn es s: Appro x. 0 . 2 cm re m o ve s h e ari n g

2 2
te m pe r S u rface area: 2 5 cm ± 5 cm m arks . C l e an u n i fo rm

H ard n e ss : 5 7 to 7 4 R B s u rfaces .

C o ppe r S AE C A1 1 4 C o l d rol l e d coppe r s h e e t o r s tri p Appro x. 8 cm l o n g ; 1 . 3 cm wi d e E d g e s m ach i n e d to

RM-1 1 H al f- h ard tem pe r Th i ckn es s: Appro x. 0 . 2 cm re m o ve s h e ari n g

2 2
H ard n e ss : 3 5 to 5 6 R B S u rface area: 2 5 cm ± 5 cm m arks . C l e an u n i fo rm

s u rfaces .

N OTE : D ri l l h o l e be twe en 4 an d 5 m m i n a d i am ete r an d appro xi m ate l y 6 m m from o n e e n d o f each s tri p. H o l e s to be cl ean an d free from bu rrs.

H ard n es s ran g es are com m e rci al l y fo r th e d es i g n ated m etal s. H ard n es s i s n o t s peci fi ed fo r th e ti n n e d i ro n becau s e i t i s n o t co n s i d ered a

practi cal re q u i rem en t.

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 1 6 o f 2 4

AP P E N D I X B – R M - 6 6 0 6 /I S O 49 2 6 C O M P ATI BI LI TY FLU I D

B. 1 FO R M U LATI O N O F FLU I D

M as s fracti o n

a
C o m po n e n ts % P u ri t y

Tri eth yl e n e g l yco l 1 9. 4 ≥ 95 %

Tri eth yl e n e g l yco l m o n o m e th yl

e th e r 25 ≥ 95 %

monobutyl ether ≤ 2 %,
D i eth yl e n e g l yco l

Triethylene glycol monobutyl ether 60 % ≤ purity ≤ 80 %

P o l ye th yl e n e g l yco l m o n o bu tyl Te trae th yl e n e g l yco l + h i g h er g l yc o l m o n o b u tyl e th ers

e th ers 3 5. 8 20 % ≤ purity ≤ 40 %
B o rate o f tri eth yl e n e g l yc o l

m o n om eth yl e th e r 1 8. 6 C o n te n t o f bo ri c aci d 1 1 . 2 % to 1 1 . 5 %

D i i s o pro pan o l am i n e 0 . 85 ≥ 98 %
n - BU TYLD I E TH AN O LAM I N E 0. 1 ≥ 98 %
B i s ph e n o l A 0. 2 ≥ 97 %
To l yl tri azo l e 0. 025 ≥ 98 %
B en zo tri azo l e 0. 025 ≥ 98 %
a.
Th e wate r co n te n t o f th e re fe ren ce fl u i d s h al l b e l es s th an o r e q u al to 0 . 2 0 %.

Th e re fere n ce fl u i d R M - 6 60 6 h as a m i n i m u m s h e l f l i fe o f 5 (fi ve ) years wh e n pu rch as ed an d s to re d i n acco rd an ce wi th S AE

J 75.
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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 1 7 o f 2 4

AP P E N D I X C - S TAN D AR D S T YR E N E - BU TAD I E N E R U B BE R ( S B R ) R M - 3 A BR AKE C U P S

FO R TE S TI N G S AE M OTOR VE H I C LE BR AKE FLU I D S

C. 1 FO R M U LATI O N O F R U B B E R C O M P O U N D

TAB LE C 1 - FOR M U LATI O N O F R U B B E R C O M P O U N D

I n g re d i e n t P arts b y W e i g h t

S BR typ e 1 50 2 1 00

N 3 3 0 S u pe rs acks 42

BBTS P e l l e ts 1

S t. Aci d P ri s te ri n e 9 4 2 9 1

Zi n c O xi d e ( 2 1 0 /672 ) 5

P o l yd e x E ( D C P - R ) 4 0 D 4. 5

S pi d er S u l fu r M C 9 8 0. 25

AG R TE S tal i te S /Octam i n e 1

An ti o x 58 /ZM TI P D R 0. 5

Fl e xo n e 6H C C P D /* Van o x 6 H 1 .5

TOTAL 1 5 6 . 75

C. 2 P R O C E D U R E FO R M I XI N G R U B BE R C O M P O U N D

Th e ru bbe r co m po u n d s h al l be m i xe d i n acco rd an ce wi th th e pro ce d u re g i ven i n AS TM D 3 1 8 5 fo r Fo rm u l a 2 B.

C. 3 P R O P E R TI E S O F R U B B E R C O M P O U N D

Vu l can i zates cu re d fo r 1 2 m in at 1 80 °C ( 3 56 ° F) fo l l o we d by a post cu re fo r 4 h at 1 00 °C (21 2 ° F) by th e pro ce d u re

d e s cri be d i n ASTM D 3 1 8 2 s h al l m e e t th e re q u i re m e n ts i n Tabl e C 2 .

TABLE C 2 - P R O P E R TI E S O F R U B BE R C O M P O U N D

P ro pert y R e q u i re m e n t AS TM M e th o d

H ard n es s 63 ± 3 D 1 41 5 o r D 2 2 40

2
Te n s i l e s tren g th 1 7. 5 M P a ( 2 5 0 0 l bf/i n , m in) D 41 2

U l ti m ate e l o n g ati o n 3 5 0 %, m i n D 41 2

Te n s i l e s tre n g th after 7 0 h at 1 2 5 ° C ( 2 57 ° F) 3 0 % d e cre as e , m ax D 865

U l ti m ate e l o n g ati o n afte r 70 h at 1 2 5 ° C ( 2 5 7 ° F) 5 0 % d e cre as e , m ax D 865

H ard n es s afte r 70 h at 1 2 5 ° C ( 2 5 7 ° F) 0 to 1 0 i n cre as e D 865

C o m pre s s i o n s e t afte r 2 2 h at 1 2 5 ° C ( 2 5 7 ° F) 1 0 to 2 0 % D 3 9 5 ( M eth o d B)

Bri ttl en e s s te m pe ratu re - 40 ° C ( - 40 ° F) , m ax D 21 37

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 1 8 o f 2 4

C. 4 BR AKE C U P S P R E P AR E D FR O M R U BB E R C O M P O U N D

Brake cu ps s h al l be pre p are d from th e ru bb er co m po u n d , by vu l can i zati o n u n d er th e co n d i ti o n s re q u i red to o b tai n th e

pro pe rti e s g i ven in S e cti o n C. 3. Th e di m en si on s o f th e cu ps s h al l b e s u i tab l e fo r th e brake c yl i n d e rs u sed to d ete rm i n e

s tro ki n g te s t pro ce d u re i n F M VS S 1 1 6 , as s h o wn i n F i g u re C 1 . C u ps m ay b e u s e d fo r te s ti n g brake fl u i d s wi th i n 6 0 m o n th s

from d ate o f m an u factu re wh en s to re d at te m peratu re s u n d e r 2 3 ° C ( 7 3 ° F) , o u t o f s u n l i g h t ( s to rag e i n d ark prefe rred ) , an d

ad eq u ate l y pro tect ed from co n tam i n an ts . R u b ber cu p s s h o u l d n o t be s to red u n d er an y s trai n an d d i ffe re n t p arts s h o u l d b e

s to red s e parate l y to avo i d m i g rati o n o f co n s ti tu e n ts . Las tl y, ru bb e r cu ps s h o u l d b e s to re d awa y fro m s o u rce s o f o zo n e .

After re m o val of cu ps fro m s to rag e , th e y s h al l be c o n d i ti o n e d b as e d o wn on a fl at s u rface fo r at l e as t 1 2 h at ro om

te m pe ratu re i n o rd e r to al l o w cu ps to re ach th e i r tru e c o n fi g u rati o n be fo re m eas u rem e n t.

FI G U R E C 1 - S AE TE S T C U P
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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 1 9 o f 2 4

AP P E N D I X D - S TAN D AR D E TH YLE N E , P R O P YLE N E , AN D D I E N E ( E P D M )

TE R P O LYM E R R U B B E R S LABS TO C K ( R M - 6 9 )

D. 1 FO R M U LATI ON O F R U BB E R C O M P O U N D

TAB LE D 1 - FO R M U LATI O N O F R U B BE R C O M P O U N D

I n g re d i e n t P arts b y W e i g h t

Vi s tal o n 2 5 0 4 1 00

N 3 3 0 S u pe rs acks 47

Zi n c O xi d e ( 2 1 0 /6 72 ) 5

Li an d o x D C P 9 9 ( B C FF) 3. 2

TM Q /AK D Q P e l l e ts 2

To tal 1 5 7. 2

D. 2 P R O C E D U R E FO R M I XI N G R U B BE R C O M P O U N D

Th e ru bbe r co m po u n d s h al l be m i xe d i n acco rd an ce wi th th e pro ce d u re s g i ve n i n AS TM D 3 1 82 .

D. 3 P R O P E R TI E S O F R U B BE R C O M P O U N D

D. 4

Vu l can i zates cu red fo r 1 2 m in at 1 80 °C ( 3 56 ° F) fo l l o we d by a post cu re fo r 4 h at 1 20 °C ( 2 48 ° F) by th e pro ced u re

d e s cri be d i n AS TM D 31 8 2 s h al l m e e t th e re q u i rem e n ts i n Tabl e D 2 .

TAB LE D 2 - P R O P E R TI E S O F R U B BE R C O M P O U N D

P ro pe rt y R eq u i re m en t AS TM M e th o d

H ard n es s , I R H D 70 ± 3 D 1 41 5

2
Te n s i l e s tre n g th , m i n 1 3 . 8 M P a ( 2 0 0 0 l bf/i n ) D 41 2

U l ti m ate e l o n g ati o n , m i n 2 2 5% D 41 2

Te n s i l e s tren g th , d e cre as e afte r 2 2 h at 1 75 ° C 1 5% D 8 65

( 3 47 ° F) , m ax

U l ti m ate e l o n g ati o n , d ecre as e afte r 2 2 h at 1 75 ° C 30% D 8 65

( 3 47 ° F) , m ax

H ard n e s s , i n cre as e afte r 2 2 h at 1 7 5 ° C ( 3 47 ° F) 0 to 1 0 D 8 65

C o m pre s s i o n s et after 2 2 h at 1 75 ° C ( 3 47 ° F) 2 0 % m ax D 3 9 5 ( M eth o d B )

Bri ttl e n es s te m peratu re , m ax - 5 4 ° C ( - 6 5 ° F) D 21 3 7

D. 5 S LAB S TO C K P R E P AR E D FR OM R U B B E R C O M P O U N D

Te s t s l abs ap pro xi m ate l y 1 50 m m x 1 50 m m x 1 . 9 m m ( 6 i n x 6 i n x 0 . 0 75 i n ) s h al l be pre p are d from th e ru bb e r co m po u n d

by vu l can i zati o n u n d er th e co n d i ti o n s s tate d in S ecti o n D. 3. Th e s e s l abs m ay be u sed in te s ti n g brake fl u i d s wi th i n

3 6 m o n th s from th ei r d ate o f m an u factu re , wh e n s to re d i n th e d ark at am bi en t te m peratu re s n o t excee d i n g 3 8 ° C ( 1 0 0 ° F)

an d ad e q u ate l y pro tecte d fro m atm o s ph eri c o r o th er co n tam i n an ts . W h e n s to re d at o th er th an 2 3 ° C ± 5 ° C ( 7 3 . 4 ° F ± 9 ° F) ,

th e m ateri al s h al l be al l o we d to s tabi l i ze at l ab o rato r y tem pe ratu re pri o r to m eas u re m e n ts .

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 2 0 o f 2 4

AP P E N D I X E - TR I E TH YLE N E G LYC O L M O N O M E TH YL E TH E R ( TE G M E ) BR AKE FLU I D G R AD E ( RM - 7 1 )

TAB LE E 1 - TR I E TH YLE N E G LYC O L M O N O M E TH YL E TH E R

(1 )
( TE G M E ) B R AKE FLU I D G R AD E ( R M - 7 1 )

P ro pe rt y R e q u i re m en t M e th o d

As s ay 9 4 are a %, m i n G as C h ro m ato g raph i c ( G C ) an al ys i s

Fu rth e r, n e i th e r th e m ate ri al pre ced i n g ( s e e bl o w)

n o r th at fo l l o wi n g TE G M E th ro u g h th e

co l u m n s h al l e xce e d 4 are a %

W ate r co n te n t 0 . 3 % b y we i g h t, m ax AS TM D 1 3 6 4

Aci d i ty 0 . 0 2 % b y we i g h t, m ax, as ace ti c aci d AS TM D 1 61 3

S u s pe n d e d m atte r S u bs tan ti al l y free —

App e aran ce C l ear l i q u i d ; 1 0 0 AP H A u n i ts , m ax AS TM D 1 2 0 9

ERBP 2 40 ° C ( 46 4 ° F) , m i n P arag raph 4. 1 o f S AE S tan d ard

J 1 70 3

1 . S tabi l i ze d by ad d i ti o n o f 1 /4% by we i g h t o f 4. 4' i s o pro pyl i d e n e d i ph en o l .

E. 1 G AS C H R O M ATO G R AP H I C AN ALYS I S

An al yze a re pres e n tati ve s am pl e u s i n g a Be n d i x M o d e l 2 2 0 0 d u al co l u m n , pro g ram m ed tem pe ratu re g as c h ro m ato g raph ,

o r e q u i val e n t i n s tru m e n t, wi th a th e rm al co n d u cti vi t y d e tecto r an d two 1 0 ft x 1 /8 i n Typ e 3 0 4 s tai n l e s s s te e l co l u m n s packe d

wi th 1 0 % C AR BOW AX 2 0M - te reph th al i c aci d o n C h ro m o s o rb T, 40 to 6 0 m e s h , as fo l l o ws :

E. 1 . 1 . 1 C o l u m n P re parati o n

U s e pre cl e an ed tu b i n g o r o btai n two 1 0 ft l e n g th s o f 1 /8 i n 3 0 4 s tai n l e s s s te e l tu bi n g ( 0 . 0 2 i n wal l th i ckn es s ) an d c l e an as

fo l l o ws :

a. R i n s e th e tu b i n g wi th 3 0 m L o f co n cen trate d n i tri c aci d .

C AU TI O N : N I TR I C AC I D C AU S E S S E VE R E B U R N S I F I T C O M E S I N C O N TAC T W I TH AN Y P AR T O F TH E B O D Y.

b. D rai n an d ri n s e th e tu b i n g wi th d i s ti l l ed wate r; d rai n an d ri n s e wi th ace to n e ; d r y wi th n i tro g e n .

E. 1 . 1 . 2 W e i g h 5 g o f C AR BOW AX 2 0 M - te re ph th al i c aci d i n to a 40 0 m L be ake r. Ad d 2 0 0 m L o f m eth yl e n e ch l o ri d e

an d s ti r wi th a m ag n e ti c s ti rre r u n ti l d i s s o l ve d . Appro x i m atel y 3 0 m i n wi l l be req u i re d .

E. 1 . 1 . 3 W e i g h 45 g o f C h ro m o s o rb T, 40 to 6 0 m e s h i n to a tare d be ake r an d tran s fe r to a 5 0 0 m L ro tary e vapo rati n g

fl ask.

E. 1 . 1 . 4 Ad d th e C AR B OW AX 2 0 M - TP A s o l u ti o n to th e fl as k an d m i x b y g en tl y s wi rl i n g . I f n e ce s s ary, ad d ad d i ti o n al

m eth yl e n e ch l o ri d e to fo rm a s e t s l u rr y.

E. 1 . 1 . 5 Al l o w th e s l u rry to s tan d fo r 1 0 m i n .
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E. 1 . 1 . 6 Attach th e fl as k to a ro tary e vapo rato r an d ap pl y vacu u m s l o wl y wh i l e d eg as s i n g . S et th e pre s s u re at

appro xi m atel y 1 0 0 m m H g . U s e d ry i ce - ace to n e traps to pro tect th e vacu u m s o u rce .

E. 1 . 1 . 7 R o tate th e fl as k at 1 0 rpm .

E. 1 . 1 . 8 P ro te ct th e co n ten ts o f th e fl as k from e xtrem e co l d o r h e at b y m e an s o f a h o t ai r g u n ( h ai r d r ye r at 5 0 to

60 °C) .

E. 1 . 1 . 9 W h e n al l o f th e s o l ve n t h as bee n rem o ve d , s to p th e e vapo rato r an d al l o w th e co n te n ts o f th e fl as k to re tu rn to

ro o m tem pe ratu re .

N O TE : I f a ro tary e vapo rato r i s n o t avai l ab l e , s ati s facto ry packi n g m ay be pre pare d u s i n g th e e vapo rati n g d i s h te ch n i q u e .

E. 1 . 1 . 1 0 Tran sfer th e d ri e d p acki n g to a b o ttl e h avi n g a vo l u m e abo u t twi ce th e vo l u m e o f th e p acki n g .

E. 1 . 1 . 1 1 Ad d 0 . 5 % b y we i g h t o f po wd ere d g raph i te an d m i x th o ro u g h l y u n ti l th e m i xtu re fl o ws fre el y.

E. 1 . 1 . 1 2 S i e ve th e m i xtu re u s i n g a c o m bi n ati o n o f 3 0 - an d 6 0 - m e s h s cree n s . R etai n th e p o rti o n th at pas s e s th ro u g h

th e 3 0 - m e s h an d i s re tai n e d o n th e 6 0 - m e s h s cre e n .

E. 1 . 1 . 1 3 U s i n g a fu n n e l , p ack th e co l u m n s wi th appro xi m ate l y 7 g o f packi n g b y g e n tl y tapp i n g th e s i d e o f th e co l u m n

wi th a s u i tab l e m e tal ro d . D o n o t ad d l arg e q u an ti ti e s o f packi n g to th e fu n n e l at o n e ti m e .

E. 1 . 1 . 1 4 C o n d i ti o n th e co l u m n s b y p ro g ram m i n g from am bi e n t te m pe ratu re to 2 0 0 ° C at 2 ° C /m i n an d h o l d at 2 0 0 ° C

fo r at l e as t 4 h . R e p e ate d l y i n j e ct a s am pl e u n ti l a g o o d bas e l i n e i s o btai n e d .

E. 1 . 2 O pe rati n g P aram e ters

a. R e co rd e r: 1 mV

b. C h art s pe ed : 0 . 5 i n /m i n

c. Tem pe ratu re s co l u m n : 1 50 to 2 2 5 ° C pro g ram m e d at 6 ° C /m i n ; h o l d at 2 2 5 ° C fo r 3 0 m i n

d. D ete cto r: 2 6 0 ° C

e. I n j e cti o n po rt: 2 3 0 ° C

f. C arri e r g as : H e l i u m at 2 0 c c/m i n

g. S am pl e s i ze : 1 mL

h. To tal el u ti o n ti m e: 45 m i n

E. 1 . 3 P ro ce d u re

I n j e ct th e s am pl e i n to th e ch ro m ato g raph an d o btai n th e ch ro m ato g ram u s i n g th e param e te rs o u tl i n e d i n E . 1 . 2 .

E. 1 . 3. 1 M e as u re th e areas o f al l co m po n en t pe aks u s i n g an e l e ctro n i c i n te g rato r o r a p l an i m e te r.

E. 1 . 3. 2 C al cu l ate an d re p o rt th e area p e rcen t o f TE G M E . Th e TE G M E e l u te s at abo u t 1 5 m i n .

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E. 1 . 3. 3 C al cu l ati o n

×
AT 1 00
= Area Pe rcent TE G M E
D
(Eq. E1 )

wh e re :

A = P e ak are a fo r TE G M E

D = To tal are a, s u m o f al l are as co rre cted fo r atte n u ati o n

T = Atte n u at i o n fo r co m po n e n t pe ak

E. 2 G AS C H R O M ATO G R AP H I C AN ALYS I S ALTE R N ATE P R O C E D U R E

An e q u i val e n t g as ch ro m ato g rap h i c pro ce d u re m ay be u s e d i n p l ace o f th at l i s te d i n App e n d i x E . 1 .

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 2 3 o f 2 4

AP P E N D I X F - R E FE R E E M ATE R I AL ( R M ) LI S T

Fo r th e cu rre n t s tatu s o n h o w to o btai n R e fe ree M ate ri al s vi s i t th e s u p pl i e r’ s web s i te at www.Greeninginc . co m .

RM Number Description Reference/Specification

R M - 0 3 a* W h e el C yl i n d e r C u p

R M - 0 4a* P ri m ary M as te r C yl i n d e r C u p

R M - 0 5 a* S eco n d ary M as te r C yl i n d e r C u p

RM -06a C orro s i o n Te s t S tri p- Ti n n e d I ro n AS TM A 62 4

RM -07 C orro s i o n Te s t S tri p- S te e l S AE 1 0 1 8

RM -08 C orro s i o n Te s t S tri p- Al u m i n u m S AE AA2 0 2 4

RM -09 C orro s i o n Te s t S tri p- C as t I ro n S AE G 3 0 0 0

RM -1 0 C orro s i o n Te s t S tri p- Bras s S AE C A2 6 0

RM -1 1 C orro s i o n Te s t S tri p- C o ppe r S AE C A1 1 4

RM -1 2* W h e el C yl i n d e r P i s to n

RM -1 3* M as te r C yl i n d e r P i s to n

R M - 1 4b * W h e el C yl i n d e r As s e m bl y

RM -1 5b* M as te r C yl i n d e r As s e m bl y

RM -20 O u tl e t tu b e co n n e cto r

RM -21 Bo l t

RM -24 W h e el C yl i n d e r C o n n e cto r

RM 25 C opp e r G as ke t

RM -26 Tu be N u t- I n verte d Fl are

RM -27 Ti n fo i l 9 9 %ti n , 0 . 5% l e ad , b e twe en 0 . 0 2

an d 0 . 0 6 m i n th i ckn e s s

RM -28 H i d i n g P o wer Tes t C h art AS TM D 3 44

RM -29 3 2 0 A Abras i ve G ri t P ape r 3 2 0 A o r P 40 0 carbo ru n d u m pape r.

R M - 49 C orro s i o n Te s t J ar- 475 m L wi th R M - 6 3 Li d

RM -51 E ffe ct o n R u bb e r Te s t J ar-2 5 0 m L

RM -52a Ti n n e d l i d fo r R M - 5 1

RM -57 Tu bi n g 1 /4" O D S AE J 5 2 7

RM -58 Tu bi n g 3 /1 6 " O D S AE J 5 2 7

RM -59 G l as s O i l S am pl e Bo ttl e w/co rk

RM -62 S cre w/N u t fo r R es i s tan ce to O xi d ati o n te s t

RM -63 Ti n n e d l i d fo r R M - 49 Ti n n ed s te e l l i d

RM -64 Ti n n e d l i d w/ ve n t h o l e Ti n n ed s te e l l i d wi th ce n tral ve n t

h o l e o f 0 . 8m m + - 0 . 1 m m i n d i am e ter

R M - 6 6 0 6* H i g h B o i l i n g C o m pati bi l i t y F l u i d I S O 49 2 6

RM -69* E PD M S to ck

R M - 70 * S i l i co n e Bas ed C o m pati b i l i ty Fl u i d

R M - 71 Tri e th yl en e G l yco l M o n o m eth yl E th e r

R M - 75 S i l i co n C arb i d e B o i l i n g S to n es #8 AS TM D 1 1 2 0

* I n d i cated re feree m ateri al s m u st be pu rch as ed from th e recom m e n d e d s o u rce si n ce th es e m ateri al s m u s t be appro ve d by th e S AE B rake Fl u i d s

S tan d ard s Com m i tte e.

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S AE I N TE R N ATI O N AL J 1 7 0 3 R e vi s e d AU G 2 0 1 4 P ag e 2 4 o f 2 4

AP P E N D I X G - S TR O KI N G TE S T R E FE R E N C E D ATA

G.1

Th e appro pri ate h i s to ri cal d ata m u s t be d e term i n e d an d th e re afte r pro vi d ed h ere i n a Tabl e .