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    3 - Algorithm A With Iterated Scale Scheme

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    Met Rizal
    This document discusses proficiency testing and outlines an 8 step protocol for conducting proficiency testing. It includes the following key points: 1. Step 1 involves sample preparation and step 2 involves testing for homogeneity criteria. 2. Steps 3 through 7 include sample distribution, testing, data collection, stability testing, statistical evaluation using outlier tests and Algorithm A. 3. Step 8 involves performance evaluation of participating laboratories based on their Z-score results. Z-scores between -2 and 2 are considered satisfactory.

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    3 - Algorithm A With Iterated Scale Scheme

    Uploaded by

    Met Rizal
    26 views8 pages
    This document discusses proficiency testing and outlines an 8 step protocol for conducting proficiency testing. It includes the following key points: 1. Step 1 involves sample preparation and step 2 involves testing for homogeneity criteria. 2. Steps 3 through 7 include sample distribution, testing, data collection, stability testing, statistical evaluation using outlier tests and Algorithm A. 3. Step 8 involves performance evaluation of participating laboratories based on their Z-score results. Z-scores between -2 and 2 are considered satisfactory.

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    3_Algorithm A with Iterated Scale Scheme

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    This document discusses proficiency testing and outlines an 8 step protocol for conducting proficiency testing. It includes the following key points: 1. Step 1 involves sample preparation and step 2 involves testing for homogeneity criteria. 2. Steps 3 through 7 include sample distribution, testing, data collection, stability testing, statistical evaluation using outlier tests and Algorithm A. 3. Step 8 involves performance evaluation of participating laboratories based on their Z-score results. Z-scores between -2 and 2 are considered satisfactory.

    Copyright:

    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    26 views8 pages

    3 - Algorithm A With Iterated Scale Scheme

    Uploaded by

    Met Rizal
    This document discusses proficiency testing and outlines an 8 step protocol for conducting proficiency testing. It includes the following key points: 1. Step 1 involves sample preparation and step 2 involves testing for homogeneity criteria. 2. Steps 3 through 7 include sample distribution, testing, data collection, stability testing, statistical evaluation using outlier tests and Algorithm A. 3. Step 8 involves performance evaluation of participating laboratories based on their Z-score results. Z-scores between -2 and 2 are considered satisfactory.

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    © All Rights Reserved
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    of 8

    Proficiency Testing:

    Algorithm A
    With Iterated
    Scale
    PROFICIENCY
    TEST SCHEME

    Chaerul Anwar, M.Si.


    Chemist – ISO 17025 &
    Protocol
    1. Persiapan Contoh
    2. Uji Homogenitas
    - Kriteria 1: Fhitung<Ftabel
    - Kriteria 2: Sdsampling<0,5SdHorwitz
    3. Distribusi
    4. Pengujian
    5. Koleksi Data
    6. Uji Stabilitas
    7. Evaluasi Statistik
    - Outlier Test
    - Algorithm A
    8. Penilaian Kinerja
    2  Chaerul Anwar
    No No Lab Hasil (mg/L) Protocol
    1 01 2,07 ± 0,42
    2 02 1,89 ± 0,02
    3 03   -  
    4 04 0,11 ± 0,02
    5 05 1,85 ± 0,18
    6 06   -  
    7 07 1,92 ± 0,01
    8 08 1,86 ± 0,07
    9 09 2,00 ± 0,09
    10 10 2,08 ± 0,12
    11 11 1,94 ±  -
    12 12 2,16 ± 0,25
    13 13 1,44 ± 0,08
    14 14 1,98 ± 0,01
    3  Chaerul Anwar
    Protocol
    Dixon's Value
    No No Lab Hasil (mg/L) Remarks
    Calculated Table
    1 04 0,11 ± 0,02 0,675 0,479 Outlier
    2 13 1,44 ± 0,08 0,641 0,502 Outlier
    3 05 1,85 ± 0,18 0,043 0,53 Pass
    4 08 1,86 ± 0,07      
    5 02 1,89 ± 0,02      
    6 07 1,92 ± 0,01      
    7 11 1,94 ±        
    8 14 1,98 ± 0,01      
    9 09 2,00 ± 0,09      
    10 01 2,07 ± 0,42      
    11 10 2,08 ± 0,12      
    12 12 2,16 ± 0,25 0,111 0,479 Pass
    4  Chaerul Anwar
    Protocol

    5  Chaerul Anwar
    Protocol
      1,5s *

    xi  x *
    Z score 
    s*

    x
    x
    n

    s * 1,134 x Sd

     x 1 
     x  x
    2
    x i
    Me   x n   x n  
    n S 2   2   1  
    2 
    n 1

    s *  1,483 x Me xi  x*
    6  Chaerul Anwar
    Protocol
    Unjuk kerja laboratorium peserta dievaluasi
    menggunakan Z-score dengan kategori:
    1) |Zscore| ≤ 2 : memuaskan (OK)
    2) 2 < |Zscore| <3 : peringatan ($)
    3) |Zscore| ≥ 3 : tidak memuaskan ($$)

    7  Chaerul Anwar
    TERIMA KASIH

    [email protected]
    081219960606

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