Vaplock - Resolution Systems
Vaplock - Resolution Systems
Vaplock - Resolution Systems
INTRODUCTION
Many labs are standardizing on Justrite 2- and 5- gallon HPLC CenturaTM waste containers. These safety cans have enough capacity for days or weeks of typical flow, vent automatically at 5 psig if pressurized, and allow users to disengage waste lines and vapor filters quickly during waste collection. Containers are available with either Polypropylene or Stainless Steel quick disconnects. Care should be taken when choosing the disconnect type. For example, at high concentrations the solvent Hexane swells Polyproplyene as much as 30%, causing the disconnect to stick and restrict fluid flow. Containers and manifolds with stainless steel quick disconnects are advised wherever such chemical compatiblity issues may arise; consult a chemical compatibility guide before selecting a container. One should also note that Justrite containers must be grounded while in use and especially while emptying the container, as static electricity has been known to ignite solvent fumes. For labs which choose not to use Justrite containers, VaplockTM products are also available to adapt to standard drum and pail closures, as well as Nalgene 83B, 53B, and 100-415 carboys. PLEASE NOTE THAT IT IS NOT POSSIBLE TO GROUND DRUM, PAIL, GLASS BOTTLE AND CARBOY (NON-JUSTRITE) CONTAINERS; THIS MAY RESULT IN A SAFETY HAZARD WITH FLAMMABLE SOLVENTS.
B A
PUMP
DETECTOR
The type and dimension of waste tubing found on an HPLC varies widely, depending on both system and user requirements. Outer and inner diameters range from microns to inches, and tubing material may be hard- or soft-wall plastic, metal, smooth-walled or corrugated. All these lines must be connected to a waste container. Adapting securely, without leaks and vapor release, poses a problem when attempting a closed system. VapLockTM manifolds adapt to tubing sizes up to 1/2 ID or OD (and larger if necessary) and can be stacked to accept additional lines. Most manifold ports permit direct connection of 1/4 or 1/2 threaded NPT fittings.
2B WASTE CONTAINER VAPOR VENT
For a closed system on a bottle, each container first requires a bottle cap with ports to fit the specific tubing sizes. When using caps with threaded ports for fittings, the fittings may be selected and replaced to accommodate different diameters of tubes. Caps with slip-through ports (non-threaded holes drilled or molded into a cap) are acceptable, provided the holes fit the tubing sizes securely. Most slip-through caps are made to accommodate 1/8 or 1/16 OD.
2006 Western Fluids Engineering and Manufacturing, LLC. All rights reserved.
In systems where sparging is not employed, to complete the closed system on a bottle each container requires a device to control the bottle cap vent. A closed bottle must function exactly like a coffee travel mug -- liquid goes out through one hole, and air comes in through a pinhole to displace the liquid removed. To manage the air flow, the simplest answer is a check valve assembly made to occupy a bottle cap port. The check valve allows air to enter a bottle as the pump moves the liquid phase out to the system. It also minimizes escape of vapors contained in the bottle. Should the bottle ever be exposed to pressure -- a result of a rise in lab temperature (over a warm weekend, for example) or a sparging line accidentally connected -- to reduce the threat of explosion a check-and-relief valve assembly is also available. The relief function allows pressure to escape while still preserving a pressure blanket of 0.5-1psi in the bottle. Although VapCheckTM units resist many standard solvents, care should be taken to consider the chemical compatibility of a solvent with VapCheckTM materials.
The most significant vapor generator in an HPLC system is the waste can, where solvents draining to the container may volatilize rapidly as solvent entering the container forces vapor into the laboratory. Activated carbon has excellent adsorptive properties for organic solvents. With a Gas Chromatograph, a number of carbon types were tested for vapor breakthrough under a flow of Acetonitrile vapor, one of the more common solvents used in HPLC. After determining the appropriate type, the carbon was similarly tested on other common solvents. The breakthrough data published in this brochure is based on use of 100% concentration of each solvent, at a flow rate of 1 mL per minute at S.T.P. (most analytical HPLCs run at 1-2 mL per minute). Disposal of spent cartridges should be conducted in accordance with local safety codes. Vaplock products may be purchased from:
01
NEW PRODUCTS
SECURE SOLVENT DELIVERY Use a Vaplock Solvent Delivery Kit to minimize release of solvent odors while supplying solvents to your system. A threaded connection for 1/8 OD tubing adapts to an inert PTFE bottle cap on a 2 Liter safety-coated borosilicate bottle, while a 1-way emission control valve allows air to enter the reservoir as solvent is removed. The valve opens at a low 0.07 psi to minimize backpressure. A 10um UHMW Polyethylene solvent filter, five replacement filter elements, Teflon 1/4-28 plug and five feet of 1/8 OD PTFE tubing are also included. For Reversed Phase solvents only. Please inquire for Normal Phase solutions.
Plumb multiple solvent lines securely to a waste container and reduce solvent odor emissions by using a Vaplock Waste Containment Kit. The heart of the system is a Justrite Polyethylene waste can, which includes 2 quick disconnects for ease of use (choose either Polypropylene with EPDM o-rings, or Stainless Steel and Teflon for more aggressive fluids). A 6-port waste manifold and fittings kit adapt to common HPLC tubing requirements, while a 5-pack of activated carbon and silica filters reduce vapors from the container vent. Antistatic wire grounds the system during use. 1, 2, and 5 gallon container sizes available.
5-GALLON
Polyethylene waste can with Stainless / PTFE disconnects
2-GALLON
Polyethylene waste can with Polypropylene / EPDM disconnects
02
SOLVENT RESERVOIRS
How to identify common laboratory solvent storage vessels
Although many container types and sizes are available, some of the more commonly used varieties in the laboratory are GL45, GL38 (sometimes known as 38-430), and GL32 glass bottles. VapLock caps are made to fit these standard sizes. Perhaps the most common reservoir of all, the GL45 lab bottle, is available for purchase. This glassware is manufactured by Schott Duran and Kontes, and is available in clear, plastic coated, and pressure-tested versions.
32mm
GL32 BOTTLE
Measures 32 mm from outside thread to ouside thread
GL38 BOTTLE
Measures 38 mm from outside thread to ouside thread
38mm
45mm
GL45 BOTTLE
Measures 45 mm from outside thread to ouside thread
03
FK-102 ALL-PTFE FILTER 10m Solvent Filter Assembly for 1/8 OD tubing
FK-202 THREADED FILTER CUP 10m Solvent Filter Assembly for 1/8 OD tubing, UHMWPE
BC-151
04
BOTTLE CAPS
Q SERIES CAPS
With 1/4-28 threaded ports Optional valved ports Anti-twist design - no twisted tubing! Solid PTFE body
Q series caps offer the simplest way to connect via 1/4-28 ports and fittings. Each port has a robust Stainless Steel thread insert to enable repeated connect and disconnect. 1/8 OD supply tubing may be press-fit into the underside of each cap. Easy operation on/off valves on each fluid line are an optional extra.
BC-109
GL45, (2) 1/4-28
BC-106
GL38, (2) 1/4-28
BC-110
GL45, (3) 1/4-28
BC-107
GL38, (3) 1/4-28
BC-111
GL45, (4) 1/4-28
BC-108
GL38, (4) 1/4-28
BC-113
GL38, 2-valved 1/4-28
BC-117
GL45, 3-valved 1/4-28
BC-114
GL38, 3-valved 1/4-28
BC-115
GL38, 4-valved 1/4-28
05
T H R E A D E D C A P S FO R NA L G ENE 3 8 -4 3 0 B OT T L ES
PTFE body with Polypropylene cap collar Expanded PTFE sealing gasket 1/4-28 threaded ports
Although similar to a standard GL38 thread, Nalgene 38-430 bottles require a slightly different bottle cap design for a proper seal. Caps include PTFE insert and gasket with Polypropylene collar and angled 1/4-28 ports.
BOTTLE CAPS
BC-322N GL45 3-port cap shown with DV-115 check valve, AQ-115 fitting kit, and plug
BC-340
3-Port cap for Nalgene 38-430 bottles
BC-440
4-Port cap for Nalgene 38-430 bottles
NO N-S T A ND A RD C A P S
Caps with 5/16-24 threaded ports Caps for 1/4 OD tubing Custom bottle caps and assemblies
We also design and manufacture bottle caps for custom applications. Below are several such designs which we now offer as part of our general product portfolio.
BC-220N
GL38 Economy Cap, 2-port
BC-222N
GL45 Economy Cap, 2-port
BCS-209
GL45 2-port cap for 1/4 OD tubing, non-threaded ports
SV-129
GL45 3-port cap with (2) 5/16-24 ports for 4.0mm or 3/16 OD tubing, and (1) 1/4-28 port
BC-320
GL38 Economy Cap, 3-port
BC-322N
GL45 Economy Cap, 3-port
NON-STANDARD CAPS
BC-420
GL38 Economy Cap, 4-port
BC-422
GL45 Economy Cap, 4-port
GL38 cap with (2) slip-through ports for 1/4 OD tube GL45 cap with (2) slip-through ports for 1/4 OD tube GL45 cap with (2) 5/16-24 and (1) 1/4-28 port GL38 cap with (2) 5/16-24 and (1) 1/4-28 port
06
EVAPORATION CONTROL
Minimize vapor loss from supply bottles Air inlet and pressure relief options Choose from Viton or perfluoroelastomer seals
Evaporation control units contain check valves that reduce the flow of vapor in and out of a solvent supply bottle. During a system run, as liquid solvent travels out of the supply bottle to the system, air must enter the bottle to displace the solvent removed. DV-115 and DV201allow air to enter the bottle, but not to escape. Part numbers DV-118 and DV-202 operate in the reverse, allowing pressure relief. DV-201 and DV-202 are constructed of PEEK and perfluoroelastomer and are our most chemically resistant option, while DV-115 and DV-118 are constructed from PTFE with Viton seals.
DV-115
Air Inlet Evaporation Control Valve, PTFE with Viton seal, 0.07 psi cracking pressure
AQ-111
For 1/16 OD tubing
AQ-112
For 1.8-2.0mm OD
AQ-117
For 2.2mm OD
DV-118
Air Outlet Pressure Relief Valve, PTFE with Viton seal, 1 psi cracking pressure
AQ-113
For 2.5mm OD tubing
AQ-114
For 3.0mm OD tubing
AQ-115
For 1/8 OD tubing
DV-201
Air Inlet Valve, PEEK with perfluoroelastomer seal, 1 psi cracking pressure
DV-202
Air Outlet Pressure Relief Valve, PEEK with perfluoroelastomer seal 1 psi cracking pressure
UC-004
1/4-28 PEEK Union, 0.05 bore
1/4-28 TUBING CONNECTIONS AND PLUGS EVAPORATION CONTROL AND RELIEF VALVES
1-WAY INLET AIR CONTROL VALVES DV-115 Air Inlet Valve, 1/4-28, 0.07 psi, Viton seal DV-201 Air Inlet Valve, 1/4-28, 1 psi, Perfluoroelastomer seal 1-WAY OUTLET AIR CONTROL (RELIEF) VALVES DV-118 Air Outlet Relief Valve, 1/4-28, 1 psi, Viton seal DV-202 Air Outlet Valve, 1/4-28, 1 psi, Perfluoroelastomer seal AQ-101X AQ-102X AQ-111X AQ-112X AQ-117X AQ-113X AQ-114X AQ-115X PL-103X For 360m OD tubing, Red / Green, 10 pack For 1mm OD tubing, Blue / Purple, 10 pack For 1/16 OD tubing, 10pk, Green, 10 pack For 1.8-2.0mm OD tubing, 10pk, Red, 10 pack For 2.2mm OD tubing, 10pk, Black, 10 pack For 2.5mm OD tubing, 10pk, Orange, 10 pack For 3.0mm OD tubing, 10pk, Yellow, 10 pack For 1/8 OD tubing, 10pk, Blue, 10 pack Delrin Plug, 1/4-28, 10 pack
07
WARNING: Viton seals in DV-115 and DV-118 are not suitable for use with some solvents, such as THF. Consult a chemical compatibility guide for further information.
PL-104X PFA Teflon Plug, 1/4-28, 10 pack SAMPLER KIT AND UNION SK-011 1/4-28 Sampler kit, includes 1 connection of each size UC-004 1/4-28 PEEK Union, 0.05 ID bore
TUBING GAUGE
Measure the inner and outer diameters of waste tubing accurately
AC-120
For 1/16 OD tubing
AC-121
For 1.8-2.0mm OD
AC-125
For 2.2mm OD tubing
INSTALLATION TOOLKIT
For quick installation of tubing connections in VaplockTM manifolds
AC-122
For 2.5mm OD tubing
AC-123
For 3.0mm OD tubing
AC-124
For 1/8 OD tubing
Easily install fittings in VaplockTM manifolds with the TK-100 installation toolkit. Includes deep socket set for 9/16 and 7/8 hex fittings, adjustable wrench, guillotine tubing cutter, sealing tape and zip tie adhesive mounts.
08
JUSTRITE
Quick-connect to Justrite CenturaTM waste cans HDPE and Polypropylene construction Locking lid with Polypropylene sealing gasket
SF- series funnels adapt to CPL safety Eco Funnels to allow quick disposal of pourable solvent waste. Locking, hinged lid minimizes leaks and spills when the funnel is closed. Standard Justrite CenturaTM containers include two quick disconnects, one for filling and one for venting; removal of the insert from the venting quick disconnect will prevent vapor release while not in use. If used in tandem with other VaplockTM products, such as manifolds and vapor filters, a closed system may also be maintained for passive wastes while the funnel is sealed. As with all solvent-based applications, chemical compatibility of the solvent and product should be noted prior to purchase. SF-series funnels are constructed of high density Polyethylene (HDPE) and Polypropylene, with a closed-cell Polypropylene sealing gasket. As Justrite Centura containers are available with two quick disconnect materials, Polypropylene (with EPDM o-ring) and Stainless Steel (with Teflon o-ring), select a safety funnel according to the type of disconnect material. .
ANTISTATIC WIRES
REDUCE FIRE RISKS FROM STATIC ELECTRICITY
Antistatic wires reduce spark danger from static electricity generated by movement and flow of flammable liquids. Bonding between containers during liquid transfer, and conecting drums to an earth ground are required under Federal and local codes.
JT-08500
Antistatic wires with 3 cable
CPLabSafety
Safety Eco Funnel TM is a trademark of CP Lab Safety.
SAFETY WASTE FUNNELS
09
Funnel with PP / EPDM disconnect Funnel with SS / Viton disconnect Funnel with SS / Teflon disconnect
M A N I F O L D S F O R J U S T R I T E C A N S
MA-701
7-ported waste manifold for PP/EPDM disconnects
MA-603
7-ported waste manifold for Stainless / PTFE disconnects
Select a manifold for a Justrite can based on the type of disconnects on the container. For a Justrite can with Polypropylene and EPDM disconnects, for example, choose part number MA-301 (3-port) or MA-601 (6-port). If a system has more waste lines than a single manifold can accommodate, use stacking manifolds to handle almost any requirement. 1-port Polyethylene adapter MA-101 has one 1/4 NPT port. 3- ported Polypropylene manifolds have three 1/4 NPT ports. 6-ported Polypropylene manifolds have five 1/4 NPT ports radially, and one 1/2 NPT top port. 9-ported PTFE manifolds have eight 1/4-28 ports radially, and one 1/4 NPT top port. To connect tubing to waste manifolds, see tubing connections on pages 7-8.
MA-601
6-ported waste manifold for PP/EPDM disconnects
MA-902
9-ported waste manifold for Stainless/PTFE disconnects
MA-300
3-ported stacking unit, Polypropylene, With 1/4 NPT male adapter
MA-600
6-ported stacking unit, Polypropylene, With 1/2 NPT male adapter
MA-301
3-ported waste manifold for PP/EPDM disconnects
MA-303
3-ported waste manifold for Stainless/PTFE disconnects
10
CARBOY MANIFOLDS
CARBOY MANIFOLDS
Various manifold options for large and small bore tubing Adapt to 83B and 53B, 70mm, 63mm, 61mm and 100-415 carboys and pails
Carboy and drum manifolds permit multiple waste lines of varying size and type to be connected to the container of your choice. If more tubing lines need connecting than a manifold will permit, use of the appropriate stacking unit will increase the number of ports to suit your needs. Panel mount manifolds may also be used if a nonstandard cap is present; either drill a 1.125 diameter hole (max 1/2 depth) in the cap and thread in place for a secure seal, or remove the lock ring to install in the 3/4 NPT knockout threads found on some carboy caps.
SV-127
11
53B 6-ported manifold, with free-spinning cap collar;with (5) 1/4 NPT ports, (1) 1/2 NPT port
BC-722
7-port manifold for GL45 bottle, with (6) 1/4-28 radial ports, (1) 1/4 NPT top port
BC-723
7-port all-PTFE manifold for GL45 bottle, with (6) 1/4-28 radial ports, (1) 1/4 NPT top port
BC-622
6-port manifold for GL45 bottle, with (5) 1/4 NPT ports radially, (1) 1/2 NPT top port
12
CARBON FILTERS
Minimize odors by adsorption before they enter the lab environment Constructed of activated coconut shell carbon and silica dessicant, with Polypropylene housing Economically priced
Reduce odors from solvent waste containers by installing a VaplockTM carbon filter, which may be adapted to a number of low pressure emission sources. Dispose of spent cartridges in accordance with local safety codes.
FA-017
Adapts filter to a female Polypropylene quick disconnect on a Justrite waste can, with elbow adapter
FA-010
Adapts filter to a female Polypropylenequick disconnect on a Justrite waste can
FA-015
Adapts filter to a female stainless steel quick disconnect on a Justrite waste can
FA-005
Adapter with 1/2 NPT male thread
13
FA-001 FA-002 FA-003 FA-004 FA-005 FA-010 FA-007 FA-015 FA-017 FA-018
Luer lock adapter, Polypropylene Male slip-type luer adapter, Polypropylene 1/4-28 adapter, long, Polypropylene 1/4 NPT adapter, Polypropylene 1/2 NPT adapter, Polypropylene Justrite can adapter, PP / EPDM Justrite can adapter, SS / Viton Justrite can adapter, SS / Teflon Justrite can adapter, elbow, PP / EPDM Justrite can adapter, elbow, SS / Viton
LEVEL CONTROL
LA-100-01
Alarm control unit with power and sensor cable connected
The LA-100 Electronic Level Alarm is designed to alarm the operator of a full or empty condition in a Polypropylene or Polyethylene tank. The sensor is a low voltage, intrinsically safe device that is connected via a 10 foot cable to the control box unit. The control is powered by a 110 VAC convertor which supplies 5 VDC power to the control box. A green operating light and red alarm light allow visual inspection of the operating condition of the level alarm. An alarm override button is easily accessible on the top. For powered relay or accessory control, such as controling a pump function or instrument shutdown, an auxiliary output is also included.
Only Polyetheylene and Polypropylene containers with a wall thickness in the range of 0.1 - 0.125 may be used with the LS-100 at present.
14
CLOSED SYSTEMS
FOR SOLVENT CONTAINMENT
VAPOR AND SPILL CONTROL FOR LABORATORY SOLVENTS
APRIL
2009