Richard MASc S2021

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The Relationship Between Lattice Structure Topology and Rapid

Investment Casting Performance

Christopher Richard

A Thesis
in
The Department
of
Mechanical Engineering

Presented in Partial Fulfillment of the Requirements


for the Degree of Master of Applied Sciences (Mechanical
Engineering) at
Concordia University
Montreal, Quebec, Canada

September 2020
©Christopher Richard, 2021
ii

CONCORDIA UNIVERSITY
School of Graduate Studies

This is to certify that the thesis prepared


By: Christopher Richard

Entitled: The Relationship Between Lattice Structure Topology and Rapid


Investment Casting Performance

and submitted in partial fulfillment of the requirements for the degree of

Master of Applied Sciences (Mechanical Engineering)

complies with the regulations of the University and meets the accepted
standards with respect to originality and quality.
Signed by the Final Examining Committee:

Dr. Martin Pugh Chair


Chair’s name
Dr. Zezhong Chen Examiner
Examiner’s name
Dr. Tsz-Ho Kwok Supervisor
Supervisor’s name
Approved by: Dr. Sivakumar Naranswamy
Chair of Department or Graduate Program Director

September 16th 2019 Dr. Mourad Debbabi


Dean of Faculty
iii

Abstract
The Relationship Between Lattice Structure Topology and Rapid Investment
Casting Performance

Christopher Richard

To leverage the unprecedented design freedom of additive manufacturing


(AM), this work aims to develop a design methodology for lattice structures
fabricated by rapid investment casting (RIC). What lattice topological proper-
ties have the most significant impact on the overall performance in RIC, and
how to improve them? The hypothesis is that the relative strut size, num-
ber of joints, joint valence, and strut angle significantly affect the performance.
There is no overarching analysis of the effect that lattice topology has on cast-
ing performance. To remedy this, various lattice topologies underwent mold
flow simulation, finite element analysis, casting experiments, and grain struc-
ture analysis. From the results, a set of design guidelines for RIC is created,
and new lattice structures are designed. The design recommendations by im-
portance are as follows. A relative strut size, number of joints, and joint valence
should be below 0.20, 9, and 8, respectively. For mechanical performance, the
strut angle distribution should include vertical, diagonal, and horizontal struts.
The two proposed topologies: proposed cell and hourglass, meet all these crite-
ria and achieve good casting and mechanical performance.
iv

Acknowledgements
I would like to acknowledge everyone who helped me during my degree.
My parents and friends for their unconditional support. I would like to thank
the Birks Family Foundation for there support throughout the entirety of my
education with special regards to Mr. J. Birks and Mrs. G. Carozza.
I would like to thank my supervisor Tsz-Ho Kwok for his incredible support,
ensuring I have all the equipment necessary to complete my Master’s and his
encouragement and tutelage.
v

Contents

List of Figures viii

List of Tables ix

1 Introduction 1

2 Related Work 7
2.1 Casting Technology . . . . . . . . . . . . . . . . . . . . . . . . . 7
2.2 Additive Manufacturing . . . . . . . . . . . . . . . . . . . . . . 9
2.3 Lattice Structures . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.4 Applications of Rapid Investment Casting Lattice . . . . . . . . 13

3 Materials and Methods 17


3.1 Materials and Equipment . . . . . . . . . . . . . . . . . . . . . . 17
3.2 Manufacturing Process . . . . . . . . . . . . . . . . . . . . . . . 18
3.2.1 Pattern Making . . . . . . . . . . . . . . . . . . . . . . . 18
3.2.2 Mold Making and Burnout . . . . . . . . . . . . . . . . . 19
3.2.3 Casting . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
3.2.4 Post-processing . . . . . . . . . . . . . . . . . . . . . . . 21
3.3 Lattice Designs . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.3.1 Set 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
3.3.2 Set 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
3.4 Characterization . . . . . . . . . . . . . . . . . . . . . . . . . . 24
3.4.1 Mold Flow Simulation . . . . . . . . . . . . . . . . . . . 24
3.4.2 Mechanical Finite Element Analysis . . . . . . . . . . . . 25
3.4.3 Microscopic Analysis . . . . . . . . . . . . . . . . . . . . 27
vi

4 Results 28
4.1 Mold Flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
4.2 Cast 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.3 Cast 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.4 Mechanical Properties . . . . . . . . . . . . . . . . . . . . . . . 32
4.5 Voids and Grain Structures . . . . . . . . . . . . . . . . . . . . 34

5 Discussion 38
5.1 Design Guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . 40

6 Conclusion 43
vii

List of Figures

1.1 Pattern Making AM Processes: a)Digital Light Processing. b)


Stereolithography Apparatus. c) Multi-Jet Modeling. d) Fused
Filament Fabrication. . . . . . . . . . . . . . . . . . . . . . . . . 3
1.2 Rapid Investment Casting Process . . . . . . . . . . . . . . . . . 5

2.1 Casting defects located in cast part. Reprinted by permission


from Springer Nature [1] © 2020. . . . . . . . . . . . . . . . . . 7
2.2 Numerical simulation and correlation with macro-structure eval-
uation of the primarily proposed design. Reprinted by permission
from Springer Nature [2] © 2020 . . . . . . . . . . . . . . . . . 8
2.3 Topology optimization of the GE bracket for multiple load cases.
Reprinted by permission from Springer Nature [3] © 2020 . . . 10
2.4 Optimized pillow bracket printed by EOS DMLS. Reprinted from
[4] © 2019, with permission from Elsevier. . . . . . . . . . . . . 12

3.1 RIC process: a) DLP additive manufacturing. b) Pattern spru-


ing. c) Plaster mold making. d) Pattern burnout. e) Vacuum
casting. f) Post processing. . . . . . . . . . . . . . . . . . . . . . 18
3.2 3D Systems FabPro 1000 prototyping resin burnout profile . . . 20
3.3 Test 1 lattice cells and structure: a) Rhombic. b) kelvin. c)
Cubic. d) Octet-Truss. e) 2 × 2 × 6 structure. . . . . . . . . . . 22
3.4 Test 2 lattice cells and structure: a) Proposed cell. b) Hourglass.
c) Rhombic. d) Octet-Truss. e) 5 × 5 × 5 structure. . . . . . . . 24
3.5 Loading conditions tensile: a) Displacement b) Force c) Fixed
support. Loading conditions shear: d) Force e) Fixed support f)
Displacement g) Displacement . . . . . . . . . . . . . . . . . . . 26
viii

4.1 Flow simulation results for rhombic and kelvin . . . . . . . . . . 28


4.2 Printed Patterns Experiment 1 a) Rhombic b) kelvin c) Cubic d)
Octet-Truss . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.3 Set 1 cast structures: a) Rhombic, b) Kelvin, c) Cubic, and d)
Octet-Truss. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
4.4 Printed Patterns Experiment 2: a) Proposed cell b) Hourglass c)
Rhombic d) Octet-truss . . . . . . . . . . . . . . . . . . . . . . . 31
4.5 Set 2 cast structures: a) Proposed cell, b) Hourglass, c) Rhombic,
and d) Octet-Truss. . . . . . . . . . . . . . . . . . . . . . . . . . 32
4.6 FEA results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
4.7 Microscopic analysis for grain structure. Images 50× magnification 36
4.8 Microscopic analysis for porosity. Images 50× magnification . . 37

5.1 Topology strut angle distribution . . . . . . . . . . . . . . . . . 39


ix

List of Tables

3.1 Mold flow Altair Inspire Cast 2019.3 material properties . . . . 25


3.2 Ansys 70/30 [Cu/Zn] brass material properties . . . . . . . . . . 27

4.1 Lattice topology comparison casting experiment 1 . . . . . . . . 30


4.2 Lattice topology comparison casting experiment 2 . . . . . . . . 33
4.3 Resultant modulus for simulated Ansys lattice structures. Eeq is
the Equivalent Tensile Modulus and Geq is the Equivalent Shear
Modulus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
4.4 Void properties. All area are in µm2 . . . . . . . . . . . . . . . . 35
4.5 Lattice topology strut size and joint characteristics. Strut size is
in mm. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

5.1 Lattice topology performance grading (from 1 to 4.) . . . . . . . 41


1

Chapter 1

Introduction

Currently, the most studied metal AM process is SLM. SLM has many positive
aspects, which make it a topic of interest, but also some limitations. According
to Aboulkair et al. [5], one of the most common defects in SLM parts in general,
irrespective of the material, is porosity. Maconachie et al. [6] also mentioned
that SLM fabrication of lattice structures is understood to result in manufac-
turing defects. Beyond that metallic additive manufacturing methods cannot
be used for mass manufacturing of complex parts. This is due to the high cost
associated with the process. Alternatively multiple patterns for RIC can be
made at a very low cost and depending on the geometry can be made hollow to
save on material usage and print time. According to Leuders et al. [7], When
comparing RIC to SLM, fatigue loadings are still a challenge for SLM, and the
same is true for selective sintering (SLS). Li et al. [8] demonstrated the presence
of residual stresses in most metal AM processes. The residual stresses are due
to high temperature gradient and rapid cooling. Given that RIC is a hybrid
AM and solidification process, it is less prone to residual stresses. In addition
of the three manufacturing processes, investment casting (IC) is already well
established in many industries that would benefit from a shift towards RIC. RIC
has similar capabilities as SLM. Both methods have their respective uses and
place in the additive manufacturing space, but RIC performs better in some ap-
plications. One example is in the manufacturing of aluminum alloy structures,
which is a challenge for SLM to process because aluminum is reflective, and the
laser has difficulties melting aluminum without causing defects [5]. Also, RIC
2 Chapter 1. Introduction

does not require sintering, which often leads to considerable shrinkage. The
use of SLM for lightweight cellular structures has been heavily iterated and
researched. The result is a vast trove of knowledge regarding materials, param-
eters, and design methodologies for metallic additive manufacturing of cellular
lattice structures. Although RIC can also be used to manufacture complex lat-
tice structures with unprecedented design freedom, little work has been done
to advance the design methodology for RIC of lattice structures. The limited
research includes using fused filament fabrication (FFF) to produce low-cost
patterns [9], studying the effect of cross-sectional shape of struts on mechanical
properties [10], and finding the optimal filling direction for honeycomb struc-
tures [11]. However, there is no current overarching analysis of the effect that
lattice topology has on casting performance and what topological properties
play the most extensive role in minimizing casting defects. Lattice topology
is defined as the properties of a lattice structure in 3D that remain the same
regardless of deformations such as twisting and stretching. For strut-based lat-
tice topologies these properties are the bounding volume, unit cell density, and
strut shape/distribution/connectivity. This analysis is required to avoid casting
defects in lattice structures to faithfully apply them to metal parts. There are
many benefits to RIC over other manufacturing processes. RIC can produce
parts with complex geometries such as: thin sections, cavities and complex in-
ternal lattice structures. Beyond that, RIC requires very little post processing
and it can produce parts with great dimensional accuracy and surface finish.
Finally, RIC components do not suffer from poor fatigue strength so it can
be used in industries like aerospace, dentistry and biomedical engineering, etc.
This work will present the background information on IC and RIC and then
delve deeper into the current open areas of research. Some areas of research
show more potential towards improving the manufacturing process as a whole
and these will be presented with the intention of identifying the most lucrative
research directions in RIC.
Given that RIC is a hybrid manufacturing method with both additive and
solidification processes, its design considerations stem from both methods. To
Chapter 1. Introduction 3

correctly print the pattern, design for AM needs to be applied. Considerations


include print direction, support location, and overhang angle. The AM perfor-
mance depends heavily on the chosen AM method, the topology of the pattern
and supports, and the material and process parameters. Some common pattern
making methods are: fused filament fabrication (FFF), stereolithography ap-
paratus (SLA), digital light processing (DLP) and Multi-Jet Modeling (MJM)
see Fig 1.1.
a) b)
Scanner System
Build Platform

Laser Beam
Laser
Resin Tank

LCD Screen Resin Tank

UV LED Bulb

Uncured Resin Platform and Piston

d) e)

Fillament

Fillament Roll
Resin Tanks
Temperature Control
Resin Jets Nozzle

UV Led Bulb
Build Platform Build Platform

Figure 1.1: Pattern Making AM Processes: a)Digital Light Process-


ing. b) Stereolithography Apparatus. c) Multi-Jet Modeling. d) Fused
Filament Fabrication.

FFF is a 3D printing process in which plastic filament made from PLA


(polylactic acid), ABS (acrylonitrile butadiene styrene) etc. is melted through
a heated nozzle and deposited following a tool path on a print bed. Tool paths
can be generated using a slicer software. The software breaks down 3D models
into layers each with its own tool path. SLA and DLP are photo-curable resin
based processes, SLA uses a laser to cure a layer point by point and layer
by layer. DLP uses a projector or LCD to cure full layers at a time. The
4 Chapter 1. Introduction

benefits of these 3D printing processes are that they can create really high
quality patterns with great surface finishes. The RIC process can be seen in
Fig 1.2. Conventional manufacturing methods impose geometric restrictions
this is not the case for RIC. IC uses a sacrificial pattern to form a mold. This is
done by encasing the pattern in refractory material. The pattern then undergoes
a burnout process leaving a mold cavity in the shape of the pattern. Molten
metal can then be poured into the mold cavity creating a metal part with the
same geometry as the pattern. Design for IC has its own set of considerations:
feeding direction, gating and feeding system design, and pattern topology. The
IC performance depends heavily on the pattern and gating system topology
and its inherent mold flow. Like many processes, topology optimization can
be applied to casting. Topology optimization for casting relies primarily on
the following properties: feed paths, flow velocity and flow connectivity. Feed
paths are used to ensure directional solidification moving from thin to thick.
Risers can be placed to allow for directional solidification that sweeps from the
extremities of the mold cavity toward the riser. Flow velocity can be optimized
to ensure molten metal does not prematurely solidify. Finally flow connectivity
can be controlled to avoid turbulence or hot spots. Minimizing the number
of intersections of metal flows will allow the casting to cool at similar rates
throughout, this will avoid the potential for hot spots which result in localized
shrinkage voids. Studying the effect of lattice topology on RIC performance
will help draw out the optimization objectives in order to be able to eventually
apply topology optimization to the casting of lattice structures. When it comes
to the design of lattice structures for RIC, the lattice topology is one of the most
critical factors that affects printability, castability, and mechanical properties.
Different objectives may have contradicting requirements on the topology, and
the research question here is: what lattice topological properties have the most
significant impact on the overall performance in RIC, and how to improve them?
In this work, a few properties are hypothesized, including the relative strut
size, number of joints, joint valence, and strut angle, significantly affect the
casting performance. These properties can be evaluated using a variety of lattice
Chapter 1. Introduction 5

topologies and structures. The relative strut size is the strut size divided by the
unit cell width, which is a property that will remain the same regardless of unit
cell width. The number of joints refers to the total number of points within
the cell where struts connect. Joint valence refers to how many struts connect
at a given joint. Strut length is the distance traveled by the metal flow in the
lattice cell. Strut angle is the angle of the strut from the filling direction of the
lattice structure. These properties were chosen as they relate to the definition
of lattice topology. Relative strut size and strut shape directly affect unit cell
density. Number of joints, joint valence and strut angle directly affect strut
distribution/connectivity.

Refractory 3D printed
pattern Broken shell Metal casting
material
slurry

Furnace

Removal from
part tree and
feeding

Shell Mold

Shell Building Pattern Burnout Shell Mold Breaking Post Processing

Figure 1.2: Rapid Investment Casting Process

By answering the research question, this work aims to develop a design


methodology for RIC lattice structures. The goal of the design methodology
would be to minimize casting defects caused by the lattice topology. Since
RIC’s design is a multi-objective optimization, only the lattice structures with
excellent printability are selected, i.e., self-supported and open-celled, and focus
on improving the castability without sacrificing mechanical performance. These
lattices will undergo mold flow and mechanical simulation to determine what
defects will occur and which properties are more critical. The casting results
will be evaluated and compared with the theoretical results to establish design
guidelines for RIC lattice structures. These design guidelines will be used to
propose new designs optimized for casting performance. Finally, a larger scale
sample of the best performing design will undergo microscopic void and grain
structure analysis to verify the simulation results further. The objective of this
6 Chapter 1. Introduction

work is to expand the limited research on lattice design for RIC as there is no
overarching analysis on the effect of lattice topology on casting performance.
The contributions of this work include:

• A methodology to study rapid RIC lattice structures’ performance is pre-


sented to test our hypothesis on the lattice topological properties.

• The properties are compared and analyzed with the test results, and a set
of design guidelines for RIC is created.

• Based on the analysis, new lattice structures are designed and optimized
for RIC.

This work is organized as follows. Chapter 2 briefly reviews the related


works. Chapter 3 details the equipment, materials and methodology used.
Chapter 4 describes the theoretical and experimental results of the study. Chap-
ter 5 evaluates the results and establishes an order of importance to the topo-
logical lattice properties for casting performance. Finally, the work concludes
in Chapter 6.
7

Chapter 2

Related Work

2.1 Casting Technology

Figure 2.1: Casting defects located in cast part. Reprinted by per-


mission from Springer Nature [1] © 2020.

IC was described as taking advantage of a fluid’s ability to assume the shape


of its container [12]. IC is a extensively developed and refined process. IC was
primarily used with precious metals for ornamentation and religious purposes.
After 1897, dentists began using the manufacturing processes to make dental
inlays. During WWII, IC became the manufacturing process of choice for mil-
itary aerospace components. Afterwards, the IC process transitioned to many
commercial and industrial applications. The applications of IC have evolved
from ornamentation to dental and finally aerospace, all these applications are
still in use today in addition to biomedical engineering. The main difference
with the modern applications is that they test the limits of the process using
8 Chapter 2. Related Work

complex design elements such as small cross sections and high dimensional ac-
curacy [13]. Given the nature of the process, IC design is principal to good mold
flow [1,14–17]. Poor gating system design could lead to casting defects, this be-
haviour can be seen in Fig. 2.1. During the optimization of casting homogeneity,
the gating system’s quality can be the most important factor affecting casting
defects occurrence [18]. One way to improve casting performance is using a
novel parabolic conical-helical sprue which reduces surface turbulence in metal
below critical velocity during mold filling [19]. Poor gating system design could
also lead to rough surface finish and accuracy, and a design where the size of
sprue and runner is unbalanced will produce unstable molten metal flow [16].
Current research is focused mainly on iterating gating system design op-
timization in the hopes of reducing the likelihood of casting defects. Gating
system design remains an iterative laborious process. There exist design guide-
lines for the process, but limited research on applying computational methods
to automate the process. One exception is the use of computing and data-
driven methods for gating and feeding system design in IC. Yu et al. present a
data-driven framework coupled with the RBF optimization method for gating
system design. The results of the optimization can be seen in Fig 2.2, it can be
observed that all the defects occur in the feeders and not the cast part.

Figure 2.2: Numerical simulation and correlation with macro-


structure evaluation of the primarily proposed design. Reprinted by
permission from Springer Nature [2] © 2020

From the optimizations the gating system’s diameter was found to be the
most influential on the volume of average shrinkage porosity [2]. This knowledge
2.2. Additive Manufacturing 9

can be added to the ever growing design methodology for IC. Conventional IC
relies primitive technologies for pattern making but AM is the most popular
option to replace the wax used in pattern making [20]. The only difference
between IC and RIC is the pattern making method, RIC relies on AM for
pattern making. This allows for RIC to take advantage of the full design freedom
of AM as it does not need to worry about pattern removal from the mold like
its wax alternatives. Let it be noted that for traditional IC the wax pattern is
melted whereas for RIC the resin pattern is burned for removal. This means
that the wax in IC can be reused to a certain extent, this is not the case for
RIC resin. There also exist wax 3D printing processes that can be used for RIC,
these processes are a bit slower and the patterns are more delicate than resin
for the molding process. For the 3D printed wax, the wax could not directly be
reused, it would have to be reprocessed for the 3D printer.

2.2 Additive Manufacturing

Design for IC and AM can be combined to cast a structurally optimized metal


components [21] such as the one in Fig 2.3. There exist many AM methods but
only several of them are used for pattern and mold making. The RIC processes,
mainly using SLA can be found in a review [22]. Given that the dimensional
accuracy of the component cast using RIC is highly pattern dependent [23, 24].
Ishida et al. [25] tested the ability of different manufacturing methods to create
dimensionally accurate full dental crowns, and they showed that all the methods
had their respective drawbacks. Monzon et al. [26] discovered the presence of
anisotropy in patterns made using DLP. The authors found that post curing
does remove the anisotropy for certain resins where UV light can pass through
the resin and pigment. This could be concerning depending on the application
for these 3D printed parts. Anisotropy can often associated with nonuniform
strength. Even in RIC, anisotropy could cause unpredictable mold cracking.
SLA was used by Huang and Huang [27] to compare RIC and traditional IC
by creating a miniature turbine blade. They found that SLA can create high
10 Chapter 2. Related Work

precision casting patterns. MJM can also 3D print using photo-curable resins,
but has the benefit of printing in wax materials as well, it can also create much
larger parts, with resolutions slightly higher than SLA and DLP. The resolution
of 3D prints are highly dependent on the machine and materials used. FDM
can be used create much larger parts than its resin based alternatives. Given
the low cost and large build volumes, a lot of research has been done to improve
its surface finishes and dimensional accuracy. Kumar et al. [28] attempted
to improve the surface finish of 3D printed patterns by observing the effect
of varying process parameters such as: geometric volume to area ratios, wax
coated or uncoated patterns, orientation, mold thickness and material grade
in order to achieve high dimensional accuracy when casting a hip joint. They
concluded, a thin coating of wax increases accuracy of the patterns being made.
Higher volume to area ratios and pattern orientations of 90 degrees lead to
higher accuracy. They were able to achieve the permissible tolerances grades
determined by the ISO standard. Hafsa [29] and Ibrahim et al. [30] compared
the use of two AM methods, MJM and FFF for creating RIC patterns. The
authors found that utilizing different internal structure for their patterns had
an effect on surface roughness. The main drawback of using FFF for IC is that
much effort is required to improve the quality of the printed patterns. Presently
FFF can not achieve the quality of patterns that DLP, SLA and MJM can. For
small scale IC, given the low cost, high speed and resolution of DLP, it is a
excellent choice for pattern making. For larger parts MJM seems to be the best
process available at the moment [13].

Figure 2.3: Topology optimization of the GE bracket for multiple


load cases. Reprinted by permission from Springer Nature [3] ©
2020
2.3. Lattice Structures 11

An alternative mold making technique is patternless mold making. This pro-


cess can improve time efficiency when compared to pattern dependent methods.
The burnout process can be omitted for patternless mold making. The main
drawback of the process is that it is dependent on SLS or binder jetting technol-
ogy. The two powder based process both undergo large amounts of shrinkage
during the mold sintering processes. The sintering process is required to fully
consolidate the ceramic or plaster refractory powders used. Generally the pow-
der based AM processes can produce surface finishes on par with sand casting.
This pales in comparison to the surface finish achievable with a pattern. The
use of ZCast binder jetting technology has been evaluated to create aluminum
castings by reducing the mold wall thickness from 12mm to 5mm. The crite-
ria were dimensional accuracy and surface roughness and were found to be in
the range of sand casting [31]. Binder jetting technology has been utilized in
combination with sand casting in order to take advantage of the design freedom
provided by AM [32]. The 3D printed molds allow sensors to be embedded.
This facilitates the collection of casting data from deep within molds. Using
binder jetting, sand molds can be made with high compressive strength without
the use of a pattern, which in turn can reduce cost and save on lead time [33].
Though patternless mold making presents a large time savings for RIC, the
powder based AM processes it relies on need improvement. The main benefit
of the patternless process is the ability to better incorporate metrology into
the casting process [13]. It is clear that in order for solidification processes to
benefit from unbounded design they must be coupled with AM.

2.3 Lattice Structures

AM processes have become increasingly relevant in different industries, espe-


cially in SLM of metals [34]. The current most prevalent application of SLM
is manufacturing of lightweight cellular structures. The use of lattice struc-
tures is desirable because AM has allowed for the fabrication of topologies with
12 Chapter 2. Related Work

Figure 2.4: Optimized pillow bracket printed by EOS DMLS.


Reprinted from [4] © 2019, with permission from Elsevier.

great geometrical complexity previously unachievable using traditional fabrica-


tion techniques [35]. Currently the only way to achieve components with very
high specific stiffness or very high specific strength is using geometric meth-
ods like ordered porous lattice structures. Lattice structures can be used in
lightweighting applications. Optimizing SLM manufacturing of lattices allows
for better mechanical properties [36]. Lattice structures can be graded based on
their SLM performance. One such example is a database evaluated by Tang et.
al. [37]. Unlike SLM, an overarching analysis of the use of lattice structures in
RIC is non existent. In some cases RIC could be better for cellular structures,
using SLM, overprinting can be observed in the radius of the lattice truss. The
truss overprinting is unpredictable [38]. This behaviour is less prevalent in RIC
as the AM process is independent of the casting process. This makes the defects
more predictable. This is just one of the few advantages of RIC for manufac-
turing of cellular structures. The two processes both have their pros and cons
and their place in the metallic AM space.
Lattice structures can used to take advantage of the boundless design space
provided by AM. Lattice structures can achieve controllable mechanical prop-
erties. This is done using ordered porous lattice structures [39, 40]. Lattice
structures can even utilize programmable joints which result in lattices with
2.4. Applications of Rapid Investment Casting Lattice 13

both stretch-dominated and bending-dominated behavior [41]. One application


for controllable lattice structures is metallic bone design. The manufactured
orthopaedic implants were found to be highly dependent on lattice geometry
and relative density [42]. Lattice structures can be optimized by varying the
unit cell topology, relative density, and base material. This optimization can be
seen in Fig. 2.4. The authors designed an aero-bracket using a lattice structure
topology optimization and manufactured using different types of AM processes.
Beyond optimizing mechanical performance, lattice structures can be designed
to be self-supporting [43]. Metal additive manufacturing (MAM) of complex
parts with overhangs typically requires the use of sacrificial support structures
to hold the part during the process [44]. The same is true for most AM processes.
Support structures are essential for the good production of parts. Vaissier et al.
presented a genetic-algorithm based framework for lattice support structure op-
timization [45]. Huang et al. utilized topology optimization to generate lattice
support structures for maximizing heat conduction in SLM [46]. Beyond that
lattice structures can be used for energy absorption. The AM of supportless
lattice structures with TPU filaments and material extrusion processes such as
FDM was evaluated for the application of energy absorption [47]. The authors
found that supportless lattice structures inspired by sea urchin shells can im-
prove the overall speed of the AM process for building customized parts. Lattice
structures can be utilized for optimizing the self-supporting, heat conduction,
energy absorption or lightweight performance of components. Although AM
of lattice structures has been heavily researched, there is no existing study on
lattice casting performance.

2.4 Applications of Rapid Investment Casting Lattice

According to Pattnaik et al. [48], IC has been used to manufacture: jewellery,


art and weapons in ancient civilization. Given that IC can create parts with
complex geometries, accurate dimensions and excellent surface finishes, it is no
14 Chapter 2. Related Work

surprise that fields such as: dental, biomedical and aerospace utilize this tech-
nology. Pattnaik et al. [49] stated that IC is superior to other casting practices
and for this reason it can be applied to many applications such as: making au-
tomobile components, aircraft engines, jewelry, statues, prosthetics, computer
hardware, electronics hardware, radar and machine tool components. With the
unbounded design freedom provided by RIC and the isotropic nature of IC it
can be used for many manufacturing applications requiring high accuracy. The
following are some of the recent RIC advancements in the fields of biomedical
engineering, dentistry and aerospace engineering.
IC as of late has showed a lot of promise for the manufacturing of implants
in the biomedical field, given that components are generally individualized.
Beyond that RIC is known for its ability to create complex 3D parts with
excellent surface finishes which lends itself well to create lightweight components
that don’t lack in strength and interface well with the human body. Singh
et al. [50] proposed the use of fused filament fabrication (FFF) for printing
biomedical implants for use in IC. The study was focused on controlling surface
roughness using three factors of the IC process such as slurry layers, slurry
viscosity and dry time of primary layer. The research found that all three
properties affected the surface quality of the cast hip joint and the research
optimized the finish to micro-level resulting in a reduction of post processing
operations. Singh et al. [51] later reviewed all the current research focused on
improving the surface finish of FFF 3D printed patterns through parameter
selection of IC and AM for biomedical implants. FFF is the AM method of
choice for pattern making in the biomedical field due to its ability to create
larger parts. One of the issues that remains to be resolved is the poor surface
finish associated with FFF.
Dentistry has been using IC since 1897, Pattnaik et al. [48] stated that many
dental laboratories employ the lost wax casting process. Given that every den-
tistry partial denture is unique to the anatomy of the patient, IC is perfect for
this application. The conventional IC process has been replaced with RIC and
instead of having crowns fit using molds, the process has been replaced by a
2.4. Applications of Rapid Investment Casting Lattice 15

combination of 3D scanning,computer aided design/computer aided manufac-


turing (CAD/CAM) and RIC. A prime example of the use of IC in dentistry is
Revilla-León and Özcan [52] who reviewed the different AM methods for pro-
cessing the alloys used in dentistry. The authors compared SLM and direct
metal laser sintering (DMLS) with casting. The results were that there are is-
sues regarding accuracy and reproducibility with SLM and DMLS and for that
reason there remains room for improvement in 3D printing metals. Alterna-
tively Dahl et al. [53] investigated if single dental crowns designed using CAD
and CAM would have as good a fit as those made with lost wax IC. Given the
limited number of crowns tested, the authors were forced to reject the hypoth-
esis that crowns made using CAD and CAM were similar to those produced
using the conventional casting method. Given the unique geometry, high ac-
curacy and surface finish requirements associated with dentistry, RIC is the
manufacturing method of choice. The main struggle with the implementation
of RIC in dentistry is the scanning and design aspect of the process rather than
the casting process itself.
RIC can create parts with very little porosity, excellent surface finish and
RIC parts can be used for applications where fatigue strength is critical. For this
reason it is the obvious choice for manufacturing aerospace components. Wu
et al [54] presented a new rapid casting process based on gelcasting and SLA.
The process relies on the addition of an aqueous colloidal silica to the mold
material slurry in order to rapidly cast hollow turbine blades. Given the need
for accurate castings that aren’t prone to creep, RIC is an ideal manufacturing
method for turbine blades that have complex freeform surfaces and complex
internal cooling channels, which can’t be made using many other manufacturing
processes. Wu et al. [55] later presented the use of the aforementioned gel casting
technology for manufacturing turbine blades with film cooling holes. Compared
to cylindrical cooling holes, abnormal cooling holes are more efficient. The
new process was less time consuming and costly which in turn resulted in a
higher production yield. Aguilar et al. [56] evaluated the use of IC to produce
low pressure turbine blades made from intermetallic titanium aluminide alloys.
16 Chapter 2. Related Work

Given these blades are 50 percent lighter than the nickel-based alternative. The
authors were able to qualify this production technology. In aerospace how much
a component weighs is of great importance, being able to create components
with more complex internal geometries instead of using assemblies can lead
to significant weight savings and better performance. It seems that complex
internal structures in aerospace have mostly been made using gelcasting, it
would be interesting to further investigate the use of RIC for this process.
17

Chapter 3

Materials and Methods

This section outlines the parameters and setup used for the theoretical and
experimental tests. The characterization methods and lattice structures used
in the tests are also detailed.

3.1 Materials and Equipment

The AM machine used in this study is the 3D Systems FabPro 1000, a DLP
printer with a resolution of 65 microns in the X and Y directions and 30-50
microns in the Z direction. The material used for this printer is the FabPro
Proto GRY plastic resin. Proto GRY is a prototyping resin manufactured by
3D systems for prototyping. This resin was used due to its great printability
when compared to casting resins. For this material, the Z direction can only
achieve a resolution of 50 microns.
The casting machine used is the Neutec® J-2R™, and the flask is the 4” di-
ameter and 6” tall Neutec® SuperPerf™ flanged flask. A high strength plaster
– the Ransom and Randolph Ultra-Vest Maxx – is used as the mold material.
The plaster is prepared with the CIMO St. Louis 92 - 4KG digital vacuum
investment mixer. Heating of the mold is done in the Lucifer L17-K12 Furnace.
Two casting materials are used in the experiments. One is the recycled 70-30
brass with a density of 8.73 × 103 g/mm3 , and the other one is the recycled 6061
aluminum with a density of 2.7 × 103 g/mm3 . The DenPlus Basic Eco Sand-
blaster is applied in post-processing, and the glass beads used in sandblasting
have a size of 50 microns.
18 Chapter 3. Materials and Methods

Samples are cut using a fret saw to perform grain structure analysis on
the casts. Next, they get mounted in Bakelite using the Bueller SimpliMet
3000 compression press. The samples get lapped using 300, 400, 600, 800, and
1200 grit sandpapers. The samples get mirror-polished using alumina powder.
Finally, they are etched using 200ml distilled water, 10gm Ferric chloride, and
50ml Hydrochloric acid. The void and grain structure analyses are done using
the Keyence VHX-6000 microscope.

3.2 Manufacturing Process

The overall RIC process is illustrated in Fig. 3.1, and the necessary details are
given in the following.
a) b) c) d)

Pattern
Furnace
Build Platform Pattern Tree
Flask Mold
Pattern
Mold Base

Resin Tank

LCD Screen Flask Mold Recycled


Metal

UV Led Bulb Scale

e) f)

Figure 3.1: RIC process: a) DLP additive manufacturing. b) Pattern


spruing. c) Plaster mold making. d) Pattern burnout. e) Vacuum
casting. f) Post processing.

3.2.1 Pattern Making

A pattern has the shape of the object to be cast, so the computer-aided model
(CAD) model is used to make the pattern. In RIC, the pattern is produced by
3.2. Manufacturing Process 19

an AM machine, in this work the DLP printer is used (see Fig. 3.1(a)). After
slicing the CAD model, DLP produces the pattern by using a projector to cure
(solidify) complete layers of liquid resin at a time. The build head lowers into the
resin tank, leaving one layer thickness between the head transparent and tank.
The projector then exposes a mask of UV light through the transparent bottom
of the tank. This mask is the two-dimensional (2D) profile of the current layer.
After the layer curing, the tank tilts to detach the print from the build plate
before moving up a layer thickness. This process repeats until the completion
of the full 3D part. The main benefit of DLP is that it can create very high-
quality patterns with great surface finishes [57]. Alternate AM processes that
can be used for pattern making are MJM, SLA, and FFF see Fig. 1.1. DLP can
achieve more complex overhangs using less supports thanks to it curing layer-
by-layer instead of point-by-point and thus having better self-support capability
of the material. Also, it is a lot faster than MJM and SLA while achieving a
comparable resolution. FFF does not produce high enough quality parts for
making delicate lattice structure patterns.
The same manufacturer offers a casting resin. The benefit of casting resin
is that it creates less stress and ash in the mold during burnout. However,
the casting resin was not rigid enough and did not print well. It also printed
a lot slower than the prototyping resin, i.e., four times slower. Although the
prototyping resin requires a higher temperature to be burnt out, it has sig-
nificantly better printability, which was important as all the lattice topologies
tested needed to be self-supporting to ensure there was no need for internal
support removal.

3.2.2 Mold Making and Burnout

The printed pattern gets placed on a mold base and a steel flask is placed on
top of the mold base. The perforated flask is then covered in masking tape to
avoid spilling the plaster, see Fig. 3.1(b). The plaster then gets weighed based
on the manufacturer’s specifications and the volume of the flask and pattern.
The plaster is placed in the mixer, and vacuum is pulled. Water is then added
20 Chapter 3. Materials and Methods

PROTOTYPING RESIN BURNOUT PROFILE


1600
1400
1200

TEMPERATURE (°F)
1000
800
600
400
200
0
0 2 4 6 8 10 12
TIME (H)

Figure 3.2: 3D Systems FabPro 1000 prototyping resin burnout pro-


file

to the mixer based on the manufacturer’s specifications, and the plaster gets
hydrated 38%. The mixer then mixes the plaster for 7 minutes, at which point
a knob is pulled to pour the plaster into the mold. Finally, the mold is vibrated
to remove any bubbles from the plaster for another 7 minutes, see Fig. 3.1(c).
The mold then gets removed from the mixer and is left for 10 minutes to dry.
The mold containing the resin pattern then gets burnt out (Fig. 3.1(d)) with
the custom burnout profile in Fig. 3.2.

3.2.3 Casting

For the casting experiment, the casting machine gets preheated to 1038◦ C, and
the mold gets preheated to 5388◦ C. 150% weight of 70-30 brass was weighed
and added to the casting machine’s crucible for melting. The brass weight is
calculated based on the density of 70-30 brass and the pattern volume. The
reason of 150% mass was chosen is to ensure that there is an excess of metal,
eliminating the lack of molten metal as a cause for casting defects. The recy-
cled brass was melted down in the casting machine using argon shielding with
a flow of 8L/min. Once the casting machine hit the melting temperature of
1038◦ C, the recycled 70-30 brass was added to the machine, causing the ma-
chine’s temperature to drop a few hundred ◦ C. Once the temperature rose back
to 1038◦ C and the metal was molten, the flask was introduced to the flask cham-
ber. Vacuum was then pulled for the flask chamber before pulling the lever that
3.3. Lattice Designs 21

introduces the molten metal to the mold, see Fig. 3.1(e). The mold was then
left under vacuum for 4 minutes to remove dissolved gases and fill the mold.
After 4 minutes, the vacuum pump was turned off, and the mold was left to cool
in the casting machine for 10 minutes. After 10 minutes the mold was removed
from the machine and left to air cool. The cooling temperatures and times are
optimal based on prior testing; these temperatures and time caused the least
defects and stress cracking. Finally, once the mold had cooled to 200◦ C, the
mold was quenched in a bucket of room temperature water.
For casting experiments involving 6061 aluminum, the whole process is ba-
sically the same. The only difference is that the casting machine preheat tem-
perature is 649◦ C, and the mold preheat temperature is 315◦ C.

3.2.4 Post-processing

The majority of the plaster dissolves away from the quenching process. After
quenching, the remaining plaster caught in small details gets sandblasted at 90
Psi, see Fig. 3.1(f). This removes minimal amounts of material without affecting
geometric accuracy. Once all the plaster is removed from the sample, the feeder
gets removed using a fret saw.

3.3 Lattice Designs

To test the casting performance of lattice structures, two sets of experiments


with different designs are conducted. Two materials are used for the experiments
as well to make sure it is the design rather than the material affecting the
performance.

3.3.1 Set 1

In the first experiment, the set of lattice topologies includes rhombic, kelvin,
cubic, and octet-truss, as shown in Fig. 3.3(a-d). These topologies were chosen
as they are commonly used structures in AM, and they vary a lot in topology
while remaining open celled and self-supporting. Each lattice unit cell is a
22 Chapter 3. Materials and Methods

a) Z
e)
n7.00mm

2 Units
(20mm)

7.00mm

b)
2.50mm 2.00mm
5.00mm

6 Units
(60mm)
c)

2 Units
(20mm)

d)

Figure 3.3: Test 1 lattice cells and structure: a) Rhombic. b) kelvin.


c) Cubic. d) Octet-Truss. e) 2 × 2 × 6 structure.

10 × 10 × 10 mm cube, and the green arrow on the wireframe cells is the Z-axis,
which is the filling direction. Their connectivity are shown in order to better
understand how they connect in 3D. All the topologies have a straight circular
strut cross-section and a cubic packing strategy. The scope of topologies was
narrowed in order to limit the amount of possible topologies. All four topologies
have a constant volume and the strut size is changed to achieve this. The density
of the unit cells is kept constant at 20%. The strut size needed to achieve
a density of 20% for different lattice topologies were obtained through trial
and error using Autodesk Inventor. The strut sizes for these topologies range
from 1.3732 mm to 1.98020 mm. To better grade their filling performance and
proneness to casting defects, the structures to be cast contain 2×2×6 unit cells
as shown in Fig. 3.3(e), and they were all fed via a 7 mm cylindrical feeder.
3.3. Lattice Designs 23

3.3.2 Set 2

For the second experiment, the main goal is to use the first experiment’s ob-
servations to create lattice topologies more optimized for casting performance.
Rhombic and octet-truss are being passed along from the previous experiment
to serve as benchmarks compared to other publications and the previous experi-
ment. Along with those two topologies, two more have been proposed. The four
unit cells are rhombic, octet-truss, proposed cell, and hourglass. The structures,
as well as their overall dimensions and orientation, can be seen in Fig. 3.4. The
hourglass structure has a balance of vertical, horizontal, and 45◦ struts. This
structure is used to evaluate further the effect of strut angle distribution on
casting performance. The second proposed structure is one that was created
purely for good casting performance. It has a low number of joints, low joint
valence; most of its struts are 45◦ , and it has a large relative strut size. The
hypothesis is that this combination of properties will lead to a better casting
performance.
The unit cell size for this experiment is 5 × 5 × 5 mm. This was chosen
to observe more casting defects without exceeding the dimensions of the flask.
In addition, the casting material was changed to 6061 aluminum. Due to the
higher solidification shrinkage of aluminum compared to the brass, set 2 is a
more challenging test beyond the geometry setting. This too will contribute to
the ability to observe more casting defects to better grade the lattice topologies.
The strut sizes for these samples ranged from 0.7 mm to 1.2 mm. This finer strut
size will increase the likelihood of premature melt solidification which will more
significantly differentiate the different topologies’ performance. The structures
to be cast contain 2 × 2 × 6 unit cells as shown in Fig. 3.4(e) In order to feed
the larger number of unit cells; the feeder size is being increased to 12 mm,
which tapers from 15 mm. The 15 mm diameter was chosen to interface with
the sprue base for the mold.
24 Chapter 3. Materials and Methods

a) Z
e)

5 Units
(25mm)

b) n 15.00mm

1.50mm
4.00mm

n 12.00mm

20.00mm

7.0mm
2.00mm

c) 1.00mm

5 Units
(25mm)

5 Units
(25mm)

d)

Figure 3.4: Test 2 lattice cells and structure: a) Proposed cell. b)


Hourglass. c) Rhombic. d) Octet-Truss. e) 5 × 5 × 5 structure.

3.4 Characterization

Analyses and characterizations based on both computer-aided engineering and


physical experiments are conducted. They are detailed here.

3.4.1 Mold Flow Simulation

Mold flow simulations on various lattice structures were performed to grade


the structures based on their casting performance. These simulations were
performed in Altair Inspire Cast. The simulations were not used as exact rep-
resentations of the different lattice structures’ mold flow but were used as a
comparison tool to see which samples performed better based on the follow-
ing criteria: filling time, porosity, and cold shuts. Cold shuts refers to when
multiple joining metal flows cool before properly fusing together.
3.4. Characterization 25

The lattice structure geometry for the mold flow simulations is the same as
the one to be cast in Fig. 3.3(e). Since the complexity of the second experi-
mental structures was increased based on the results of the first. They were too
complicated to simulate on a standard PC, and thus, this simulation was not
conducted.
The mold flow simulation was performed using the parameters listed in Ta-
ble 3.1. The simulation was a gravity process with the fill parameter set as
a constant liquid level on the sprue. The casting method is IC, and a shell
mold was chosen to simplify the simulation. The shell thickness of 50 mm is
quite large and comparable to the casting experiments’ flask mold. The 7 mm
cylindrical feeder fed the molten metal as in Fig. 3.3(e). The elements utilized
by the mold flow simulations are tetrahedral, and the software chose their size.
Table 3.1: Mold flow Altair Inspire Cast 2019.3 material properties

Property Value Unit


Material CW502L Brass N/A
Molding Material Plaster N/A
Melting Temp. 1093 ◦C

Preheat Temp. 538 ◦C

Shell Mold Thickness 50 mm

3.4.2 Mechanical Finite Element Analysis

Mechanical simulations were performed using Ansys Workbench 19.2. The ma-
terial properties used for the simulations were 70-30 brass found in Table 3.2.
Two static structural, mechanical simulations were performed per lattice sam-
ple: tension/compression and shear. Bending was omitted because if a lattice
topology performed well under tension and compression, it also performed well
under bending since bending is a combination of the two [58]. For the lattice
topologies observed, the focus was lightweight, rigid topologies. Therefore the
topologies were only loaded right up till the onset of plastic deformation. The
results were only used to determine the equivalent tensile and shear modulus.
Given that the only deformation observed was plastic and this Ansys simulation
26 Chapter 3. Materials and Methods

Tensile Loading Shear Loading


Z
X Y
a) b)
d)

f)

g)

c) e)
Figure 3.5: Loading conditions tensile: a) Displacement b) Force c)
Fixed support. Loading conditions shear: d) Force e) Fixed support
f) Displacement g) Displacement

did not take into account struts colliding with each other, the compressive simu-
lations were the same as the tensile simulations, so they are not reported. Also,
two large blocks of material were added to both ends of the lattice structure to
ensure the loads are applied uniformly to the structure. For tensile loading, a
force was applied to the top face 15 kN at a time. A fixed support was added
to the bottom face, which restricts movement in every direction. Finally, a dis-
placement constraint was added to the top face that only allows displacement
in the direction of the applied load. For shear loading, a force was applied to
the front face 15 kN at a time. A fixed support was also added to the bot-
tom face, which restricts movement in every direction. Finally, a displacement
constraint was added to both inner faces that only allowed displacement in the
applied loading direction. The geometry for the mechanical tests was simplified
as shown in Fig. 3.5, this was done to save on computation time. The purpose
of the simulations was not to determine the exact deformation or maximum
principal stress in the structures but rather to serve as a comparison tool for
the different topologies to establish which ones have good cast-ability without
sacrificing mechanical performance. The loading conditions and fixed supports
3.4. Characterization 27

as well as the geometry utilized for the simulation, can be seen in Fig. 3.5. The
observed results for mechanical performance are the max deformation in the
applied load direction and the max principal stress. From these results, stress-
strain graphs can be generated, and the resultant modulus for tensile and shear
of the structure can be determined. These moduli will be used to compare the
mechanical performance of the different lattice topologies.
Table 3.2: Ansys 70/30 [Cu/Zn] brass material properties

Property Value Unit


Density 8530 kg / m3
Young’s Modulus 10E+10 Pa
Poisson’s Ratio .331 Pa
Bulk Modulus 8.08678E+10 Pa
Shear Modulus 3.080390E+10 Pa

3.4.3 Microscopic Analysis

A scaled-up lattice structure of the best performing lattice topology will be


3D printed, molded, and cast. The sample will then be cut into three smaller
samples. The first sample will represent a joint of valence 2, the second one
of four valence, and the last one six valence. Two sets of these six samples
will be prepared. The samples will then be mounted in Bakelite, and their
surfaces polished. The brass samples can then be etched and observed under
the microscope for voids and grain structure analysis. Using the microscopic
analysis images, each sample’s void ratio can be determined, and the grain
structure can be analyzed. The result should be an understanding of the effect
that a lattice structure’s joint valence has on the porosity and grain structure.
The prediction is that that porosity will increase with joint valence. The struts
will most likely exhibit a similar grain structure as most cast samples with a
visible chill zone, columnar zone, and equiaxed zone.
28

Chapter 4

Results

4.1 Mold Flow

a) Filling Time b) Porosity c) Cold Shuts


Rhombic Kelvin Cell Rhombic Kelvin Cell Rhombic Kelvin Cell

Figure 4.1: Flow simulation results for rhombic and kelvin

The results of the mold flow simulation can be seen in Fig. 4.1. The 3D
plots of only the rhombic and kelvin structures are presented because both the
cubic and octet-truss samples solidified before filling according to the simula-
tion, so their results were not plotted. The three observed casting properties
that showed the largest deviation across the lattice topologies were filling time,
porosity, and cold shuts. Firstly, from the comparison of filling time, it can be
seen that the rhombic structure fills fastest, and the filling time does not differ
much in the x and y direction, only in the filling direction. Secondly, a porosity
of 20% was chosen to be unacceptable and highlighted. The kelvin structure
has repeatable porosity located at the horizontal struts (90◦ from filling direc-
tion). The rhombic structure shows almost no porosity of 20% in the body, but
just at the top. This could be caused by the highly directional filling, which
4.2. Cast 1 29

would cause the feeder to solidify last. Finally, cold shuts were observed. The
magnitude of cold shuts in the kelvin sample is higher than that of the rhombic
sample. Cold shut locations for these two structures were consistently located
on horizontal struts (90◦ from filling direction).

4.2 Cast 1

a) b) c) d)

Figure 4.2: Printed Patterns Experiment 1 a) Rhombic b) kelvin c)


Cubic d) Octet-Truss

20.23mm

a) b) c) d)
Figure 4.3: Set 1 cast structures: a) Rhombic, b) Kelvin, c) Cubic,
and d) Octet-Truss.
30 Chapter 4. Results

Table 4.1: Lattice topology comparison casting experiment 1

Rhombic
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 47.162 20.00 1.980
Printed N/A 20.23 2.013
Cast 49.000 20.19 2.077
% Fill 103.90
Kelvin
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 47.163 20.00 1.976
Printed N/A 20.21 2.090
Cast 45.840 20.15 2.047
% Fill 97.19
Cubic
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 47.142 20.00 1.629
Printed N/A 20.20 1.723
Cast 40.350 20.15 1.693
% Fill 85.59
Octet-Truss
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 47.163 20.00 1.373
Printed N/A 20.08 1.447
Cast 38.500 20.11 1.417
% Fill 81.63

Following the presented manufacturing pipeline, all the lattice structures


were successfully printed without supports, molded, and cast see Fig 4.2. Through
visual inspection, the location and severity of casting defects can be observed.
The octet truss and cubic structures did not fill, contrarily the rhombic and
kelvin did. The kelvin has consistent defects on its horizontal struts (90◦ from
filling direction) this was also visible in castings from other publications [59].
The rhombic structure also has defects on a few horizontal and diagonal struts,
but this was not a consistent defect. Furthermore, the weights and dimensions
of the CAD models, casts, and printed patterns are listed in Table 4.1. The
measurements were taken using a caliper at three points on the structure’s width
and the struts. These three measurements get averaged, and they were taken
randomly on the sample. For the width, any unfilled portions were avoided to
make the measurements more accurate. Let it be noted that all the printed
4.3. Cast 2 31

lattice structures were around 1% larger in structure width than the CAD ge-
ometries. The biggest contributor to the inaccuracy in size seems to be caused
by the 3D printing process, but this could be accounted for and corrected in the
CAD models or the printer software. Because some samples are more filled than
others, the measurements may not be a perfect representation as the unfilled
samples will have a more significant variation in dimensions. The percent fill
was calculated by comparing the cast part’s mass from the CAD model to what
it is. The percentage fill is based on the weight of the cast samples with the
feeder removed compared to the CAD model’s weight. According to the per-
cent fill, the rhombic structure filled the most, followed by the kelvin, cubic and
octet-truss. The percentage fill and visual inspection are in agreement. Overall
the rhombic structure has the best casting performance. The structure seems
to have flowed well based on the number of defects. The casting performance
from best to worst was rhombic,

4.3 Cast 2

a) b) c) d)
Figure 4.4: Printed Patterns Experiment 2: a) Proposed cell b)
Hourglass c) Rhombic d) Octet-truss

All the four lattice structures in the second set are also successfully printed
without supports, molded, and cast, as shown in Fig. 4.4 and Fig. 4.5. There
was no significant variation in the samples’ weight (see table 4.1). According
to the percent fill, although the difference of the top-three was low, the most
successful structure was the hourglass proceeded by the proposed cell, rhombic,
32 Chapter 4. Results

25.02mm

a) b) c) d)
Figure 4.5: Set 2 cast structures: a) Proposed cell, b) Hourglass, c)
Rhombic, and d) Octet-Truss.

and finally the octet-truss. However, from visual inspection, it is clear that
the proposed cell structure showed the fewest visible defects, followed by the
hourglass, rhombic, and finally octet-truss. The proposed cell sample only had
one visibly unfilled strut. The hourglass sample had many visible defects present
in its vertical (0◦ struts) as well as its joints among the vertical (0◦ ), horizontal
(90◦ ) and diagonal (45◦ ) struts. The rhombic structure had many defects similar
to the first casting experiment with voids at the perpendicular (90◦ ) struts and
the high joint valence joints. Finally, the octet truss sample did not fill. From
these results, it can be seen that the two new structures designed based on the
observation from experiment 1 are indeed better.

4.4 Mechanical Properties

The tensile stress vs. strain for elastic deformation can be seen in Fig. 4.6. From
the graph, it can be seen that under tensile loading, the hourglass, proposed
cell and cubic samples performed the best. These three topologies had the
highest resultant tensile modulus see Table 4.3. The resultant modulus of the
structures describes the structures’ rigidity under different loading conditions.
The rigidity of the structures under tensile loading from highest to lowest is
cubic, hourglass, proposed cell, rhombic, kelvin, and octet-truss. Similarly, the
line’s slope for shear stress against strain tells how much deformation occurs
for a given applied shear load. The resultant shear modulus of the structures
can be seen in Table 4.3. The structure’s rigidity under shear loading from
4.4. Mechanical Properties 33

Table 4.2: Lattice topology comparison casting experiment 2

Hourglass
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 12.005 25.00 1.022
Printed N/A 25.19 1.013
Cast 13.030 25.01 1.157
% Fill 108.54
Proposed Cell
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 12.004 25.00 1.111
Printed N/A 25.02 1.147
Cast 12.750 24.93 1.113
% Fill 106.21
Rhombic
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 12.005 25.00 0.989
Printed N/A 25.180 1.028
Cast 12.540 24.86 1.003
% Fill 104.46
Octet-Truss
Mass (g) Cell Width (mm) Strut Diameter (mm)
CAD 12.005 25.00 0.686
Printed N/A 25.10 0.743
Cast 11.740 20.080 1.447
% Fill 97.79

highest to lowest is hourglass, proposed cell, octet-truss, rhombic, kelvin, and


cubic. In terms of overall mechanical performance for shear and tensile, the
hourglass structure performed the best closely followed by the proposed cell.
The rhombic structure was the only other structure that performed well for
both loading conditions. None of the other structures performed well for both
loading conditions.
Table 4.3: Resultant modulus for simulated Ansys lattice structures.
Eeq is the Equivalent Tensile Modulus and Geq is the Equivalent Shear
Modulus

Topology Eeq (Mpa) Geq (Mpa)


Rhombic 14528 3387.3
kelvin 12849 2005.9
Cubic 24941 1214.8
Octet-Truss 11710 3478.2
Proposed Cell 23501 3978.4
Hourglass 24847 36225.0
34 Chapter 4. Results

Tensile Stress vs. Strain Casting Samples


Stress From Applied Load (Mpa) Stress From Applied Load (Mpa) 3000 Rhombic Kelvin Octet Truss

2500 Cubic Hourglass Proposed Cell

2000

1500

1000

500

0
0 0.05 0.1 0.15 0.2 0.25

Strain From Deformation


Shear Stress vs. Strain Casting
400 Hourglass Proposed Cell Octet Truss Kelvin Cubic

350

300 Rhombic

250

200

150

100

50

0
0 0.05 0.1 0.15 0.2 0.25 0.3 0.35

Strain From Deformation


Figure 4.6: FEA results

4.5 Voids and Grain Structures

The proposed cell structure is cut on a plane containing 2-valence, 4-valence,


and 6-valence joints. The results of the microscopic analysis can be broken
down into two parts. The first is the analysis of resultant grain structure,
and the second is the analysis of porosity in the cast samples. The resultant
grain structure for the 2-valence, 4-valence, and 6-valence joints can be seen
in Fig 4.8. The 2-valence and 4-valence joints both show clear indications of a
chill, columnar, and equiaxed zone. The 6-valence joint seems to lack a fully
formed equiaxed zone. This is most likely due to the cooling rate of this joint.
4.5. Voids and Grain Structures 35

Table 4.4: Void properties. All area are in µm2

Property 2-Valence 4-Valence 6-Valence


Sum of void area 28946 199025 786608
Max void area 1555 129721 82656
Min void area 20 20 20
Total void # 154 326 1209
Total strut area 13579304 13729209 23476110
Void ratio (%) 0.21 1.45 3.35

Table 4.5: Lattice topology strut size and joint characteristics. Strut
size is in mm.

Property Proposed Hourglass Rhombic Cubic Kelvin Octet-Truss


Rel. Strut Size 0.22 0.20 0.20 0.16 0.20 0.14
Number of Joints 9 9 9 27 24 14
Max Joint Valence 6 6 8 6 4 16
Min Joint Valence 4 4 8 6 4 16
Mean Joint Valence 4.58 5.74 8 6 4 16

The grain area distribution was not determinable due to voids limiting the
ability for software to determine the grain boundaries. The porosity results can
be seen in Fig. 4.8, which shows the microscopic images at 50x magnification
without having etched the sample. The area and frequency of each void were
tabulated. The results for void ratio, number of voids, and max/min void area
are summarized in Table 4.4. A clear trend from the results can be observed.
With the increase in the joint valence, a higher void ratio is observed. The void
ratio increases from 0.21% in the 2-valence joint to 1.45% in the 4-valence joint
and finally to 3.35% in the 6-valence joint. The void ratio is based on the sum
of the void area, so the void area shows the same trend. The number of defects
also increases with the increase in joint valence. The only outlier in terms of
behavior is the max void size. The max is higher for the 4-valence joint than
the 6-valence joint. The large defect in the 4-valence joint is quite close to the
strut’s surface and could be a surface defect when looking at the structure as a
whole. Regardless of this outlier, the overall void ratio still ends up being lower
than the 6-valence one. These results show that the higher the valence number,
the worse the casting performance.
36 Chapter 4. Results

Sample 1: Sample 2:
a) 2-Valence Joint

1000μm
Outer Edge of casting

b) 4-Valence Joint

Equiaxed Zone Columnar Zone Chill Zone

c) 6-Valence Joint

Figure 4.7: Microscopic analysis for grain structure. Images 50×


magnification
4.5. Voids and Grain Structures 37

2-Valence Joint Void

40
Frequency

30
20
1000μm
10
0

82656
1100
1500
1900
130
190
250
300
700
10
70

More
Void Area (μm²)

4-Valence Joint Void

80
Frequency

60
40
20
0
82656
1100
1500
1900
130
190
250
300
700
10
70

More

Void Area (μm²)

6-Valence Joint Void

200
Frequency

150
100
50
0
82656
1100
1500
1900
130
190
250
300
700
10
70

More

Void Area (μm²)

Figure 4.8: Microscopic analysis for porosity. Images 50× magnifi-


cation
38

Chapter 5

Discussion

In terms of geometric accuracy, the printed lattice structures were larger in


structure width than the CAD geometries, see table 4.1, and table 4.2. Some
shrinkage was also observed in the cast part when compared to the printed
pattern but this was less significant of a size change than the CAD geometry
to the printed pattern. Overall the biggest contributor to the inaccuracy in
final cast size seems to be caused by the 3D printing process but this could be
accounted for and corrected in the 3D models or the printer software due to it
being consistent.
From all the results, mold flow, the two casting experiments, and the FEA,
The factors that significantly affect casting performance have been narrowed
down. The properties that play a role in the success of the cast lattice topolo-
gies are: relative strut size, number of joints, joint valence, and strut angle
distribution. The casting experiments’ results and the overall performance of
each lattice topology can be explained using these properties. The above prop-
erties are listed in Table. 4.5 for each lattice topology tested. Strut length is
the distance traveled by the metal flow in the lattice cell. Strut length can be
measured for different strut angles and divided by the total to determine the
strut angle distribution (see Fig. 5.1).
When analysing the casting and mold flow results, the effect of relative strut
size can be seen most significantly in the cubic and octet-truss topolgies. The
two structures have lower relative strut sizes of 0.16 and 0.14 when compared
to the more successful proposed cell and hourglass topologies (0.20-0.22) (see
Chapter 5. Discussion 39

Table 4.5). Lower relative strut sizes result in slower filling times which often
results in premature melt solidification. Therefore, it is clear that the relative
strut size plays the largest role in the success of a lattice structure casting. This
ratio gives a idea of the negative effect that adding more struts for rigidity has
on the strut size and in turn the metal flow. From this the structures that
create an efficient short path for the metal to flow through can be determined.

Rhombic
90.00
Cubic
80.00
Kelvin Cell
70.00
% Total Strut Lenght

Octet-Truss
60.00
Proposed Cell
50.00
Hourglass
40.00
30.00
20.00
10.00
0.00
0° (Vertical) 35°-55° (Diagonal) 90° (Horizontal)
Absolute Value of Strut Angle from Filling Direction
Figure 5.1: Topology strut angle distribution

Next in the level of importance is the number of joints. From the mold
flow and experimental castings, it is clear that the topologies with the highest
number of joints performed very poorly. The effect can be seen in the cubic
(27), kelvin (24) and octet-truss (14) topologies. The remaining three topologies
with a joint number of 9 all performed well. To add a level of granularity to
the analysis, these three topologies can be further classified based on their joint
valence. The proposed cell structure performed better than the other two due
to its low joint valence (4.58), this trend continues for the hourglass (5.74) and
then the rhombic (8). This behaviour can be further supported by the void
analysis results. A higher void ratio can be observed as the joint valence is
increased from 2 to 4 to 6. In the 2-valence and 4-valence joints, fully formed
equiaxed zones can be seen unlike the 6-valence joint. Equiaxed grains are more
40 Chapter 5. Discussion

desirable as they exhibit better mechanical performance. The presence of the


chill, columnar, and equiaxed zones are typical of cast or extruded parts due to
the way they cool from the outside inward.
Finally, the effect of strut angle can definitely be seen in the casting results
and the mold flow results, with defects often occurring at vertical or horizontal
struts. Regardless, strut angle seems to have the smallest effect on the per-
formance. The hourglass topology illustrates this as it was the second most
performant but it has a balance of vertical, diagonal, and horizontal struts.
This topology would have performed worse due to its horizontal and vertical
struts if strut angle had more of an impact on the performance. From the FEA
results, the presence of horizontal, diagonal, and vertical struts is important for
mechanical strength under tensile and shear. Some of the structures were tested
by Després et al. [58]. The authors observed similar behaviour as was observed
in our FEA results. The diagonal struts contribute to the shear performance
whereas the vertical struts contribute to the bending, tension and compression
performance.
Overall looking at a balance of casting performance and mechanical strength,
optimizing for relative strut size, number of joints, and joint valence seem to
be the best way to avoid negatively affecting mechanical performance while im-
proving casting performance. Mechanical performance can be achieved through
strut angle distribution.

5.1 Design Guidelines

In order to better establish and understand the design guidelines for RIC, the
performance grading of all the topologies can be seen in Table 5.1. The topolo-
gies are graded from 1 to 4 with 4 being the best and 1 being the worst perfor-
mance. This table also includes the tensile and shear performance for reference.
The topological properties are listed in decreasing order of casting perfor-
mance from left to right. The two topologies (proposed cell and hourglass)
performed the best experimentally, as shown from the table. They scored 3 and
5.1. Design Guidelines 41

Table 5.1: Lattice topology performance grading (from 1 to 4.)

Property Proposed Hourglass Rhombic Kelvin Cubic Octet-Truss


Rel. Strut Size 4 4 3 3 2 1
Number of Joints 4 4 4 1 1 2
Joint Valence 3 3 3 4 3 1
Strut Angle Dist. 4 3 3 3 2 3
Tensile/Compressive 4 4 3 3 4 2
Shear 4 4 4 2 1 4

4 across the board and scored 4 in the most important categories (relative strut
size, number of joints, and joint valence). The mechanical performance was not
sacrificed due to the angle distribution, which includes vertical, horizontal, and
diagonal struts [58].
The number of joints and joint valence also affect mechanical strength. This
effect was observed in the FEA results and is supported by Li et al. [60].
The authors stated that lattice cells’ deformation mode changes from bending-
dominated to stretch-dominated with the increase of the joint valence. Stretch
dominated is the more rigid of the two behaviors. Although, rigidity can be
achieved without a high number of joints and joint valence, as Maxwell’s crite-
rion of rigidity is limited as demonstrated by Chen et al. [61]: if finite element
analysis shows a rigid lattice, then the net lattice is rigid.
The design guidelines in order of importance are as follows. The relative
strut size should be kept below 0.20. The number of joints should be kept
below 9. The max and mean joint valence of 8 or less is recommended. Finally,
for mechanical performance, the strut angle distribution should include vertical,
diagonal, and horizontal struts. The following minimum conditions must be met
for faithful use of the design guidelines.

• The lattice must be open celled, circular cross-sectioned, straight strut


topologies with a cubic packing strategy.

• The lattice unit cell must range from 20 mm3 to 1000 mm3 and the strut
size should range approximately from 1 mm to 5 mm.

• Lattice topologies should be oriented with the filling direction as demon-


strated throughout the work.
42 Chapter 5. Discussion

• The materials cast should be similar in fluidity and solidification shrinkage


to 70-30 brass or 6061 aluminum.

• The materials must be cast using some sort of assisted method such as
vacuum or centrifugal with some sort of inert shielding gas.

• The pattern must be 3D printed using a resin or wax based process with
a resolution of at least 100 µm in x, y and z.

By far from what has been tested, the proposed cell, hourglass and rhombic
topologies meets all these criteria and achieve good casting and mechanical
performance.
43

Chapter 6

Conclusion

In summary, it is clear that, much like other metallic AM processes, RIC can
take full advantage of AM’s unprecedented design freedom. RIC was success-
fully used to create a variety of lattice structures. These structures were utilized
to determine the topological lattice properties critical to casting performance.
From those results, a methodology to study the performance of RIC lattice
structures has been established. In this methodology, topological properties are
compared and analyzed using the test results. This analysis results in a set of
design guidelines for RIC. The properties established to affect casting perfor-
mance in descending importance are relative strut size, number of joints, joint
valence, and strut angle distribution. These properties differ slightly but rely
on the same logic as the design guidelines for casting. Feed paths and flow ve-
locity/connectivity play a large role in design for casting. Without controlling
these properties, hot spots, porosity and premature solidification can occur. All
four proposed topological lattice properties directly affect a lattice’s feed paths
and flow velocity/connectivity. The design guidelines developed throughout
this work differ in that they are specifically tailored towards optimizing cellular
structures. Cellular structures by nature have a high potential for flow restric-
tion or high connectivity. For this reason the design guidelines need to be more
targeted than the general casting ones. The properties deemed to have the most
significant effect on tensile and shear mechanical performance are strut angle
distribution, number of joints, and joint valence. With the design methodology,
44 Chapter 6. Conclusion

the proposed cell and hourglass topologies were created. These lattice topolo-
gies had the best overall casting and mechanical performance of all the tested
lattices. The limitations of the current work include testing only strut-based
lattice topologies. Future work could expand beyond this. Future work could
also further refine the design methodology and automate the design process
using software-driven methods.
45

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