Brazilian Test Journal
Brazilian Test Journal
Brazilian Test Journal
a r t i c l e i n f o a b s t r a c t
Article history: The experimental study in this paper focuses on the effects of the layer orientation and sample shape on
Received 3 July 2012 failure strength and fracture pattern of samples tested under Brazilian test conditions (i.e. diametrical
Received in revised form 6 November 2012 loading of cylindrical discs) for one particular layered sandstone which is from Modave in the south of
Accepted 2 January 2013
Belgium. The variations of the strength in combination with the failure patterns are examined as a function
of the inclination angle between the layer plane and the loading direction. The experimental, results clearly
Keywords:
show that the induced fracture patterns are a combination of tensile and/or shear fractures. In shape effect
Layered sandstone
experiments the layer thickness and the number of layer boundaries are investigated. Different blocks
Brazilian test
Fracture pattern
of Modave sandstone are used to prepare samples. The layer thickness is different among the various
Layer activation blocks, but the layer thickness in each studied rock block can be considered to be constant; hence, the
Shape effect number of layer boundaries changes according to the sample diameter for samples of the same block. The
experimental study shows that the layer thickness plays a more important role than the number of layer
boundaries per sample.
© 2013 Institute of Rock and Soil Mechanics, Chinese Academy of Sciences. Production and hosting by
Elsevier B.V. All rights reserved.
1. Introduction Experimental methods are the most important and reliable way
to study rock properties and rock failure mechanisms. The failure
The knowledge of the anisotropic properties of rock material mechanism of rock materials due to their mineralogical texture is
is required in the fields of civil, mining, geoenvironmental and complex and it is more problematic for anisotropic rock.
petroleum engineering, as in general, rock material near the earth’s In rock mechanics, the uniaxial (unconfined) compressive
surface is anisotropic. Material properties of anisotropic rock are strength (UCS) test and Brazilian tensile strength (BTS) test are
directionally dependent, as opposed to isotropic rock that implies the most widely used methods to obtain rock strength properties.
identical properties in all directions. An additional characteristic of Change in rock strength properties (e.g. UCS and BTS) with sample
rock material is the large spatial variation of its properties, even at size is referred to as scale effect. In this context, the so-called scale
small distance, which makes a rock mechanical study even more effect is divided into two categories: size effect and shape effect
difficult. More and more this anisotropy is taken into account when (Thuro et al., 2001; Pan et al., 2009). The size effect can be stud-
testing the rock material, as input for design and for numerical ied by comparing the rock strength values from specimens with
modelling. The engineering applications without considering the the same shape but different sizes (the same length/diameter ratio
rock anisotropic behaviour produce errors of different magnitudes, but with different diameters). The shape effect can be studied by
depending on the extent of rock anisotropy (Amadei, 1996; Cho comparing the rock strength values from specimens with the same
et al., 2012). diameter (or length) but a variation in length/diameter ratio (see
further, Thuro et al., 2001; Pan et al., 2009).
In this study, the focus is on stratified rock material as one spe-
cific form of anisotropy that is often present in geological material.
∗ Corresponding author. Tel.: +32 16321171. Transverse isotropy (as a form of anisotropy) is a characteristic
E-mail address: [email protected] (A. Tavallali). of intact foliated metamorphic rocks (slates, gneisses, phyllites,
Peer review under responsibility of Institute of Rock and Soil Mechanics, Chinese
schists) and intact laminated, stratified or bedded sedimentary
Academy of Sciences.
rocks (shales, sandstones, siltstones, limestones, coal, etc.) (Chen
et al., 1998).
The tests are conducted on hard and brittle stratified sand-
stone (psammite) and the Brazilian method (diametrical loading of
cylindrical discs) is applied. The stratified (layered or banded) rock
1674-7755 © 2013 Institute of Rock and Soil Mechanics, Chinese Academy of
Sciences. Production and hosting by Elsevier B.V. All rights reserved.
material is sometimes called transversely isotropic rock material
http://dx.doi.org/10.1016/j.jrmge.2013.01.004 (Ye et al., 2009), i.e. rocks with one dominant direction of planar
A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377 367
drill bits with different diameters from 30 mm to 115 mm are used. a 2.62–2.63 2.0–3.0 4.5–4.7 4.9–5.0
The direction of coring is parallel to the layers. For all samples a b 2.57–2.58 2.8–3.2 4.3–4.4 4.5–4.6
c 2.58–2.61 2.1–3.0 4.5–4.6 5.0
constant thickness of 25 mm is taken. All tests are carried out by
368 A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377
wave velocities are always measured perpendicular and parallel to groups (Reineck and Singh, 1986). The grains of the three sub-types
the layers, respectively (see Table 1). The minimum difference of are in the class of subangular.
wave velocities is measured in samples of sub-type b. In this sub- For quartz grain size measurements, the point-counting method
type, wave velocity perpendicular to the layers is from 4.3 km/s to is applied too. Three hundred points in each thin section are
4.4 km/s while in direction parallel to the layers it is from 4.5 km/s counted in a similar pattern to the composition quantification.
to 4.6 km/s. Similar to sieving analysis the smallest dimension of the grain is
considered as the grain size. The average (and minimum, maxi-
2.2. Petrographical study of untested samples mum) values (in m) of the quartz grains size in sub-types a, b and
c are 69 (22, 141), 107 (42, 218), and 82 (29, 146), respectively. The
For petrographical purpose, thin sections with a thickness of grain size calculation is done by arithmetic method. By considering
30 m from an untested sandstone sample from each sub-type the British Standards (Craig, 1990), the grains of studied sub-types
are prepared and analysed. Thin section observation is done by are in the size range of fine sand. The measurements are in agree-
petrographical microscope with transmitted polarised light. In all ment with the study of Thorez et al. (2006) of the sandstone in the
samples, quartz, carbonate and mica are observed. Pores, organic same area. They have mentioned that the sandstone of Famennian
material, clay minerals and feldspar are also observed, although in stage in the south of Belgium is fine grained with the average grain
very small quantities. Clays are found usually mixed with micro- size of 45–120 m.
scopic crystals of carbonates, feldspars, micas and quartz. These The nature of minerals suggests that the presence of strong ele-
minerals are very common in fine grain sedimentary rocks such as ments such as quartz increases the rock strength and, on the other
the studied sandstone. Determining precisely the clay mineral by hand, the abundance of weak minerals such as mica and carbonate
means of X-ray analysis and some spectroscopic methods is pos- decreases the rock strength. It is widely accepted that for higher
sible. By referring to some studies, it is understood that the clay quartz content, rock strength increases. Contrary to quartz, the
minerals in the studied sandstone are dominated by illite (Thorez abundance of easily cleavable minerals would result in lowering the
et al., 1988; Han et al., 2000). strength values (Tavallali, 2010). It should be noted that sub-type
To quantify the relative amount of minerals, the point-counting a has the highest weak minerals percentage (23.5%) and sub-type
method is applied (Chayes, 1956; Přikryl, 2001). The thin section is b has the lowest weak minerals percentage (7.9%).
put in the point-counting apparatus which is attached to the petro-
graphical microscope. Above-mentioned apparatus moves the thin 3. Brazilian test results
section with a given interval. After each movement, the mineral in
the centre of the microscopic view is observed. For example, if in The rock layers are inclined at different angles (see Fig. 1) ran-
100 steps of movement 75 times a quartz grain is observed in the ging between 0◦ (perpendicular to the loading direction) and 90◦
centre of microscopic view, it is concluded that quartz content in (parallel to the loading direction). It should be highlighted that
that rock material is 75%. the orientation of the layers with respect to loading direction is
In this study, 500 points in each thin section are counted in a evaluated. As the loading direction in this study is always vertical,
regular pattern with a fixed interval of 400 m between the points. changing the layer orientation implies that the angle between the
Direction of counting is perpendicular to the layers. The distance of layer direction and the loading direction changes. Seven different
800 m is taken between the lines of point-counting. Fig. 2 presents values are considered: 0◦ , 20◦ , 45◦ , 60◦ , 70◦ , 80◦ and 90◦ . Since one
the percentage of different minerals in each sub-type. sample is not necessarily representative for the failure behaviour
In the three Modave sandstone sub-types, the main constitutive corresponding to a specific inclination angle, four to six samples
mineral is quartz (from 72% to 88%). The shape and roundness of are tested per inclination angle value per sub-type. The number
the quartz grains are the same in all the sub-types. For roundness of tested samples for the sub-types a, b and c is 29, 30 and 30,
of sand grains, Powers (1953) and Shepard (1963) distinguished six respectively (89 samples in total).
The variation in the average failure strength with the inclination
angle for the sub-types is presented in Fig. 3. All the curves show a
(1) Some fractures are parallel to the isotropic layers which are
further called “layer activation”.
(2) Some fractures are roughly parallel to the loading direction and
they are located in the central part of the sample between the
two loading lines. The central part is arbitrarily defined as 10%
of the diameter on both sides of the central line. These fractures
are further called “central fractures”.
(3) Fractures outside the central part are also observed. If they do
not correspond to layer activation, they are further called “non-
central fractures”. The latter are often curved lines, starting at
or around the loading platens.
Fig. 7. Observed failure patterns of samples from different layered Modave sandstone sub-types in Brazilian tests. Inclination angle of 70◦ for all samples. Set of inclined
parallel lines symbolises average layer direction (bedding). The predominant and secondary failure mode are given in parentheses, CF: central fracture, LA: layer activation.
4. Shape effect
In this part of the study, the effect of sample shape on the failure
behaviour of disc-shaped samples after conducting Brazilian tests
is investigated for Modave sandstone. To be sure that the same
material is tested, the samples coming from each block are consid-
ered separately. So, in one way, with this condition, the amount of
rock material is limited. Therefore, size effect experiments are not
possible, as for the same length/diameter (or thickness/diameter)
ratio a large amount of rock material is needed for large diameters.
Therefore, only the shape effect is investigated.
Fig. 8. Variation in fracture length percentage corresponding to layer activation,
central fracture(s) and non-central fracture(s) for different sandstone sub-types.
It is observed that the number of layer boundaries (e.g. over
1 cm) of the three sandstone sub-types is not the same, and also
their failure patterns are different. It is essential to know whether
the number of layer boundaries per sample is important or the
372 A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377
Fig. 9. Observed failure patterns (one side) in Brazilian test for samples in different diameters from Modave sandstone sub-types a, b and c (one typical sample for each
diameter). Inclination angle for all samples is 70◦ . Sample number and the predominant failure mode(s) are put under the samples. The first part of the numbers is the sample
diameter in mm. CF: central fracture, NCF: non-central fracture, LA: layer activation, #LB: number of layer boundaries.
distance between the layers plays the main role in failure sandstone sub-type b (2.6). It means that a sample from sub-type
behaviour. By preparing larger samples, the number of layer a with “D” in diameter has the same number of layer boundaries as
boundaries per samples increases; however, the distance between a sample from sub-type b with “2D” in diameter. However, the dis-
them does not change. For example, the number of layer bound- tance between the layer boundaries in the sample from sub-type
aries over 1 cm for sub-type a (5.4) is about two times that for b is two times larger than that for the sample from sub-type a.
A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377 373
Table 2
Quantity of sandstone samples for shape effect analyses.
a 4 4 4 2 2 – 16
b 4 – 4 3 – 4 15
c 4 – 4 – 3 4 15
The aim of the following experiments can be summarised by the An effort has been made to answer these questions. For this
following two questions: purpose, several samples with different diameters from different
sub-types of sandstone should be tested.
The blocks of sandstone sub-types a, b and c are cored in the
(1) What is the effect of sample diameter on failure behaviour of laboratory by using drill bits with different diameters from 30 mm
disc-shaped samples from a particular sandstone sub-type? to 115 mm. The direction of coring is parallel to the layering. For
(2) Is there any similarity in failure pattern of samples from differ- all samples a constant thickness of 25 mm is taken. Therefore,
ent sub-types which have (roughly) the same number of layer the thickness/diameter ratio varies from 0.2 to 0.9. Variation in
boundaries? mentioned ratio in some studies is executed by changes in the
Fig. 10. Shape effect on failure behaviour of disc-shaped samples after conducting Brazilian test. Samples with different diameters but constant thickness (25 mm) from
sandstone sub-types a, b and c are tested. The inclination angle for all the samples is 70◦ .
374 A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377
Table 3
Number of layer boundaries per sample in the tested diameter range for the three sandstone sub-types.
D = 30 mm D = 40 mm D = 50 mm D = 80 mm D = 100 mm D = 115 mm
Fig. 12. Correlation of average failure strength and average relative layer activation
fracture length for the three sandstone sub-types.
Fig. 13. Variation in relative layer activation fracture length as a function of number
relative layer activation fracture length for the tested samples is
of layer boundaries per sample. Items 1 to 5 show the samples with (roughly) the
clearly presented by Fig. 12. This figure shows that higher strength same number of layer boundaries (see Table 4).
corresponds to the samples with lower layer activation fracture
length.
As can be seen in Fig. 11, although the number of total layer sandstone sub-type b and the samples with 4 cm diameter from
boundaries is larger in samples of sandstone sub-types b and c sandstone sub-type a are the other example (see Table 3 and also
by increasing the samples diameter, their relative layer activation item 4 in Table 4). Five pairs with relatively similar numbers of layer
fracture length does not change considerably. It means that the boundaries can be found in Table 3. These five pairs are presented
failure patterns of samples from different sub-types of sandstone in Table 4 as items 1–5 with their sandstone sub-types, diameters
which have (roughly) the same number of layer boundaries per and individual numbers of layer boundaries (#LB/sample).
sample are not similar. Mentioned conclusion is verified by com- Variation in relative layer activation fracture length for samples
paring the failure patterns of samples with similar number of layer with (roughly) the same number of layer boundaries (items 1–5
boundaries. in Table 4) is presented in Fig. 13. Fig. 13a shows that the effect
By knowing the number of layer boundaries per centimetre for of the number of layer boundaries on layer activation cannot be
each sub-type of sandstone, the number of layer boundaries in observed. Furthermore, this figure shows that by increasing the
each sample with different diameters is calculated. Table 3 presents number of layer boundaries per sample (by increasing the sample
the number of layer boundaries per sample in the tested diameter diameter), any positive trend of relative layer activation fracture
range for the three sandstone sub-types. From Table 3 the samples length does not exist. Fig. 13b presents the variation in average
with similar numbers of layer boundaries per sample are grouped. relative layer activation fracture length as a function of number
For example, the numbers of layer boundaries in the samples with of layer boundaries per sample in every item. In this figure, only
3 cm diameter from sandstone sub-type a is 15.7, close to the num- item 2 shows the same average relative layer activation fracture
bers of layer boundaries in the samples with 11.5 cm diameter from length for the samples with roughly the same number of layer
sandstone sub-type c (16.0). The samples with 8 cm diameter from boundaries and for the other four items no correlation can be
Table 4
Sandstone samples with (roughly) the same number of layer boundaries per sample.
1 c 50 7.0 7.5 30 b 1
2 b 50 13.0 14.0 100 c 2
3 a 30 15.7 16.0 115 c 3
4 b 80 20.8 21.1 40 a 4
5 a 50 27.0 29.6 115 b 5
376 A. Tavallali, A. Vervoort / Journal of Rock Mechanics and Geotechnical Engineering 5 (2013) 366–377
tested diameter range. Samples of sandstone sub-type b with the Rocco C, Guinea GV, Planas J, Elices M. Size effect and boundary conditions
lowest weak minerals percentage (7.9%) have the lowest relative in the Brazilian test: experimental verification. Materials and Structures
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Szwedzicki T. A hypothesis on modes of failure of rock samples tested in uniaxial
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Tavallali A. Failure of layered Modave sandstone: effect of layer orientation and
material properties. Leuven: KU Leuven; 2010 [Ph.D. thesis].
The financial support of the Research Council of the Katholieke Tavallali A, Vervoort A. Effect of layer orientation on the failure of layered sandstone
Universiteit Leuven (OT-project OT/03/35) is gratefully appreci- under Brazilian test conditions. International Journal of Rock Mechanics and
Mining Sciences 2010a;47(2):313–22.
ated. The work is part of the Ph.D. study by A. Tavallali. Authors Tavallali A, Vervoort A. Failure of layered sandstone under Brazilian test conditions:
acknowledge their sincere thanks to Prof. Rudy Swennen from the effect of micro-scale parameters on macro-scale behaviour. Rock Mechanics and
Geology Section of KU Leuven for helpful comments and also per- Rock Engineering 2010b;43(5):641–53.
Tavallali A, Vervoort A. Failure of transversely isotropic rock material: effect of layer
mitting the use of their microscopic instruments. The authors also
orientation and material properties. In: Proceedings of the 6th international
thank An De Cleyn for her helpful comments in the geological part symposium on ground support in mining and civil engineering construction.
of the study. Johannesburg: The Southern African Institute of Mining and Metallurgy; 2008.
p. 317–28.
Tavallali A, Debecker B, Vervoort A. Evaluation of Brazilian tensile strength in
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Abbass Tavallali is an Advisor Engineer at International
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Marine and Dredging Consultants (IMDC) in Belgium. He
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graduated as a Civil Engineer in 1995 from Shiraz Uni-
axial compression using 3D cellular automata. International Journal of Rock
versity in Iran. He had an opportunity to participate in
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the huge geotechnical and structural projects in Iran.
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He gained nine years of professional experience in the
tives. Belgium: Ouvrage publié par le Ministère de la Region Wallonne; 2004.
field of dam construction and tunnelling projects prior to
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continuing his studies for Ph.D. He got his Ph.D. degree
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in geotechnical engineering from KU Leuven (Katholieke
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Universiteit Leuven) in Belgium in 2010. Then (in 2011) he
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joined IMDC and he carries out a diverse range of geotech-
Reineck HE, Singh IB. Depositional sedimentary environments. Berlin, Germany:
nical and dredging subjects.
Springer-Verlag; 1986.