Jis g03302 Table of Content
Jis g03302 Table of Content
Jis g03302 Table of Content
INDUSTRIAL
STANDARD
Translated and Published by
Japanese Standards Association
(JISF)
Hot-dip zinc-coated steel sheet and strip
ICS 77.140.50
Reference number : JIS G 3302 : 2019 (E)
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G 3302 : 2019
JSA 2019
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized
in any form or by any means, electronic or mechanical, including photocopying and microfilm, without
permission in writing from the publisher.
Printed in Japan HN
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Contents
Page
Introduction ································································································· 1
1 Scope ································································································· 1
2 Normative references ············································································ 1
3 Symbol of grade and applicable nominal thickness ···································· 2
4 Chemical composition ··········································································· 3
5 Coating ······························································································ 4
5.1 Plating bath composition ······································································· 4
5.2 Type of coating ···················································································· 4
5.3 Coating mass ······················································································ 5
5.4 Coating surface finishes ········································································ 6
5.5 Coating adherence ··············································································· 7
6 Chemical treatment ·············································································· 8
7 Oiling ································································································· 9
8 Mechanical properties ··········································································· 9
8.1 Applicable mechanical properties ··························································· 9
8.2 Bendability ························································································ 10
8.3 Tensile test characteristics ··································································· 10
9 Dimensions ························································································ 11
9.1 Expression of dimensions ····································································· 11
9.2 Standard dimensions ··········································································· 12
9.3 Dimensional tolerances ········································································ 13
10 Shape ································································································ 16
10.1 Camber ····························································································· 16
10.2 Squareness ························································································ 17
10.3 Flatness ···························································································· 17
11 Mass ································································································· 18
11.1 Mass of sheet and corrugated sheet ························································ 18
11.2 Mass of coil ························································································ 18
11.3 Calculation of mass ············································································· 19
11.4 Tolerances on theoretical mass of sheet and corrugated sheet ···················· 20
12 Appearance ························································································ 20
13 Tests ································································································· 20
13.1 Chemical analysis ··············································································· 20
13.2 Plating bath composition test ································································ 20
(i)
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(ii)
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Foreword
(iii)
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Blank
JAPANESE INDUSTRIAL STANDARD JIS G 3302 : 2019
Introduction
This Japanese Industrial Standard has been prepared based on ISO 3575 : 2016,
Edition 5, and ISO 4998 : 2014, Edition 6, with some modifications of the technical
contents.
The vertical lines on both sides and dotted underlines indicate changes from the cor-
responding International Standards. A list of modifications with the explanations is
given in Annex JF. Annex JA to Annex JE are unique to JIS and not given in the cor-
responding International Standards.
1 Scope
This Standard specifies requirements for hot-dip zinc-coated steel sheet (hereafter
referred to as sheets), steel strip (hereafter referred to as coils), and corrugated sheet
manufactured by processing sheets into the shapes and dimensions specified in JIS G
3316 (hereafter referred to as corrugated sheets).
NOTE The International Standards corresponding to this Standard and the
symbol of degree of correspondence are as follows.
ISO 3575 : 2016
2 Normative references
The following standards contain provisions which, through reference in this text,
constitute provisions of this Standard. The most recent editions of the standards (in-
cluding amendments) indicated below shall be applied.
JIS G 0320
JIS G 0404
JIS G 0415
JIS G 3316
JIS K 0119
JIS K 8847
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JIS Z 2241
JIS Z 8401
Table 1 Symbol of grade and applicable nominal thickness (hot-rolled base metal)
Unit: mm
Symbol of grade Applicable nominal Application
thickness
SGHC Commercial
SGH340
SGH400 1.6 or over up to and
High strength commer-
SGH440 incl. 6.0
cial
SGH490
SGH540
For those with a nominal thickness of 1.6 mm or over up to and in-
cluding 3.2 mm, unless the use of hot-rolled base metal is specifically re-
quired, the cold-reduced base metal which satisfies the specifications for
hot-rolled base metal may be used.
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Table 2 Symbol of grade and applicable nominal thickness (cold-reduced base metal)
Unit: mm
Symbol of grade Applicable nominal Application
thickness
SGCC 0.19 or over up to and Commercial
incl. 3.2
SGCH 0.11 or over up to and Commercial hard
incl. 1.0
SGCD1 0.30 or over up to and Drawing, Class 1
incl. 2.3
SGCD2 0.40 or over up to and Drawing, Class 2
incl. 2.3
SGCD3 Drawing, Class 3
0.60 or over up to and
SGCD4 Drawing, Class 4,
incl. 2.3
non-ageing property a)
SGC340
SGC400 0.25 or over up to and
SGC440 incl. 3.2 High strength com-
SGC490 mercial
SGC570 0.25 or over up to and
incl. 2.0
Note a) Non-ageing property indicates the property by which steels
are free from the stretcher strain marks when being formed.
4 Chemical composition
The base metal of sheets, coils and corrugated sheets shall be tested for chemical
composition in accordance with 13.1, and the heat analysis values shall be as given in
Table 5.
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5 Coating
5.1 Plating bath composition
Plating bath shall be tested for composition in accordance with 13.2 and shall be as
given in Table 6.
NOTE In the hot-dip coating process, the base metal is immersed in a molten
metal bath at a high temperature, and then cooled to form a coating on
the base metal surface. This molten metal bath is called plating bath.
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Note 2) Alloy coating indicates the coating obtained in such a way that the entire
coating comprises the alloy layer of zinc and iron by heating after coating.
5.3 Coating mass
5.3.1 Symbol for coating mass
The coating applied shall be of equivalent thickness on both surfaces. The symbols
for coating mass shall be as given in Table 7.
5.3.2 Coating mass
The sheets, coils and corrugated sheets shall be tested for coating mass in accord-
ance with 13.3.2 and shall satisfy the following requirements.
a) The coating mass of sheets, coils and corrugated sheets shall be expressed by the
total mass on both surfaces and shall meet the minimum triple-spot average coat-
ing mass value and the minimum single-spot coating mass value given in Table 7.
The minimum triple-spot average coating mass shall apply to the average of the
measured values of three test pieces taken from the sample, and the minimum sin-
gle-spot coating mass shall apply to the smallest value among the measured values
of the three test pieces of which the average value is obtained. When coating mass
is measured in accordance with Annex JD, the minimum coating mass values in
the table shall apply to the average coating mass and minimum coating mass ob-
tained according to JD.6.5.
NOTE It is desirable that the coating mass on one side be not less than 40 % of
the required value for the minimum single-spot coating mass (total mass
on both surfaces).
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b) For sheets and coils used for roofing and architectural siding, the coating mass
shall be as given in Table JA.1.
c) The coating mass for corrugated sheets shall apply to pre-corrugated sheets and
shall be as given in Table JB.1.
d) The upper limit value of the coating mass (total mass on both surfaces) of sheets,
coils and corrugated sheets may be as agreed between the purchaser and the man-
ufacturer.
5.4 Coating surface finishes
5.4.1 Classification and symbol of surface finish for non-alloy coating
The classification and symbols of the surface finish for non-alloy coating shall be as
given in Table 8.
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6 Chemical treatment
The classification and symbols of chemical treatment for sheets, coils and corrugated
sheets shall be as given in Table 11. Unless otherwise specified, the non-alloy coating
shall be subjected to the chromate-free treatment 3) and the alloy coating shall be un-
treated.
Note 3) Chromate-free indicates that the coating formed by chemical treatment is
free from hexavalent chromium.
Chromate treatment c) C
Phosphate treatment c) d) P
Untreated M
Notes a) The term chromate-free treatment comprises both chro-
mate-free treatment and chromate-free phosphate treatment
that are specified in JIS G 3302 : 2012.
b) The symbol of chromate-free treatment shall be as agreed
between the purchaser and the manufacturer. The symbols
NC and NP may be used for chromate-free treatment and
chromate-free phosphate treatment, respectively, that are
specified in JIS G 3302 : 2012.
c) Requirements for chromate treatment and phosphate treat-
ment are to be deleted in the next revision.
d) In phosphate treatment, chromate treatment is generally
applied to the phosphate-treated surface in order to improve
the corrosion resistance.
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7 Oiling
The classification and symbols of oiling for sheets, coils and corrugated sheets shall
be as given in Table 12. Unless otherwise specified, non-alloy coating shall be unoiled
and the alloy coating shall be oiled.
8 Mechanical properties
8.1 Applicable mechanical properties
Mechanical properties applicable to sheets and coils shall be as given in Table 13.
The mechanical properties of the corrugated sheets shall apply to pre-corrugated
sheets and shall be as given in Table 13.
SGCH
SGCD1
SGCD2
SGCD3
SGCD4
SGC340
SGC400
SGC440
SGC490
SGC570
Notes a) Bendability applies to the non-alloy coating and
not to the alloy coating.
b) For those under 0.25 mm in nominal thickness,
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8.2 Bendability
When non-alloy coated sheets, coils and pre-corrugated sheets are tested for benda-
bility in accordance with 13.4.2, the external surface of the test piece (not less than 7
mm from both side edges of test piece) shall be free from cracks and breakage that are
visible to the naked eye.
NOTE For the details of bend test, see 13.4.2.
8.3 Tensile test characteristics
The sheets, coils and pre-corrugated sheets shall be tested for tensile test character-
istics in accordance with 13.4.3 and shall satisfy the requirements given in Table 14 or
Table 15. The values given in Table 14 or Table 15 shall apply to those which undergo
delivery inspection 4).
Note 4) Age-hardening of sheets, coils and pre-corrugated sheets may cause an
increase in yield point or proof stress and a decrease in elongation.
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9 Dimensions
9.1 Expression of dimensions
9.1.1 Denomination of thickness
The denomination of thickness of sheets, coils and corrugated sheets shall be as fol-
lows. For corrugated sheets, the following denominations of thickness shall be applied
to pre-corrugated sheets.
a) The thickness of base metal before coating shall be taken as the nominal thickness.
b) The thickness of base metal after coating shall be taken as the product thickness.
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The product thickness, which is the base of tolerances, shall be the nominal thick-
ness plus the equivalent coating thickness and shall be obtained by adding the
equivalent coating thickness given in Table 16 to the nominal thickness expressed
to the third decimal place. The resultant value shall be rounded to the second dec-
imal place according to Rule A of JIS Z 8401.
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b) Standard width and standard length of sheets The standard width of sheets and
coils and the standard length of sheets shall be as given in Table 18.
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10 Shape
10.1 Camber
The camber of sheets, coils and corrugated sheets shall be as follows.
a) The measurement of camber shall be as shown in Figure 1.
b) The camber shall be as given in Table 26 or Table 27. For corrugated sheets, these
tables shall apply to pre-corrugated sheets.
c) The requirements for camber shall not apply to the irregular portions of coils.
d) The measurement of camber may be omitted 5); however, when specified by the
purchaser, the measurement shall be performed.
Note 5) The measurement of camber may be omitted at the discretion of the
manufacturer provided that the products satisfy the requirements for
camber.
Unit: mm
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10.2 Squareness
The squareness of sheets and corrugated sheets shall be in accordance with either of
the following. For corrugated sheets, it applies to pre-corrugated sheets.
In the case of dispute, the method given in a) shall apply.
a) Method using perpendicular line The squareness of sheets and corrugated sheets
shall be expressed by the ratio (A/W), where A indicates the distance between a
perpendicular line from an edge drawn at a corner point and the corner point of the
opposite edge, and W indicates the length of the perpendicular line, as shown in
Figure 2, and this value shall not exceed 1.0 %.
W (Measured width)
b) Method using diagonal lines Half of the absolute value of the difference between
the lengths of two diagonal lines (X1 and X2 in Figure 3) of the sheet and corrugated
sheet shall be obtained, and this value (| X1 X2 | /2) shall not exceed 0.7 % of the
measured width of the sheet and corrugated sheet.
L (Length)
W (Measured width)
Figure 3 Squareness of sheets and corrugated sheets (method using diagonal lines)
10.3 Flatness
The flatness of sheets and coils shall be as follows.
a) Flatness of sheet The flatness of sheets shall be as given in Table 28 or Table 29.
The flatness shall be obtained as follows : place a sheet on a surface plate; measure
the maximum strain of the sheet; from the measured value subtract the product
thickness of the sheet, to take as the value for the top surface of sheet.
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b) Flatness of coil The flatness of coils shall be as given in Table 28 or Table 29;
however, the requirements for bow do not apply. In addition, the flatness of coils
shall not apply to the irregular portions of coils. The flatness of coils shall be in-
spected on the inspection station installed on the production line. When the meas-
ured values are required to be reported, the measurement shall be performed after
the purchaser and the manufacturer agree upon the measurement including the
measurement method.
The measurement of flatness of coils may be omitted 6).
Note 6) The measurement of flatness may be omitted at the discretion of the man-
ufacturer provided that the coils satisfy the requirements for flatness.
11 Mass
11.1 Mass of sheet and corrugated sheet
Unless otherwise specified, the mass of sheets and corrugated sheets shall generally
be given in the theoretical mass in kilogrammes.
11.2 Mass of coil
The mass of coils shall be given in either the actual mass or theoretical mass in kilo-
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grammes.
11.3 Calculation of mass
The calculation method of mass of sheets, coils and corrugated sheets shall be as
given in Table 30.
Mass of a single coil Unit mass of coil (kg/m) × length (m) Rounding off to an
kg integer in kg
Total mass kg Total mass of each coil (kg) An integer in kg
Notes a) The rounding of numerical values shall be in accordance with Rule A of JIS Z 8401.
b) Basic mass of base metal per thickness 1 mm × area 1 m2
c) The coating mass constants shall be as given in Table 31.
d) The width dimensions used for the calculation of the area of corrugated sheet shall
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12 Appearance
The sheets, coils and corrugated sheets shall be free from defects detrimental to use.
Coils may contain some irregular portions or welds because the inspection usually does
not afford the manufacturer the opportunity to readily detect and remove defective
portions over the entire length. Treatment of coil defective portions, if necessary, may
be agreed upon between the purchaser and the manufacturer.
The requirements for surface defects shall apply to one surface 7) of sheets, coils and
corrugated sheets, unless otherwise specified.
NOTE Defects include holes, laminations and surface flaws.
Note 7) One surface generally refers to the upper surface of package for sheets
and corrugated sheets, and the outside surface for coils.
13 Tests
13.1 Chemical analysis
13.1.1 General requirements for chemical analysis and sampling method
The chemical composition of sheets, coils and corrugated sheets shall be determined
by heat analysis, and the general requirements for chemical analysis and the sampling
method shall be as given in Clause 8 of JIS G 0404.
13.1.2 Analytical method
The analytical method shall be in accordance with JIS G 0320.
13.2 Plating bath composition test
The test method of plating bath composition shall be determined at the discretion of
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the manufacturer. The test of plating bath composition may be omitted 8); however, if
requrested by the purchaser, the test shall be performed by the method agreed upon
between the purchaser and the manufacturer.
Note 8) The test may be omitted at the discretion of the manufacturer provided
that the requirements for plating bath composition are satisfied.
13.3 Coating test
13.3.1 Sampling method
The sampling method for each product of same dimensions and coating mass shall be
as follows.
For corrugated sheets, the sample shall be taken from the pre-corrugated sheet.
a) For the continuously coated coils or their cut lengths, one sample shall be taken
from every 50 t or its fraction.
b) For the sheets prepared by applying coating to the base metal having been cut to
specified lengths, one sample shall be taken from every 3 000 sheets or its fraction.
13.3.2 Coating mass determination
The coating mass shall be determined as follows.
a) Test method Coating mass shall be measured on both surfaces of the test piece, in
accordance with either of Annex JC, Annex JD or Annex JE. In the case of dispute,
Annex JE shall apply.
For the tests in accordance with Annex JD, the measurement shall be performed
for every 50 t or its fraction of products of the same size and coating mass.
b) Sampling of test pieces The test pieces shall be sampled as follows.
1) For the tests in accordance with Annex JC, the sampling position, size and num-
ber of test pieces shall be as specified in JC.5.
2) For the tests in accordance with Annex JD, the coating mass of the product shall
be measured on the production line without sampling a test piece.
3) For the tests in accordance with Annex JE, the sampling position and number of
test pieces shall be as specified in JC.5.2. The size of the test piece shall be 1 200
mm2 or over.
13.3.3 Coating adherence determination
The coating adherence determination by the bend test shall be as follows.
a) Sampling position and size of test piece The test piece shall be taken at any posi-
tion of the sample. The test piece shall have a width of 75 mm to 125 mm and a
suitable length of about twice the width. Unless otherwise specified, one test piece
shall be taken from the sample in the direction parallel to the rolling direction of
the base metal.
b) Test method The test piece shall be bent manually using a vice at 180° in the lon-
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gitudinal direction of the test piece, as shown in Figure 4, with the specified num-
ber of sheets being sandwiched. The number of sheets is specified in Table 9 or Ta-
ble 10 as the internal spacing of bend. When a vice is not available, testing by other
suitable means may be adopted. After the bending, the test piece shall be examined
for flaking of the coating.
Internal spacing
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surface of the test piece shall be examined for cracks and breakage which are visible to
the naked eye.
The bend test may be omitted 9). If specified by the purchaser, however, the test shall
be performed.
Note 9) The bend test may be omitted at the discretion of the manufacturer pro-
vided that the requirements for bendability are satisfied.
13.4.3 Tensile test
The tensile test shall be as follows.
a) Test piece Take one Test piece No.5 specified in JIS Z 2241 from the sample, in
the direction given in Tables 14 and 15.
b) Test method The test method shall be in accordance with JIS Z 2241.
c) Thickness used for calculation of yield point or proof stress, and tensile strength
The thickness used for calculation of yield point or proof stress, and tensile
strength shall be either of the following.
Actual measured thickness after the removal of coating
Thickness obtained by subtracting the equivalent coating thickness from the
actual measured thickness including the coating
Thickness obtained by subtracting the coating thickness obtained through
conversion of the actual measured coating mass 10) from the actual measured
thickness including the coating
Note 10) The converted coating thickness is obtained by dividing the actual
measured coating mass by the density of coating (7.14 g/cm3 for
non-alloy coating and 7.21 g/cm3 for alloy coating). The resultant value
is rounded to three decimal places and expressed in millimetres.
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14.2 Reinspection
The sheets, coils and corrugated sheets having failed the coating mass determination,
coating adherence determination, bend test or tensile test, may be subjected to the re-
test according to 9.8 of JIS G 0404 for further acceptance judgement.
15 Marking
The sheets, coils and corrugated sheets having passed the inspection shall be marked
with the following items by a suitable means on each package or bundle. When agreed
between the purchaser and the supplier, the following items may be marked on each
sheet or corrugated sheet by a suitable means.
a) Symbol of grade
b) For those for roofing or architectural siding, the symbol given in Table 3 which is
suffixed to the symbol of grade
c) For corrugated sheets, the symbol given in Table 4 which is suffixed to the symbol
of grade. For corrugated sheets for roofing or architectural siding, the symbol given
in Table 4 is suffixed to the symbol given in Table 3.
d) Symbol for surface finish; symbol for skin-pass treatment and/or symbol for chemi-
cal treatment; and symbol for oiling, all of which are marked when specified by the
purchaser
e) Symbol for coating mass
f) Dimensions (See 9.1. For one sheet, only the nominal thickness is marked.)
g) Product identification number
h) Number of sheets or mass (For one sheet, this item may be omitted.)
i) Manufacturers name or its identifying brand
Marking examples are as follows.
Example 1 Sheet
SGCC Z18 0.27 × 914 × 1 829
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17 Report
The manufacturer shall submit an inspection document to the purchaser when the
document is previously requested by the purchaser. In this case, the report shall con-
form to the requirements in Clause 13 of JIS G 0404. The measured values of carbon,
phosphor and sulfur among chemical compositions may be expressed to three decimal
places in the report. Unless otherwise specified, the type of the inspection document to
be submitted shall be in accordance with 5.1 of JIS G 0415.
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Annex JA (normative)
Coating mass of sheet and coil for roofing and
architectural siding
Table JA.1 Nominal thickness and symbol for coating mass (applicable to symbols of
grade given in Table 2)
Application Nominal thickness Symbol for coating mass a)
mm
0.35 or over up to and incl. 1.0 Z25, Z27
Roofing
Over 1.0 Z27
0.27 or over up to and incl. 0.50 Z18, Z22, Z25, Z27
Architectural
Over 0.50 up to and incl. 1.0 Z22, Z25, Z27
siding
Over 1.0 Z27
Note a) Z35, Z37 Z45 and Z60 may be applied if agreed between the purchaser
and the manufacturer.
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Annex JB (normative)
Coating mass and standard dimensions of corrugated sheet
Table JB.1 Nominal thickness and symbol for coating mass (applicable to symbols of
grade given in Table 2)
Nominal thickness Symbol for coating mass a)
mm
0.11 or over to and excl. 0.16 Z12 b)
0.16 or over to and excl. 0.27 Z12
0.27 or over up to and incl. 0.30 Z12 b), Z18, Z22, Z25, Z27
Over 0.30 up to and incl. 0.50 Z18, Z22, Z25, Z27
Over 0.50 up to and incl. 1.0 Z22, Z25, Z27
Notes a) Z35, Z37 Z45 and Z60 may be applied if agreed be-
tween the purchaser and the manufacturer.
b) Application of Z12 to corrugated sheets with a
nominal thickness of 0.11 mm or over to and ex-
cluding 0.16 mm and of 0.27 mm or over up to and
including 0.30 mm shall be as agreed between the
purchaser and the manufacturer.
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Annex JC (normative)
Off-line coating mass determination of hot-dip zinc-coated
steel sheet and strip by fluorescent X-ray method
JC.1 Outline
The coating mass of a test piece is determined using an off-line fluorescent X-ray test
apparatus.
JC.3 Apparatus
The apparatus shall be as specified in Clause 5 of JIS K 0119.
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Unit: mm Unit: mm
Direction of coating
Figure JC.1 Sampling position of test Figure JC.2 Sampling position of test
pieces (continuous zinc-coating method) pieces (sheet-by-sheet zinc-coating
method)
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the average coating mass of two Test pieces B to take as the coating mass on the
measurement surface of Test piece A.
d) Preparation of calibration curve Carry out procedures a) to c) on test pieces with
at least three different levels of coating mass, and prepare the calibration curve
based on the relation between the intensity of fluorescent X-ray and the coating
mass.
JC.6.1.3 Dual-test-piece method
The preparation of the calibration curve by the dual-test-piece method shall be as
follows.
a) Test piece Take two test pieces of at least 1 200 mm2 in size from the sample for
preparing the calibration curve.
b) Measurement of fluorescent X-ray intensity Decide which surface of the one test
piece to irradiate with fluorescent X-ray to take as the measurement surface. Irra-
diate the measurement surface of the test piece with X-ray under the condition
specified in JC.7 a), and measure the intensity of fluorescent X-ray. Measure the
intensity of fluorescent X-ray of the other test piece on the same surface in the
same manner. Obtain the average intensity of fluorescent X-ray of the two test
pieces to take as the intensity of fluorescent X-ray on the measurement surface.
c) Measurement of coating mass Pretreat the test pieces so as to prevent the elution
of coating from other surfaces than the measurement surface. Prevent the elution
of coating in such a way that, on the back of measurement surface, lacquer is ap-
plied and then dried, or a wide tape is applied. After pretreatment, measure the
coating mass on the surfaces of the two test pieces, according to Annex JE. Obtain
the average coating mass of the two test pieces to take as the coating mass on the
measurement surface.
d) Preparation of the calibration curve Carry out procedures a) to c) on test pieces
with at least three different levels of coating mass, and prepare a calibration curve
based on the relation between the intensity of fluorescent X-ray and the coating
mass.
JC.6.2 Correction of calibration curve
Mount the calibration test piece on the test apparatus, periodically 1) measure the
intensity of fluorescent X-ray or obtain the value converted to coating mass, and cor-
rect the calibration curve.
Note 1) This calibration should be performed, for example, every 8 h or 24 h.
JC.7 Procedure
The procedure shall be as follows.
a) Mount on the apparatus the test piece of symbol for the minimum coating mass
among all measured coating mass values. Set the apparatus conditions under
which the relative standard deviation 2) after 10 consecutive measurements can be
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within 1 %, and which the coating mass can be obtained to the nearest 0.1 g/m2.
Repetitive measurements are not required when the X-ray intensity obtained by
counting is 10 000 or more.
Note 2) The term indicates the quotient obtained by dividing the standard devia-
tion of measured values (absolute value of square root of variance) by the
average value (see 3.10 of JIS K 0211).
When measuring a coating mass smaller than that of the symbol for coating
mass used in setting the conditions, confirm that the above conditions are satisfied
by using a test piece of the relevant symbol for coating mass. If the above condi-
tions are not satisfied, new conditions shall be defined.
b) Set the test piece properly in the sample chamber.
c) Irradiate the test piece with X-ray under the specified conditions, and measure the
intensity of fluorescent X-ray.
d) Convert the intensity of fluorescent X-ray to coating mass per square metre (one
side, g/m2), by using the calibration curve.
e) Repeat procedures b) to d) on the rear surface of the test piece to determine the
coating mass. Take the total of the coating masses on the front surface and rear
surface as the coating mass of the test piece (both sides, g/m2).
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Annex JD (normative)
Online coating mass determination of hot-dip zinc-coated
steel strip by fluorescent X-ray method
JD.1 Outline
Coating mass is measured by means of a fluorescent X-ray test apparatus installed
on the production line without taking a test piece from coils.
WARNING Proper safety measures shall be taken in measurement and mainte-
nance of a facility performed in accordance with this Annex. Thorough safety control
shall be in place especially to avoid exposure to radiation.
NOTE Examples of laws and regulations regarding the installation and han-
dling of the apparatus used in this test method are the Industrial Safety
and Health Act and the Regulation on Prevention of Ionizing Radiation
Hazards.
JD.3 Apparatus
The apparatus shall be composed of an X-ray generating section; spectroscopy, light
scanning and counting sections; and apparatus controlling and data processing sec-
tions; and shall be as follows. The apparatus shall be installed in a place where there is
no variation of temperature or humidity that may significantly affect the measurement
results.
JD.3.1 X-ray generating section The X-ray generating section shall be capable of
directly irradiating the position of a coil specified in JD.6.3 with X-ray (including
ray).
JD.3.2 Spectroscopy, light scanning and counting sections The spectroscopy, light
scanning and counting sections shall be capable of measuring the intensity of fluores-
cent X-ray generated at the measuring point specified in JD.6.3.
JD.3.3 Apparatus controlling and data processing sections The apparatus control-
ling and data processing sections shall be capable of controlling the X-ray generating
section and the spectroscopy, light scanning and counting sections for irradiating the
position specified in JD.6.3 with X-ray (including ray) and measuring the intensity of
the resultant emission of fluorescent X-ray, and shall be capable of keeping interrelat-
ed records of their irradiating points and the measurement results.
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The coating mass shall be measured on both the front and rear surfaces of the coil.
The measuring points of width direction shall be the same for both the front and rear
surfaces of the coil, and measuring points of longitudinal directions of the front and
rear surfaces of the coil shall be as close as possible.
Unit: mm
Coating direction Coating direction
Edge Edge
X-ray
beam
locus
Edge
Edge
Centreline Centreline
of coil width of coil width
JD.6.4 Measurement
The measurement shall be as follows.
a) The measuring time for one point shall be 4 s or less. Mount on the apparatus the
test piece of symbol for the minimum coating mass among all coating mass values
measured on the production line on which the apparatus is installed. Set the ap-
paratus conditions under which the relative standard deviation after 10 consecu-
tive measurements 1) in the specified time can be within 1 %, and which the coating
mass can be obtained to the nearest 0.1 g/m2. Repetitive measurements are not re-
quired when the X-ray intensity obtained by counting is 10 000 or more.
Note 1) The term indicates the quotient obtained by dividing the standard devia-
tion of measured values (absolute value of square root of variance) by the
average value (see 3.10 of JIS K 0211).
When measuring a coating mass smaller than that of the symbol for coating
mass used in setting the conditions, confirm that the above conditions are satisfied
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by using a test piece of the relevant symbol for coating mass. If the above condi-
tions are not satisfied, new conditions shall be defined.
b) Irradiate the coil with X-ray under the set conditions and measure the fluorescent
X-ray intensity.
c) Convert the intensity of fluorescent X-ray to coating mass per square metre (one
side, g/m2), by using the calibration curve.
When the coil area changes after measurement of the coating mass due to e.g.
skin-pass treatment, correct the coating mass using the rate of change of area.
d) Take the total of the coating masses on the front surface and rear surface as the
coating mass at one point of the coil (both sides, g/m2).
JD.6.5 Measured value of coating mass
Obtain the average coating mass and the minimum coating mass using coating mass
values at three points of arbitrary one pass 2). The measurement may be performed
over more than one pass, in which case the average coating mass shall be the average
of all measured coating mass values and the minimum coating mass shall be the min-
imum value among all measured coating mass values.
Note 2) One pass means the measurement performed while the X-ray generating
section is moved in one direction from a side edge at an arbitrary point of
the coil to the other side edge.
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Annex JE (normative)
Coating mass determination by gravimetric method
JE.1 Outline
The coated test piece is weighed and then the coating is dissolved in the test solution.
The test piece is again weighed, and from the gap between the two masses obtained,
the coating mass is determined.
JE.4 Procedure
The procedure shall be as follows.
a) Measure the mass of test piece before dissolving the coating. The mass shall be
measured to an accuracy within ±1 % of the estimated coating mass (prospective
coating mass).
b) Select the volume of test solution so that at least 10 ml of solution is available for
each 100 mm2 of the coated surface area (one side) of test piece. The test solution
may be reused as long as it is capable of easily removing the coating.
c) Immerse the test piece completely in the test solution at ordinary temperature, and
leave until the coating thoroughly dissolves. The cessation of originally brisk evo-
lution of hydrogen in the test solution indicates the completion of dissolution. Rinse
the test piece in running water, wipe well with cotton cloth and dry sufficiently, or
alternatively immerse the test piece in alcohol and dry quickly. Then weigh the
mass again. The mass shall be measured to an accuracy within ±1 % of the esti-
mated coating mass (prospective coating mass).
d) After weighing, determine the area (mm2) of the coated surface (one side) of test
piece. Measure the surface area to an accuracy within ±1 %.
In the case of known surface area, e.g. punching, the measurement may be omit-
ted.
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_______________________________________________________________________________
Bibliography JIS G 0594
JIS H 8502
JIS K 0211
JIS K 5600-7-9
JIS Z 2371
ISO 16539
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Annex JF (informative)
Comparison table between JIS and corresponding International Standards
JIS G 3302 : 2019 ISO 3575 : 2016
(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
1 Scope Hot-dip zinc-coated ISO 3575 1 Hot-dip zinc-coated Alteration The scope in JIS covers JIS and ISOs have
steel sheet, strip and steel sheet and strip specifications of the two ISO different standard
corrugated sheet of commercial and standards. structures.
drawing qualities Addition Requirements for corrugated
sheets have been added to
ISO 4998 1 Hot-dip zinc-coated
JIS.
steel sheet and strip
of structural quality
3 Symbol of Applicable nominal ISO 3575 1 Applicable thickness, Alteration JIS specifies classification of The difference arises due
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grade and thickness, and symbols 4.1 and symbols of 1 hot-rolled and cold-reduced to the different market
applicable of 3 grades of grade of commercial base metal. JIS specifies needs.
nominal commercial quality, 4 quality and 4 grades more numbers of grades
thickness grades of drawing of drawing quality than ISOs. The range of
quality and 10 grades ISO 4998 1 Applicable thickness, applicable thickness in JIS is
of high strength 4.1 and symbols of seven wider than that in ISOs.
commercial quality grades of structural Addition Requirements for coating on
quality steel sheets have been added
to JIS.
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40
(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
G 3302 : 2019
No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
4 Chemical Chemical composition ISO 3575 5.3 Chemical Alteration Requirements for chemical The difference arises due
composition (four elements) of base ISO 4998 5.1 composition (four composition differ between to the difference in
metal to be coated elements) of base JIS and ISOs. specified mechanical
metal, upper limit JIS does not specify the properties between JIS
value of alloy upper limit value of alloy and ISOs.
elements not elements not specified and JIS does not specify
specified and permissible variation in requirements for product
permissible variation product analysis. analysis due to the lack of
in product analysis market demand.
5 Coating 5.1 Plating bath Addition Requirements for plating Submission of a proposal
composition bath composition have been regarding this addition to
added to JIS. ISOs will be considered.
5.3 Coating mass 5.5.1 Coating mass Alteration The requirements for coating The difference arises due
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5.3.1 mass specified in JIS are to the different market
more detailed than that in needs.
ISOs.
5.4 Coating surface 8.4 Designation by a Alteration JIS specifies separate JIS and ISOs have
finishes combination of symbols for the type of different standard
spangle and spangle and the application structures.
skin-pass treatment of skin-pass treatment.
5.5 Coating adherence 5.5.2 Evaluation of coating Addition While JIS and ISOs specify Test methods common in
adherence by the the same requirements for Japan have been added to
bend test the evaluation by the bend JIS.
test, JIS also specifies
requirements for the
evaluation by other test
methods.
(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
6 Chemical Four types of chemical ISO 3575 5.8.1 Two types of Addition Requirements for chemical Submission of a proposal
treatment treatments ISO 4998 5.6.1 chemical treatments treatment capable of regarding this addition of
supporting environmentally chemical treatment
restricted substances (chromate-free treatment)
(chromate-free treatment) to ISO will be considered.
has been added to JIS.
8 Bendability, tensile 5.2 Tensile test Addition Requirements for bendability The bend test specified in
Mechanical test characteristics characteristics (yield have been added to JIS. JIS may be omitted. This
properties (yield point or proof point or proof stress, item will be considered for
stress, tensile strength tensile strength and exclusion from JIS in the
and elongation) as elongation) future.
mechanical properties Alteration Requirements for tensile test The difference arises due
characteristics differ to the different market
between JIS and ISOs. needs.
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9 9.1 Expression of 4.2 The ordered Alteration Base metal thickness applies Base metal thickness has
Dimensions dimensions Annex A thickness shall be in JIS. been conventionally used
either the product in Japan. Although ISOs
thickness or base used to specify the
metal thickness. application of product
thickness only, ISO then
accepted the proposal of
addition of the application
of base metal thickness
and made a modification
in the 2005 revision.
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(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
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No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
9 9.2 Standard ISO 3575 Addition Requirements for standard Requirements for
Dimensions dimensions ISO 4998 dimensions have been added standard dimensions is
(concluded) to JIS. necessary in JIS due to
business practices
performed in Japan.
9.3 Dimensional 5.7 ISOs refer to ISO Alteration JIS and ISOs specify The difference arises due
tolerances Annex A 16163 for different dimensional to the different market
dimensional tolerances. needs.
tolerances.
10 Shape Shape 5.7 Shape tolerances. Alteration JIS specifies shape JIS and ISOs have
ISOs refer to ISO tolerances separately for different standard
16163 for shape hot-rolled and cold-reduced structures.
tolerances. base metal.
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JIS and ISOs specify
different values for shape.
11 Mass Mass Addition Application of actual mass Requirements for mass are
and theoretical mass are necessary in JIS due to
specified in JIS. business practices
performed in Japan.
13 Tests 13.1 Chemical analysis 5.1 Heat analysis shall Alteration ISOs do not specify concrete JIS and ISOs have
be performed by the sampling method or different standard
manufacturer. analytical method. structures. Concrete
Product analysis JIS specifies both concretely. specifications are required
shall be performed in JIS.
by the purchaser,
where necessary.
(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
13 Tests 13.2 Plating bath ISO 3575 Addition JIS specifies the test method Submission of a proposal
(concluded) composition test ISO 4998 of plating bath composition. regarding this addition,
along with the addition of
specifications of plating
bath composition, to ISO
will be considered.
13.3 Coating test 6.2 Coating mass Addition Requirements for corrosion The item has been added
7.2 determination and resistance test of coating, as to JIS because the
coating adherence agreed between the purchaser may request the
determination Alteration purchaser and the submission of corrosion
manufacturer, have been resistance test data.
added to JIS. No technical deviation.
JIS states coating mass
determination, which is
specified in ISO, in Annex JC
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to Annex JE
13.4 Mechanical test 6.1 Test pieces and test Alteration Requirements for the shape The shape of tensile test
7.1 methods for bend of tensile test piece and the piece specified is unique to
test and tensile test test method differ between JIS.
JIS and ISOs.
14 14.1 Inspection 12 Inspection Alteration JIS specifies requirements JIS and ISOs have
Inspection for inspection for each item. different standard
and structures.
reinspection 14.2 Reinspection 9 Reinspection Alteration JIS specifies that the retest No technical deviation.
shall be performed in
accordance with 9.8 of JIS G
0404.
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(I) Requirements in JIS (II) Inter- (III) Requirements in (IV) Classification and details of technical (V) Justification for the
national International Standard deviation between JIS and the Interna- technical deviation and
Standard tional Standard by clause future measures
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No. and Content number No. of Content Classifica- Detail of technical deviation
title of clause tion by
clause clause
15 Marking Marking ISO 3575 8 Marking Alteration Symbols for roofing and JIS and ISOs have
ISO 4998 14 architectural siding and different standard
symbols for corrugated structures.
sheets have been added to
JIS.
16 Items to Items to be confirmed 15 Items to be Alteration Requirements for JIS and ISOs have
be at the time of ordering confirmed at the dimensions for corrugated different standard
confirmed time of ordering sheets have been added to structures.
at the time JIS.
of ordering
17 Report Report Addition Report requirements have Report requirements are
been added to JIS. necessary in JIS because
reporting has been
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conventionally performed
in Japan.
Annex JA Nominal thickness and Addition Requirements for sheets and Requirements are
(normative) symbol for coating coils for roofing and necessary due to the
mass of sheet and coil architectural siding have particular uses.
for roofing and been added to JIS.
architectural siding
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3 Terms and Deletion The clause has been deleted Terms are defined in JIS G
definitions from JIS. 0203.
10 Resubmission for Deletion The clause has been deleted The item is specified in
acceptance when from JIS. JIS G 0404.
products have been
rejected during
earlier inspection
12 Attendance Deletion The clause has been deleted The item is specified in
inspection from JIS. JIS G 0404.
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