Aisyah 2018 J. Phys. Conf. Ser. 1007 012063
Aisyah 2018 J. Phys. Conf. Ser. 1007 012063
Aisyah 2018 J. Phys. Conf. Ser. 1007 012063
Series
E-mail: *[email protected]
Abstract. UMM Vertical Ball M ill (UVBM) was intended to be the apparatus to produce metal
powder with superior characteristic in production rate while retaining good quality of metal
powder. The concept of design was adopting design theory of Phal and Beitz with emphasis on
increasing of probability of success in engineering and economy aspects.Since it was designed
as vertical ball mill, a new way to produce powder, then it need to be tested for the
performance after manufactured. The test on UVBM was carried out by milling of alu miniu m
chip for 5 (five) d ifferent milling time of 0.5 hours, 1 hour, 3 hours, 5 hours and 7 hours, and
the powder product then be characterized fo r it mo rphology and size using Scanning Electron
Microscope (SEM) and Sieve.The results of the study were the longer of the milling time, the
finer of the powder. Fro m the test results of SEM, the morphology of the powder with 5
variations of milling time were most of the powder in form of flake (flat), s mall round and
angular (irregular). The distribution of powder size was best obtained on the variation of
milling time 3 hours, 5 hours, and 7 hours with percentage of 200 mesh in size of 22.14 %, 64
% and 91.25 % respectively.
1. Introduction
Powder metallurgy is a process in transforming metal powder or its alloy with certain size and
distribution into product without melting process [1]. Aluminium is categorized as light material and
has good corrosion resistant, good conductor properties and other superior properties compared to
other. Because of its popular application, it is one of the materials available in metal powder stock.
Ball mill (BM) is one of the instruments / apparatus to produce metal powder. In terms of the
capability, the powder may have micrometers or even nanometers in size. The mill consists of a vial
(cylinder tube) to contain the materials and crusher balls. The mill then is rotated or vibrated in high
frequency, depend on the necessity. It makes the materials which are trapped between ball crusher and
vial wall will be deformed caused by crushing action between ball and vial wall. The deformation of
material makes fragmentation of material structures to smaller structure [2].
Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution
of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.
Published under licence by IOP Publishing Ltd 1
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
In industry, BM has important role in industry to produce powder both for big and small scale
industry. To produce fine metal powder, it always need a crusher which suitable with its function and
design. There are many type of ball mill to produce powder, one of them are Electric Discharge
Assisted Mechanical Milling (EDAMM). This type of ball mill combined ball mill action and electric
discharge to synthesize and process metal by promoting rapid transformation of freshly fracture
particles and ions associated with the generated dusty plasma. Therefore, it works on the principle of
interface transformation rather than diffusional transformation. In was proven that ball mill was able to
produce powder both SiC and HfCN [3] [4].
In this research, we designed and tested of indigenous design and less advance of UVBM to
produce aluminium powder with further goal to produce micro or even nano in size. This effort is
important because nano size particles have taken over the material for drugs to be more efficient;
cellular phone and laptop which is smaller in size and more efficient; and the car which more eco-
friendly, etc.
2.1. Aluminium
Aluminium was f founded by Sir Humphrey Davy in 1809, it was first reduced from its ore by H.C.
Oersted in 1825. Aluminium also found in alloyed metal to increase it mechanical properties by
adding Cu, Mg, Si, Mn, Zn, Ni. The addition also makes the alloys have good corrosion resistant, wear
resistant and low expansion coefficient [5]. There are many application of aluminium powder such as
for rocket propellant, personal hygiene equipment, boosting reliability of computer, refine several
exotic materials, as frame materials for car and aircraft to save weight. Its application includes the
parts for structural and non-structural one and is the key for developments of aluminium alloys [6].
2
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
START START
Redesign Preparation
SEM Sieving
Assembly
Data Analysis
Comply with
Design Objective?
Conclusion
Yes
No
END END
(a) (b)
Figure 2. Flow chart of (a) design of UVBM and (b) testing of UVBM.
3. UVBM
3
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
220 V electric motor (Aliens) with 1400 rpm, reduced to 60 rpm by a pulley drive.
Pulleys was manufactured from cast iron with dimensions of 13 mm, 78 mm, and 300 mm
V-belt was type A.
Shaft was manufactured from cast iron with 12 mm in diameter.
And frame was manufactured from steel box with dimension of 30 x 30 x 2 mm.
3.3.1. Morphological analysis by SEM.Figure 4 shows SEM microphotograph of grinded aluminiu m alloy
(powder) by varying of milling times of 0.5 hours, 1 hour, 3 hours, 5 hours, and 7 hours. It was shown that most
of the powder is in flake form and small fraction has circular, oval or irregular shape. In time variat ion of 0.5
hours, it can be seen that powder size is bigger and coarser than other time variation and mostly in flake shape.
When the milling time getting longer, then the powder become finer. For milling time of 1 hour, the powder also
became finer eventhough the shape still in flake. 3 hour of milling time variation made the powder became finer
and other shape of powder, i.e. oval, circular and irregular, start to form. For last two time variations, i.e. 5 an d 7
hours, the trend was also observed. More powder has finer size and the shape also varied in form of oval, circu lar
and irregular shape. Also, it was observed that the thickness of the powder become thinner. The shapes for time
variation of 5 hours were do minated by flake and irregular shape while for t ime variation of 7 hours was flake.
(d) (e)
Figure 4. SEM of aluminium powder with milling time variations of
4
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
(d) (e)
Figure 5. SEM of alu miniu m powder for size analysis with milling time variations of
Determination of powder size was conducted by SEM and sieving. Figure 5 show SEM microphotograph of
alu min iu m powder with 5 milling time variations of 0.5 hours, 1 hour, 3 hours, 5 hours, and 7 hours. It can be
seen that the size of powder was varied because of deformat ion effect caused by crushing fo rce fro m crusher ball
on aluminiu m. The tabulation of size of powder was given in Tab le 2 and the distribution was presented in
Figure 6 above. Fro m the table, the average size of powder fro m time variation of 0.5 hours, 1 hour, 3 hours, 5
hours, and 7 hours was 2028 µm, 753.6 µm, 259.6µm, 158.4µm, and 135.2 µm respectively .
5
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
Graph in Figure 6 above shows mass percentage of metal powder for time varying of 0.5, 1, 3, 5,
and 7 hours using 24 ball crusher of 16 mm. From the graph, it was shown that longer milling time
gives finer size distribution. The centrifugal force act on rusher ball initiated by rolling ball mill’s vial
makes balls fell into the powder in the top curvature of ball mill and gave crushing effects. This
crushing effect made chips deformed and broke into powder. The longer of milling time made
crushing effect become obvious and finer powder was produced in larger number.
Another method of ball mill, i.e. horizontal one [8], produced finest powder at 500 rpm, followed
by 700 rpm and 450 rpm. The crusher ball which gave finest one were 5 crusher balls with diameter of
42 mm, then 8 crusher balls with diameter of 27 mm, followed by 6 crusher balls with diameter of 42
mm then 6 crusher balls with diameter of 27 mm, and the last ones were 4 crusher balls with diameter
of 42 mm and 7 crusher balls with diameter of 27 mm, the results from this results is better as depicted
in Figure 7 below.The main differences in the process was for vertical ball mill gave stronger crusher
effect compare to horizontal one so that finer powder produced.
Figure 7. Comparison between our research and Oksaria’s [8] one on percentage of sieving mass.
4. Conclusion
Regarding the results of the research, it can be concluded that longer the milling time will give finer
powder. The morphology of the powder shows that the dominant shape was flake followed by circular
and angular (irregular). Milling time of 7 hour produced finest powder with flake shape. Size
distribution of 5 (five) different milling time shows different trends and mainly caused by deformation
on aluminium chip caused by crusher balls.
6
MECnIT IOP Publishing
IOP Conf. Series: Journal of Physics: Conf. Series 1007 (2018)
1234567890 ‘’“” 012063 doi:10.1088/1742-6596/1007/1/012063
The size distributions of powder product are as follows. On 5 (five) variations of milling time, i.e.
0.5 hours, 1 hour, 3 hours, 5 hours, and 7 hours the average size were 2028 µm, 753.6 µm, 259.6 µm,
158.4 µm, and 135.2 µm. The finest size distribution was on 7 hours of milling time, followed by 5
hours and 3 hours with mesh 200 were 91.25%, 64%, and 22.14% respectively.Compared to another
type of ball mill, i.e. horizontal one, the trend for size distribution were similar with the longer time to
mill and more crusher ball employed will give finer powder but our design give faster time.
References
[1] Suresh S., Mortensen A., and Needleman A., (1993). Fundamentals of Metal-matrix
Composites, Butterworth-Heinemann
[2] Maurice, D., and Courtney, T. H., (1996). Milling dynamics: Part II Dynamic of SPEX mill and
a One-dimensional Mill, Metallurgical and Materials Transactions A, Volume 27A, July,
pp.1973-1979
[3] Aisyah I.S.,Wyszomirska M., Calka A., and Wexler, D. (2017). Nitrogenation of hafnium
carbide powders in AC and DC plasma by Electrical Discharge Assisted Mechanical Milling.
Journal of Alloys and Compounds. 715, pp. 192-198
[4] Aisyah I.S., Wyszomirska M., Calka A., and Wexler, D. (2016). Rapid transformation of
hexagonal to cubic silicon carbide (sic) by electric discharge assisted mechanical milling. 36,
pp. 1177-1186
[5] Surdia,T., and Saito,S., 1995, Pengetahuan Bahan Teknik, PT. Pradnya Paramita, Jakarta
[6] Gurganus, T.B., 1995, Aluminum Powder Application, Advanced Materials and Processes
Journal, Volume 148, Issue 2
[7] Phal. G, and Beitz. W (1977), Engineering Design. Berlin, Heidelberg
[8] Tasha Oksaria.(2014). Pengaruh kecepatan putar drum dan jumlah bola penumbuk pada ball
mill terhadap distribusi ukuran serbuk duralumin. Jurnal, Universitas Brawijaya