CH PJ
CH PJ
CH PJ
TEACHER’S SIGNATURE
S. NO. TITLE PAGE NO.
1. Aim 1
2. Introduction 2-3
3. Theory 4-09
4. Experiment 10
5. Procedure 11-12
6. Observations 13
7. Result 13
8. Bibliography 14
AIM OF THE
EXPERIMENT
Extraction of
essential oils
present in
Saunf(Aniseed),
Ajwain (Carom)
and Elaichi
(Cardamom)
INTRODUCTION
An essential oil is a concentrated
hydrophobic liquid containing
volatile aroma compounds from
plants. They are also known as
volatile oils, ethereal oils, aetherolea
etc. Essential oils are made up of
highly volatile substances which can
be extracted from numerous plant
species. Distillation based recovery
processes such as steam and
vacuum distillation are preferred for
the extraction of essential oils from
plant materials. Virtually all
naturally occurring essential oils are
made up of hydrocarbons such as
camphene, pinene, limonene,
phellandrene, cedrene, and
oxygenated hydrocarbons such as
alcohols, aldehydes, esters, ethers,
ketones, lactones, phenols and
organic acids.
The essential oil get their odours from the
oxygenated
d compounds contained in them
and these confer stability on the oil against
oxidation. The hydrocarbons are less stable
and they are responsible for the
degradation observed in the oils. The
hydrocarbons contained in the essential oils
are often removed so that the oils can be
more stable and still retain their odours and
flavours. Essential oils made up of highly
numerous plant species, Distillation based.
ANISEED OIL (SAUNF)
Common Method of
Extraction: Steam Distillation
Botanical Name:
Pimpinella anisum
Colour: Clear
Aromatic Description: Distinctive scent of
licorice. Rich and sweet.
Constituents: a-pinene, camphene, B-
pinene, linalool, cis-anethole,
transanethole, safrole, anisaldehyde,
acetoanisole.
Uses:
In aromatherapy, aniseed essential oil is
used to treat colds and flu
Aniseed oil can be made into a liquid
scent and is used for both hunting and
fishing. It is put on fishing lures to attract
fish.
a Anethole, the principal component of
anise oil, is a precursor that can
eventually produce 2,5-
dimethoxybenzaldehyde which is can be
used in the clandestine synthesis of
psychedelic drugs such as 2C-B, 2C-I and
DOB.
Oil of aniseed is also reported to be used
as an aromatic carminative to
relieve flatulence, and as an ingredient of
cough lozenges in combination with
liquorice.
Essential oil is also used externally as an
insecticide against small insects such as
head lice, mites and vermin. It also has
fungicidal properties.
CAROM OIL(AJWAIN)
Botanical name: Trachyspermum
ammi
Common Method of Extraction:
Distillation
Aroma: Warm, Pungent, Peppery
Extraction: Ajwain oil is extracted
from the crushed seeds of ajwain by
the method of steam distillation.
Chemical composition:
The main constituents of the ajwain
oil are thymol, gamma-
terpinene,pcymene, and beta-
pinene. Alpha-pinene, alpha-
thujene, beta-myrcene, carvacrol.
limonene,
d and terpinene-4-ol. There are
variations in the composition of ajwain
oils, depending upon the region where it is
cultivated. For instance, ajwain oil
collected from Southern India is rich in
thymol.
Uses:
Skin Ailments: Ajwain can help with
pimples.
Digestive Aid: One can treat indigestion,
ulcers, and various other bacterial
infections of the gut with ajwain seeds
and essential oil.
Aromatherapy: Useful in aromatherapy,
ajwain oil offers calming sensations that
relieves neuralgia and migraines.
CARDAMOM OIL
(ILLAICHI)
Extraction: Cardamom oil is extracted
using steam distillation method.
Botanical Name: Elettaria
cardamonum
Common Method Of Extraction:
Steam Distillation
Aroma: Very complex and smooth
spice aroma ,the fruit are used just
before they ripe. The yield through this
process is normally 1 to 5 per cent.
Chemical Composition:
Cardamom oil contains sabinene,
myrcene, a-pinene, b-pinene,
aphellandrene, limonene, p-cymene,
terpinolene, 1,8-cineole, y-terpinene,
linalool, linalyl acetate, a-terpineol
acetate, citronellol, nerol, terpinen-4-
oil, aterpineol, geraniol, methyl
eugenol and trans-nerolidol.
e
Uses:
Cardamom oil has a vast range of usage
for treatment of sciatica, coughs,
abdominal pains, spasm and nervous
disorders.
Traditionally, it is used for pulmonary
disease, fever, digestive and urinary
problems in India and China for over
3000 years. It is also used to flavour
pharmaceutical products.
Apart from pharmaceutical usage,
cardamom oil is also used as a fragrant in
soaps, perfumes and cosmetic products.
EXPERIMENT
Materials Required:
Steam Generator (Copper Vessel)
Round Bottom Flask (500 Ml)
Conical Flask
Condenser
Glass Tubes
Iron Stand
Sand Bath
Separatory Funnel
Tripod Stands
Burners
Ajwain (carom)
Petroleum Ether (60-80°c)
Saunf (aniseed)
PROCEDURE:
1. Set the apparatus as shown in the
picture of Experimental Setup. The
apparatus consists of a steam generator
connected to the round bottom flask
through a glass inlet tube. The flask is
connected to a water condenser
through a glass outlet tube. Condenser
is further attached to a receiver through
an adaptor.
2. Take about 750ml of water in the
steam generator and start heating to
produce steam.
3.In the round bottom flask take about
75g of crushed saunf (aniseed).
4. A vigorous current of steam from
steam generator is passed through the
round bottom flask.
5. A part of the steam condenses in
the round bottom flask. As more and
more steam is passed, the steam
volatile components of saunf pass
through condenser along with steam.
These contents on condensation are
collected in the receiver.
6. The contents in the round bottom flask
may be heated by a Bunsen burner to
prevent excessive condensation of steam.
a The process of steam distillation is
7.
continued for about half an hour.
8. Transfer the distillate to a separating
funnel and extract with 20ml portions of
petroleum ether 3 times.
9. Combine the petroleum ether extracts in
a 250ml conical flask and dry it with the
help of anhydrous sodium sulphate.
10. Remove the solvent from the dried
filtrate by careful distillation in a water
bath. The essential oil is left behind in the
distillation flask.
11. Find the weight of the extracted
essential oil. Note the color, odour and
weight of the essential oil.
OBSERVATIONS:
Saunf (aniseed):
Weight Of Saunf Taken = 100g
Weight Of Bottle + essential Oil = 11.25g(y)
Initial Weight Of The Bottle = 10g(x) Weight Of
Essential Extracted= (y-x) = 1.25g
Percentage Of Essential Oil= (y/100)*100 =1.25%
Color Of The Oil = Colorless
Odour Of The Oil = Saunf Like Smell
Ajwain (carom):
Weight Of Ajwain Taken =75g
Initial Weight Of The Bottle =10g(x)
Weight Of The Bottle + essential Oil =11g(y)
Weight Of Essential Oil Extracted= (y-x) =1g
Percentage Of Essential Oil (Y/75)*100 = 1.33%
Colour Of The Oil = Colorless
Odour Of The Oil = Ajwain Like Smell
Result:
Essential Oils Present In Aniseed, carom And
Cardamom Are Extracted From This Method.
BIBLIOGRAPHY
www.slideshare.net
www.zemvelocare.com
www.katyaniexports.com
www.icbse.com