1300 EC1986 Signed

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MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC1986 Date : 23.10.2023


Invoice No.:WIF/EX/23-24/ Date :
P.O. No.: 4500789133 Line Item: 00010 PO Date : 06.10.2023 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)
P.O. Ver. 3
Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT PLUG Forged,
1300 VALVE 2 ULT150 F/UNION P537156 Rev D Normalized 7.21 : 1 176 Nos AISI 4140 BF-EOF-LRF-VD-CCP
ENDS AISI 4140 ALLOY STEEL Quenched &
FMC SPEC M25070 Tempered, - JSW STEEL LTD
Shot Blasted
Heat Code: OTP DU500006672 Rev B
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Ni Grain Size
F17881 0.40 0.91 0.20 0.007 0.012 1.05 0.22 0.22 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 - -
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AG-717 HT Batch No. of Q&T:- AG-718 Qty :- 176 Nos
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 7.21 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 31°C 47°C 570°C 5 Hrs (Air Cool)
Forging 7.21 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 31°C 47°C 570°C 5 Hrs (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details


Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure


Note :- We hereby guarantee no weld repairs performed.
. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, heat treatment batch "AG-718" stamped near to Heat code.
The above material meets the requirement of ASTM A788/A788M : 23
Forging Method - Closed Die Forging

Ajay Joshi (HEAD-MQC, HT & NDT)


Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819


Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) [email protected]
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC1986


P.O. No.:- 4500789133 Line Item: 00010 PO Date : 06.10.2023 Date : 23.10.2023
BODY FORGING, ULT PLUG VALVE 2
Item : ULT150 F/UNION ENDS AISI 4140 ALLOY Material : AISI 4140
STEEL FMC SPEC M25070

Part No : P537156 Rev D Heat No. : F17881


Drawing No.: DU500006672 Rev B Ambient Temp : 26°C
Die No.: 1300 Hardness Range:- 277 - 331 HBW
Qty.: 176 Nos Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AG-717 QT: AG-718 Sr No.: 09/2021-036
Reference Standard: ASTM E10 Machine Make: SAROJ
Load Applied: 3000 Kgs Calibration Agency: MTMS
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: MATRIX/CAL/2022-23/12/4205

Std Block Details: SH-2831/23 (Hardness value - 304.0 HBW) Calibrated On: 09.12.2022

Entity Performing Test: WIF Sanaswadi Calibration Due On: 08.12.2023


Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 11 & 14.10.2023
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW


176 Nos 285-321 HBW

Test Performed By Reviewed By Approved By :


Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016


CERTIFICATE OF COMPLIANCE
Customer : TechnipFMC TC No.: EC1986
Date: 23.10.2023
Die No. : 1300 Heat Code : OTP
PO No : 4500789133 Line Item No : 00010
Offer Qty. : 176 Nos
Part No/ Rev : P537156 Rev D Drg No / Rev : DU500006672 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
2 ULT150 F/UNION ENDS AISI 4140
ALLOY STEEL FMC SPEC M25070

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F17881

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 8 Nos.
III. Secondary Process : Heat Treatment
A. Process Name : Normalised
Heat Lot No. : AG-717 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : AG-718 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI
Certificate No : NA Process Spec : NA

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, heat treatment batch "AG-718" stamped near to Heat
code.
The above material meets the requirement of ASTM A788/A788M : 23
Sign with Stamp
Ajay Joshi (HEAD-MQC, HT & NDT)
Mechanical Test Annexure
Die No.: 1300 Material Grade: AISI 4140

Heat No.: F17881 HT Lot No. : AG-718

Heat Code: OTP TC No. : EC1986

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA


Test Temp. NABL Lab Sample
Specimen 4710045571 H.T. 0.2 % Offset
(⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below
L 311, 321 Ambient G-23-1105-P 1 146.22 126.54 21.11 64.49
HT Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
86 70 70 75.33
Single - 32 J Min
LE - 0.51 mm Min -29°C G-23-1106-P 1.00 0.86 0.87 0.91

%Shear - Report 60 55 55 56.67


L 1
Avg. - 27 J Min
56 50 42 49.33
Single - 20 J Min
LE - Report -40°C G-23-1107-P 0.67 0.61 0.52 0.60

%Shear - Report 45 40 35 40.00


0.5" below
HT Surface Avg. - 28 J Min
56 52 38 48.67
Single - 18.7 J Min
LE - Report
-29°C G-23-1108-P 0.78 0.72 0.51 0.67

%Shear - Report 45 45 30 40.00


T 1
Avg. - 20 J Min
48 32 48 42.67
Single - 14 J Min
LE - Report -40°C G-23-1109-P 0.62 0.47 0.61 0.57

%Shear - Report 40 25 40 35.00

Ajay Joshi (HEAD-MQC, HT & NDT)


Authorised Signatory

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