Test Work
Test Work
Test Work
material. The status of the mine production schedule is very • Waste and dilution from mining
important. Using a preliminary mine plan that is likely to The inclusion of an appropriate percentage of dilution
change, as a basis for the composite sample preparation can material is important to the development of the physical and
lead to poor correlations between the mine and metallurgical chemical testwork program. Particular types of waste
testwork head grades or ore, which can reduce the accuracy material can have deleterious effects on the metallurgical
of the BFS. response of ore types, for example the content of a graphitic
• Use of specialised consultants for some sections of the component in a gold or flotation plant. The inclusion of
testwork program, eg filtration and thickening. waste should be representative of the mining plan, eg if the
• Factorial designed metallurgical testwork can significantly physical testwork is carried out on 30 per cent dilution, yet
reduce the timing of metallurgical testwork programs due to the mining plan has only 15 per cent dilution, then the
a number of factors: testwork can lead to an oversized comminution circuit.
- reduce the amount of sample required per test; Alternatively the inclusion of waste into the program can
indicate that from particular ore zones no more than X per
- reduce the amount of time per test; cent of the hanging or footwall can be delivered to the
- statistically verify a circuit or reagent regime with a process plant. This can then set key performance indicators
higher level of confidence; and for the project design for the mine as well as the process
- simple to set up. plant.
The level of detail required for the metallurgical testwork The selection of the amount of waste/ore ratio that should be
program governs the BFS. Generally the data presented above is included in the sizing of the comminution circuit must be
a good starting point for considering deadlines for the BFS and carefully scrutinised. Grinding circuits are generally the
important points to consider with the schedule of the highest power user and the highest capital cost item of the
metallurgical testwork program. plant. In using a too high or low number for the waste/ore
ratio in sizing the grinding circuit can result in either an
oversized or undersized grinding circuit.
PLAN FOR THE METALLURGICAL TESTWORK
• Composite samples should represent the orebody as mined.
PROGRAM
The number of composite samples selected should be based
Planning of a metallurgical testwork program requires careful on the number of different ore types and aim to represent the
consideration of a number of factors to ensure that the data mining production schedule. One of the important outcomes
produced meets that required for a BFS. The metallurgical from the metallurgical testwork program is the predicted
testwork should also generate sufficient information for the cash flow forecast based on the mining production schedule.
optimisation of the process economics and reliable data to be Hence the metallurgical testwork must represent the expected
used in the process plant design. ore feed grades from the mining schedule for an accurate
The initial plan for the testwork will be most likely based on performance prediction of the metal grade and tonnage
the previous testwork. The following are points that should also produced. Different ore types affect the cash flow generated
be raised at this stage: from the project due to the metal tonnes produced and the
• what other orebodies of this type are globally mined? operating costs. Hence if different ore types react quite
differently and are mined in different periods, the effect of
• what is the process used for extraction? this must be included in the financial model.
• who are the experts in this field? The composite samples should represent the orebody as
• can operations with similar process unit operations and ore relevant treatment periods, including any deleterious material
types be contacted to understand their experiences? that will be expected during the production period.
In developing the metallurgical testwork program the • Testwork schedule in reference to the BFS requirement
following should be considered: There are a number of key milestones that need to be met to
• Geological and mineralogical features of the orebody. finish the BFS on time. This becomes very important if a
The mineralogical assessment of the orebody is an important presentation to the decision-makers is required at a set date
initial phase and money invested correctly initially can and the BFS schedule is aimed at this date. This sets the
significantly improve the process economics of the orebody. focus on the testwork program output and can define the
This is especially the case for flotation studies and the use of project success.
diagnostic leaching for gold. There are cases where the same • Selection of an appropriate laboratory facility
orebody has been proven uneconomical for some companies There are a number of laboratory facilities with differing
and proven economical by others due to the mineralogical capabilities and this can be important in optimising the
information. This includes the assessment of the different ore testwork program data. The criteria for laboratory selection
types, grain size of valuable mineral, association of valuable should involve some of the following; delivery of reports, the
mineral to contaminants and liberation characteristics. The quality control practices in use, experience with similar types
mineralogical program should be compiled to highlight of material, examples of testwork programs being completed
differing ore types and be combined with the geological on schedule and budget, how often does the company review
structure of the ore horizon. testwork or brain storm ideas throughout a program. A
The geological structures can provide hints to the behaviour laboratory can be effective with a gold testwork program but
of the ore types. For example a drilling program may find not so with flotation.
that the ore was competent to drill in some sections and drill • Consideration for tailings disposal
bits were worn frequently, giving an indication to the
hardness/abrasiveness of certain ore zones. Major faults can This is an area that needs special consideration, depending
provide the basis for differing ore types and certain on the location of the project and the environmental
geological zones can contain excessive states of oxidation, considerations. The timing of this type of testwork is also an
which highlights mine to mill planning issues during ore important factor due to the length of time required for the
extraction. This can lead to a specific metallurgical testwork environmental and backfill testwork, if required. For an
program that confirms these preliminary inferences. underground operation the advantage of storing tailings
underground can be very attractive and can improve the
mining production schedule and environmental factors. The • a record of which samples were in each drum was displayed
testwork required for the potential of the sulphide flotation on the side of each drum.
tailings to be acid producing and the detoxification of a These samples arrived at the metallurgical laboratory with no
cyanide gold tail is very important and needs special oxidation evident.
consideration.
The tailings treatment can add significant costs to the project, Detail of the metallurgical testwork program
depending on the size, storage requirement, type of tailings
and environmental considerations and hence is an important Common to both gold and flotation testwork programs are the
section of any BFS metallurgical program. The curing times following:
for the backfill strength determination can be in the order of • size by size head assaying and mineralogical or diagnostic
30 to 60 days and this then becomes a critical path item for leaching for gold on composite samples and intermediate
the testwork program. Hence if backfill testwork is required products;
then a tailings sample may need to be produced as a priority. • specific gravity determination and bulk density of the
composites; and
Example of a composite sample preparation • physical testwork.
On a recent feasibility study, before commencing composite Following the initial leach/float tests the final grind size is
sample preparation, all the drill hole intercepts from the drilling determined and from this the Bond Ball Mill Work Indices
program were listed and those for which samples were available (BBMWI) can be determined for the various composites. In
for metallurgical testwork identified. The available intercepts conjunction with the leach tests other grinding testwork can
were then reviewed to assess whether they would fall within a be started. If SAG milling is to be part of the treatment route
mineable zone. This was done in conjunction with the consultant than the SAG Mill determination could be carried out, such
mining engineers. as the JKTECH Drop Weight Test or Advance Media
Competency Test (AMC). If no SAG milling testwork is to
To meet the mineable criteria an intercept had to: be completed then Impact Crushing Work Indices,
• include a minimum of 0.5 m hanging wall waste and 0.5 m of Unconfined Compression Tests (UCS) and Bond Rod Mill
foot wall waste to allow for mining dilution; Work Indices (BRMWI) should be determined. For the UCS
• have a minimum mining width of 4 m, if necessary by the data it is the type of breakage, axial or cleavage that is
inclusion of more hanging wall and foot wall dilution; important, as well as the number generated. Abrasion Indices
• after inclusion of the above dilution, exceed a cut-off grade (AI) do provide a guide to the type of material, however the
of one per cent Cu; and method of AI determination results in a wide variation of
• fall within an area that would be mined. results.
Each 1 m interval was assayed for copper and sulphur and then • Scoping tests based on previous results.
composite samples of each drill hole were made up from the 1m It is generally a good idea to reproduce the previous test
intervals and included the required percentages of the hanging results such that a statistical base line can be developed and
wall and footwall dilution. subsequently use this for the optimisation tests.
• Optimisation testwork and grade/recovery.
Sample handling - use of factorial design; and
Delivering the sample in the best condition to the laboratory - reagent screening – completed to a level of detail that
reduces the risks and optimises the project economics.
facility requires a number of controlling factors:
• the need for a well defined procedure for sample collection, • Tailings testwork.
bagging and delivery to the laboratory; - backfill testwork, tailings dam and environmental tests
can all take considerable time and hence the schedule
• a disciplined field team that understands the importance of
should highlight these as key milestones.
sample preservation and procedure;
For a typical Gold BFS the following tests are carried out:
• minimising the amount of times the sample is handled; and
• minimising the movement of the sample in and out of a • Leach tests on variable grind size, cyanide or alternative
extraction levels, leach times.
freezer.
The storage and transportation of the core is very important
- economic evaluation of the optimum grind size;
when dealing with sulphidic ores that are subject to oxidation. - determines what the grind size for BBMWI
Not only does the metallurgical testwork program aim to determination should be;
measure the oxidative effect but the program also requires fresh - can compare resin vs carbon;
unoxidised sample. A recent procedure below was used - predict the leaching kinetic behaviour of the ore for plant
successfully on a highly oxidative ore: predictions; and
• PQ core extraction and frozen at approximately minus19°C; - determine level of, for example, kerosene required.
• removed from the freezer; • Leach tests with variable degrees of dissolved oxygen levels.
• geological logged; - determine if supplied oxygen is a requirement.
• samples were then cut for metallurgical testwork; • Diagnostic leaching to determine gold deportment with size
• each cut metallurgical sample was wrapped in a foil bag, by size analysis.
which was purged with nitrogen and then wrapped in cloth. • Rheology of slurry.
A nametag describing each sample was placed inside the The rheology of the slurry is important in the design of the
cloth bag. layout of the leach tanks due to head losses. The maximum
• the cloth bag was then placed in a drum, and a document feed density can often be set by the slurry rheology and
placed on top of all the samples in the drum describing what hence can have a tremendous impact on the volume of cells
was in the drum; required. The slurry rheology is also a critical parameter for
• the drum was then purged with nitrogen and sealed; and the design of mixers and interstage screens.
• Carbon adsorption kinetics. - the final per cent moisture is important in determining
Determine the amount of carbon per leach tank that is concentrate transport operating costs and self-heating
required to produce a targeted final solution gold and/or properties.
silver grade. • Bulk density of filtered concentrate.
Loading of the precious metal onto carbon determines the This information is used for the sizing of the concentrate
size of the desorption circuit and the rate of change that this storage area, which can be a significant cost in some cases.
occurs is an important design number. In most studies benchmark numbers are used.
• Carry out cyanide detoxification testwork on tailings. • Regrind of intermediate concentrates.
- Determine the amount of reagents and retention time - fine grinding testwork can require up to 20 kg of sample
required to reduce the total cyanide to the accepted level. for a BFS standard and hence a pilot plant is required.
• Residence Time Distribution techniques • Full suite of assays for concentrate analysis.
Aids in determining the retention time required in the leach Normally an ICP analysis is completed for marketing and
system and combined with the leach kinetic data can aid in evaluating the impact the penalty elements and/or minor
predicting plant behaviour and thus improve the level of payable elements on the sale of concentrate. An accurate
confidence of the BFS. picture of the concentrate metal and gangue content is useful
For a typical flotation BFS the following tests are carried out: as base line assays.
• Mineralogical examination of the selected composites • Use of site and aged water tests.
This is an important phase that can determine the The determining of the likely effect of recycling process
dissemination of minerals and classification of the various water is very important to deciding on maximum or
ore types. For larger corporations with a technical base, the minimum water recovery. Recycling of water from tailings
mineralogical information can be compared with an internal and concentrate thickeners can be very important for some
database, which can be very valuable to understanding the operations. If water cannot be recycled or requires alternative
ore treatment options. The information is helpful in treatment before being used, this can add a significant cost to
understanding the association of the valuable mineral with the process design.
penalty elements and defining these zones within the • Aged ore tests
orebody.
Determine the expected oxidation rate of the ore, which can
• Factorial design to select optimum conditions produce a guide to the type of reagent regime required, if
- only requires 500 grams per test and produces results for pre-aeration is required and what the live crushed ore
reagent screening, pH conditions and grind size stockpile retention times should be. In some cases the size of
determination in a timely manner. the ore feed can be defined as a way of trying to reduce the
• Batch flotation tests on the selected flowsheets. oxidation rate. A highly reactive ore, that is relatively soft,
The flowsheet selection is based on the grade/recovery would be best left as coarse as possible until it was ready for
required to achieve a targeted NSR value for the project. For processing.
example a 55 per cent Zn grade @ 80 per cent recovery may
be good enough but by adding a regrind and cleaning a COSTS OF METALLURGICAL TESTWORK
higher recovery can be achieved, however the cost of the
PROGRAM
extra installation must be considered. Sometime achieving
the highest recovery may be at the detriment of grade and The metallurgical testwork program costs are dependent on the
actually result in lower cash flows due to higher treatment type and number of tests and the required consultants time. The
and refinery charges. The opposite can occur, when the costs, exclusive of GST inclusive of sample preparation, for
highest recovery may be lower cash value of the valuable typical metallurgical testwork are presented in Table 1.
mineral, but higher precious metal recovery and result in Supervision of the testwork program by the metallurgical
higher cash flows. consultant requires about 24 to 32 hours per week for a BFS of 1
• Lock cycle tests on the selected flowsheet option. to 1.5 Mtpa. In addition, the engineer would also be required on
Correctly balanced locked cycle tests, based on density and a full time basis at beginning of the program for two weeks and
mass flow, can correlate well to the full production plant and towards the end for two weeks.
produces a guide to the type of recirculating loads expected. For a simple gold or flotation orebody (1 to 1.5 Mtpa) where
The densities in the cycle tests should aim to mimic those the testwork requirement is standard, with four composites and a
expected in the plant, sometimes this is difficult due to the bulk composite, the testwork expenditure can be of the order of
low mass recovery and maintaining balances. $A 160 000 to $A 180 000. Some simple gold or flotation
• Specific gravity of concentrate and tails samples. testwork programs can be of the order of $A 40 000 to
• Size by size data of concentrate and tailings sample. $A 70 000 for smaller orebodies or where the study may be an
The size-by-size analysis by assay, provides an invaluable expansion of an existing facility.
guide to the valuable mineral and gangue deportment which For a complex gold orebody (1 to 1.5 Mtpa) where the
can lead to the selection of reagents, determining the testwork requirement includes various process option
optimum grind size and flowsheet. assessments, such as gravity, flotation, bioleaching, pressure
• Concentrate/tailing filtration and thickening testwork. oxidation on four composites the testwork expenditure can vary
- this generally requires a pilot plant to generate enough from $A 180 000 for gravity/flotation option, up to $A 350 000
sample for concentrate testing. In some cases it could be for pressure oxidation.
cheaper to run a pilot plant to generate the quantity of For a complex flotation orebody (1 to 1.5 Mtpa) where the
sample required than from batch tests; testwork requirement includes various process option
- in some cases the concentrate sample is required for assessments, such as fine grinding on four composites the
potential buyers to test and analyse; testwork expenditure can vary from $A200 000 to $A300 000.
- the Transportable Moisture Limit needs to be determined The detail of the costs for completion of one composite for a
during this testwork and then either pressure or vacuum flotation and gold metallurgical testwork program are shown in
filtration should be decided upon; and Appendix 3. To use these numbers for the prediction of a
APPENDIX 1
Metallurgical schedule and BFS schedule.
APPENDIX 2
Detailed metallurgical schedule for a gold BFS.
APPENDIX 3
Detailed costs for a gold and flotation testwork program.
APPENDIX 3
Detailed costs for a gold and flotation testwork program.
APPENDIX 3
Detailed costs for a gold and flotation testwork program.