Designation: C88 − 05

Standard Test Method for

Soundness of Aggregates by Use of Sodium Sulfate or
Magnesium Sulfate1
This standard is issued under the fixed designation C88; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.

1. Scope C136 Test Method for Sieve Analysis of Fine and Coarse
1.1 This test method covers the testing of aggregates to Aggregates
estimate their soundness when subjected to weathering action C670 Practice for Preparing Precision and Bias Statements
in concrete or other applications. This is accomplished by for Test Methods for Construction Materials
repeated immersion in saturated solutions of sodium or mag- C702 Practice for Reducing Samples of Aggregate to Testing
nesium sulfate followed by oven drying to partially or com- Size
pletely dehydrate the salt precipitated in permeable pore D75 Practice for Sampling Aggregates
spaces. The internal expansive force, derived from the rehy- E11 Specification for Woven Wire Test Sieve Cloth and Test
dration of the salt upon re-immersion, simulates the expansion Sieves
of water on freezing. This test method furnishes information E100 Specification for ASTM Hydrometers
helpful in judging the soundness of aggregates when adequate E323 Specification for Perforated-Plate Sieves for Testing
information is not available from service records of the Purposes
material exposed to actual weathering conditions. 3. Significance and Use
1.2 The values given in parentheses are provided for infor- 3.1 This test method provides a procedure for making a
mation purposes only. preliminary estimate of the soundness of aggregates for use in
1.3 This standard does not purport to address the safety concrete and other purposes. The values obtained may be
problems associated with its use. It is the responsibility of the compared with specifications, for example Specification C33,
user of this standard to establish appropriate safety and health that are designed to indicate the suitability of aggregate
practices and determine the applicability of regulatory limita- proposed for use. Since the precision of this test method is poor
tions prior to use. (Section 12), it may not be suitable for outright rejection of
aggregates without confirmation from other tests more closely
2. Referenced Documents related to the specific service intended.
2.1 ASTM Standards:2 3.2 Values for the permitted-loss percentage by this test
C33 Specification for Concrete Aggregates method are usually different for fine and coarse aggregates, and
attention is called to the fact that test results by use of the two
salts differ considerably and care must be exercised in fixing
1
This test method is under the jurisdiction of ASTM Committee C09 on proper limits in any specifications that include requirements for
Concrete and Concrete Aggregatesand is the direct responsibility of Subcommittee these tests. The test is usually more severe when magnesium
C09.20 on Normal Weight Aggregates.
Current edition approved July 15, 2005. Published August 2005. Originally
sulfate is used; accordingly, limits for percent loss allowed
approved in 1931. Last previous edition approved in 1999 as C88 – 99a. DOI: when magnesium sulfate is used are normally higher than
10.1520/C0088-05. limits when sodium sulfate is used.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM NOTE 1—Refer to the appropriate sections in Specification C33 estab-
Standards volume information, refer to the standard’s Document Summary page on lishing conditions for acceptance of coarse and fine aggregates which fail
the ASTM website. to meet requirements based on this test.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
Copyright by ASTM Int'l (all rights reserved); Tue May 7 08:41:41 EDT 2013
1
Downloaded/printed by
(Turkey MOU- Online Access) pursuant to License Agreement. No further reproductions authorized.
 C88 − 05
4. Apparatus 5.1.1 Sodium Sulfate Solution—Prepare a saturated solution
4.1 Sieves—With square openings of the following sizes of sodium sulfate by dissolving a USP or equal grade of the salt
conforming to Specifications E11 or E323, for sieving the in water at a temperature of 77 to 86 °F (25 to 30 °C). Add
samples in accordance with Sections 6, 7, and 9: sufficient salt (Note 4), of either the anhydrous (Na2SO4) or the
crystalline (Na2 SO4·10H2O) form,3 to ensure not only satura-
150 µm (No. 100) 8.0 mm (5⁄16 in.)
9.5 mm (3⁄8 in.) tion but also the presence of excess crystals when the solution
300 µm (No. 50) 12.5 mm (1⁄2 in.) is ready for use in the tests. Thoroughly stir the mixture during
16.0 mm (5⁄8 in.)
600 µm (No. 30) 19.0 mm (3⁄4 in.)
the addition of the salt and stir the solution at frequent intervals
25.0 mm (1 in.) until used. To reduce evaporation and prevent contamination,
1.18 mm (No. 16) 31.5 mm (11⁄4 in.) keep the solution covered at all times when access is not
2.36 mm (No. 8) 37.5 mm (11⁄2 in.)
50 mm (2 in.) needed. Allow the solution to cool to 70 6 2 °F (21 6 1 °C).
4.00 mm (No. 5) 63 mm (21⁄2 in.) Again stir, and allow the solution to remain at the designated
larger sizes by temperature for at least 48 h before use. Prior to each use, break
4.75 mm (No. 4) 12.5-mm (1⁄2-in.)
spread up the salt cake, if any, in the container, stir the solution
4.2 Containers—Containers for immersing the samples of thoroughly, and determine the specific gravity of the solution.
aggregate in the solution, in accordance with the procedure When used, the solution shall have a specific gravity not less
described in this test method, shall be perforated in such a than 1.151 nor more than 1.174. Discard a discolored solution,
manner as to permit free access of the solution to the sample or filter it and check for specific gravity.
and drainage of the solution from the sample without loss of NOTE 4—For the solution, 215 g of anhydrous salt or 700 g of the
aggregate. decahydrate per litre of water are sufficient for saturation at 71.6 °F (22
°C). However, since these salts are not completely stable and since it is
NOTE 2—Baskets made of suitable wire mesh or sieves with suitable desirable that an excess of crystals be present, the use of not less than 350
openings are satisfactory containers for the samples. g of the anhydrous salt or 750 g of the decahydrate salt per litre of water
4.3 Temperature Regulation—Suitable means for regulating is recommended.
the temperature of the samples during immersion in the sodium 5.1.2 Magnesium Sulfate Solution—Prepare a saturated so-
sulfate or magnesium sulfate solution shall be provided. lution of magnesium sulfate by dissolving a USP or equal
4.4 Balances—For fine aggregate, a balance or scale accu- grade of the salt in water at a temperature of 77 to 86 °F (25 to
rate within 0.1 g over the range required for this test; for coarse 30 °C). Add sufficient salt (Note 5), of either the anhydrous
aggregate, a balance or scale accurate within 0.1 % or 1 g, (MgSO4) or the crystalline (MgSO4·7H2O) (Epsom salt) form,
whichever is greater, over the range required for this test. to ensure saturation and the presence of excess crystals when
the solution is ready for use in the tests. Thoroughly stir the
4.5 Drying Oven—The oven shall be capable of being
mixture during the addition of the salt and stir the solution at
heated continuously at 230 6 9 °F (110 6 5 °C) and the rate
frequent intervals until used. To reduce evaporation and
of evaporation, at this range of temperature, shall be at least 25
prevent contamination, keep the solution covered at all times
g/h for 4 h, during which period the doors of the oven shall be
kept closed. This rate shall be determined by the loss of water when access is not needed. Allow the solution to cool to 70 6
from 1-L Griffin low-form beakers, each initially containing 2 °F (21 6 1 °C). Again stir, and allow the solution to remain
500 g of water at a temperature of 70 6 3 °F (21 6 2 °C), at the designated temperature for at least 48 h before use. Prior
placed at each corner and the center of each shelf of the oven. to each use, break up the salt cake, if any, in the container, stir
The evaporation requirement is to apply to all test locations the solution thoroughly, and determine the specific gravity of
when the oven is empty except for the beakers of water. the solution. When used, the solution shall have a specific
gravity not less than 1.295 nor more than 1.308. Discard a
4.6 Specific Gravity Measurement—Hydrometers conform- discolored solution, or filter it and check for specific gravity.
ing to the requirements of Specification E100, or a suitable
combination of graduated glassware and balance, capable of NOTE 5—For the solution, 350 g of anhydrous salt or 1230 g of the
measuring the solution specific gravity within 60.001. heptahydrate per litre of water are sufficient for saturation at 73.4 °F (23
°C). However, since these salts are not completely stable, with the hydrous
salt being the more stable of the two, and since it is desirable that an
5. Special Solutions Required excess of crystals be present, it is recommended that the heptahydrate salt
5.1 Prepare the solution for immersion of test samples from be used and in an amount of not less than 1400 g/litre of water.
either sodium or magnesium sulfate in accordance with 5.1.1 or 5.1.3 Barium Chloride Solution—Prepare 100 mL of 5 %
5.1.2 (Note 3). The volume of the solution shall be at least five barium chloride solution by dissolving 5 g of BaCl2 in 100 mL
times the solid volume of all samples immersed at any one of distilled water.
time.
NOTE 3—Some aggregates containing carbonates of calcium or mag-
nesium are attacked chemically by fresh sulfate solution, resulting in 3
Experience with the test method indicates that a grade of sodium sulfate desig-
erroneously high measured losses. If this condition is encountered or is nated by the trade as dried powder, which may be considered as approximately
suspected, repeat the test using a filtered solution that has been used anhydrous, is the most practical for use. That grade is more economically available
previously to test the same type of carbonate rock, provided that the than the anhydrous form. The decahydrate sodium sulfate presents difficulties in
solution meets the requirements of 5.1.1 and 5.1.2 for specific gravity. compounding the required solution on account of its cooling effect on the solution.

Copyright by ASTM Int'l (all rights reserved); Tue May 7 08:41:41 EDT 2013
2
Downloaded/printed by
(Turkey MOU- Online Access) pursuant to License Agreement. No further reproductions authorized.
 C88 − 05
6. Samples of the separated fractions after final sieving and place in
6.1 The sample shall be obtained in general accordance with separate containers for the test.
Practice D75 and reduced to test portion size in accordance 7.2 Coarse Aggregate—Thoroughly wash and dry the
with Practice C702. sample of coarse aggregate to constant weight at 230 6 9 °F
6.2 Fine Aggregate—Fine aggregate for the test shall be (110 6 5 °C) and separate it into the different sizes shown in
passed through a 9.5-mm (3⁄8-in.) sieve. The sample shall be of 6.3 by sieving to refusal. Weigh out quantities of the different
such size that it will yield not less than 100 g of each of the sizes within the tolerances of 6.3 and, where the test portion
following sizes, which shall be available in amounts of 5 % or consists of two sizes, combine them to the designated total
more, expressed in terms of the following sieves: weight. Record the weights of the test samples and their
fractional components. In the case of sizes larger than 19.0 mm
Passing Sieve Retained on Sieve
(3⁄4 in.), record the number of particles in the test samples.
600 µm (No. 30) 300 µm (No. 50)
1.18 mm (No. 16) 600 µm (No. 30) 8. Procedure
2.36 mm (No. 8) 1.18 mm (No. 16)
4.75 mm (No. 4) 2.36 mm (No. 8) 8.1 Storage of Samples in Solution—Immerse the samples in
9.5 mm (3⁄8 in.) 4.75 mm (No. 4)
the prepared solution of sodium sulfate or magnesium sulfate
6.3 Coarse Aggregate—Coarse aggregate for the test shall for not less than 16 h nor more than 18 h in such a manner that
consist of material from which the sizes finer than the No. 4 the solution covers them to a depth of at least 1⁄2 in. (Note 6).
sieve have been removed. The sample shall be of such a size Cover the containers to reduce evaporation and prevent the
that it will yield the following amounts of the indicated sizes accidental addition of extraneous substances. Maintain the
that are available in amounts of 5 % or more: samples immersed in the solution at a temperature of 70 6 2 °F
Size (Square-Opening Sieves) Mass, g (21 6 1 °C) for the immersion period.
9.5 mm (3⁄8 in.) to 4.75 mm (No. 4) 300 ± 5 NOTE 6—Suitably weighted wire grids placed over the sample in the
19.0 mm (3⁄4 in.) to 9.5 mm (3⁄8 in.) 1000 ± 10 containers will permit this coverage to be achieved with very lightweight
Consisting of: aggregates.
12.5-mm (1⁄2-in.) to 9.5-mm (3⁄8-in.) material 330 ± 5
19.0-mm (3⁄4-in.) to 12.5-mm (1⁄2-in.) material 670 ± 10 8.2 Drying Samples After Immersion—After the immersion
37.5-mm (1 1⁄2-in.) to 19.0-mm (3⁄4 in.) 1500 ± 50 period, remove the aggregate sample from the solution, permit
Consisting of:
25.0-mm (1-in.) to 19.0-mm (3⁄4-in.) material 500 ± 30
it to drain for 15 6 5 min, and place in the drying oven. The
37.5-mm (1 1⁄2-in.) to 25.0-mm (1-in.) material 1000 ± 50 temperature of the oven shall have been brought previously to
63-mm (2 1⁄2 in.) to 37.5-mm (1 1⁄2 in.) 5000 ± 300 230 6 9 °F (110 6 5 °C). Dry the samples at the specified
Consisting of:
50-mm (2 in.) to 37.5-mm (1 1⁄2-in.) material 2000 ± 200
temperature until constant weight has been achieved. Establish
63-mm (2 1⁄2-in.) to 50-mm (2-in.) material 3000 ± 300 the time required to attain constant weight as follows: with the
Larger sizes by nominal 12.5-mm (1⁄2-in.) spread in sieve oven containing the maximum sample load expected, check the
size, each fraction
Consisting of:
weight losses of test samples by removing and weighing them,
75-mm (3-in.) to 63-mm (2 1⁄2-in.) material 7000 ± 1000 without cooling, at intervals of 2 to 4 h; make enough checks
90-mm (3 1⁄2-in.) to 75-mm (3-in.) material 7000 ± 1000 to establish required drying time for the least favorable oven
100-mm (4-in.) to 90-mm (3 1⁄2-in.) material 7000 ± 1000
location (see 4.5) and sample condition (Note 7). Constant
6.4 When an aggregate to be tested contains appreciable weight will be considered to have been achieved when weight
amounts of both fine and coarse material, having a grading loss is less than 0.1 % of sample weight in 4 h of drying. After
with more than 10 weight % coarser than the 9.5-mm (3⁄8-in.) constant weight has been achieved, allow the samples to cool
sieve and, also, more than 10 weight % finer than the 4.75-mm to room temperature, when they shall again be immersed in the
(No. 4) sieve, test separate samples of the minus No. 4 fraction prepared solution as described in 8.1.
and the plus No. 4 fraction in accordance with the procedures
NOTE 7—Drying time required to reach constant weight may vary
for fine aggregate and coarse aggregate, respectively. Report
considerably for several reasons. Efficiency of drying will be reduced as
the results separately for the fine-aggregate fraction and the cycles accumulate because of salt adhering to particles and, in some cases,
coarse-aggregate fraction, giving the percentages of the coarse- because of increase in surface area due to breakdown. The different size
and fine-size fractions in the initial grading. fractions of aggregate will have differing drying rates. The smaller sizes
will tend to dry more slowly because of their larger surface area and
7. Preparation of Test Sample restricted interparticle voids, but this tendency may be altered by the
effects of container size and shape.
7.1 Fine Aggregate—Thoroughly wash the sample of fine
aggregate on a 300-µm (No. 50) sieve, dry to constant weight 8.3 Number of Cycles—Repeat the process of alternate
at 230 6 9 °F (110 6 5 °C), and separate into the different sizes immersion and drying until the required number of cycles is
by sieving, as follows: Make a rough separation of the graded obtained.
sample by means of a nest of the standard sieves specified in 8.4 After the completion of the final cycle and after the
6.2. From the fractions obtained in this manner, select samples sample has cooled, wash the sample free from the sodium
of sufficient size to yield 100 g after sieving to refusal. (In sulfate or magnesium sulfate as determined by the reaction of
general, a 110-g sample will be sufficient.) Do not use fine the wash water with barium chloride (BaCl2). Wash by
aggregate sticking in the meshes of the sieves in preparing the circulating water at 110 6 10 °F (43 6 6 °C) through the
samples. Weigh samples consisting of 100 6 0.1 g out of each samples in their containers. This may be done by placing them

Copyright by ASTM Int'l (all rights reserved); Tue May 7 08:41:41 EDT 2013
3
Downloaded/printed by
(Turkey MOU- Online Access) pursuant to License Agreement. No further reproductions authorized.
 C88 − 05
in a tank into which the hot water can be introduced near the Sieve Used to
bottom and allowed to overflow. In the washing operation, the Size of Aggregate Determine Loss
samples shall not be subjected to impact or abrasion that may 100 mm (4 in.) to 90 mm (3 1⁄2 in.) 75 mm (3 in.)
tend to break up particles. 90 mm (3 1⁄2 in.) to 75 mm (3 in.) 63 mm (2 1⁄2 in.)
75 mm (3 in.) to 63 mm (2 1⁄2 in.) 50 mm (2 in.)
NOTE 8—Tap water containing sulfates when used for the wash water 63 mm (2 1⁄2 in.) to 37.5 mm (1 1⁄2 in.) 31.5 mm (1 1⁄4 in.)
will cloud when tested with the barium chloride solution. The cloudiness 37.5 mm (1 1⁄2 in.) to 19.0 mm (3⁄4 in.) 16.0 mm (5⁄8 in.)
of a solution of tap water and the barium chloride solution should be 19 mm (3⁄4 in.) to 9.5 mm (3⁄8 in.) 8.0 mm (5⁄16 in.)
judged so that tested wash water with the same degree of cloudiness can 9.5 mm (3⁄8 in.) to 4.75 mm (No. 4) 4.0 mm (No. 5)
be assumed to be free of sulfates from the test.
10. Qualitative Examination
9. Quantitative Examination 10.1 Make a qualitative examination of test samples coarser
9.1 Make the quantitative examination as follows: than 19.0 mm (3⁄4 in.) as follows (Note 9):
10.1.1 Separate the particles of each test sample into groups
9.1.1 After the sodium sulfate or magnesium sulfate has
according to the action produced by the test (Note 9).
been removed, dry each fraction of the sample to constant
10.1.2 Record the number of particles showing each type of
weight at 230 6 9 °F (110 6 5 °C). Sieve the fine aggregate
distress.
over the same sieve on which it was retained before the test,
and sieve the coarse aggregate over the sieve shown below for NOTE 9—Many types of action may be expected. In general, they may
the appropriate size of particle. For fine aggregate, the method be classified as disintegration, splitting, crumbling, cracking, flaking, etc.
and duration of sieving shall be the same as were used in While only particles larger than 3⁄4 in. in size are required to be examined
qualitatively, it is recommended that examination of the smaller sizes be
preparing the test samples. For coarse aggregate, sieving shall made in order to determine whether there is any evidence of excessive
be by hand, with agitation sufficient only to assure that all splitting.
undersize material passes the designated sieve. No extra
manipulation shall be employed to break up particles or cause 11. Report
them to pass the sieves. Weigh the material retained on each 11.1 Report the following data (Note 10):
sieve and record each amount. The difference between each of 11.1.1 Weight of each fraction of each sample before test,
these amounts and the initial weight of the fraction of the 11.1.2 Material from each fraction of the sample finer than
sample tested is the loss in the test and is to be expressed as a the sieve designated in 9.1.1 for sieving after test, expressed as
percentage of the initial weight for use in Table 1. a percentage of the original weight of the fraction,

TABLE 1 Suggested Form for Recording Test Data (with Illustrative Test Values)
Percentage
Grading of Weight of Test
Passing Weighted
Sieve Size Original Sample, Fractions
Designated Percentage Loss
% Before Test, g
Sieve After Test
Soundness Test of Fine Aggregate
Minus 150 µm (No. 100) 6 ... ... ...
300 µm (No. 50) to No. 100 11 ... ... ...
600 µm (No. 30) to No. 50 26 100 4.2 1.1
1.18 mm (No. 16) to No. 30 25 100 4.8 1.2
2.36 mm (No. 8) to No. 16 17 100 8.0 1.4
4.75 mm (No. 4) to No. 8 11 100 11.2 1.2
9.5 mm (3⁄8 in.) to No. 4 4 ... 11.2A 0.4
Totals 100.0 ... ... 5
Soundness Test of Coarse Aggregate
63 mm (2 1⁄2 in.) to 50 mm (2 in.)
50 mm (2 in.) to 37.5 mm (1 1⁄2 in.)
2825 g
1958 g J 2 1⁄2 to 1 1⁄2 in. 20 4783 4.8 1.0

37.5 mm (1 1⁄2 in.) to 25.0 mm (1 in.)

25 mm (1 in.) to 19.0 mm (3⁄4 in.)
1012 g
513 g J 1 1⁄2 to 3⁄4 in. 45 1525 8.0 3.6

19.0 mm (3⁄4 in.) to 12.5 mm (1⁄2 in.)

12.5 mm (in.) to 9.5 mm (in.)
675 g
333 g J ⁄ to 3⁄8 in.
34 23 1008 9.6 2.2

9.5 mm (3⁄8 in.) to 4.75 mm (No. 4) 298 g 12 298 11.2 1.3

Totals 100 ... ... 8

A
The percentage loss (11.2 %) of the next smaller size is used as the percentage loss for this size, since this size contains less than 5 % of the original sample as received.
See 11.1.3.4.

Copyright by ASTM Int'l (all rights reserved); Tue May 7 08:41:41 EDT 2013
4
Downloaded/printed by
(Turkey MOU- Online Access) pursuant to License Agreement. No further reproductions authorized.
 C88 − 05
TABLE 2 Suggested Form for Qualitative Examination (with Illustrative Test Values)
Qualitative Examination of Coarse Sizes
Particles Exhibiting Distress
Total No. of
Splitting Crumbling Cracking Flaking
Sieve Size Particles
Before
No. % No. % No. % No. %
Test
63 mm (2 1⁄2 in.) to 37.5 2 7 ... ... 2 7 ... ... 29
mm (1 1⁄2 in.)
37.5 mm (1 1⁄2 in.) to 5 10 1 2 4 8 ... ... 50
19.0 mm (3⁄4 in.)

11.1.3 Weighted average calculated in accordance with Test test, and (2) the number of particles affected, classified as to
Method C136 from the percentage of loss for each fraction, number disintegrating, splitting, crumbling, cracking, flaking,
based on the grading of the sample as received for examination etc., as shown in Table 2, and
or, preferably, on the average grading of the material from that 11.1.6 Kind of solution (sodium or magnesium sulfate) and
portion of the supply of which the sample is representative whether the solution was freshly prepared or previously used.
except that: NOTE 10—Table 1, shown with test values inserted for purpose of
11.1.3.1 For fine aggregates (with less than 10 % coarser illustration, is a suggested form for recording test data. The test values
than the 9.5-mm (3⁄8-in.) sieve), assume sizes finer than the shown might be appropriate for either salt, depending on the quality of the
300-µm (No. 50) sieve to have 0 % loss and sizes coarser than aggregate.
the 9.5-mm (3⁄8-in.) sieve to have the same loss as the next
smaller size for which test data are available. 12. Precision
11.1.3.2 For coarse aggregate (with less than 10 % finer 12.1 Precision—For coarse aggregate with weighted aver-
than the 4.75-mm (No. 4) sieve), assume sizes finer than the age sulfate soundness losses in the ranges of 6 to 16 % for
4.75-mm (No. 4) sieve to have the same loss as the next larger sodium and 9 to 20 % for magnesium, the precision indexes are
size for which test data are available. as follows:
11.1.3.3 For an aggregate containing appreciable amounts Coefficient of Difference Between
of both fine and coarse material tested as two separate samples Variation Two Tests (D2S %),
as required in 6.4, compute the weighted average losses (1S %), %A % of AverageA

separately for the minus No. 4 and plus No. 4 fractions based Multilaboratory:
on recomputed gradings considering the fine fraction as 100 % Sodium sulfate 41 116
and the coarse fraction as 100 %. Report the results separately Magnesium sulfate 25 71
Single-Operator:
giving the percentage of the minus No. 4 and plus No. 4 Sodium sulfate 24 68
material in the initial grading. Magnesium sulfate 11 31
11.1.3.4 For the purpose of calculating the weighted
A
average, consider any sizes in 6.2 or 6.3 that contain less than These numbers represent, respectively, the (1S %) and (D2S %) limits as
described in Practice C670.
5 % of the sample to have the same loss as the average of the
next smaller and the next larger size, or if one of these sizes is 12.2 Bias—Since there is no accepted reference material
absent, to have the same loss as the next larger or next smaller suitable for determining the bias for this procedure, no state-
size, whichever is present. ment on bias is being made.
11.1.4 Report the weighted percentage loss to the nearest
whole number, 13. Keywords
11.1.5 In the case of particles coarser than 19.0 mm (3⁄4 in.) 13.1 aggregates; magnesium sulfate; sodium sulfate; sound-
before test: (1) The number of particles in each fraction before ness; weathering

ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.

This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above
address or at 610-832-9585 (phone), 610-832-9555 (fax), or [email protected] (e-mail); or through the ASTM website
(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/
COPYRIGHT/).

Copyright by ASTM Int'l (all rights reserved); Tue May 7 08:41:41 EDT 2013
5
Downloaded/printed by
(Turkey MOU- Online Access) pursuant to License Agreement. No further reproductions authorized.