Group Meeting Problems 2023/01/21

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Group Meeting Problems - 2023/01/21

Pd(PPh3)4 (5 mol%)
MeO2C
1 BocO DMAP (20 mol%)
OHC
CO2Me OH
O + CH2Cl2, 40 C O
N OBoc 5 h, Ar N
Me Me
87%, dr = 18:1

B. D. Cui et al., J. Org. Chem., 88, 371 (2023)


Group Meeting Problems - 2023/01/21

2
PMBO OPMB
O
TBSO OH
H NaHMDS O
TBS O
Me THF Me
PhMe2Si –80 to –15 °C
O PhMe2Si
80%

K. Takeda et al., J. Org. Chem., 75, 3941 (2010)

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