SVM 3000 g2 Instruction Manual
SVM 3000 g2 Instruction Manual
SVM 3000 g2 Instruction Manual
WHAT IS MEASURABLE
AND MAKE MEASURABLE
THAT WHICH IS NOT
'ALILEO 'ALILEI
SVM 3000 / G2
Stabinger Viscometer
Nor is any liability assumed for damages resulting from the use of the information contained in this
instruction manual.
Anton Paar GmbH does not make a commitment to update the information in this manual. Specifications
are subject to change without notice.
All rights reserved (including translation). No part of this document may be translated, reproduced or
distributed in any form (print, photocopy, microfilm or any other process) without the prior written
permission of Anton Paar GmbH.
Trade marks may be used in this instruction manual without being marked as such. These are the
property of their respective owners and are legally protected.
E-mail: [email protected]
Web: http://www.anton-paar.com
SVM 3000/G2 5
9.2 Rinsing and Drying the Measuring Cells ............................................................................... 37
9.2.1 Solvents ................................................................................................................. 38
9.2.2 Cleaning the Measuring Cells ............................................................................... 38
9.2.3 Drain and Tube Rinsing System (External Rinsing) .............................................. 39
9.3 Disassembling the Viscosity Measuring Cell ........................................................................ 40
10 Menu Structure .............................................................................................................................. 44
Appendix A:Technical Data .............................................................................................................. 47
Appendix B:Menu Tree "Administrator" .......................................................................................... 49
Appendix C:Maintenance Schedule ................................................................................................. 53
Appendix D:Declaration of Conformity............................................................................................. 54
6 SVM 3000/G2
SVM 3000/G2 7
1 About the Instruction Manual
The instruction manual at hand describes the most important features and
functions. Find further information about the instrument on the enclosed CD.
Reference Manual This manual on the CD-ROM contains among other things detailled descriptions
about:
Video Manual For your SVM 3000 additionally a video manual on CD-ROM is available. It
contains among other things short video sequences and instructions regarding
sample handling, filling, measuring and cleaning. Additionally some maintenance
work such as replacing O-rings or replacing the drive shaft seal unit is shown.
Supplementary the CD-ROM contains a spare parts list.
8 SVM 3000/G2
1 About the Instruction Manual
Warning:
This symbol calls attention to the risk of accidental injuries or damage to
goods. Do not proceed until the indicated conditions for averting this threat
are fully understood and met.
Caution:
This symbol calls attention to the risk of instrument damage or
measurement errors. Do not proceed until the indicated conditions for
averting this threat are fully understood and met.
Information:
This symbol calls attention to any additional information of use to the
operator.
SVM 3000/G2 9
2 Safety Instructions
2 Safety Instructions
• Read the instruction manual at hand before using SVM 3000/G2.
2.1.1 Liability
• The instruction manual at hand does not claim to address all safety issues
associated with the use of the instrument and samples. It is your
responsibility to establish health and safety practices and determine the
applicability of regulatory limitations.
• Anton Paar GmbH only warrants the proper functioning of SVM 3000/G2 if
no adjustments have been made to the mechanics, electronics, and
firmware.
• Only use SVM 3000/G2 for the purpose described in this instruction manual.
Anton Paar GmbH is not liable for damages caused by incorrect use of SVM
3000/G2.
• Do not use any accessories or spare parts other than those supplied or
approved by Anton Paar GmbH.
• Make sure all operators are trained to use the instrument safely and correctly
before starting any applicable operations.
• Check SVM 3000/G2 for chemical resistance to the samples and solvents.
• Refer to Chapter 2.3, for the explanations of the safety sign ( ) on the
instrument.
10 SVM 3000/G2
2 Safety Instructions
• The results delivered by SVM 3000/G2 not only depend on the correct
function of the instrument, but also on various other factors. We therefore
recommend to have the results checked (e.g. plausibility tested) by skilled
personnel before consequential actions are taken based on the results.
2.1.4 Disposal
2.1.5 Returns
• For repairs send the cleaned SVM 3000/G2 unit to your Anton Paar
representative. Only return the instrument together with the filled out
"Malfunction Report". Find this form on the supplied CD-ROM.
• Observe and adhere to your national safety regulations for handling the
measured samples (e.g. use of safety goggles, gloves, respiratory protection
etc.).
• Only store the minimum required amount of sample, solvents and other
inflammable materials near the SVM 3000/G2.
• Make sure that the setup location is sufficiently ventilated. The environment
of SVM 3000/G2 must be kept free of inflammable gases and vapors.
• Connect SVM 3000/G2 to the mains via a safety switch located at a safe
distance from the instrument. In an emergency, turn off the power using this
switch instead of the power switch on SVM 3000/G2.
SVM 3000/G2 11
2 Safety Instructions
• Do not use SVM 3000/G2 to measure fluids of the IIC group according to EN
60079-14, such as e.g. carbon disulfide, hydrogen or acetylene.
• When using the magnetic particle trap (optional accessory): The metal parts
of this device will be heated to a temperature of max. 80 °C. Do not use
sample and solvents with a boiling point lower than 80 °C. This can form
flammable gasses.
• When moving or lifting the SVM 3000 measuring assembly, hold the
SVM 3000 at the front and the rear to prevent your fingers from squeezing
between the SVM 3000 and the table. When carrying the instrument, keep it
close to your body.
• Check the chemical resistance of the materials which come into contact with
sample liquids and solvents before filling the liquids to the cells. See
Appendix B, Reference Manual (on CD-ROM).
• Prior to starting a measurement, make sure that the filling and waste hoses
and the cell connection tube are properly connected.
• To extract explosive vapors from the measuring cell area, a "suction hose"
can be connected to the "INTERNAL" inlet.
• Compressed air for drying the measuring cells must be dry, free of oil and
dust. The pressure must be limited safely to a max. pressure of 100 kPa (= 1
bar = 14.5 psi). Suitable air preparation kits are available from Anton Paar.
See Chapter 4.3 and 11, Reference Manual (on CD-ROM).
12 SVM 3000/G2
2 Safety Instructions
Fig. 2 - 1
Fig. 2 - 2
Fig. 2 - 3
SVM 3000/G2 13
3 SVM 3000/G2 - An Overview
The SVM 3000 is designed to measure mainly oily substances. The following list
gives an overwiew about sample types which can be measured within the
instrument’s specifications. If you have questions regarding your sample, contact
you local Anton Paar representative.
Considering sufficient lubrication of the outer rotor bearings and the chemical
compatibility also the following sample types can be measured with restrictions
using the SVM 3000.
• polymer solutions
• aqueous solutions
• acids and bases
• other chemicals
14 SVM 3000/G2
3 SVM 3000/G2 - An Overview
Never try to measure samples, which harden during the time they are in the
measuring cells. This leads to costly repairs.
SVM 3000 can be operated by using the 7 built-in keys (see Chapter 6.2) or an
external keyboard. The instrument can also be controlled with a PC via the PC
interface. See Appendix A, Reference Manual on CD-ROM. When pressing any
internal key, you will hear a key click. For other events like the instrument
prompting a user interaction or the measurement is valid or an error has occurred,
an acoustic signal will be emitted. Information on the acoustic signals see Chapter
12.2.3 and Appendix C, both in the Reference Manual on CD-ROM.
3.3 Interfaces
The instrument has two serial interfaces (RS232-C), and a keyboard connector
(PC-AT; DIN). The two S-BUS interfaces can be used to connect two SVM 3000
for automatic temperature adjustments and calibrations with MKT thermometers.
Where to find the interfaces on the instrument see Chapter 5.3.
• baudrate: 9600
• format: 7E1
• flow control: hardware: RTS-CTS
• line delimiter: <CR><LF>
• baudrate: 19200
• format: 7E1
• flow control: none
• data delimiter: semicolon (;)
• line delimiter: <CR><LF>
SVM 3000/G2 15
4 Unpacking and Checking the Supplied Parts
4.1 Unpacking
SVM 3000/G2 was tested and packed carefully before shipment. However,
damage may occur during transport.
1. Keep the packaging material (box, foam pieces, transport protection) for
possible returns and further questions from the transport and insurance
company.
2. Check the delivery for completion by comparing the supplied parts to those
noted in the table in Chapter 4.2.
4. If a part is damaged, contact the transport company and your Anton Paar
representative.
16 SVM 3000/G2
4 Unpacking and Checking the Supplied Parts
1 U-tube PTFE with Luer cone (spare part for cell 7429
connection tube)
2 O-ring 2x1 FPM 75 Viton Extreme with assembly
tool
3 O-ring 6x1 FPM 75 Viton Extreme 18877
1 O-ring 5x1 FPM 75 Viton Extreme 15752
1 O-ring 4.5x1 FPM 75 Viton Extreme 42612
1 O-ring 4x1 FPM 75 Viton Extreme 15751
supplies for O-rings:
O-ring set SVM 3000/G2 including the above 17064
listed O-rings, further 1 pc. O-ring 5x1.1 FPM 75
Viton Extreme and 1 pc. O-ring 6x1.1 FPM 75
Viton Extreme
O-ring set SVM 3000, 5 pcs. 2x1 FPM 75 Viton 10538
Extreme
(All these O-rings made of Viton 981 Extreme =
ETP-600S)
5 Cartridge sealing unit 17764
SVM 3000/G2 17
4 Unpacking and Checking the Supplied Parts
4.2.2 Accessories
This list contains only some common accessories. For all available accessories
and consumables see Chapter 4.3, Reference Manual on CD-ROM.
- 20.0 10
170
50110
210
1 Low temperature options
°C
More information:
Packing the instrument for transport see Chapter 4.4, Reference Manual on
CD-ROM.
A detailed description of keyboard, printer and barcode reader see Chapter
17, Reference Manual on CD-ROM.
18 SVM 3000/G2
5 Preparing the Instrument
• SVM 3000 does not require any special installation conditions. The setup
location and surroundings should meet the requirements of a typical
laboratory. Place the instrument on a flat lab desk.
1 Remove the transport protection
before switching on the instru-
ment. To do this, open the front
flap and take out the foam block
(1). Position (2) shows the key for
viscosity inlet nozzle (measuring
cell key).
Fig. 5 - 2 and 5 - 3 show the positions of all connectors, the type plate and the
power switch.
SVM 3000/G2 19
5 Preparing the Instrument
The fixing point (C) for the cell connection tube (J) is a thread which is directly
mounted onto the measuring cell block. It is foam-covered together with the block
for better thermal insulation. Fix the cell connection tube by inserting it securely
into the density outlet nozzle (B) and the viscosity inlet nozzle (F). Screw the fixing
screw into the fixing point (C).
D2
D1
K
J
A
20 SVM 3000/G2
5 Preparing the Instrument
B
A
SVM 3000/G2 21
5 Preparing the Instrument
All mentioned hoses are supplied in the accessory kit. Connectors see Fig. 5 - 2
and 5 - 3, the instrument with connected hoses is shown in Fig. 5 - 5.
The FEP hoses 250x3x2 mm have a marker ring (before the screw connector).
This ring stops the hose slipping, which is especially important for the hose end
in the waste bottle (it prevents the hose becoming immersed in the liquid in the
waste bottle).
5 2
3 H
G
Connect a FEP hose 250x3x2 mm (1) to the waste tube (E = viscosity outlet
nozzle in Fig. 5 - 2) and lead it to the waste bottle (2). Attach it to one of the three
holes in the lid.
Information:
The waste hose must be laid correctly otherwise a sucking effect can occur
and bubbles may be sucked into the measuring cells. Low viscous samples, in
particular, could run out of the measuring cell. Lead the waste hose so that it
runs slightly upwards into the waste bottle.
Air hose:
1. To prepare the air hose (3), cut a piece of 25 cm (10") from the supplied
silicone hose 3x5 and attach an adapter Luer cone to one end of this hose.
22 SVM 3000/G2
5 Preparing the Instrument
2. Plug the other end to the "AIR OUT" connection (I in Fig. 5 - 2).
This hose is for drying the cells (connect to D1) and the drain and tube rinsing
system (connect to D2).
The instrument is equipped with drain hoses for the drive shaft seal, further with
a system for cleaning the thermostat tube and the outer surface of the measuring
rotor and the rotor bearings. These items can be cleaned by filling the system with
solvent and drying afterwards.
1. Connect a 250 mm FEP hose (4) to the inner connection (D2) on the filling
support (D) and the RINSE IN connection (G).
2. Connect a further 250 mm FEP hose (5) to the RINSE OUT connection (H).
Attach the free end to the waste bottle (3).
Information:
After the first installation, rinse and dry the measuring cells as described in
Chapter 9 before carrying out measurements.
All connectors are placed on the rear of the instrument see Fig. 5 - 3.
4. Connect the computer with the supplied RS-232 cable to the PC interface on
the SVM 3000 (C in Fig. 5 - 3); if applicable.
SVM 3000/G2 23
6 Functional Components
6 Functional Components
To switch on SVM 3000, press the power switch (F in Fig. 5 - 3) on the rear of the
instrument.
24 SVM 3000/G2
6 Functional Components
Information:
The air density value can be seen as an indicator for the cleaning and drying
quality of the measuring cell. See Chapters 6.1 and 10, Reference Manual on
CD-ROM.
Measuring windows:
The measuring variables shown in the first three lines of the display can be
selected by the user. Measuring values can also be displayed in the first three
lines of the second measuring window (press the INFO key to switch over). In the
fourth line the sample name and the consecutive number of measurement is
displayed. The third window (measurement precision window) displays the repeat
deviations and the obtained precision. How to select an instrument mode see
Chapter 7.
2 3
state display (blinks every second on the right side of the window):
> state indicator, shows the current instrument state:
FILLING, MEASURING
results are frozen (RESULT VALID)
! error message or warning (ERROR)
More information:
All possible display settings see Chapter 12, Reference Manual on CD-ROM.
Description of all measuring windows, the information windows and the
context sensitive help see Chapter 6, Reference Manual on CD-ROM.
State display, see Chapter 6.4 of this manual and in the Reference Manual on
CD-ROM.
SVM 3000/G2 25
6 Functional Components
The TEXT in the lower part of the key describes its function in the measuring
window. The SYMBOL in the upper part of the key describes its function when
navigating the menu structure and entering characters.
opens the main menu
prints the measuring values and stores the data
for entering the set temperature and sample name
for selecting the instrument mode
starts and stops a measurement
switches the air pump on and off
opens the other measuring and the information windows
menu navigation: browse within a menu level
text entry: scroll through the character set
data memory: change between data sets
menu navigation: browse within a menu level
text entry; move the cursor to the character to be changed
data memory: change between results within a data set
opens the submenu of the selected menu
confirms a selection or data entry
26 SVM 3000/G2
6 Functional Components
Data (= text and numerals), e.g. sample names or reference values of a standard
oil, can be entered using an external keyboard, a barcode reader, or the built-in
keys of the instrument. Use the optional external keyboard for easy data entry.
Key functions of the external keyboard see Chapter 17.1, Reference Manual on
CD-ROM.
Overwrite mode:
By default, every data field - no matter whether letters or numerals - opens in the
overwrite mode. Data can be entered here using an external keyboard or a
barcode reader. An existing line of data will be overwritten completely.
Edit mode:
To edit data using the instrument’s keys, just press ENTER once again to switch
to the "edit mode". The first sign of the data field will start to blink. Use the
ARROW keys to edit data. When you are ready, confirm with ENTER.
SVM 3000/G2 27
6 Functional Components
RESULT VALID The "" shows that the display is frozen. The measurement
values are valid (RESULT VALID) and the instrument is ready
to be refilled or cleaned (FILLING).
ERROR The "!" and ">" blink alternately in the 4th line of the state
No measurement display. This shows an error. To read the error message,
possible! press the INFO key. For details see Chapter 19.2, Reference
Manual on CD-ROM.
WARNING e.g.: Dependent on the instrument state, either ">" and "!" or ""
Perhaps only and "!" blink alternately in the corresponding line of the state
limited display. This shows a warning. To read the warning message,
measurements press the INFO key. For details see Chapter 19.2, Reference
possible! Manual on CD-ROM.
28 SVM 3000/G2
7 Instrument Modes
7 Instrument Modes
There are 10 predefined standard settings for the instrument modes. However,
these can be adapted to suit your own requirements in the user level
"administrator" (in the "mode settings" menu).
Key functions:
To select a mode press to switch to the modes menu
In this window:
to browse through the list of modes
FILLING
MEASURING
RESULT VALID to confirm the selection
ERROR
to leave the menu without changing the
instrument mode
Overview:
M1-SINGLE POINT UF ultra fast measurement, e.g. for high throughput at low
accuracy
M2-REPEAT UF ultra fast measurement with repetitions
M3-SINGLE POINT F fast measurement at one temperature
M4-REPEAT F fast measurement with automatic repetitions
M5-SINGLE POINT S standard measurement with high accuracy at one
temperature
M6-REPEAT S standard measurement with automatic repetitions
M7-VISCOSITY INDEX measurement at 40 °C and 100 °C, calculated viscosity
index according to ASTM D2270, ISO 2909; precision
class standard
M8-TEMP. TABLE SCAN scan over a temperature table, precision class standard,
you enter: table of measuring temperatures
M9-TEMP. RANGE SCAN scan over a temperature range, precision class fast,
you enter: start / stop temperature, step
M0-ASTM (PRECISE) measurement of highest accuracy with repetitions
for tests according to the ASTM D7042 standard
More information:
Detailed description of all preset instrument modes see Chapter 7.2,
Reference Manual on CD-ROM.
How to create user specific instrument modes see Chapter 7.3, Reference
Manual on CD-ROM.
SVM 3000/G2 29
30
DEFAULT SETTINGS OF THE 10 PRESET INSTRUMENT MODES
M1- M2- M3- M4- M5- M6- M7- M8- M9- M0-
7 Instrument Modes
SINGLE REPEAT SINGLE REPEAT SINGLE REPEAT VISCOSITY TEMP. TABLE TEMP. RANGE ASTM
POINT UF UF POINT F F POINT S S INDEX SCAN SCAN (PRECISE)
temp. unit °C °C °C °C °C °C °C °C °C °C
temp. change yes yes yes yes yes yes no no no yes
allowed
set temperature 40 °C 40 °C 40 °C 40 °C 40 °C 40 °C 40 °C 20 °C 20 °C 40 °C
filling temp. cell -100 °C -100 °C -100 °C -100 °C -100 °C -100 °C -100 °C -100 °C -100 °C -100 °C
temperature
Xsample* / magazine * 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C 60 °C / 60 °C
offset
Xsample* / magazine * ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0 ±0.0 / ±0.0
display eta eta eta eta eta eta ny 40°C eta eta eta
settings ny ny ny ny ny ny ny 100°C ny ny ny
rho rho rho rho rho rho VI rho rho rho
API-D De.15C API-D De.15C API-D De. 15C API-D De.15C API-D De.15C API-D De. 15C eta 40°C
eta 100°C
rho 15°
measurement automatic automatic automatic automatic automatic automatic viscosity temp. table temp. range automatic
mode index scan scan
meas. precision ultrafast (UF) ultrafast (UF) fast (F) fast (F) standard (S) standard (S) standard (S) standard (S) fast (F) precise (P)
equilibration time 000 000 000 000 000 000 000 030 000 000
repetition number 0 3 0 3 0 3 0 0 0 3
data memory all determin. all determin. all determin. all determin. all determin. all determin. all determin. all determin. all determin. all determin.
options
viscosity limit 0.00 % 0.00 % 0.00 % 0.00 % 0.00 % 0.00 % 0.00 % 0.00 % 0.00 % 0.00 %
density limit 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
air pump timeout 50 50 50 50 60 60 60 80 80 80
start temp. 20 20 20 20 20 20 20 20 20 20
stop temp. 100 100 100 100 100 100 100 100 100 100
temp. step 10 10 10 10 10 10 10 10 10 10
SVM 3000/G2
7 Instrument Modes
Base values:
eta ... mPa·s dynamic viscosity
(a * in the result indicates, that the calibration correction was applied)
ny ... mm²/s kinematic viscosity
(a * in the result indicates, that the calibration correction was applied)
rho ... g/cm³ true density (predetermined value)
VI values:
40°C ... mm²/s kinematic viscosity at 40 °C
100°C ... mm²/s kinematic viscosity at 100 °C
VI viscosity index
40°C ... mPa.s dynamic viscosity at 40 °C
100°C ... mPa.s dynamic viscosity at 100 °C
15°C ... g/cm³ calculated density at 15 °C (extrapolated from 40 °C and 100 °C)
API functions:
API-D De. 15C ... g/cm³ API density at 15°C (calculated), here for product group D - lube oils
filling temperature allows filling and cleaning at higher temperatures than the measuring
temperature.
measuring precision ultrafast (UF), fast (F), standard (S), precise (P)
equilibration time additional delay in seconds before the evaluation procedure begins
More information:
Detailed description of all preset instrument modes see Chapter 7.2,
Reference Manual on CD-ROM.
All possible mode settings and the explanations see Chapter 12.2, Reference
Manual on CD-ROM.
SVM 3000/G2 31
8 Measurements
8 Measurements
Before starting the measurement, select the desired instrument mode (see
Chapter 7) and enter a measuring temperature and a sample name.
measuring window
Sample name:
The instrument must display the "measuring window". Press the SET key to
change to the "various settings" menu. Press ENTER to select "edit sample
name". The following screen will be displayed:
Enter the sample name (16 characters maximum)
using the optional external keyboard or a bar code
reader (overwrite mode) or by pressing ENTER again
and using the ARROW keys (edit mode). Confirm data
entry with ENTER.
Counter:
32 SVM 3000/G2
8 Measurements
Measuring temperature:
Information:
This menu item is only accessible if "temp. change allowed" is set to "yes"
in the "mode settings", or if the SVM 3000 is used in the user level
"administrator".
More information:
For a detailed description of entering a sample name (overwrite mode, edit
mode) and the measurement counter see Chapter 8.1, Reference Manual on
CD-ROM.
1. Ensure that the cells are clean and dry, then fill the sample (filling/cleaning
see Chapter 9).
2. Press the START key.
The motor starts up to filling speed, the state display changes from "FILLING" to
"MEASURING" and the first measuring values appear on the display. These are
unstable at first, but become more accurate as the averaging period increases.
When the values are stable, the state changes to "RESULT VALID", indicated by
the arrow. The motor slows down to filling speed. The instrument asks you to "refill
and press ENTER".
3. Refill 1 mL (at least 250 µL) from the syringe and press again the START
key.
During the measurement you can view the current repeat deviation for viscosity
and density (RDV, RDD) by pressing the INFO key twice.
If the results of the first repetition are within the limits for viscosity and density, the
state changes to "RESULT VALID", indicated by two diamonds. The motor slows
to filling speed and the display is frozen until the START key is pressed again.
In addition the "FILLING" state is displayed. The instrument is now ready to be
refilled or to be rinsed and dried and then newly filled.
If the result is not within the limits the repeat deviation for viscosity and density will
be displayed and you are asked once more to refill.
SVM 3000/G2 33
8 Measurements
Measuring data are automatically stored in the "data memory" and sent to the
printer port.
Aborting a measurement:
Press the SET key and proceed as described in Chapter 8.1. A sample name
entered during the measurement comes into effect for this measurement. It is not
possible to change the measuring temperature, when the first determination has
become already valid (message: "access denied!").
More information:
Measurements generally see Chapter 8, Reference Manual on CD-ROM.
Measurement according to ASTM D7042-04: See this standard, further
Chapter 8.2.3 in the Reference Manual on CD-ROM.
Precision and Bias of SVM 3000 see Chapter 8.4, Reference Manual on CD-
ROM.
34 SVM 3000/G2
8 Measurements
Viewing data:
1. Press the MENU key to switch to the menu "data memory" and confirm with
ENTER.
3. To switch between values within a data set, use the ARROW RIGHT / LEFT
keys.
4. To browse between all data sets, use the ARROW UP / DOWN keys.
Connect the optional protocol printer to the PRINTER port of SVM 3000.
Alternatively you can transfer the measuring data directly to a computer. See
Appendix A, Reference Manual on CD-ROM.
1. Press the MENU key to switch to the menu "data memory" and confirm with
ENTER.
2. Select the menu item "print data" and confirm with ENTER.
3. Select either "all new data" (prints all data sets which were not printed
before) or "starting from ..." (prints all data sets from a the date which you
can enter here) and confirm with ENTER.
Information:
Measurement results either printed directly after measurement or printed from
the data memory look always the same
More information:
Communication via the serial interfaces see Appendix A, Reference Manual
on CD-ROM.
AP SoftPrint for SVM see Appendix A.2, Reference Manual on CD-ROM.
VisioLab for SVM see Appendix A.3, Reference Manual on CD-ROM.
Recording a continuous protocol see Chapter 8.3.4, Reference Manual on
CD-ROM.
SVM 3000/G2 35
9 Filling and Cleaning the Measuring Cells
More information:
All filling options for different sample types (e.g. highly viscous oils, volatile
substances, heavy oils), separate filling of the cells (e.g. as required for
adjustment), see Chapter 9, Reference Manual on CD-ROM.
Sample handling and preparation see Chapter 9.1, Reference Manual on CD-
ROM.
For all cleaning options and information about solvents see Chapter 10,
Reference Manual on CD-ROM.
For the filling and cleaning procedures see also the SVM 3000 Video Manual.
9.1 Filling
Caution:
• Before filling, check whether the wetted parts are resistant to the sample
and solvents (see Appendix B, Reference Manual on CD-ROM).
• Check also whether the wash bottle (PE) is resistant to the solvents used.
• Do not use disposable syringes with rubber plunger for petrochemical
substances. They are often chemically not resistant and tend to sucking
small bubbles.
• Hold the syringe with the tip pointing upwards. The bubble rises to the top.
Remove it by carefully pushing the plunger upwards.
• For very small bubbles place the syringe with the tip in the connector for
the external rinsing. Wait until the bubbles have moved upwards to the
plunger and will not be filled into the cells.
Caution:
The filling pressure also for highly viscous samples must not exceed 1.5 bar
(22 psi) otherwise sample may pass out at the rotor bearings. This applies
also for pressing out the sample after a measurement. This pressure
corresponds to a force of approx. 20 N on the plunger of a 5 mL syringe.
An increased pressure may also lead to damage in the measuring cell. In this
case Anton Paar is not liable for damage.
36 SVM 3000/G2
9 Filling and Cleaning the Measuring Cells
6. Fill another 1 mL from the syringe - or at least until the sample is visible in
the waste hose. Then press START again.
This prewetting helps you achieve a better filling quality and a more precise
measuring result.
Caution:
• After measurement and cleaning the cells, make sure that samples and
solvents are disposed correctly. For details, refer to the safety information
sheet for the solvent used. These are available from the manufacturer.
• Ensure that the solvent is suitable for the sample. If there are any doubts,
perform solubility tests outside the instrument.
Have the required solvent(s) ready in the supplied wash bottles before the first
measurement is carried out.
SVM 3000/G2 37
9 Filling and Cleaning the Measuring Cells
9.2.1 Solvents
For clean oils usually a single solvent is satisfactory - for most samples you can
use cleaner’s naphtha (100/140).
Required solvent For a single solvent or a second solvent: "chemically pure" or "for synthesis".
quality The purity of the first solvent (prewash) is not important.
Samples Solvents
Low and medium viscous oils Cleaner’s naphtha (boiling range 100/140 °C),
toluene
High viscous oils, most of all As before, or a combination of two solvents may
heavy oils and crude oils be more effective; e.g. 1st kerosene + 2nd
cleaner’s naphtha.
Samples which are not soluble e.g.: 1st toluene/xylene for solving the sample and
in cleaner’s naphtha (some rinsing it out of the cells; 2nd cleaner’s naphtha for
kinds of lube oils, some heavy removing the residues from solvent 1 and to
oils and crude oils) accelerate drying the cells.
Precleaning:
Caution:
When pushing out the sample after a measurement, the pressure must not
exceed 1.5 bar (22 psi). This pressure corresponds to a force of approx. 20 N
on the plunger of a 5 mL syringe. An increased pressure may also lead to
damage in the measuring cell. In this case Anton Paar is not liable for damage.
Push out the sample from the cells using the empty syringe. Low viscous oils can
be sucked back from the cells with the syringe. You can also connect the air hose
to the filling adapter and switch on the air pump to push out the sample.
1. Attach the tip of the wash bottle to the connector D1 on the filling support.
2. Only fill the cells with solvent until you can see 2 - 3 cm of solvent in the
waste hose (leading upwards) but not so much that the solvent reaches the
highest point in the waste hose. This prevents the solvent running out of the
cells (suction effect) when removing the tip.
3. Squeeze the wash bottle this way, that the liquid in the waste hose comes to
a standstill.
4. Now detach the wash bottle and at the same time stop squeezing it. This
prevents sucking contaminated solvent back into the bottle. Check whether
the liquid is still not in motion.
5. Allow the motor to run on measuring speed for approx. 10 seconds. This
improves the cleaning action.
6. If required, repeat this procedure a few times.
38 SVM 3000/G2
9 Filling and Cleaning the Measuring Cells
7. To dry the cells attach the air hose to the connector D1 on the filling adapter
(D) and press the PUMP key.
When using two solvents, remove the residues of solvent 1 by blowing air through
the cells for some seconds using the air pump.
Information:
The density value for a filled cell is higher than 0.6 g/cm³.
The density value for a clean and dry cell is approx. 0.0015 ± 0.0005 g/cm³;
this depends on temperature, air pressure and waiting time after drying.
More information:
Solvents and recommended drying times see Chapter 10.1, Reference
Manual on CD-ROM.
Chemical resistance of sample and solvent wetted parts see Appendix B,
Reference Manual on CD-ROM.
The SVM 3000 is equipped with an additional drain and tube rinsing system
("external rinsing"). This allows to draw away liquids in case of leaks, further to
rinse the rotor bearings, the outer surface of the measuring rotor, the thermostat
tube and the drive shaft seals.
1. To perform such a rinsing cycle fill solvent into the inner connector (D2 in Fig.
5 - 5) on the filling adapter until it can be seen in the waste hose fixed on the
RINSE OUT connector.
2. Start the motor for approx. 10 seconds. This improves the cleaning action on
the outer surface of the measuring rotor.
3. Refill solvent until the solvent in the outlet becomes clear.
4. For drying connect the air hose to the connector D2 on the filling adapter (D)
and switch on the air pump.
Caution:
The drain and tube rinsing cycle is no substitute for the regular disassembly of
the viscosity measuring cell for cleaning and checking of all parts.
More information:
Rinsing the outside of the rotor and the drive shaft seal, Chapter 10.3,
Reference Manual on CD-ROM.
Drive shaft seals: handling leakage, replacement, leak test; see Chapter 18,
Reference Manual on CD-ROM.
SVM 3000/G2 39
9 Filling and Cleaning the Measuring Cells
The viscosity measuring cell contains a measuring rotor which is made of two
rotors and two rotor bearing rings. The outer rotor is a hastelloy tube and inside
this tube is a sensitive titanium rotor. Disassemble the measuring rotor if the usual
rinsing and drying procedure is not sufficient.
Caution:
• The SVM 3000 should only be opened by trained personnel as it
contains very sensitive components. The drive shaft can be bent very
easily. The inner titanium rotor has a very thin wall. Take care when
cleaning.
• Anton Paar GmbH is not liable for components which have been handled
incorrectly.
Working steps:
The motor must turn on filling speed, the instrument stays switched on.
1. Disconnect the cell connection tube (J in Fig. 5 - 2) and unscrew the waste
hose from the viscosity outlet nozzle.
2. Open the front flap.
Fig. 9 - 2
2 Fig. 9 - 3
40 SVM 3000/G2
9 Filling and Cleaning the Measuring Cells
Fig. 9 - 4
Warning:
The measuring rotor could still be hot from the last measurement. To prevent
injury, make sure that the temperature of the measuring cell has decreased
before removing or disassembling the measuring rotor.
Fig. 9 - 5
Caution:
Make sure that the drive unit is pushed back to the left as far as it will go so
that the drive shaft cannot be damaged by the brush.
8. Carefully push the titanium rotor out of the hastelloy rotor using the 5 mm
cleaning brush.
SVM 3000/G2 41
9 Filling and Cleaning the Measuring Cells
Caution:
The titanium rotor has a very thin wall and can easily be damaged. Do not use
tools such as pliers or tweezers to handle the rotor. Do not use polishing
agents, abrasive paper or other cleaning aids other than the supplied brushes
and a soft cleaning paper.
If dried sample residues cannot be removed, place the titanium rotor in a
suitable solvent. If the titanium rotor is damaged mechanically during cleaning,
check the adjustment of the instrument with a control measurement.
Fig. 9 - 7
10. Wipe the other components clean with lint-free paper dipped in solvent. Dry
all parts.
2 5
1
3 4
Note: Your SVM 3000 can also be equipped with a conical titanium rotor. See Fig.
9 - 9.
2 5
1
3 4
1 ... Rotor bearing ring drive side PEEK (Mat. No. 87455)
2 ... Hastelloy rotor (Mat. No. 6004)
3 ... Conical titanium rotor (Mat. No. 80708)
4 ... Rotor bearing ring fill side PEEK (Mat. No. 87456)
5 ... Marking for direction of assembly
42 SVM 3000/G2
9 Filling and Cleaning the Measuring Cells
11. Lubricate the O-rings to make them slide easier. The rotor bearing rings have
one and two grooves. The hastelloy rotor has one end with one locating key
and one end with two locating keys. This design should prevent wrong
assembling.
12. Push the titanium rotor into the hastelloy rotor. The marking on the titanium
rotor must point into direction of the arrow on the hastelloy rotor. If the
titanium rotor is inserted in wrong direction, this may lead to measuring
deviations.
13. Swivel the unlock lever for the motor into the instrument to the end stop. This
engages the drive unit to the right.
14. Insert the measuring rotor in direction of the arrow into the thermostat tube.
15. Screw in the viscosity inlet nozzle carefully.
16. Close the viscosity inlet nozzle with a Luer plug and screw an adapter Luer
UNF into the waste tube.
17. Fill the supplied glass syringe or a new 5 mL disposable syringe up to the
4 mL mark with air.
18. Connect the syringe to the adapter Luer UNF.
19. Press in the plunger of the syringe up to the 1 mL mark and let it move back
out again. The plunger must move back to at least the 2 mL mark. Repeat
the procedure several times. The plunger must return to the almost same
position as it reached the first time.
20. Remove the Luer plug and the adapter Luer-UNF and mount again the cell
connection tube.
More information:
Disassembling the viscosity measuring cell, measuring rotor and parts see
Chapter 10.4, Reference Manual on CD-ROM.
Drive shaft seals, handling leakage, leak test and replacing wearing parts see
Chapter 18, Reference Manual on CD-ROM.
For disassembling, cleaning, leak test and wearing parts see also the SVM
3000 Video Manual.
SVM 3000/G2 43
10 Menu Structure
10 Menu Structure
To ease operating the instrument for routine jobs, in the lowest user level
"operator" many functions are hidden. In the user level "administrator" the
instrument modes can be adapted to the requirements of the customer and further
settings can be done. In the following a short description of the user level
"operator" is given. Other than the temperature, no instrument settings can be
changed.
Information:
The option of changing the temperature setting can be deactivated in the
menu "mode settings - measuring temp. - temp. changes allowed". This
can only be carried out at the "administrator" level.
More information:
Detailed description user level "operator" see Chapter 12.1, Reference
Manual on CD-ROM.
User level "administrator" (password: 3000) see Chapter 12.2., Reference
Manual on CD-ROM.
"user level"
Enter the appropriate password to access different user levels.
44 SVM 3000/G2
10 Menu Structure
"data memory"
Contains the chronologically stored measuring data sets. Data is stored
automatically and always when printed (when pressing the PRINT key.)
"browse"
Here you can view the data.
ARROW UP/DOWN:
Browse between the data sets.
ARROW RIGHT/LEFT:
Browse between the measuring values of one data set.
The letters at the end of the date and time field show whether the data set
has been read out by a computer (f/F="fetched") or if it has been printed
out (p/P ="printed"). Capital letters mean "Yes", small letters mean "No".
The "printed" (P) state can be reset in "data memory - browse" for the
current data set by pressing ENTER. This allows a second printout. The
command "reset data" can be sent from a PC via the serial interface (PC)
to reset all stored data sets to the state "f" and "p".
"print data"
The results in an instrument mode are printed out according to the date,
beginning with the oldest measuring value.
The number in the last line of the display is the number
of the memory content which is being printed at that
time (0 to 383).
Information:
Make sure there is enough paper in the printer. For results from max. 384
measurements, each with up to 16 lines (= max. 6144 lines), you would require
approx. 24 m of paper - this is nearly a third of a new paper roll!
SVM 3000/G2 45
10 Menu Structure
"calibration"
Calibration menu. The settings cannot be changed in the level "operator".
To perform calibration measurements refer to Chapter 14, Reference Manual on
CD-ROM. The calibration reminder is set to 0 days by default (deactivated).
"new calibration"
Select this menu to perform calibration measurements.
"temperature"
Starts the temperature calibration by pressing ENTER.
"check measurement"
Automatic viscosity and density verification measurement at maximum 5
temperature points. The settings cannot be changed in the level "operator".
To perform a check measurement refer to Chapter 15, Reference Manual on CD-
ROM.
"print results"
Prints the results of the last performed verification measurement.
"measuring window"
Press ENTER to return to the measuring window.
More information:
Complete menu tree (user level "administrator") see Appendix B.
Complete description of the menu (user levels "operator" and "administrator")
see Chapter 12, Reference Manual on CD-ROM.
46 SVM 3000/G2
Appendix A: Technical Data
Measuring temperature :
• Maximum: +105 °C
• Minimum without cooling: 20 °C below ambient temperature
• With cooling at -20 °C: -40 °C (at max. 23 °C/73 °F room temperature)
• With cooling at -40 : -56 °C (at max. 23 °C/73 °F room temperature)
Reproducibility (Special calibration might be required outside the works adjustment range.):
• Viscosity: ±0.35% of the measured value within the works adjustment range
(typical values for clean base oils) under conditions of the instructions in Chapter 8.4.3, Reference
Manual on CD-ROM)
• Density: ±0.0005 g/cm³ from 0.65 to 1.5 g/cm³
±0.0020 g/cm³ outside this range
• Temperature: ±0.02 °C (±0.04 °F) from 15 to 105 °C (59 to 221 °F)
±0.05 °C (±0.09 °F) outside this range
Repeatability * :
• Viscosity: ±0.1% of the measurement value
• Density: ±0.0002 g/cm3
• Temperature: ±0.005 °C
SVM 3000/G2 47
Appendix A: Technical Data
Materials in contact with the sample: PTFE, PEEK, Hastelloy C276, titanium, stainless steel A4, Viton 981
Extreme (ETP 600S), borosilicate glass
Solvent consumption:
• Minimum: 5 mL per sample
• Typical: 10 mL per sample
Dimensions (L x W x H): 440 x 315 x 220 mm
Weight: approx. 16 kg
Caution:
All serial interfaces conform to the SELV regulations (Separated Extra-Low
Voltage) according to EN 60950. Interfaces which do not conform to the SELV
regulations must not be connected.
More information:
Description of the interfaces see Chapter 20, Reference Manual on CD-ROM.
48 SVM 3000/G2
SVM 3000/G2
FILLING
MEASURING
RESULT VALID
ERROR
49
Appendix B: Menu Tree "Administrator"
50
mode settings mode name M0-A...A - M9-A...A
temperature unit °C, °F
measuring temp. temp. change allowed yes, no
set temperature ±xxx.xx °C
filling temperature cell temperature ±xxx.xx °C
set Xsample heating Xsample temperature ±xx °C
(to be used with Xsample temp offset ±x.x °C
heated Xsample) magazine temperature ±xx °C
magazine temp offset ±x.x °C
display settings page 1/2: line 1/2/3 base values dynamic viscosity
kinemat. viscosity
equilib. density
predeterm. density
shear rate D
Appendix B: Menu Tree "Administrator"
SVM 3000/G2
mode settings display settings
continued continued raw values Q-1 raw
SVM 3000/G2
Q-1 time average
raw density
oscillator period
raw dyn. viscosity
raw kin. viscosity
Xsample heating act. temp. Xsample
(to be used with heated act. temp. magazine
Xsample)
measurement mode automatic
viscosity index
viscosity index
temp. table scan
temp. range scan
manual control
meas. precision ultrafast
fast
standard
precise
equilibration time delay: xxx seconds
automatic repetition repetition number maximum: x
data memory options all determinations
final result only
viscosity limit RDV xx.xx %
density limit RDD x.xxxx g/cm3
air pump timeout xxx seconds
temp. range scan start temperature ±xxx.xx °C
stop temperature ±xxx.xx °C
temperature step xx.xx °C
51
Appendix B: Menu Tree "Administrator"
52
instrument settings
continued
printer interface baudrate 19200, 9600, 4800, 2400, 1200
format E71, O71, N81, N82
line delimiter <CR><LF>, <CR>, <LF>, <LF><CR>
flow control hardware: RTS/CTS, none, software: Xon/Xoff
date and time 20xx xx xx xx:xx:xx
admin. password 3000
external keyboard US english (QUERTY)
german (QUERTZ)
sound settings play all sounds
warnings and prompts
warnings only
all sounds off
print configuration only for Xsample: prints the hardware and firmware version numbers
Xsample activation use heating (for Xsample heating attachment)
Appendix B: Menu Tree "Administrator"
yes, no
user level
measuring window
SVM 3000/G2
Appendix C: Maintenance Schedule
More information:
Detailed mainenance schedule see Appendix D in the Reference Manual on
CD-ROM and the listed chapters in this schedule for performing the
maintenance work.
SVM 3000/G2 53
Appendix D: Declaration of Conformity
54 SVM 3000/G2