Electron Diffraction

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Vellore Institute of Technology BPHY101P Engineering Physics Lab Manual

Demonstration of wave nature of electrons through


electron diffraction
Objective
To calculate the interplanar spacing of polycrystalline graphite from electrondiffraction pattern
and to obtain de Broglie wavelength of electrons at different accelerating voltages.

Apparatus to be used

Electron diffraction tube, High voltage (up to 10 kV) power supply, Connecting wires, ruler.

Basic theory
In this experiment we form an electron diffraction pattern consisting of circular rings, after the
electron gets transmitted through a very thin polycrystalline graphite sheet. Figure showssheet of
graphite with hexagonal arrangements of carbon atoms.

Consider this arrangement as two sets of inter-penetrating planes of atoms each with its own
interplanar distances 1 and 2 in order of Angstroms. These planes can be further considered as
two sets of inter-penetrating multiple slits. If electrons behave like waves and if they are allowed to
pass through these slits, they would get diffracted just as EM waves get diffracted (provided their
wavelength is comparable to interplanar distances).

The apparatus shown in the figure below depicts that electrons are produced at filament,
accelerated and passed through the thin graphite crystal. To accelerate electrons,a power supply is
used. There are sets of circular disks inside evacuated tube in which the right most is anode with
graphite crystal and left most is cathode. Remaining disks are to focus electrons. Electrons passing
through the graphite hit the florescent screen on the right end of the tube. As graphite has two
different lattice spacing, two diffraction rings are seen at each voltage..
Vellore Institute of Technology BPHY101P Engineering Physics Lab Manual

Now, we can apply law to this case. For the first order diffraction
= d sin (1)

From theory, de Broglie wavelength of an electron accelerated through a potential V is


= 12.3 Å/ (2)
From the geometry of the above figure,

(3)

Procedure
First, turn ON the voltage controller and make sure the initial voltage is set to zero. After that,
turn thevoltage knob slowly so that we can see a set of two rings on the florescent screen. Since
diffraction is property of waves, we demonstrate that electrons too exhibit wave nature. By this
demonstration, interplanar distances can be also be found by measuring the diameter of the
rings. For the inner ring, first measure the inner diameter and then the outer diameter
using a ruler. Find out the average diameter . Similarly for outer ring, measure the
inner and outer diameters and find out the average . Now, Repeat these
steps for different accelerating voltages 3.5 to 5 kV, at voltage intervals of 0.5 kV.

Precautions
Never accelerate beyond 5 kV.
Never touch any controls on the power supply other than the switch and
the voltage varying knob.
Never apply force while measuring the ring diameters.
Keep a ruler gently over the tube to measure the diameters of rings. Metalrulers are strictly
prohibited.
Vellore Institute of Technology BPHY101P Engineering Physics Lab Manual

Observations
Distance between graphite sheet and screen (L) = 13.5 cm. For inner ring, d1 =

sin d1(Å)
(kV) (cm) (cm) (cm ) (nm)
(kV)-1/2

For outer ring, d2 =

(kV) sin d2(Å)


(cm) (cm) (cm ) (nm)
(kV)-1/2

Calculations
By using the values from table, calculate sin , , d1 and d2 with the help of equations (3),
(2) and (1), respectively. And then calculate the average of d for inner and outer rings.

Results
Interplanar distances of the graphite are found to be and
Vellore Institute of Technology BPHY101P Engineering Physics Lab Manual

Inferences/Conclusions

Questions on related concepts (Self-assessment)

Q1. Why cannot we explain diffraction by assuming particle nature of electrons?


Q2. What is/are the source of error in this experiment?
Q3. Why does the diameter change with voltage?

Q4. What does the inner and out circle indicate?

Q5. How can you get the interplanar spacing graphically?

Q6. Why do we have a circular pattern?

Further references

[1] https://www.youtube.com/watch?v=IYnU4T3jbgA

[2] https://www.youtube.com/watch?v=AM8LcaKxZGg

[3] https://www.youtube.com/watch?v=l2OXawoAD6M

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