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    Exp 7

    Uploaded by

    Savar Jaiswal
    The document describes an experiment to calculate the interplanar spacing in a graphite sample using electron diffraction. Key steps included: 1) Using an electron diffraction tube with a high voltage power supply up to 4kV. 2) Measuring the angles of diffraction peaks when different accelerating voltages were applied. 3) Calculating the interplanar spacing using the diffraction formula. 4) The average interplanar spacing measured for graphite was 20.56nm.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    Exp 7

    Uploaded by

    Savar Jaiswal
    18 views7 pages
    The document describes an experiment to calculate the interplanar spacing in a graphite sample using electron diffraction. Key steps included: 1) Using an electron diffraction tube with a high voltage power supply up to 4kV. 2) Measuring the angles of diffraction peaks when different accelerating voltages were applied. 3) Calculating the interplanar spacing using the diffraction formula. 4) The average interplanar spacing measured for graphite was 20.56nm.

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    The document describes an experiment to calculate the interplanar spacing in a graphite sample using electron diffraction. Key steps included: 1) Using an electron diffraction tube with a high voltage power supply up to 4kV. 2) Measuring the angles of diffraction peaks when different accelerating voltages were applied. 3) Calculating the interplanar spacing using the diffraction formula. 4) The average interplanar spacing measured for graphite was 20.56nm.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    18 views7 pages

    Exp 7

    Uploaded by

    Savar Jaiswal
    The document describes an experiment to calculate the interplanar spacing in a graphite sample using electron diffraction. Key steps included: 1) Using an electron diffraction tube with a high voltage power supply up to 4kV. 2) Measuring the angles of diffraction peaks when different accelerating voltages were applied. 3) Calculating the interplanar spacing using the diffraction formula. 4) The average interplanar spacing measured for graphite was 20.56nm.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 7

    Sunit

    Dals
    ExPERIMENT -1 20BMEO 651
    Sowa Jois wa
    ELECTRON OIFPRACTiON

    Atm To (olcuulake He inteplanak Spacina


    n
    gkaphute m diprachn paie

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    e kawe
    Sin 8 R
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    Simpliui9 wit E 13:5 Cm

    Sing
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    Kre ceduse:
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    Step-2 F te unne uing, meaouhe tidiate (28)
    Step3 l b a He uken 9u aeao wMe He diawttes(2 Ra)_
    Stepy alculate sinG and d
    SHep:5- epeot He Steps fo dipjoet orcelerakng
    Voltagep
    Shep:6 alcuote He Ouerage fe boH unnerand
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    CalculaHos

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    Cose V 4-o EV d /sine
    A 12.3 A 6.194 A O-q4/. 099
    4ooo d 2064 A
    o-o99
    ( + (3.s/(.215 ) 2) 2
    Sunil
    Pogo
    Dalo
    Case.2 V= 4-5kv A dsin e
    Ri R2 = 20D C
    A 12:3
    d Aine
    A° o.1B3A os d o 183/o.o 89
    4.5x looo
    d 2.o56 A°
    Sin9 O.089
    I+(13.5/1-200)2)|2

    Case.3 V 5 kv
    Sin9 + O o8 5
    (13.5/1-15)2)V2
    Rie R2 1-15ocn
    A 12 3 =O-174A° ol O.l74 2- o4T4°
    JSx1o oo Sine O o85

    For Oute
    Cane V=4 KV O 159
    R R2 2-175 tm L3-5/R-115)2 ) *2
    A 12-3 0 19 A° d a O-19491-22oA
    Jxlo o0 Sine o-59

    Cabe V 4-5 kV
    E
    sin8 O.154
    Ri R2 =
    2.1 cm C1+C13sl2-1)2) \n
    A 12:3 O.183AA d : o183= 18 8 A
    .SX looD Sin O.IS

    Cane 3 V V d: O.174
    Sin O 4S
    RiE R2 1.97 5
    12.3 O.174A 1-2oo A
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    sio9
    ( (13 s/(.9 75)2) 2
    d fo wne eug
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    de ditdet d3 v
    3 oosia 9
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    ecso b
    3 oolxd
    2 oS6 A &

    AveAage d for owweh iug

    A e do 22o t 1 8 8 +120O
    3

    2o3 A |
    -
    oss SEA
    TLDHU9 20BMEO651
    oedo Diaq r a n aTB9491C
    L

    F
    8
    2R
    ol9

    loo K2
    Schemahc diag ram of enpt
    Setup hg-1)
    - 2R -
    d

    da

    2R2
    The duff rachibn ings
    2 diffenent ypeb o poLe duced by these
    olkice planes otice plane
    O bsew akon
    Table
    QoBMEO651
    Sava Jais wa9
    2R (o1) Ri os P2
    Ring
    Rin9 V(EU) 2R2 (cm) Sin9 d
    (cm) (A°) (deg CA)

    255 -215 O-194 Oe94 2054


    Tnnes
    4.5 24o 1-200 O-183 0-089 2 oS6
    5:0 2-301-15o O.74 Ooo85 2-o47

    4-35 2115 O194 o.159 -220


    Oude
    4.5 2 0 2ooO183 154 188
    5.03.a5191s 0.174 O145 1-200
    unil
    Pagps
    Dalo
    PHecauHoo:

    Neue acceleuake pekenhial beuad5Ev


    2 ee toud ay utels 9 the p9uue &uppu
    heh Han ONMOe Sutc of V' kngb
    Neve uoe foue L9 'aeasuhë he ui diometers
    p AoQyg mea0Lo He teng dfameteHo uwtt80+
    kands
    S99 not touc ay oHen_paut_of waclie emept
    enfSwltt fo Baeypurpase
    Reult:

    Thewteuplaak Spacing in 9ap kte ha


    meapLed O
    20.56nm
    Inne ung (di) = 2 os6 A
    0uteing (do) 1203 A° l2-o3 nm

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