AFTES - Slurry For Use in Slurry Shield TBM
AFTES - Slurry For Use in Slurry Shield TBM
AFTES - Slurry For Use in Slurry Shield TBM
ET DE L’ESPACE SOUTERRAIN
AFTES
Recommendations
Text prepared by
P. LONGCHAMP (Bouygues Travaux Publics)
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CONTENTS
Pages Pages
1 – FOREWORD – PURPOSE OF THE RECOMMENDATIONS - - 165 4.1.3 – Plastic viscosity (PV) - - - - - - - - - - - - - - - - - - - - - - - - 168
2 – BASIC ROLES AND FUNCTIONS - - - - - - - - - - - - - - - - - - - - - 166 4.1.4 – Yield point - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 168
2.1 - General - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 166 4.1.5 – Thixotropy and gels - - - - - - - - - - - - - - - - - - - - - - - - 169
2.2 – Primary functions of slurry - - - - - - - - - - - - - - - - - - - - - - - - 166 4.2 – Physical properties - - - - - - - - - - - - - - - - - - - - - - - - - - - - 169
2.3 – Secondary functions and qualities of slurry - - - - - - - - - - - 166 4.2.1 – Density of slurry - - - - - - - - - - - - - - - - - - - - - - - - - - - 169
3 – BASIC PRINCIPLES FOR USING SLURRY - - - - - - - - - - - - - - - 167 4.2.2 – Sand content (particles > 80 µm) - - - - - - - - - - - - - - 169
3.1 – Confinement function - - - - - - - - - - - - - - - - - - - - - - - - - - 167 4.2.3 – Filterability - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 169
3.1.1 – General - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 167 4.2.4 – Quality of cake - - - - - - - - - - - - - - - - - - - - - - - - - - - 169
3.1.2 – Filtration - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 167 4.3 – Chemical properties - - - - - - - - - - - - - - - - - - - - - - - - - - 169
3.1.3 – Stiffening of slurry - - - - - - - - - - - - - - - - - - - - - - - - - - 167 4.3.1 – Presence of electrolytes - - - - - - - - - - - - - - - - - - - - - 169
3.1.4 – Types of cake - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 167 4.3.2 – pH variation - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 170
3.1.5 – Speed of cake formation - - - - - - - - - - - - - - - - - - - - - 167 5 - MATERIELS AND PROCEDURES FOR MEASURING SLURRY
3.2 – Transport function - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 167 QUALITY - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 170
3.3 – Separation function - - - - - - - - - - - - - - - - - - - - - - - - - - - - 167 5.1 – Test equipment - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 170
3.4 – Changes to slurry during excavation - - - - - - - - - - - - - - - - 167 5.2 – Procedures - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 170
3.4.1 – Physical contamination of slurry by solid load - - - - - - 167 6 – CHOICE OF MAIN SLURRY CHARACTERISTICS - - - - - - - - - 170
3.4.2 – Chemical contamination of slurry - - - - - - - - - - - - - - - 167 6.1 – Properties - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 170
4 – BASIC PROPERTIES OF SLURRY AND THEIR MEASUREMENT 167 6.2 – Guiding the choice of slurry type - - - - - - - - - - - - - - - - - 170
4.1 – Rehological properties - - - - - - - - - - - - - - - - - - - - - - - - - - 168 7 – COMPONENTS OF SLURRY - - - - - - - - - - - - - - - - - - - - - - - - 171
4.1.1 – Introduction - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 168 7.1 – Composition - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 171
4.1.2 – Apparent viscosity (AV) - - - - - - - - - - - - - - - - - - - - - - - 168 7.2 – Choice of components - - - - - - - - - - - - - - - - - - - - - - - - - 171
CONTENTS
Pages Pages
8 – TREATMENT OF EXCESS SLURRY (see Appendix 6) - - - - - - 171 2 - Types of polymers used in tunnelling slurry - - - - - - - - - - - - - 174
9 – SLURRY SCHEDULE - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 172 2.1 – Starches and amylase derivatives - - - - - - - - - - - - - - - - - 174
9.1 – Objectives - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 172 2.5 – Polyacrylamides - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 174
9.2 – Preparation - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 172 2.6 – Polyacrylates - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 174
9.2.1 – Regulatory considerations: environment / health 3 - Bentonite - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 174
and safety - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 172 3.1 – Structure of bentonite- - - - - - - - - - - - - - - - - - - - - - - - - - 175
9.2.2 – Site conditions: project geometry, geology, 3.2 – Bentonite properties - - - - - - - - - - - - - - - - - - - - - - - - - - 175
geotechnics, and landtake - - - - - - - - - - - - - - - - - - - - - - 172 3.3 – Bentonite for underground works - - - - - - - - - - - - - - - - - 175
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S
lurry is an indispensable aspect in the use of closed face slurry-shield tunnel boring machines (TBMs), for tunnel support and for slurry remo-
val. The AFTES Recommendations on the choice of mechanized tunnelling techniques (TOS No. 157, January/February 2000, paragraphs
4.3.4, 6.3.3, 7.3.3, and 8.5) provide more information on this.
AFTES Working Group GT 4 dealing with mechanized excavation considered it important to publish recommendations on slurry.
The science of slurry for this kind of application is indeed relatively complex. It consists of a combination of experience and theory, as the slurry
itself combines rehological, physical, and chemical phenomena. It also has to take account of another range of complex sciences, the earth
sciences.
Use of slurry for tunnelling can undoubtedly trace its origins back to drilling fluid (mud) for vertical holes. Because of their immense resources and
the economic issues involved, oil companies played a leading role in the development of the technology. Civil engineering thus benefited from a
wealth of prior knowledge, first in respect of deep foundations and drill holes for ground improvement, and then, some years later, for excavation
of tunnels in loose water bearing granular soils.
While the composition of tunnelling slurry is essentially the same as that of the drilling mud used in the oil industry, it does have its own special
requirements. Some examples are given below:
➬ For vertical drilling: the hole by laminar flow to prevent erosion of ➬ For tunnelling:
the borehole walls. This calls for low flow velo-
• The volume and sectional area of the bore- • Support conditions are generally more diffi-
cities and a mud whose viscosity enables it to
hole are relatively small, and any ground insta- cult , with a high risk of instability.
carry the cuttings at that speed.
bility is localized. • Slurry pressure is produced and controlled
• The borehole generally goes through a series
• The mud pressure is governed directly by its mechanically.
of sub-horizontal geological strata, but gene-
density and the hydrostatic head. • Spoil is carried by a turbulent flow regime
rally crosses them at nearly perpendicular
• Cuttings from the cutterhead are carried up angles. which requires high flow velocity; the suspen-
ded solids (cuttings) carrying capacity is is to impart to the tunnel walls and excava- Excavation of the tunnel produces a change
governed by the dynamics of the turbulence . tion face the qualities that will hold up the in the state of initial stress around the ope-
• Since the geological strata encountered are excavation. To achieve this, its components ning. σv is assumed to be constant whereas
sub-horizontal and sub-parallel to the axis of and physical properties must: σh tends to 0. The initial Mohr circle (➀)
excavation, ground at the face is often strati- • create an impermeable membrane at the expands until it reaches the critical circle ➃
fied and heterogeneous. ground interface (at the face and around the beyond which stability is no longer guaranteed.
• The excavation volumes involved and the shield, in the case of overcutting). The This diagram has been simplified. It corres-
sectional face areas of the excavation are ground interface must be made imper- ponds to the stability of an infinitely large
large with meable so that the slurry can develop ade- tunnel face with a two dimensional stress
quate confinement pressure, or, more preci- state. In practice, stability calculations involve
The basic solids mixing component for sely, extra confinement pressure above the three-dimensional stress mechanisms.
mud/slurry is bentonite, a type of clay with hydrostatic ground water pressure.
very special physical and components pro- 2.3 – SECONDARY FUNC-
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3 - BASIC PRINCIPLES • Impregnation cake: in moderately to required for tunnel support. A trade-off must
highly permeable ground of varying porosity, therefore be found to meet the opposing
FOR USING SLURRY the slurry penetrates relatively deeply into requirements of ground support and solids
the pores in the ground before it stops and separation.
3.1 – CONFINEMENT sets. It is this impregnation that constitutes
FUNCTION The basic operation of a slurry separation
the impermeable interface. This zone can
and treatment plant is described in
vary between several tens of centimetres and
Appendix 6.
3.1.1 – General several metres thick.
3.4 – CHANGES TO SLURRY
Slurry penetrates the ground at the face and 3.1.5 – Speed of cake formation
DURING EXCAVATION
along the tunnel walls (especially in the case
of overcutting). As commented above in § 3.1.2, the filter
cake at the tunnel face is partially or totally A variety of external contaminates blend into
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In accordance with the permeability of the destroyed with each sweep of a cutting tool, the slurry as excavation proceeds, and can
ground and its intrinsic properties, the but re-forms behind it immediately. modify its initial characteristics.
slurry’s penetration into the ground will gra-
dually slow down, then stop, as a result of Rheograms (cf. Section 4.1) show that the 3.4.1 – Physical contamination of
two interdependent, simultaneous pro- yield point of the slurry after agitation is slurry by solid load
lower than its initial value.
cesses: filtration (pressure filtration) and an
increase in the stiffness of the slurry. It therefore takes some time period before Slurry treatment plants cannot filter out the
the slurry returns to its initial consistency. finest soil particles. The concentration of
3.1.2 – Filtration This time should be as short as possible in external contaminates particles in the recy-
order to reinstate watertightness to its full cled slurry therefore increases with continued
The pressure in the cutterhead chamber value. It is characterized by the “0-10 min. use of the slurry and the density of the slurry
forces the slurry through the soil at the tunnel gel strength” test (cf. § 4.1.5). gradually increases, generally to the detri-
face and walls and into the ground. As it per- ment of its properties (yield point, filtrate,
meates the ground, the liquid and solid com- 3.2 – TRANSPORT etc.) (cf. § 4.2).
ponents of the slurry are separated, gra- FUNCTION It then becomes necessary to regenerate the
dually leaving the solids at or near the slurry by adding fresh slurry.
surface, The apparent viscosity of the slurry (cf. 4.1.2)
must be as low as possible for the hydraulic
The filtered solids themselves enhance the 3.4.2 – Chemical contamination of
mucking system. One of the properties of
filtering process until the barrier is imper- slurry
Bingham fluids is that above the yield point,
meable. When the face is excavated, the
the apparent viscosity decreases with increa- Minerals or pollutants in the soil and/or
filter is partially or totally destroyed by each
sed agitation. Sufficiently intense agitation is groundwater can also modify the characteris-
cutting tool, but the process resumes imme-
obtained by creating a turbulent flow regime tics of the slurry. They should therefore be
diately once the tool has passed.
in the slurry pipes. taken into account when the slurry compo-
This continuing process results in creation of
nents are chosen (cf. section 4.3).
a filter cake of varying thickness, depending 3.3 – SEPARATION
on the permeability of the ground and the FUNCTION Attention should also be paid to the possibi-
characteristics of the slurry. lity of contamination of the slurry by cement
Use of slurry to excavate and support a tunnel and other chemical products (silicates etc.)
3.1.3 – Stiffening of slurry and to remove excavation spoil necessarily used for ground improvement prior to tunnel
implies that the slurry is treated in order to: excavation.
The filtration effect of slurry penetrating into
the ground immediately reduces the velocity • separate solid spoil from the slurry so that
of slurry flow into the ground. the slurry can be recycled into the mucking
circuit 4 – BASIC PROPERTIES OF
Bentonite slurry is a non Newtonian (ref.
• separate in excess slurry as new slurry is SLURRY AND THEIR MEASU-
chapter 4). Therefore, as a consequence of
its reduction in flow velocity, it gradually stif-
added REMENT
fens and “sets”. • treat in excess slurry for disposal. The slurry used for closed face shield TBMs is
Setting is directly linked the conventional The first two of these operations are carried a water-based fluid with a variety of solids
yield point or “yield value” of the slurry. out in real time, and the separation rates are added to form a colloidal suspension. The
governed by the instantaneous penetration solid components are essentially:
3.1.4 – Types of cake rate of the TBM. Slurry in excess can be trea-
• mineral colloids (chiefly bentonite)
ted as a background task, and is governed by
There are two types of cake: the mean advance rate (limited to a certain • organic colloids (chiefly polymers).
• Membrane cake: this is obtained in ground time interval), taking account of shutdowns, There are hundreds of branded products
of low permeability by using a relatively stiff lining erection, etc. throughout the world described as bento-
slurry. The slurry does not penetrate very far The components and physical characteristics nites or polymers. This can lead to conside-
into the ground, and creates only surface of a slurry must take into account this requi- rable confusion, for although they may be
imperrmeabilization of the ground interface. rement for separation. These characteristics similar, they often have very different physico-
It will be several millimetres thick. may be inconsistent with the characteristics chemical, rehological, or filtration properties.
4.1 – RHEOLOGICAL Apparent viscosity is the relationship between 4.1.3 – Plastic viscosity (PV)
PROPERTIES the shear stress and the velocity gradient.
Consequently it is not a constant quantity: Plastic viscosity concerns non-Newtonian
fluids and characterizes Bingham fluids. It
4.1.1 - Introduction corresponds to the gradient of the linear part
of the rheogram, as shown
Rheology is the science devoted to the study Newtonian fluid
of deformations and flow of matter under the
effects of internal and external stresses. In
Bingham fluid
rehological terms, tunnelling slurries are defi-
ned by a number of characteristics whose
Apparent viscosity
measurement and verification are of the
greatest importance since they govern:
Shear stress
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Apparent viscosity
• stabilization of the tunnel face and control
Shear stress
of ground water
• muck removal
• slurry preparation and treatment perfor- Velocity gradient
mance.
Refer to Appendix 5 (Slurry rheology) for Velocity gradient
more information.
Slurry
4.1.2 – Apparent viscosity (AV)
Slurry
The apparent viscosity of slurry is its “real vis-
cosity”. However, since these kinds of fluids
are non-Newtonian, their viscosity depends Apparent viscosity
on their flow velocity. Their viscosity is high
Shear stress
Apparent viscosity
for low velocities (during filtration into the
Shear stress
ground, in storage tanks), but conversely, is
low for high velocities (in muck pipes, in
hydrocyclones), as can be seen from the fol-
lowing graphs:
Velocity gradient
Viscosity-velocity gradient graphs are not
often used. Since viscosity is determined by Velocity gradient
the shear
Viscosity-velocity gradient graphs are not Rheogram: solid lines
In the case of tunnelling slurries, the plastic
often used. Since viscosity is determined by Apparent viscosity: dotted lines viscosity is deemed to be constant, as a first
the shear forces at play between layers of
Apparent viscosity is expressed in mPa◊s approximation. It is determined by extrapo-
liquid, it has become customary to use a gra-
these days, and formerly in centipoise (cP). lating the linear part of the rheogram (as
phic representation of the shear stress ver-
shown above). This physical quantity is
sus velocity gradient; commonly called a 1 mPa.s = 1 cP
important for calculation of pressure losses in
rheogram. Viscosity is no longer explicitly
the slurry pipes. It depends above all on the
discussed.
solids content of the slurry and the nature of
those solids.
Plastic viscosity is also expressed in mPa.s
(or cP).
Newtonian fluid Slurry
4.1.4 – Yield point
The yield point determines the ability of a
Apparent viscosity
point, and since its viscosity is infinite, it and 10-min. gel strengths (refer to the (cyclone split ratio). Any sand remaining in
behaves like a solid. The actual yield point “Thixotropy” entry in the glossary). the slurry directly affects the permeability of
depends on initial conditions and increases Bentonite has this thixotropic behaviour. the cake and its stability on the ground
with time at rest. In slurry-tunnelling practice, Other commonly used additives such as interface.
the convention is to use a value determined water-soluble polymers contribute other pro-
from the intersection on the rheogram of the perties (viscosity, filtrate reduction, electroly- 4.2.3 - Filterability
straight line obtained with the Fann rheome- tic stability, etc.).
ter and the vertical scale of co-ordinates. Filterability is the ability of a slurry to imper-
The rheogram below illustrates the concepts meabilize the ground interface by forming a
This extrapolation is called the Yield Value described above.
(cf. below). filter cake. It depends on the quality and
quantity of the components making up the
4.2 – PHYSICAL PROPERTIES
slurry.
Filterability is generally inversely related to
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the clay-layers and can produce coagulation ❑ Testing chemical properties the thickness of the cake. It will sometimes
and flocculation of the suspension. These ➘ pH: indicator strips, pH meter limit hydration of geological strata contai-
ions modify ion balances, resulting in phase ning clay or evaporite.
separation due to liberation of free-water ➘ Conductivity: conductivity meter
❸ Density
molecules initially attached to clay platelets ➘ Specific surface (“activity”): methylene
or polymer chains: this results in flocculation. blue value The density of a tunnelling slurry depends on
Special attention must be paid to the chemi- its components, on physical contamination
➘ electrolyte content by fines from the ground that are recycled
cal composition of water (lime-bearing water,
sea water, etc.) throughout the excavation through the slurry circuit, and on regenera-
5.2 - PROCEDURES tion by fresh slurry and additives.
process.
Most slurry tests required already have stan- It has an effect on viscosity and therefore on
4.3.2 – pH variation dardized test procedures, principally develo- pressure losses in the slurry circuit.
ped by the oil industry (cf. American
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A change to the pH of the slurry also affects The thickness and permeability of the cake
Petroleum Institute: section 13),
its ion balances and physico-chemical pro- increase with greater density, which is there-
("Recommended Practice Standard
perties. Beyond a pH range from 8 to 10, fore detrimental to the resistance of mem-
Procedure for Field Testing Water Based
there is a significant risk of poor slurry perfor- branes and the impermeability of the tunnel
Drilling Fluids"), and also the ISO 13500 stan-
mance in both acid environments (in contact walls.
dard. Other test equipment has its own spe-
with organic matter, for instance) and in basic cific test method pertaining to applications in ❹ Other characteristics:
environments (in contact with cement, for other fields.
instance). Other characteristics (pH, polymer or soluble
The methylene blue value is obtained using a salt types and contents, etc.) have to be iden-
standardized test tified for better characterization of a slurry
(French standard NF P18-592). and to meet environmental requirements:
5 - MATERIELS AND • ground/slurry interaction during excavation
PROCEDURES FOR (contaminated sites and grouted areas)
MEASURING SLURRY 6 - CHOICE OF MAIN • recycling in the slurry circuit,
QUALITY SLURRY CHARACTERISTICS • disposal of liquid waste.
5.1 – TEST EQUIPMENT 6.1 - PROPERTIES For guidance, Appendix 4 gives a table sho-
wing representative values for slurry parame-
Many types of equipment can be used for When tunnelling using a closed face slurry ters for different ground permeabilities.
measuring the different physical, chemical, shield TBM, the main characteristics of the
and rehological parameters of slurries. We slurry must be determined in accordance 6.2 – GUIDING THE CHOICE
have selected only the following equipment with:
for continuous measurement.
OF SLURRY TYPE
• the type of ground to be excavated,
❑ Testing rehological properties: measure- • the possible presence of a groundwater, The number of parameters to be taken into
ment of AV, PV, YP, gels together with its chemical properties, account when choosing a slurry type is so
➘ Marsh funnel viscometer (not very mea- great that these Recommendations cannot
• the risks identified (geological, environ- define an exhaustive, “ready-made” proce-
ningful in this field) mental hazards, etc.). dure. Further difficulty arises in the case of
➘ Fann rheometer Among the most important criteria for defi- mixed faces (relative to variation in geology
➘ Possibly, a rheometer with imposed velo- ning a slurry are the following: over short distances).
city gradient (Rhéomat or similar) ➊ Rehological parameters, essentially yield For guidance and training, an elementary
point (YP) and plastic viscosity (PV) classification of ground types on the basis of
- It should be pointed out that many automa- From the yield point and plastic viscosity can their permeability is given below, with sug-
tic viscometers found on tunnelling projects be defined: gestions for the appropriate slurry types:
are derived from the geometry of the Fann • the conditions of impregnation of the ➊ Highly permeable ground with granular or
rheometer and can thus be used to deter- ground interface (formation of cake), intensely fractured structure.
mine the characteristic rehological parame- Solution: bentonite slurry with rheology sui-
• the conditions of fluid flow and solid sepa-
ters of slurry on a “quasi-continuous” basis table for high porosity; in particular, appro-
ration in the slurry circuit and treatment
by measuring values at 600 and 300 rpm. priate yield value, 0/10-min. gel strengths,
plant,
❑ Testing physical properties filtrate.
Methods for calculating these parameters
➘ Density: Baroid mud balance, densimeter are presented in Appendix 3. ❷ Silty to sandy semi-permeable ground.
➘ Sand content kit (sieve analysis apparatus) ❷ Filtration properties Solution: bentonite slurry (pure or with addi-
➘ Filtration and cake: API fluid-loss-test filter Filtration properties govern cake formation. tive) with low filtrate and suitable rheology
press and, for a more realistic approach to The cake must be sufficiently impermeable, (as per above).
interface problems, a large permeameter (cf. strong and flexible (deformable) to guaran- ❸ Impermeable ground with no particular
Appendix 7). tee there will be a pressure gradient across reactivity or sensitivity to water.
Solution: water or bentonite slurry and/or - water-soluble polymers (cf. Appendix 2) throughout the world described as bento-
polymer. - special organic products (defoaming nites or polymers. This can lead to conside-
❹ Impermeable, reactive ground. agents, antifriction agents, etc.). rable confusion, for although they may be
similar, they often have very different phy-
To find the right type, it is necessary to: • Chemical additives: sico-chemical, rehological, or filtration pro-
• have perfect knowledge of the mineralogi- • Various chemical additives such as KCl, perties.
cal composition of the ground, sodium carbonate, sodium polyphosphate, The choice of the polymers or bentonites to
• analyze the physical and chemical interac- etc. for modifying the initial properties of be used will depend on economic considera-
tions of the associated minerals and organic clayey colloids by ion exchange. tions, the specific performance of each pro-
matter. ❹ Groundwater and solids from the ground. duct, the circumstances in which it will be
This makes it possible to quickly define the used, and the following requisite functions:
Active clays and additives are chosen in
best system for inhibiting hydration of clay accordance with the effect desired: • Viscosity level,
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• Limiting the cost of treatment to the exact be required. The geological report should 9.3 – TESTING IMPLEMENTA-
need, specify the physical, chemical, and mineralo- TION AND FOLLOW-UP
• Making provision for the site footprints gical nature of the ground and ground water
necessary for treatment plant in the project that will be encountered, including any parti- Tests should be carried out to establish a sys-
planning stage. cular or localized features. It is also useful to tem for checking the required instructions
include on a longitudinal geological profile and specifications. These tests will concern:
Slurries are stable colloidal suspensions
the prior ground improvement carried out, • Slurry types and components,
of particles that do not easily settle out
with indication of the products used. The
naturally. • Requisite characteristics. The checks are
profile should specify and demarcate the
It is generally necessary to use physico-che- succession of different formations. This data carried out by means of standardized tests
mical treatments to flocculate them and cla- will serve to identify the sequence of diffe- and/or other measuring systems (e.g. real-
rify the water extracted from them. time logging system).
rent slurries best adapted to the individual
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A P P E N D I X 1 : G L O S S A RY
• Activity of clay: The activity of clay is repre- used to determine the values of different • Plastic viscosity (PV): See Article 4.1.3.
sentative of ion charge that gives it the ability rehological parameters (apparent viscosity, With the Fann rheometer, plastic viscosity is
to swell due to adsorption. plastic viscosity, yield point) calculated by testing at 600 rpm and redu-
• Adsorption: Fixing of water molecules on • Filter press: A filter press consists of a cing from the reading the reading taken at
the surface of elementary soil particles (clay series of hollow trays clamped between a 300 rpm. , The unit of measurement is the
platelet for example). mobile plate and a fixed plate by a hydraulic millipascal second (1 millipascal second =
cylinder. The edges of the chambers thus 1 centipoise (former unit)).
• Apparent viscosity (AV): Ratio of the shear
stress to the velocity gradient. The unit of created are covered with filter cloth. Slurry is • Polymers: See Appendix 2, Chapter 2.
measurement is the pascal second (or milli- pumped into the chambers, generally from • Rheogram: Graphic representation of the
pascal second). With the Fann rheometer, it the centre of the trays, and the filtrate is col- behaviour of a fluid subject to shear. Shear
is calculated by testing at 600 rpm and divi- lected in a channel at the side. stress is plotted against the velocity gradient.
ding the result by 2. The unit of measure- • Filtrate test: Laboratory test characterizing • Rheology: Branch of mechanics which stu-
ment is the millipascal second (1 millipascal the ability of a slurry to retain water. Filtrate dies the deformation of materials or their
second = 1 centipoise (former unit)). measurement is expressed as the quantity of flow under stress (see Appendix 5).
• Bentonite: Cf. Appendix 2, Chapter 3. fluid collected in a test tube after 30 minutes
at a pressure of 7 bars exerted by an appara- • Shear stress: Force exerted on a surface by
• Bingham fluid: Fluid requiring exertion of a a fluid and causing shear (refer also to
tus known as the filter press. The unit of mea-
minimum stress to set it in movement. The Appendix 5, Chapter 3).
surement is the millilitre. All things being
Yield Value determines the value of that
equal, the volume of filtrate is proportional • Slurry: Also known as drilling mud/fluid.
stress.
to the area of filtration, to the pressure, and Colloidal clay suspension, with or without
• Cake: In laboratory testing, the thickness of to the square root of the test duration. water-soluble polymers and/or salts to
a layer of solid materials deposited on filter enhance its original characteristics, that has
• Flocculants: Products with inter-particle
paper in the filtrate measurement test (filter- desirable rehological and filtration properties
action due to bridging. They include high-
cake); the unit is the millimetre. For the mea- and possibly the ability to stabilize ground to
molecular-weight polymers, bentonite, etc.
ning in the context of excavation, refer to the be excavated.
definitions in Chapters 3.1.2 and 3.1.4 . • Fluid: See Appendix 5, Chapter 3.
• Stiffness: See Article 4.1.4.
• Coagulants: Products that neutralize or • Gradient or velocity (or shear velocity):
See Appendix 5, Chapter 3. • Thixotropy: Reversible phenomenon of
invert surface charges of suspended matter:
certain colloidal suspensions whereby they
ferric chloride, lime, aluminium sulphate, etc. • Marsh viscosity (MV): Laboratory test
fluidify when agitated and gel when left to
• Density: Ratio of the mass of a given where the time in seconds for 946 ml of slurry
to flow through a 4.75 mm nozzle rest. Thixotropy can be estimated from the
volume of one body to the mass of the same evolution of gelling over time. With the Fann
volume of a reference body, under condi- (water = 26s). The reading obtained depends
on YP, PV, thixotropy, and density. rheometer, gels are measured by testing at
tions which must be specified for both no more than 3 rpm after a waiting period of
bodies (water at 4°C for liquids). It is expres- Consquently this measurement is hardly
representative of the characteristics of a 10 sec. (gel 0) and 10 min. (gel 10). The unit
sed as a dimensionless number. of measurement is lbs / 100ft
slurry.
• Fann rheometer: A.P.I standardized appa- • Yield point: See Article 4.1.4.
ratus for applying shear to a fluid by means • Newtonian fluid: Fluid for which the shear
of an immersed cylinder rotating at a control- stress is directly proportional to the shear • Yield value (YV): An extrapolated yield-
led speed and for determining the response rate. point value (see Article 4.1.4) derived from a
of the fluid by measuring the stress applied • pH: Expresses the acidity or alkalinity of an Fann rheometer test. Calculated by testing
to a concentric cylinder left free to turn. The aqueous solution. The pH value of pure at 300 rpm and deducting from the reading
preset speed of rotation are 3, 6, 100, 200, water is 7. The products used in tunnelling the reading for the plastic viscosity, PV. The
300, and 600 rpm. Stress is read off in slurry achieve their optimum yield when the unit of measurement is the lb/100 Square
lbs/100 Square feet. Simple calculation colloidal state of the slurry is in the pH range feet. To convert to Pa, divide by 2.
methods enable the data obtained to be from 8 to 10. • Yield point (YP): See Yield value
APPENDIX 2:
P O LY M E R S A N D B E N T O N I T E S F O R T U N N E L L I N G S L U R R I E S
This appendix presents the main types of polymers used for underground works.
1- GENERAL • They consist of amylose and amylopectin. • Their degree of purity, i.e. their active-mat-
• They are hydrolyzed by heat to increase ter content: the other products they contain
Polymer: chemical compound obtained by are salts, which are by-products of the reac-
their water solubility.
polymerizing molecules of a given com- tion (degree of purity = 50 to 99%).
pound known as a monomer. • They are sensitive to fermentation and are
Cellulose ethers are not stable under bacte-
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3.1 - STRUCTURE OF the platelets. In an aqueous medium, water • behaviour under heat (up to 1000°C),
BENTONITE molecules attach between the plates, cau- • possible presence of electrolytes (stabili-
sing them to move apart, causing intra-struc- zing or flocculating action).
The elementary Montmorillonite platelet tural swelling of the bentonite. The space
between layers becomes the seat of cation The properties of a bentonite also depend
consists of two tetrahedral layers of Si4+ on
exchange. Some important properties of on the physical state it is in. It can be solid,
either side of a third octahedral layer whose
bentonites depend closely on the type and semi-solid, plastic, semi-liquid, or liquid,
centre is occupied by a cation such at Al3+.
number of cations exchanged: swelling, vis- depending on the proportions of bentonite
The three layers comprise an elementary pla-
cosity of suspensions, plasticity, Atterberg and water. The essential properties of bento-
telet about 10 Å thick. The smallest volume
nite as a slurry component in tunnelling are
with all the characteristics of crystal is a sand- limits, and some other characteristics of
as follows:
wich of two layers of these elementary plate- interest for foundry work. The type of
lets. In practical terms, bentonite always exchangeable cations provides a basis for • adsorbant properties,
takes the form of primary particles of about classifying natural bentonites into two cate-
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APPENDIX 3:
P R I N C I P L E F O R E VA L U AT I O N O F T H E R H E O L O G I C A L
CHARACTERISTICS OF TUNNELLING SLURRIES
The principle of ground support using slurry required to ensure stability can be be calcula- where K is the horizontal permeability of the
pressure relies on the possibility of mobili- ted from the relationship: in situ soil, and A is an adimensional coeffi-
zing a pressure in a liquid against a soil sub- ϕ cient between 5 and 10 which in theory
ject to a state of stress, be it saturated or not. f = (1 – n ) (γg – γs ) sin (α – ) increases with the degree of scatter of soil
sinϕ
Soil is a porous medium through, which a pore diameters and decreases with gradual
clogging of the ground by slurry.
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APPENDIX 4 :
S L U R RY PA R A M E T E R TA B L E
The table below gives orders of magnitude in the form of bracket values for slurry parameters against different permeabilities in homogeneous
ground. These values are merely orders of magnitude for the purposes of illustration.
SOLS TYPES
Parameters Unit Type 1 Type 2 Type 3 Type 4
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AV cp 15 - 40 10 - 20 8 - 20
PV cp 5 - 20 5 - 10 5 - 10
YP Pa 8-5 5 - 10 < 15
0/10 gel strengths lbs/100ft 10 - 30 3 - 20 Not applicable
Filtrate ml 20 - 50 15 - 30 Not applicable
Cake (API test) mm 2-6 1-5 1-5
Marsh viscosity s/946 ml 40 - 120 35 - 50 30 - 50
Density 1.02 - 1.15 1.02 - 1.20 1.02 - 1.60 1.02 - 1.30
pH 7 - 10 7 - 10 7 - 10
Sand % 1–5 1-5 1-5
(standardized test methods “Recommended Practice Standard Procedure for Field Testing Water-Based Drilling Fluids API RP 13 B-1, 1 June 90)
APPENDIX 5 :
S L U R RY R H E O L O G Y
over each other, each driven at its own In practical terms, these very simple theoreti- If:
speed. The velocity gradient between any cal models do not fit tunnelling slurries per- a = 0, the plot is a straight line passing
two layers of a fluid is therefore the quotient fectly. Since they can define a fluid only over through the origin; the fluid is Newtonian,
of the velocity difference between those a limited range of velocity gradients, they
layers divided by the distance between with viscosity h = 1/c (1)
cannot take account of the plastic or visco-
them. The dimensional measurement of the plastic behaviour of tunnelling slurries. a < 0, is meaningless
velocity gradient (sometimes called the shear Consequently other models have been deve- a > 0, the liquid is pseudo-plastic or plastic,
gradient or the shear rate) is the reciprocal of loped. Most of them are based on the basic depending on whether c is positive or negative
a time; it is measured in s-1. models above.
c< 0, in addition to the origin, the plot has
Shear stress: Herschel-Bulkley model: τ = YP + K x G N two further intersections with the vertical
Shear stress is the result of forces of internal This model is a synthesis of the above three scale. There is a yield point. The liquid is plas-
friction opposing the flow of liquid. It models, for, depending on the values of YP, tic and close to being a Bingham fluid (2)
depends on the velocity gradient of the fluid,
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Shear stress
Shear stress
APPENDIX 6 :
P R I N C I P L E O F O P E R AT I O N O F A S L U D G E T R E AT M E N T P L A N T
silt has residual humidities of between 10 and After desanding and desilting, most of the
large particles (> 6 mm approx.): slurry is fed back into the slurry circuit, after
gravel and pebbles, but also 20%, depending on the characteristics of the
mucking slurry. compensating with fresh slurry to maintain
lumps and flakes of earth that the required rehological characteristics. The
have not been broken down. • Unlike screens, there is a “self desatura- excess is disposed of, to maintain the correct
tion” phenomenon in a dewatering unit: with weight/volume balance (density and levels).
a) Scalping with vibrating screen: For sandy a given circulating load, an underlying layer
and stoney ground that does not stick of filter material is formed. 6.3 - TREATMENT OF EXCESS
b) Scalping with drum screen: Especially • Because of the diversity of the ground SLURRY: (in real time, part-
good for sticky, clogging clayey ground. types encountered and the broad range of ly as a background task)
viscosities of mucking slurries, a desanding
6.1.2 - Desanding: Separation of unit with 2 separation stages plus dewatering The treatment of excess slurry is closely lin-
sand from slurry is generally necessary for most tunnelling ked to the required spoil consistency (liquid,
projects. The second separation stage refines paste, or solid) and the quality of the ground
Sand is separated out from the slurry in 1, 2 or the relatively coarse split of the first. water absorbed and of the water discharged
3 series stages of hydrocyclones. Centrifuges
from the plant (pH, SS, hydrocarbons, etc.).
may also be used to separate out silt.
How a hydrocyclone works: (from French
documentation: Mines et Carrières /
L’épuration physico-chimique des eaux)
Cycloning is a process for separating liquids from solids that uses centrifugal force. Slurry is injected tangentially into the cylindrical part of the
cyclone. The vortex created causes the heavy, i.e. coarse particles to be thrown against the walls of the cyclone and to be carried down the coni-
cal section with downward flow while the finest particles, which are less affected by centrifugal force, are carried by
the upward flow. The fineness of separation increases with increasing inlet velocity, and a small-diameter hydrocy-
clone also separates out finer particles.
The split size, or d50, is the particle dimension which has equal chances of being in the overflow or underflow. It is
the grain size that is split exactly into two equal amounts by the hydrocyclone. The empirical Yoshioka and Hotta
formula can be used to calculate the d50 integrating viscosity:
Filter-press treatment Solid 1,70 – 2,00 0 to 10% slaked lime added to slurry (by weight of
dry solids)
6.3.1 - Thickening by flocculation- resistance (r0.5 < 1011 m.kg-1) and is compres- P: filter pressure in Pa
settlement of thick slurry paste sible (s>1), for the filter pressures that can be A: slope of straight plot for filterability test, in
applied are relatively low (0.3 to 1 bar). s.m-6
• Flocculation requires effluent concentra- S: filtration surface in m2
• In most cases a filter-press produces hard,
tions of about 20 to 30 g per litre of dry
solid cakes from slurrys with high specific η: dynamic viscosity of filtrate in Pa.s
solids, which generally implies addition of
resistances (r0.5 = 1015 m.kg-1), using the pos- (approximately 1.1 x 10-3 Pa.s at 20°C)
considerable quantities of water for dilution
sible filtration pressures of 0 to 20 bars. It is C: dry solids at 105°C divided by the volume
before treatment.
generally necessary to treat the slurry before- of slurry in kg.m-3
• Clay particles consist of a stack of elemen- hand by adding lime or some other filtration
tary platelets of variable specific surface aid to dewater a slurry with a specific resis- ➬ Different slurries are generally compared
(≈ 20 m2/g for kaolinite / ≈ 100-150 m2/g for tance of r0.5 = 1012 m.kg-1. in terms of their r0.5 values (0.5 bar pressure):
construction bentonite): this structure ➬ If r0.5 = 1014 to 1015 m.kg-1: slurry not easily
explains the high swellability of bentonite. 6.3.3 - Slurry filter index: (from pressed, requiring an admixture such as lime
There is a layer of adsorbed water on the sur- Degrémont technical report on to assist filtration
face of the particle (ionic double layer) which water)
is electrically charged with easily exchan- ➬ If r0.5 = 1x1011 to 5x1011 m.kg-1: slurry easily
geable cations (+). Its potential increases pressed, requiring no filtration admixture.
6.3.3.1 - Specific resistance to filtration
with the specific surface of the particles. The
presence of more or less bentonite usually • Use a filtration cell of the Baroid filter-press 6.3.3.2 - Compressibility factor
requires there to be a phase of coagulation type using compressed air and a paper filter. • Measure the specific resistance to filtration,
by adsorption of cations to reduce the • Pour 100 to 150 ml of slurry into the cell. r, at several pressures, P.
potential of the ionic double layer, followed
• Allow the filtrate to flow off and record the • Plot curve log r = f (log P)
by addition of a flocculant (generally a syn-
thetic polymer such as polyacrylamide) to volume V0 The value of s is determined from the slope
form inter-particle bridges (coagulant Apply the required pressure (0.5 to 16 bars) of the straight line
consumption ≈ 100 - 200 ml/T of dry solids – and record the volume of filtrate every 10, = (log r1 – log r) / (log P1 – log P)
flocculant consumption ≈ 100 - 200 g/T of 15, 20, 30, or 60 seconds, depending on the ➬ If s < 1: the filteration flow rate increases
dry solids). filtrate flow velocity. as P increases => the slurry is not very com-
• Filtrate volumes V0, V1, V2… correspond pressible and high pressures are recommen-
6.3.2 - Additional treatment by to times T0, T1, T2… ded (15-16 bars).
pressing to obtain solid bulk
waste that can be handled easilty: • Plot points against Vx horizontally and ➬ If s > 1: the filtration flow rate decreases as
Tx / ( Vx – V0) vertically, and measure slope a P increases => the slurry is compressible and
The filterability of bentonite slurries is gene- of the linear part of the curve. it is recommended that the pressure be rai-
rally poor ( r0.5 = 1014 to 1015 m.kg-1 ) Specific resistance r in sed gradually to facilitate drainage.
• If a belt filter is used, the slurry must be m.kg-1 = ( 2 A P S2 ) / ( η C )
flocculated beforehand, and belt filters can Where
only be used if the slurry has a low specific
APPENDIX 7
PERMEAMETER
Additionnal equipment
Valve Scales for soil weight
Scales for water weight
Compressed air in
Tube
T
Levels Boue - (15 litres)
Overflow
Translucent cylinder
Service pressure up to 0.15 MPa
Attachment
NB
It would be useful to have the permeater
To a tilting base so that filter cake
Performance under compressed air can be
4 legs allowing permeameter handling Tested and to facilitate emptying
The following forms are given to illustrate standard documentation for monitoring tunnelling slurry:
• Daily monitoring report
• Test report
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• 183 •
test on parent slurry
Parent slurry addition
Concentration
Additive type
Additive addition
Concentration
Slurry for use in SLURRY SHIELD TBM
Slurry pH
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