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    Ar2775lot751219 PDF

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    This certificate of analysis provides the results of testing conducted on a certified reference material (CRM) coal sample. The testing analyzed the sample's proximate analysis, ultimate analysis, mineral analysis, sulfur forms, and ash fusion temperatures. The certificate explains the intended use of the standard is for test method verification and describes the statistical analysis and coordination that was conducted in certifying the sample. The material used was produced according to ISO 17034 accreditation standards and the certificate is valid for two years once opened.

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    Ar2775lot751219 PDF

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    lab ic
    27 views1 page
    This certificate of analysis provides the results of testing conducted on a certified reference material (CRM) coal sample. The testing analyzed the sample's proximate analysis, ultimate analysis, mineral analysis, sulfur forms, and ash fusion temperatures. The certificate explains the intended use of the standard is for test method verification and describes the statistical analysis and coordination that was conducted in certifying the sample. The material used was produced according to ISO 17034 accreditation standards and the certificate is valid for two years once opened.

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    This certificate of analysis provides the results of testing conducted on a certified reference material (CRM) coal sample. The testing analyzed the sample's proximate analysis, ultimate analysis, mineral analysis, sulfur forms, and ash fusion temperatures. The certificate explains the intended use of the standard is for test method verification and describes the statistical analysis and coordination that was conducted in certifying the sample. The material used was produced according to ISO 17034 accreditation standards and the certificate is valid for two years once opened.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    27 views1 page

    Ar2775lot751219 PDF

    Uploaded by

    lab ic
    This certificate of analysis provides the results of testing conducted on a certified reference material (CRM) coal sample. The testing analyzed the sample's proximate analysis, ultimate analysis, mineral analysis, sulfur forms, and ash fusion temperatures. The certificate explains the intended use of the standard is for test method verification and describes the statistical analysis and coordination that was conducted in certifying the sample. The material used was produced according to ISO 17034 accreditation standards and the certificate is valid for two years once opened.

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    of 1

    Value Beyond Measure

    Certificate of Analysis
    AR-2775
    ULTIMATE COAL CRM
    LOT # 751219 LID # 751219
    DRIED BASIS VALUES
    Proximate Analysis n= k= ASTM Ultimate Analysis n= k= ASTM
    % Ash………………… 6.31 ± 0.68 12 2.2 D3174/D7582 % Carbon……………… 69.69 ± 1.67 12 2.2 D5373
    % Volatile Matter………. 43.54 ± 1.22 11 2.2 D3175/D7582 % Hydrogen…………… 5.09 ± 0.84 12 2.2 D5373
    % Fixed Carbon(calculated) (50.15) -- -- D3172 % Nitrogen……………… 1.00 ± 0.12 12 2.2 D5373
    % Sulfur……………… 0.41 ± 0.03 36 2.0 D4239 % Oxygen (calculated)… (17.5) -- -- D3176
    Btu/lb.………… 11888 ± 209 12 2.2 D5865 MAF/DAF BTU (calculated) (12688) -- -- D3180

    Mineral Analysis n= k= ASTM Sulfur Forms ASTM


    % Silica……………… 27.05 ± 1.65 8 2.36 D4326/D6349 % Pyritic………… (0.02) D2492
    % Alumina…………… 15.35 ± 0.64 8 2.36 D4326/D6349 % Organic (calculated)… (0.38) D2492
    % Titania………… 1.24 ± 0.06 8 2.36 D4326/D6349 % Sulfate…………… (0.01) D2492
    % Ferric Oxide…………… 4.79 ± 0.26 8 2.36 D4326/D6349
    % Calcium Oxide……… 25.55 ± 1.55 8 2.36 D4326/D6349 Ash Fusion Temperature Degrees F Degrees F
    % Magnesium Oxide…… 6.69 ± 0.54 8 2.36 D4326/D6349 ASTM D1857 Reducing Oxidizing
    % Potassium Oxide………… (0.40) -- -- D4326/D6349 Initial deformation… (2283) (2261)
    % Sodium Oxide………… 1.79 ± 0.31 8 2.36 D4326/D6349 Softening…………... (2309) (2312)
    % Sulfur Trioxide…… 14.99 ± 2.49 8 2.36 D4326/D6349 Hemispherical……... (2313) (2318)
    % Phosphorus Pentoxide 0.55 ± 0.07 8 2.36 D4326/D6349 Fluid/Final………… (2319) (2328)
    % Strontium Oxide……… (0.51) -- -- D4326/D6349
    % Barium Oxide……… 0.61 ± 0.06 8 2.36 D4326/D6349 % Chlorine D4208/D6721 (0.0011)
    % Manganese Oxide… (0.03) -- -- D4326/D6349 % Fluorine D3761/D5987 (0.0042)
    % Undetermined(calculated) (0.44) -- --
    REFERENCES USED: Sulfur - NIST SRM 2693; BTU - NIST 39j(Benzoic Acid); C/H/N – Phenylalanine, EDTA; Form of Sulfur – QAR-RM-6, RM-1
    SRM1635a; Mineral Analysis – NIST 634a, 2689, USGS AGV-2; Chlorine – SRM2693, 2682c; Fluorine – 1632d, SARM18. () Indicates
    reference only value

    The intended use of this standard is for the verification of various tests by the above-mentioned methods. Typical sample size for
    analytical testing and minimum size is subject to the test method and instrumentation used. The uncertainty values represent the
    expanded uncertainty obtained through analytical testing by the mentioned ASTM methods utilizing ANOVA, ISO Guide 35, and the
    Guide to Uncertainty Measurement. Metrological traceability is to the SI derived units expressed as mass fraction percent,
    temperature, or BTU/lb. Normal test procedures should be employed when using this standard; this includes using the reproducibility
    and repeatability factors of the method for establishing analytical uncertainty if needed. When necessary, professional judgment is
    applied toward consideration of data and statistical information. The statistical analysis and the overall direction and coordination of
    the analytical measurements leading to certification were performed by K.E. Dyer, Chief Chemist at Alpha Resources.

    The material used in production of this standard was identified in accordance with ARI 041. The samples for round-robin testing were
    selected in accordance with ARI 031. The above values relate only to the material used to produce this standard. The analytical
    samples should be dried or corrected for moisture as per the test method you are using. This bottle contains 50g fine coal powder (-60
    mesh). While unable to determine a definite shelf life this reference standard should be reviewed 20 years from the data of
    certification. Once opened this certificate is valid for two years. Keep sealed tight and store under normal laboratory conditions. This
    certificate cannot be reproduced except in full. Remedies for any claimed defect in this product will be limited to product
    replacement or refund of the purchase price. In no event shall Alpha Resources be liable for incidental or consequential damages.

    This is a Certified Reference Material (CRM) and is traceable to the above-mentioned references. For good laboratory practice it is
    recommended that all standards be verified as fit for purpose prior to use. This standard was produced in accordance to ISO 17034
    (RMP) accreditation issued by ANSI-ASQ/ANAB. Refer to certificate and scope of accreditation AR1920.

    EXPIRATION DATE
    THIS CRM IS VALID FOR TWO YEARS FROM THE DATE OF OPENING
    CERTIFIED February 17, 2020

    3090 Johnson Rd. • Stevensville, MI 49127-0199 • Phone (269) 465-5559 • Fax (269) 465-3629 • alpharesources.com

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