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    Siflon Drugs: Sy. No. 25/4, Rachanapalli (V)

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    bharath kumar
    The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

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    Siflon Drugs: Sy. No. 25/4, Rachanapalli (V)

    Uploaded by

    bharath kumar
    31 views4 pages
    The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

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    The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    31 views4 pages

    Siflon Drugs: Sy. No. 25/4, Rachanapalli (V)

    Uploaded by

    bharath kumar
    The document summarizes an automatic potentiometric titration experiment. The experiment involved titrating a sample of closantel sodium against a 0.1M perchloric acid solution to determine its concentration. The titration reached the endpoint of 6.79 mL at 2585 mV. Analysis of the results found the closantel sodium sample had an assay of 94.1559% and 99.16% on an anhydrous basis.

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    © All Rights Reserved
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    of 4

    VEEGO

    AUTOMATIC POTENTIOMETRIC
    TITRATION APPARATUS

    SIFLONDRUGS
    Sy. No. 25/4, Rachanapalli (V).
    Anantapur 515004. Andhra Pradesh

    MODEL: AUTOPOT-KF SERIAL NO.: 20/1218


    TIME: 14:57.27 DATE: 28/02/2022

    FILE NAME : CLOSANTEL SODBP


    SAMPLE NAME CLOSANTELSODIUM
    SAMPLE D : CLOSANTEL SODIUM
    BATCH NO : CLS0620222
    TITRATION NO :2
    TITRANT :0.1M PERCHLORICDTHE TI.. AN
    ELECTRODES : GLASS
    : CALOMEL
    OPERATOR NAME : V. SREEKANTH REDDY
    TITRATION MODE SINGLE END POINT
    TITRATION METHOD STEP VOL DOSING
    SENSITIVITY 25
    END mV 900

    SETTINGs Direet Vol: 5.00 ml Dosing Vol 0.10 ml


    End Vol: 20.00 ml Dosing Int: 10 sec

    Vol(ml) mV
    Difference
    0.00 2075
    1.00 2133 0
    2.00 2186 0
    3.00 2234 0
    4.00 2283 0
    5.00 2340 0
    5.00 2348
    5.110 2359 11
    5.20 2367 8
    5.30 2375
    5.40 2380
    5.50 2392 12
    5.60 2406 14
    5.70 2417 11
    5.80 2419
    5.90 2430
    6.00 2442 12
    6..10 2463 2
    6.20 2469
    .30 2476 1
    40 2491 15
    50 2509 18
    6.60 2522 13
    6.70 2549 27
    6.80 2588 39
    6.90 2626 38
    7.00 2707 81

    Page 1 of 4
    EndPoint @ 6.7900 ml and 2585 mV

    Peak Magnitude: 81 mV

    REMARK : TITRATION OVER

    Page 2 of 4
    VEEGO
    AUTOMATIC POTENTIOMETRIC
    TITRATION APPARATUS

    SIFLON DRUGS
    Sy. No. 25/4, Rachanapalli (V).
    Anantapur - 515004, Andhra Pradesh

    MODEL: AUTO/POT-KF SERIAL NO.: 20/1218


    TIME 14:57:27 DATE: 28/02/2022

    FILE NAME : CLOSANTEL SODBP


    SAMPLENAME :CLOSANTELSODIUM
    SAMPLE ID CLOSANTEL SODIUM
    BATCH N0 :CLSO620222
    TITRATION NO :2
    TITRANT :0.IM PERCHLORICDTHE TI.. AN
    ELECTRODES :GLASS
    CALOMEL
    OPERATOR NAME V. SREEKANTH REDDY
    TITRATION MODE SINGLE END POINT
    TITRATION METHOD STEP VOL DOSING
    SENSITIVITY 25
    END mV :900

    SETTINGS Dire:ct Vol 5.00 ml Dosing Vol: 0.10 ml


    End Vol: 20.00 ml Dosing Int: 10 sec

    PARAMETER VALUE REMARK

    READING 6.7923 ml
    BLANK READING 0.0290 ml

    SAMPLEQUANTITY 0.50240 g
    MOLARITY . 0.10186 M

    STANDARD MOLARITY 0.1000 M

    STANDARD FACTOR 0.068500 g

    WATER CONTENT. 5.05 %

    ASSAY AS IS 94.1559 %

    ASSAY ANHYDROUS BASIS 99.16 %

    AnalyzedBy: Checked By: Approved By:


    28 lo22 022

    COMMENT:
    pwl Comphie pen Apec

    Page 3 of 4
    GRAPHI DETAILS
    TIME: 14:57:27 DATE: 28/02/2022

    SAMPLE ID: CLOSANTEL SODIUM BATCH NO. : CLS0620222

    SAMPLE NAME: CLOSANTELSODIUM TITRATION NO. : 2

    2800

    28 00

    E 2400

    2200

    2000

    Vonme

    100

    40

    VolumB

    80

    20

    olumE

    40

    20

    AMA

    Valu me

    Page 4 of 4

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