Plan. Sampling

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SUPPORT DOCUMENT Doc No.

: S-DC-001

Topic : Sampling Plan Revision :0

Dept : Quality Control (QMS) Issue Date : 1/9/2021

Activity Sample Type Packaging Sampling Point/Frequency Sample Quantity References Remark
Sampling 1 time per vehicle Refer to RM Specification
1 Raw Material (30% Sampling) Grains and Animal Sampling the bags that possible to be reached (Top Composite Total for Corn
for Release Parameter,
Based Protein in Bag and Back Side) (3-5 Kg)/Vehicle, Others (1 EC. No 152/2009 refer to Sampling Plan -
truck Kg)/Vehicle for Insect Matrix
Depth is random depends on the sampling probe.
Sampling 1 time in sampling house/per vehicle.
Sampling 10 points (Corn) (as pic - top),
Sampling min. 3 points (other than corn) (as pic -
bottom), point of deepness is random (max. 1.8 m)

Grains in bulk & Composite Total for Corn


Truck
Bulk (3-5 Kg)/Vehicle, Others (1 AAFCO Feed Inspector Refer to RM Specification
for Release Parameter
Manual
Kg)/Vehicle

Sampling per vehicle


Grains in Sampling bags that can be reached, Composite Total for Corn
Container Bag & Bulk (3-5 Kg)/Vehicle, Others (1 AAFCO Feed Inspector Refer to RM Specification
for Release Parameter
6 points for Bulk (Left, Right, Center) Depth is random Kg)/Vehicle Manual
depends on the sampling probe.
Animal Based Sampling per vehicle 9
Protein meal in Bulk points depends on sampling probe for deepness Composite Total 500 g - 1 Refer to RM Specification
container Kg/Vehicle for Release Parameter
AAFCO Feed Inspector
Manual
RM in truck Jumbo Bag Min. 10% of total jumbo bags @1 Ton Composite Total 500
g/Jumbo Bag/Lot

Oil/Liquid IBC Tank/Drum Sampling 3 points ( Top, Middle, Bottom and composite) Composite Total 1 L
AAFCO Feed Inspector Refer to RM Specification
for Release Parameter
Total 1 L Manual

Sampling 3 points ( Top, Middle, Bottom and composite) AAFCO Feed Inspector
Oil/Liquid Bulk Oil Tank Vessel Composite Total 1 L
Total 1 L Manual

AAFCO Feed Inspector Refer to RM Specification


Oil/Liqud Pail Sampling 1 pail / 20 Pail / Lot Composite Total 1 L/Lot for Release Parameter
Manual

min. 10% of total bags, with point first and mid only for
Refer to RM Specification
Raw Material (100% Sampling) RMs in truck Bag safety purpose, samples are composite, 100% Composite Total 1 Kg EC. No 152/2009 for Release Parameter
check for visual checking (occasional condition)
Grains in bulk &
Truck Bulk Covered by 30%

Grains in
Container Bag & Bulk Covered by 30%

RMs in truck Jumbo Bag Covered by 30%

Oil/Liquid IBC Tank Covered by 30%

Oil/Liquid Bulk Oil Tank Vessel Covered by 30%

Oil/Liqud Pail Covered by 30%

Egg, Egg derivate, Feed Additive, Special Solid/Liquid Bag/Box/Drum 1 bag/box per lot min. 200 g or mL/Lot
RM, Pallatants
Bulk.Bag/Box/
Sampling for Microbiology testing Solid/Liquid Drum/Tank 1 sample per lot min. 200 g or mL/Lot

2 Dry Pet Food (Level 1) per 30 minutes for 2 hours (first) and per 3 hours
(categorize middle and last) until finalize packing Refer to Product
All packaging Min. 2 x 0.8 - 1 Specification for release
Dry Pet Food In house sampling
Chemical and Microb Size and Form Samples are composite represent first/middle/last Kg/frequency/Lot parameter
pallets
Aflatoxin and Salmonella Composite first, Middle, Last
Dry Pet Food (Level 2 and 3) per 30 minutes for 2 hours Refer to Product
Chemical and Microb All packaging Samples are composite represent first Min. 2 x 0.8-1
Dry Pet Food Size and Form Kg/Frequency/Lot
In house sampling Specification for release
parameter
Aflatoxin and Salmonella Samples are composite represent first
3 Checked by Production Staff
Batching- Physical & Nutrition Solid/Powder Plastic Bag per 20 minutes (per batch), min. 1 Kg In house sampling Nutrition Spec by RD
Kibble from Extruder Process
Physical Dry Pet Food - Plastic Bag per hour, min. 600 grams min. 600 grams In house sampling
Refer to Product
Kibble Specification (RD/QA)
Dry Pet Food - Refer to Product
Nutrition Kibble Plastic Bag per batch (from FM bin batching) 200 grams/batch In house sampling Specification (RD/QA)
Kibble from Packing Line
Refer to Product
Physical Dry Pet Food Bag per pallet 1 bag/min. 1 kg for woven In house sampling Specification (RD/QA)
Checked by QPI
Batching - Physical Solid/Powder Plastic Bag Sampling represent first, middle, last (3x tp 6x based 1 bag/min 1 Kg for woven In house sampling Refer to Product
on level inspection) Specification (RD/QA)
Sampling represent first, middle, last (3x tp 6x based Refer to Product
Batching - Chemical Solid/Powder Plastic Bag 1 bag/min 1 Kg for woven In house sampling
on level inspection) Specification (RD/QA)
Kibble from Extruder Process
Start up : per 30 minutes for est. 2 hours. Reguler
Physical Dry Pet Food - Plastic Bag checking based on level inspection (per hour to per 3 min. 600 grams In house sampling
Refer to Product
Kibble hours)
Specification (RD/QA)

Nutrition Dry Pet Food - Plastic Bag based on level inspection per batch to per 3 hours min. 200 gram In house sampling
Refer to Product
Kibble Specification (RD/QA)
Kibble from Packing Line
Refer to Packing
Physical Dry Pet Food Bag based on level inspection per hour 5-10 bags In house sampling Specification (Packing
Spec./QA)
4 Checked by Lab - Food Safety
Raw Material Solid/Liquid (Oil) Bag/IBC Tank Annual min. 500 gram/500 mL per In house sampling Refer to RM Specification
type of RM
Premix/Special
RM Bag/IBC Tank Annual by COA/Lot In house sampling Refer to RM Specification

Solid/Liquid (Oil) Bag/IBC Tank Annual Min. 200 gram In house sampling Refer to Product Spec.
RM Microbiology Monitoring
Pallatant/Special Bag Annual min. 200 gram In house sampling Refer to RM Specification
RM - Solid
Bag/Plastic Bag per packaging/min. 500
Dry Pet Food Product Dry Pet Food taken from Annual gram (represent 1 lot/year)
In house sampling Refer to RM Specification
Woven
Propose Verification Points to QPI

Checking Activity Sample Type Packagin Sampling Point/Frequency Ver by Sample AQL/Acceptability
WI WI Reference
g Quantity Records at s
Sampling Analysis
Remark
SUPPORT DOCUMENT Doc No. : SDC-PCIM-010
Topic : Sampling Plan Revision :1
Dept : Quality Control (QMS) Issue Date : 4/2/2022
Activity Sample Type Packaging Sampling Point/Frequency Sample Quantity AQL References Remark
Checked by Lab - Hygiene (Environment)
Water RO Water Plastic Bottle Weekly (2 points), RO unit, RO Tank 2 x 250 mL CR - TR in house method

Weekly (5 points) Packing : Chronos - Chute


Air Air N/A Area, Bosch : Radial Area, Extruder : DCC 1 and 2 petrifilms per point CR - TR in house method
DCC 2, Tipping Powder 4th
Production Line Swab Swab Kit Weekly and Additional
Extruder Line 1
outlet of extruder
airlock dryer
airlock coater
coater bin 1st floor
coater bin 2nd floor
nozzle coater
tipping manual
airlock cooler
cooler bin 1st floor
cooler bin 2nd floor
screener cooler

Turn Head (Total 8)


Piping Turn Head (Total 32)
Extruder Line 2
Outlet Extruder
Dies Extruder
Air Lock Coater 1st Floor
Sampler Coater 1st Floor
Coater Bin 1st Floor
Cooler Bin 1st Floor
Air lock cooler 1st Floor
Sampler Cooler 1st Floor
Bin Dryer 1st Floor
Airlock dryer 1st floor
Sampler dryer 1st floor
Cooler Bin 2nd Floor
Screener Cooler 2nd Floor
1 swab per point CR - TR
in house
5 method
1 swab per point CR - TR
in house
5 Coater bin 2nd Floor
method
Tipping manual coating powder 4th Floor
Turnhead packing 7th floor
Pipping turn head tank 7th Floor
Nozzle coater 2nd Floor
Packing Machine Line (Toyo, Bosch, Chronos)
Toyo
chute
shutter
Tray additional
Collection chute Refer to Product
rotary table Specification for
Contamination and
Discharge chute Food Safety
funnel Release Parameter
Mainhole hopper
vibrating tray
radial trough
weight hopper
Bosch
Mainhole hopper bosch
vibrating tray bosch
radial trough bosch
weight hopper bosch
head of bosch machine
forming tube bosch
Roll guide packaging bosch
Chronos
Mainhole hopper cronos
small hopper cronos
Middle inside hopper
chute cronos
FG Bin
FG Bin No. 01 - 32
Pathogen Monitoring (Personel Swab Swab Kit Monthly
Attire & Factory Floor) Packing hygiene junction
Packing floor
packing with WH FG border
Production hygiene junction
Pathogen Monitoring (Personel
Attire & Factory Floor)

Tipping manual 4th floor


3rd floor oil tank floor
DCC 2nd floor
DCC 1st floor
Extruder 1st floor
Pellet mill floor
extruder with WH RM border
WH RM hygiene junction 1 swab per point
in house
method
WH RM floor
SMX floor
Outlet WH RM floor
Lift floor - Extruder
Waste area floor - utility area
Sampling oil tank yard
Extruder - Safety Shoes
Extruder - Safety Shoes
Packing - Safety Shoes
Packing - Safety Shoes
Batching - Safety Shoes
RM - Safety Shoes
SUPPORT Doc No. : SDC-PCIM-010
DOCUMENT
Topic : Sampling Plan Revision :1

Dept : Quality Control (QMS) Issue Date : 4/2/2022

Sample Sampling Point Sample


No. Activity
Type
Packaging
Quantity
AQL References Remark
/Frequency

Sampling 1 time per vehicle ≤ 2/20 sample (10% for life insect, dead insect
1 Raw Material (30% Rice/approach Bag Sampling the min. 20 is still acceptable (dead
Sampling) for grains bags that possible to be reached from Total population MIL-STD 105E insect that normal in rice
(Top and Back Side) samples) with less severity)

Tight ≤ 2/32 Normal ≤


91 - 150
5/32
Bags are sorted, and
rejected the remaining if
Raw Material (100% Rice/approach All Bags during/after unstuffing, AQL already reached, tight
2 Bag MIL-STD 105E can be used if new
Checking) for grains min. 3 stabs per bag Tight ≤ 3/32 , Normal
151 - 280 supplier and bad
≤ 7/32
performance supplier

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