8890 Installation

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Agilent 8890 Gas Chromatograph

Installation and First Startup


Notices
© Agilent Technologies, Inc. 2018 Warranty Safety Notices
No part of this manual may be reproduced in The material contained in this document is
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Installation and First Startup


Contents
1 Installing the GC
Overview of Installation 8
Purpose of this procedure 8
Customer responsibilities 8
About Agilent’s installation service 8
Tools and additional parts required 8
Performing checkout 9
System installation 9
Configuring the GC 9
Connecting to the Browser Interface 10
The 8890 GC 11
Unpacking 12
Place the GC on the bench 13
Verify line voltage, voltage settings, and power cord 15
Line voltage 15
Power consumption 16
Power cords available 17
Grounding 21
Connect GC to LAN, Local Computer, or Tablet 22
Connect the power cord and turn on the GC 24
View the System Setup Wizard 25
Configure the GC IP address 26
Set the Date/Time 27
Set the Pressure Units 28
Configure Carrier Gas Types 29
Connect Gases and Traps 30
Install the gas regulators 30
Connect the tubing to the gas source 32
Install traps 33
Plumb to EPC flow modules 33
Install Aux EPC module frits for your application 34
Install hydrogen sensor calibration gas 36
Leak test all connections and set source pressures 38
Set source gas pressures 40

Installation and First Startup 3


Install inlet checkout parts 41
Install ALS, if ordered 42
Configuring GC-MSD communications 43
Connect the external cables 44
Back panel connectors 44
Connecting cables 45
GC / MS / Agilent data system / ALS 47
Additional cabling configurations 47
Vent ECD or uncombusted hydrogen to a fume hood 48
Connect cryogenic cooling (if present) 49
Connecting liquid carbon dioxide 49
Connecting liquid nitrogen 50
Connecting air to the multimode inlet 51
Connect valve actuator air (if present) 53
Configure Headspace Communications 54
Configure the checkout column 55
Checkout column 55
Install the checkout column 57
Transfer the checkout sample to a screw-top sample vial 59
When the system stabilizes, run one injection 60
Prepare for the Next Analysis 61

A Making Swagelok Connections


Making Swagelok Connections 64
Using a Swagelok Tee 67

B Cabling Diagrams and Remote Start/Stop


Using the Remote Start/Stop Cable 70
Connecting Agilent products 70
Connecting non-Agilent products 70
Multi-instrument Cabling Examples 73
GC / ALS / Non-Agilent Data System 73
GC / 3395A/3396B Integrator / ALS 74
GC / 3396C Integrator / ALS 74
Example: Using a Y-Cable in a setup (GC/MSD/Data System/Headspace
Sampler) 75
GC / External Events (unspecified, non-Agilent instrument) 76

4 Installation and First Startup


Cable Diagrams 77
Analog signal cable, general use, G1530-60560 77
Agilent analog signal cable, G1530-60570 78
Remote start/stop cable, general use, 35900-60670 78
Agilent APG remote start/stop cable, 03396-61010 79
Agilent APG remote start/stop cable, G1530-60930 79
Agilent remote start/stop Y-cable, G1530-61200 80
External event cable, G1530-60590 82
External valve cable, G1580-60710 83
Pulser module power supply cable, G1580-60730 83

Installation and First Startup 5


6 Installation and First Startup
1 Installing the GC
Overview of Installation 8
Connecting to the Browser Interface 10
The 8890 GC 11
Unpacking 12
Place the GC on the bench 13
Verify line voltage, voltage settings, and power cord 15
Connect GC to LAN, Local Computer, or Tablet 22
Connect the power cord and turn on the GC 24
View the System Setup Wizard 25
Configure the GC IP address 26
Set the Date/Time 27
Set the Pressure Units 28
Configure Carrier Gas Types 29
Connect Gases and Traps 30
Leak test all connections and set source pressures 38
Install ALS, if ordered 42
Connect the external cables 44
Vent ECD or uncombusted hydrogen to a fume hood 48
Connect cryogenic cooling (if present) 49
Configure the checkout column 55
Install the checkout column 57
Transfer the checkout sample to a screw-top sample vial 59
When the system stabilizes, run one injection 60
Prepare for the Next Analysis 61

This section contains installation procedures for the Agilent 8890 GC. Depending on the
ordered options, some steps are optional, such as “plumbing” cryogenic cooling or valve
actuator air.
Instructions for connecting cables from the GC to other instruments in a typical 8890 Series
system are included here and in Appendix B, “Cabling Diagrams and Remote Start/Stop” on
page 69“.

Installation and First Startup 7


1 Installing the GC

Overview of Installation
Purpose of this procedure
This procedure ensures that instruments and systems are installed and functioning as
designed. Correct installation is the first step in ensuring that instruments and systems
operate reliably over their lifetimes.

Customer responsibilities
1 Make sure your site meets the basic requirements, including the necessary space,
electrical outlets, gases, tubing, operating supplies, consumables and other
usage-dependent items, required for a successful installation. Refer to the Agilent 8890
Gas Chromatograph GC, GC/MS, and ALS Site Preparation Guide.
2 If Agilent is delivering installation and familiarization services, users of the instrument
should be present throughout these services; otherwise, these users will miss important
operational, maintenance, and safety information.
Additional information is available via the GC Touchscreen, Browser Interface help &
information suite, and the Agilent GC and GC/MS User Manuals & Tools DVD.

About Agilent’s installation service


The installation service does not include:
• Network setup with other computers, or to the site or building LAN.
• Customization of the system.
• Method development and testing.
• Analysis of customer standards or samples.
• Testing against the instrument performance specification.
If you need assistance beyond this installation service, please contact your local Agilent
office. Assistance with installation and with user-specific services and applications is
available and will be contracted separately.

Tools and additional parts required


Installation requires the following tools, fittings, and hardware. These items are not included
with the instrument.
• Precleaned copper tubing, 1/8-inch or 1/4-inch od.
• Fittings.
• Tubing cutter.
• Filters for gas supplies.
• 7/16-inch and 9/16-inch wrenches for assembling Swagelok fittings.
• Carrier and other gas supplies.

8 Installation and First Startup


1 Installing the GC

• Pressure regulator for each gas supply.


• A computer, tablet, or other LAN capable device (for accessing GC user information and for
updating GC firmware when needed).
• Any additional LAN components, such as cables and a switch or hub, for connection to the
site LAN (not included in Agilent installation services).
The Agilent 8890 Gas Chromatograph GC, GC/MS, and ALS Site Preparation Guide contains a
listing of Agilent installation kits and a description of parts included with each kit. These kits
contain filters, fittings, tubing, tools (wrenches, tubing cutter, drivers, and so on), and other
required parts for installing a GC.

Performing checkout
Checkout requires a system that can produce a chromatogram.
• If using an Agilent data system, you can perform the checkout procedure. Read these GC
installation instructions and the instructions for installing the data system.
• If connected only to an integrator or site system (for example, a LIMS system) that
captures the GC output signal, you must connect to that system to obtain the
chromatogram.

System installation
If installing an ALS, the ALS can be used for checkout. Refer to the ALS installation
documentation for details.
When installed as part of a complete system including an Agilent data system (for example,
Agilent OpenLAB CDS), first install the GC up to the checkout column bakeout step. Once the
bakeout ends, configure the new GC in the data system and open the online instrument
session. Use the data system to perform the checkout test.
When installed as part of other complete systems, for example in an Agilent GC/MSD or
GC/MS system, refer to the installation instructions for that system.

Configuring the GC
To configure the various components of your GC, you must use either the Touchscreen or
access the Browser Interface from a computer on the same network as your GC. For more
information about connecting to the Browser Interface, see “Connecting to the Browser
Interface”.
To access the copy of this manual stored on your GC, enter http://<your GC’s IP
address>/install into the web browser of your choice.

Installation and First Startup 9


1 Installing the GC

Connecting to the Browser Interface


To connect to the GC using a browser:
1 If you do not know the GC's IP address or host name, use the touchscreen to find it.
2 Open a web browser. Supported browsers include Chrome, Safari (on a tablet), Internet
Explorer 11, and Edge. Make sure the browser version is up to date.
3 Enter http://xxx.xx.xx.xxx, where xxx.xx.xx.xxx is the GC's IP address. (If
using a host name, enter it instead.) In this example, the GC IP address is 10.1.1.101.
Accessing the Browser Interface only requires that the tablet or computer be connected to
the same gateway as the GC; no internet connection is required.

Browser Interface

http://10.1.1.101

X
8890 GC

http://10.1.1.101/install

LAN switch or hub


LAN cable

10 Installation and First Startup


1 Installing the GC

The 8890 GC
Detectors

Inlets

Oven

Power switch
Touchscreen

Figure 1. Front of the 8890 GC

Oven exhaust
vents
Inlet vents

Gas supply
connections

Electronic
cable
connections

EPC cooling
intake
Power
connection
Figure 2. Back of the 8890 GC

Installation and First Startup 11


1 Installing the GC

Unpacking
Be careful when lifting the GC. Because it is heavy, two people should lift it. When moving the
WAR N IN G GC, be aware that the back is heavier than the front.

1 Inspect the shipping containers for damage.


2 If a container is damaged or shows signs of stress, do the following:
a Notify both the carrier and your local Agilent sales office.
b Keep all shipping materials for inspection by the carrier.
3 Check the items received against the packing lists.
4 If there are discrepancies, notify your local Agilent sales office immediately.
5 Retain the shipping containers until you check their contents for completeness and verified
instrument performance.

12 Installation and First Startup


1 Installing the GC

Step 1 Place the GC on the bench


The GC requires a bench that can support its weight plus that of other equipment you will use
with it. The area must be free of overhanging obstructions that might interfere with
autosamplers, or that limit access to the top of the instrument. The area must include
sufficient space behind the GC to allow for cooling.
1 Remove the GC from its shipping box.

2 Place the GC on the bench top. Make sure gas and power supplies are accessible. Place
related equipment near the GC.

The power cord is the power disconnect device. Do not position the instrument such that
WAR N IN G access to the coupler or plug is impaired.

Make sure your GC has adequate distance from the wall and other instruments.
C AU T I O N

3 If space is limited behind the GC, attach the optional oven exhaust deflector to the back of
the GC as shown below. (Order Option 306 or part number G3450-81650.) The deflector
hangs from the exhaust vents on four hooks.

Installation and First Startup 13


1 Installing the GC

Oven exhaust
deflector

Figure 3. Correct position of the oven exhaust deflector

The oven exhaust deflector accepts a 10-cm (4 in.) diameter exhaust duct, and adds
about 13 cm to the depth of the GC, but this additional depth does not increase the depth
required for proper ventilation.

14 Installation and First Startup


1 Installing the GC

Step 2 Verify line voltage, voltage settings, and


power cord
1 Locate the power label near the power cord connector on the back of the GC. Compare the
instrument power settings with the laboratory line voltage. See “Power consumption” on
page 16.
2 Verify that the power cord is correct for the voltage and location. “Power cords
available” on page 17.

Electrical shock hazard. To avoid injury, only a qualified person should measure line voltage.
WAR N IN G

3 Have a qualified person measure the actual power outlet voltage and verify that it meets
the tolerance requirements listed in Table 1 on page 16. See “Grounding” on page 21“ and
“Line voltage” on page 15.
The following sections detail the power specifications and requirements for reference.

Line voltage
Typical GC System - 8890 GC with computer and printer.

Use isolated circuits with


dedicated grounds for GC and

31-in. (79 cm)


(without heat
deflector)

Leave 12-in. (31 cm) 26-in. (66 cm)


open space for (with heat
operational access deflector)

Installation and First Startup 15


1 Installing the GC

To protect users, the metal instrument panels and cabinet are grounded through the
WAR N IN G three-conductor power line cord in accordance with International Electrotechnical
Commission (IEC) requirements.

A proper earth ground is required for GC operations. Any interruption of the grounding
conductor or disconnection of the power cord could cause a shock that could result in
personal injury.

Be sure to verify proper receptacle grounding.

Do not use extension cords with Agilent instruments. Extension cords normally are not rated
WAR N IN G to carry enough power and can be a safety hazard.

1 Make sure that each instrument in your GC system can be connected to a dedicated circuit
with an isolated ground. (Note that ALS instruments receive their power from the GC.)
2 Power requirements are printed near the power cord attachment on the rear panel of each
instrument. Although your GC should arrive ready for operation in your country, compare
its voltage requirements with those listed in Table 1 on page 16. If the voltage option you
ordered is not suitable for your installation, contact Agilent.

Power consumption
The number and type of electrical outlets required for installation depends on the size and
complexity of your system. A GC system with a computer, monitor, printer, and hub requires 5
outlets. The outlet for the GC must be a dedicated circuit.
Each GC has a label next to the power cord connector that lists its line voltage requirements.
See the examples below.

The GC power consumption and requirements depend on the type of oven that you ordered
and the country the unit shipped to. Fast oven options 002 and 003 require more power than
the standard oven.
See your Site Preparation Guide for a list of the power cords available for the GC. If your power
cord is incorrect, order the cord appropriate for the country.

Table 1 GC power requirements

Oven Line voltage Frequency Current Power Power outlet


current rating

Standard Americas: 120 V AC (1) single phase, 48-63 Hz 18.8 amps 2250 VA 20 A
+10 to –10%

Standard 220/230/240 V single/split phase,  48-63 Hz 10.2 / 9.8 / 2250 VA 10 A


+10 to –10% 9.4 amps

16 Installation and First Startup


1 Installing the GC

Table 1 GC power requirements (continued)

Oven Line voltage Frequency Current Power Power outlet


current rating

Fast Japan: 200 V split phase, +10 to –10% 48-63 Hz 14.8 amps 2950 VA 15 A

Fast 220/230/240 V (2)(3) single/split phase, +10 to 48-63 Hz 13.4 / 12.8 / 2950 VA 15 A
–10% 12.3 amps

Notes
1 Some US labs have 3 phase service resulting in 208 V at the wall receptacle. It is important
for a qualified person to measure the line voltage at the receptacle for the GC. Option 003,
208 V fast oven, uses a 220 V unit with operating range of 193 to 231 V.
2 Power line conditioners should not be used with the GC.

Power cords available


Table 2 lists the power cords available for the GC. If your power cord is incorrect, order the
cord appropriate for the country.

Table 2 Power cords by country

Part number Country Description Wall termination Plug termination

8120-1369 Australia, New Power Cord, Australia/NZ, C13, 10 amp AS 3112


Zealand

8120-1378 Americas Cable Assembly-Power Cord 18AWG NEMA 5-15


2.3m-LG

8120-1689 Europe Cable Assembly-Power Cord 17AWG CEE/7/V11


2m-LG PV

8120-2104 Switzerland Cable-Assembly-Power cord 250VAC 10A Swiss/Denmark 1302


3-C

Installation and First Startup 17


1 Installing the GC

Table 2 Power cords by country (continued)

Part number Country Description Wall termination Plug termination

8120-3997 Denmark, Greenland Power Cord, DK/Greenland, C13, 10 amp AFSNIT 107-2-01

8120-4211 India, South Africa Power Cord, India/S Africa, C13, 10 amp AS 3112

8120-4753 Japan Power Cord, Japan, C13, 125V NEMA L6-20P

8120-5182 Israel Power Cord, Israel, C13, 10 amp Israeli SI32

8120-6360 Taiwan, South Power Cord, Taiwan/S America, C19, 20A NEMA 5-20P
America
G

8120-6869 Argentina Power Cord, Argentina, C13 250V 10A AS 3112


RA/3

8120-6894 US Power Cord, US 120V, C19, 20 amp NEMA 5-20P

18 Installation and First Startup


1 Installing the GC

Table 2 Power cords by country (continued)

Part number Country Description Wall termination Plug termination

8120-6903 Japan Power Cord, Japan, C19, 20 amp NEMA L6-20P

8120-6978 Chile Power Cord, Chile, C13, 10 amp CEI 23-16

8120-8619 Australia Power Cord, Australia, 16 amp AS 3112

8120-8620 Great Britain, Hong Power Cord, GB/HK/SG/MY, C19, 13 amp BS1363
Kong, Singapore,
Malaysia

8120-8621 Europe Power Cord, Europe, 16 amp CEE7/V11

8120-8622 Switzerland, Denmark Power Cord, Swiss/DK, C19, 16 amp Swiss/Denmark 1302

8120-8705 Great Britain, Hong Power Cord, GB/HK/SG/MY, C13, 10 amp BS89/13
Kong, Singapore,
Malaysia

8121-0070 China Power Cord PRC Fast GB 1002

Installation and First Startup 19


1 Installing the GC

Table 2 Power cords by country (continued)

Part number Country Description Wall termination Plug termination

8121-0075 US Power Cord, US 240V, C19, 15 amp NEMA L6-15P

8121-0161 Israel Power Cord, Israel, C19, 16 amp Israeli SI32

8121-0675 Argentina Power Cord, Argentina, C19, 20 amp AS 3112

8121-0710 India, South Africa Power Cord, India/S.Africa, C19, 15 Amp AS 3112

8121-0723 China Power Cord, China, C13, 10 amp GB 1002

8121-1222 Korea Power Cord, Korea, C19, 16 amp CEE7/V11

8121-1226 Korea Power Cord, Korea C13, 10 amp CEE7/V11

8121-1301 Thailand Power Cord, Thai 220V, 15 A, 1.8M, C19

20 Installation and First Startup


1 Installing the GC

Table 2 Power cords by country (continued)

Part number Country Description Wall termination Plug termination

8121-1787 Brazil Power Cord, Brazil, C19, 16 A, 250V Max IEC 60906-1

8121-1809 Brazil Power Cord, Brazil, C13, 10 A, 250V Max IEC 60906-1

Grounding
To protect users, the metal instrument panels and cabinet are grounded through the
three-conductor power line cord in accordance with International Electrotechnical
Commission (IEC) requirements.
When plugged into a properly grounded receptacle, the three-conductor power line cord
grounds the instrument and minimizes shock hazard. A properly grounded receptacle is one
that is connected to a suitable earth ground. Proper receptacle grounding should be verified.
Make sure the GC is connected to a dedicated circuit.

Installation and First Startup 21


1 Installing the GC

Step 3 Connect GC to LAN, Local Computer, or


Tablet
If you intend to connect your system to your site’s LAN network, you must have an additional
shielded twisted pair network cable (8121-0940).
Use a network cable to connect the GC LAN port to your site LAN or directly to a local
computer.

Figure 4. LAN connection

A single LAN communications cable is supplied with the GC. The switch (or hub) and other
cables must be ordered separately, if needed.

22 Installation and First Startup


1 Installing the GC

Figure 5. Simple supported LAN configuration: LAN Switch or hub

Agilent is not responsible for connecting to or establishing communication with your site
NOTE LAN network. The Agilent representative will test the system’s ability to communicate on a
mini-hub or LAN switch only.

Installation and First Startup 23


1 Installing the GC

Step 4 Connect the power cord and turn on the GC


1 Verify that the power switch is in the Off position.

Power
Switch

Figure 6. Power switch location

2 Plug the power cord into the back of the GC and the power outlet.

Attach power
cord here

Figure 7. Power cord location

24 Installation and First Startup


1 Installing the GC

Step 5 View the System Setup Wizard


The system setup wizard walks through the most important steps needed to install and
configure the GC. It provides a way to enter only the critical settings needed to get started
quickly, leaving all other configuration settings at their default values. These steps include:
• Unpacking
• Setting the system date, time, and IP address
• Setting the gas units, gas types, and similar choices
• Connecting gases and checking for leaks
• Installing a sampler, if available
• Running a checkout sample

You can follow the system setup wizard, or cancel it and follow the procedures here instead.
Whether using the wizard or not, this guide provides all of the supporting information needed
for installation.
After exiting the system setup wizard, you can re-launch it at any time. On the GC touchscreen,
navigate to Settings > System Setup and touch Run System Setup.

Installation and First Startup 25


1 Installing the GC

Step 6 Configure the GC IP address


If you intend to connect your system to your site’s network, each piece of equipment must
have a unique IP address assigned to it. For an isolated LAN installation, see Table 3 for typical
IP addresses.

Table 3 Typical IP addresses for an isolated LAN

GC Computer

IP address 10.1.1.101 10.1.1.100

Subnet mask 255.255.255.0 255.255.255.0

1 Select Settings > System Settings > Network.

2 Manually enter the GC Host Name, IP address, Gateway, and Net Mask (subnet mask), or
enable DHCP to propagate these fields.

26 Installation and First Startup


1 Installing the GC

Step 7 Set the Date/Time


Select Settings > System Settings > Date and Time and set the GC clock.
• The Current Time is based on a 24 hour clock.
• The time set here is important for the time and date stamps used when collecting data and
recording log entries (such as maintenance tasks and errors). The GC time also controls
resource conservation for connected samplers.

Installation and First Startup 27


1 Installing the GC

Step 8 Set the Pressure Units


To set the pressure units, select Settings > Configuration > Misc, and select the desired
pressure units to use in methods.

28 Installation and First Startup


1 Installing the GC

Step 9 Configure Carrier Gas Types


Select Settings > Configuration > Inlets and use the dropdown menu to select the Carrier Gas
Type connected to the selected inlet. Repeat for any additional inlets installed in your GC.

Installation and First Startup 29


1 Installing the GC

Step 10 Connect Gases and Traps


Most of installation involves plumbing gas to tanks, filters, and flow modules. Swagelok fittings
are used to make leak-tight connections. If you are not sure how to make a Swagelok
connection, see Appendix A, “Making Swagelok Connections” for instructions.

Hydrogen is a flammable gas. If hydrogen or any other flammable gas is used, periodic leak
WAR N IN G tests should be performed. Be sure that the hydrogen supply is off until all connections are
made, and insure that the inlet fittings are either connected to a column or capped at all times
when hydrogen gas is present in the instrument.

Substituting parts or performing any unauthorized modification to the instrument may result
in a safety hazard.

The insulation around the inlets, detectors, valve box, and the insulation cups is made of
refractory ceramic fibers (RCF). To avoid inhaling RCF particles, we recommend these safety
procedures: ventilate your work area; wear long sleeves, gloves, safety glasses, and a
disposable dust/mist respirator; dispose of insulation in a sealed plastic bag; wash your
hands with mild soap and cold water after handling RCFs.

Install the gas regulators


1 Select the appropriate CGA regulator for each gas type. (In other countries, refer to local
standards. See the Agilent GC, GC/MS, and ALS Site Preparation Guide for requirements.)

Table 4 Gas regulators, 1/8-inch, U.S. only *

Description Part number

CGA 346, 125 psig max (8.6 bar), Air 5183-4641

CGA 350, 125 psig max (8.6 bar), H2, Ar/Me 5183-4642

CGA 540, 125 psig max (8.6 bar), O2 5183-4643

CGA 580, 125 psig max (8.6 bar), He, Ar, N2 5183-4644

CGA 590, 125 psig max (8.6 bar), Air 5183-4645

* For 1/4-inch tubing, purchase a 1/4-inch to 1/8-inch adapter, U.S. only.

Never use a liquid thread sealant on gas fittings. Liquid thread sealants introduce
C AU T I O N contamination into the GC plumbing.

2 Confirm that the outlet fitting of the regulator is 1/8-inch Swagelok. If not, install the
appropriate adapter fitting. Wrap the fitting threads using PTFE tape. Wrap the tape in a
clockwise direction so that the adapter threads do not unwrap the tape. Be careful to keep
the tape away from the end of the fitting. Two to three tightly wound wraps are sufficient.
Tighten the Swagelok adapter fitting securely to the NPT pipe thread fitting.

30 Installation and First Startup


1 Installing the GC

3 Install the regulator onto the compressed gas cylinder main fitting.
• Check the thread type. Some regulators use left-hand thread fittings. For left-handed
threads, the nut will have a groove in it.

Groove indicates
left-hand thread

4 Purge the air from the regulator by repeating the following procedure 5 times:
a Fully close the regulator knob, then open the main tank valve.
b Turn the regulator knob fully counter-clockwise to open the tank main valve,
pressurizing the primary side of the regulator.
c Turn OFF the tank main valve.
d Slowly turn the regulator knob clockwise to release (“bleed off”) the gas pressure.
e Close the regulator knob.
The image below illustrates a typical pressure regulator installation. In the example shown
below, which uses an optional shutoff valve, open the shutoff valve and leave open during
purging.

Installation and First Startup 31


1 Installing the GC

Secondary gauge Primary gauge


Shutoff valve
(optional) Main tank valve

Regulator knob

Swagelok adapter

Connect the tubing to the gas source


If you need more than 4.5 m (15 feet) of supply tubing to connect to a gas source, use
NOTE 1/4-inch tubing with appropriate hardware. See the Agilent GC, GC/MS, and ALS Site
Preparation Guide for part numbers.

1 Turn off all gases at their sources. Measure the length of tubing needed to connect the gas
supply outlet to the inlet fitting on the GC. Take into account any traps or tees you will need.
2 Cut the tubing to length with a tubing cutter. See Figure 8.

Cutting wheel

Good cut

Figure 8. Typical tubing cutter

3 Connect the tubing to the gas source with a Swagelok fitting. See Appendix A, “Making
Swagelok Connections”.

32 Installation and First Startup


1 Installing the GC

Install traps
1 Determine where you will install the traps in your supply tubing line. Figure 9 shows the
recommended trap order for the carrier gas and the recommended locations for On/Off
valves. Also see the Site Preparation Guide.
Tank valve Two-stage regulator

On/Off valve

Gas Clean Filter


system

On/Off valve

Gas supply
Figure 9. Plumb the gas supplies

2 Cut the tubing to length with a tubing cutter.


3 Connect the traps and tubing. On/Off valves are not essential, but are very useful when a
tank or trap must be changed. (If purchasing Agilent compliance services, install an on/off
valve for each inlet gas supply.)

Plumb to EPC flow modules


Inlet and detector EPC flow modules are mounted very close together across the back of the
GC. See Figure 10.

Detector EPCs Inlet EPCs

Figure 10. Plumb flow modules

Installation and First Startup 33


1 Installing the GC

Purge the supply lines for a few minutes before connecting them to the GC flow modules.

Be sure to vent uncombusted hydrogen to a fume hood or other safe location.


WAR N IN G

When two inlets use the same carrier gas, we recommend using a Tee fitting that includes
shutoff valves for performing leak tests.
When two detectors use the same gases, we recommend using a Tee fitting. Shutoff valves
are not required.

TCD connections The carrier gas and reference gas must come from the same source.
Because of the close spacing of the EPC modules, the simplest way to do this is to attach
lengths of tubing to each input to bring the ends outside the back panel, then join them with a
Tee.

Side mounted detector connections If the GC is equipped with a side-mounted TCD or ECD,
attach the carrier gas to the single gas connection at the back of the side mount enclosure.
(For TCD, an internal Tee feeds the reference gas and input.)

Install Aux EPC module frits for your application


Skip this section if an Aux EPC module is not installed.
The AUX EPC module ships with brown (FID air) restrictors in all channels. For certain
applications, you will have to replace this restrictor (frit) so the EPC module can provide flows
in the correct ranges. See Table 5. Also refer to the other instrument’s or application’s
documentation.

Table 5 G3470-60502 Aux EPC restrictor kit

Kit contains Part number Marking Flow Resistance Often used with

O-rings, 6/pk 5181-3344

None G3430-80061 1 ring 400 ± 30 SCCM air Low FID air, purged splitters, Deans
Brown @ 40 psig switch

3 G3430-80062 2 rings 30 ± 1.5 SCCM H2 Medium FID hydrogen


Red @ 15 psig

3 G3430-80063 3 rings 3.33 ± 0.3 SCCM H2 High NPD hydrogen


Blue @ 15 psig

3 G3430-20011 None Zero (none) Purged splitter, Deans switch


when using backflush

Notes for this table


• Frit G3430-80061 ships in each AUX channel.
• Restrictor kit G3470-60502 is included in the AUX module ship kit.
• Always use new O-rings (part number 5181-3344, O-rings, 6/pk).
• Install tubing and connectors as needed for each additional gas supply required.

34 Installation and First Startup


1 Installing the GC

• Do not install an external flow restrictor.

Installation and First Startup 35


1 Installing the GC

Install hydrogen sensor calibration gas


If available, install the hydrogen sensor calibration gas. The hydrogen sensor ship kit includes a
pressure regulator that installs directly onto the calibration gas cylinder. Agilent also provides
sufficient copper tubing and hardware to connect the pressure regulator to the hydrogen
sensor assembly calibration gas input fitting.
1 Set the gas cylinder stand upright on the lab bench near the GC.

The gas cylinder is pressurized. Do not place the cylinder on its side or behind the oven
WAR N IN G exhaust vent!

1/8-inch Swagelock
nut and ferrule
Pressure
regulator
To hydrogen sensor
input fitting

Calibration
gas cylinder
1/8-inch copper
tubing, cut to
length needed

Gas cylinder
stand

2 Turn the pressure regulator completely off and set the output pressure as low as possible
(full CCW).

3 Install the pressure regulator onto the calibration gas cylinder (it screws on).

36 Installation and First Startup


1 Installing the GC

4 Connect the calibration gas cylinder output tubing to the hydrogen sensor module.
• Use the tubing, nuts, and ferrules provided in the hydrogen sensor kit.
• See the figure under step 1.
5 Install the calibration gas cylinder into the stand and secure using the screw.
6 Turn on the supply pressure at the pressure regulator. (You will adjust it later.)
7 Check for leaks in the fittings using a leak detection fluid. Correct any leaks.

Installation and First Startup 37


1 Installing the GC

Step 11 Leak test all connections and set source


pressures
Liquid leak detectors, such as soapy water, are not recommended, especially in areas where
cleanliness is very important. If there is a leak, these liquids can contaminate the plumbing and
affect your analyses. If you do use leak detection fluid, immediately rinse the fitting to remove
the soapy film.
When checking for leaks of hydrogen or helium, Agilent recommends the G3388B leak
detector, or similar.

To avoid a potential shock hazard when using liquid detection fluid, turn the GC off and
WAR N IN G disconnect the main power cord. Be careful not to spill leak solution on electrical leads.

Perform a pressure drop test.


1 Turn off the GC.
2 Set the regulator pressure to 415 kPa (60 psi).
3 Fully turn the regulator pressure adjustment knob counterclockwise to shut the valve.
4 Wait 10 min. If there is a pressure loss greater than 7 kPa (1 psi), there is a leak in the
external connections. Use the leak detector to check each fitting for leaks. See Figure 11.

38 Installation and First Startup


1 Installing the GC

Figure 11. Locations to check for leaks

5 Correct leaks by tightening the connections and then retest the connections. Continue
tightening until all connections are leak-free.

Installation and First Startup 39


1 Installing the GC

Set source gas pressures


The pressure set at a tank regulator depends on these factors:
• The inlet pressure needed to achieve the highest column flow rate required by your
method.
The pressure/flow relationship depends on the column or device involved. The best way
to address this is to begin at a moderate pressure level and adjust upward as needed.
• A pressure difference of about 170 kPa (25 psi) across flow controlling devices enables
them to work properly.
• The pressure limit of the weakest part of the supply system.
Swagelok fittings and copper tubing are more than adequate for the highest pressures
used in gas chromatography.
We recommend a maximum continuous operating pressure of 1170 kPa (170 psi) to
avoid excessive wear and leaks.
Traps are often the weakest part of the system. They should be labeled, either on the trap
itself or in accompanying literature, with a maximum operating pressure. Source
pressure must not exceed the lowest maximum operating pressure in the supply
system.
Table 6 suggests starting values of source pressure.

Table 6 Suggested starting pressures

Gas Use Source pressure

Carrier Packed column 410 kPa (60 psi)

Capillary columns 550 kPa (80 psi)

Air for FID, FPD Detectors 550 kPa (80 psi)

Hydrogen Detectors 410 kPa (60 psi)

Makeup gas Detectors 410 kPa (60 psi)

TCD Reference TCD 410 kPa (60 psi)

Air for valve actuators Valves 345 kPa (50 psi)

40 Installation and First Startup


1 Installing the GC

Step 12 Install inlet checkout parts


If using a split/splitless or multimode inlet, install the liner and O-ring needed for checkout. See
the Operation manual, and the procedures listed in Maintaining Your GC.
If installing a GC/MS system, refer to the GC/MS installation manuals for the correct inlet
hardware to install, as needed.

Installation and First Startup 41


1 Installing the GC

Step 13 Install ALS, if ordered


If installing an ALS, install it now. Refer to its instructions.
Prepare the sampler for checkout. See the checkout procedures and information in the
Operation Manual.
1 Prepare a 2-mL screw-top sample vial with checkout sample.
2 Prepare 4-mL waste vials and place them into the turret.
3 Prepare fresh solvent solutions as needed for the checkout sample for your detector type.
Place the solvent vials into the injector turret. For details on the solvent needed, see the
Operation Manual:

42 Installation and First Startup


1 Installing the GC

Step 14 Configuring GC-MSD communications


If connected to an MSD such as 5977A or 7000C/D, use the GC touchscreen to identify the
connected MSD’s IP address and to select the part information (for example, source type, and
pump type). Touch Settings > Configuration > Detectors, then select the tab for the MSD. The
MSD IP address entered here must exactly match the IP address entered in the data system
and at the MSD keyboard.
Once the instruments have IP addresses and are connected to the LAN, complete the GC/MS
configuration and enable enhanced communications, Parts Finder data, and MS-friendly
features such as the MS Vent method as follows:
1 Select Settings > Configuration > Detectors.
2 If configuring a 5977B MSD, select LCOMM from the dropdown menu under Connection
Type, and input the MSD’s IP Address, Gateway, and Net Mask. Otherwise, select DCOMM
and input the MSD’s IP address.
3 Enter details for the MSD.

Installation and First Startup 43


1 Installing the GC

Step 15 Connect the external cables


In addition to the LAN cable as referenced in “Connect GC to LAN, Local Computer, or
Tablet” on page 22, other cables may be installed for control of the GC’s automatic liquid
sampler (ALS), connecting signal output to integrators, synchronizing the start and end of a
run between various instruments, sensing conditions external to the GC, and controlling
devices external to the GC.

Back panel connectors


The figure below shows the connectors on the back panel of the GC.

SIG1
SIG2
BCD
ELVDS1
ELVDS2
LAN

USB1
ALS1
EVENT
USB2
ALS2

TRAY REMOTE

See also “Cable Diagrams” on page 77.

Sampler connectors
If using an ALS, connect it to the GC using the following connectors:
ALS 1 Optional. An injector or 150-position sample tray.
ALS 2 Optional. An injector or 150-Position sample tray.
TRAY Optional. The 150-position sample tray (includes optional barcode
reader/heater/mixer control, if purchased).

The SIG (analog output) connectors


Optional. Use SIG1 and SIG2 for analog output signals.

REMOTE connector
Provides a port to remotely start and stop other instruments using the APG protocol. A
maximum of 10 instruments can be synchronized using this connector. See “Using the
Remote Start/Stop Cable” on page 70 for more detail.

44 Installation and First Startup


1 Installing the GC

EVENT connector
This connector provides two passive contact closures and two 24-volt outputs for controlling
external devices. The outputs are controlled by valve drivers 5 through 8.

BCD input connector


This connector provides two control relays and a BCD input for a stream selection valve or a
BCD generating device.

BCR/RA connector
This connector is reserved for the optional G3494B RS-232 Barcode Reader. Refer to the GC
Operation Manual.

LAN connector
Standard Local Area Network (LAN) connector, for communication with data systems and
other devices via TCP/IP.

Connecting cables
Use the supplied LAN cable to connect the GC to a LAN switch or hub as shown below in
Figure 12. Other LAN configurations are possible. Refer to your Agilent data system
documentation for details about its supported LAN configurations.

LAN switch or hub

LAN cable
Crossover LAN cable 5183-4648
8121-0940
LAN cable
8121-0940

OR

GC Computer GC Computer

Figure 12. Simple supported LAN configurations: LAN switch or hub (left) and direct connection (right)

Table 7 Typical IP addresses for an isolated LAN

GC Computer

IP address 10.1.1.101 10.1.1.100

Subnet mask 255.255.255.0 255.255.255.0

Installation and First Startup 45


1 Installing the GC

A single LAN communications cable is supplied with the GC. The switch (or hub) and other
cables must be ordered separately, if needed. See Table 8 and Table 9 for cabling
requirements for other configurations.

Table 8 Cabling requirements

8890 Series GC connected to: Required Cable(s) Part number

Samplers
7693A Automatic Liquid Sampler Injector cable or tray cable G4514-60610

7650 Automatic Liquid Sampler Injector cable G4514-60610

7683 Automatic Liquid Sampler Injector cable is integral


Tray cable G2614-60610

7697A Headspace Sampler Remote, 9-pin male/6-pin connector G1530-60930

G1289B/G1290B Headspace Sampler Remote, 9-pin male/6-pin connector G1530-60930

CTC automatic sampler Cable, 4 conductor, remote start G6500-82013

Mass Spectrometers and MS


systems
Mass Selective Detector Remote, 2-m, 9-pin male/9-pin male G1530-61200

GC / Agilent external sampler / MS or MSD Y-Cable, remote start/stop G1530-61200


system (for example, GC/HS/MSD or
GC/Thermal Desorber/MSD)

GC / TMS-9800/ MS or MSD system Y-Cable, remote start/stop G1530-61200


Interface cable for Agilent 6890/7890/8890 to P&T 14-6689-086

Integrators
3395B/3396C Integrator Remote, 9 pin/15 pin 03396-61010
Analog, 2 m, 6 pin G1530-60570

Non-Agilent Integrator General purpose analog signal cable 2 m, 6 pin G1530-60560

Non-Agilent data system General use remote, 35900-60670 (2 m), 


9-pin male/spade lugs 35900-60920 (5 m),
(various lengths) 35900-60930 (0.5 m)

Other devices
Non-Agilent External event, 8 pin/spade lugs (No label. See “Labeling G1530-60590
instrument, unspecified BCD and EVENT cables” on page 56.)

Valco pulser module (used with PDHID) Valve pulser module power supply cable (includes green G1580-60730
EVENT label)

Stream selection valves See documentation accompanying the valve


Gas sampling valves (external)

External valve cable (includes green EVENT label) G1580-60710

LAN
LAN Cable, networking CAT 5, 25 feet 8121-0940
Cable, LAN, crossover 5183-4648

46 Installation and First Startup


1 Installing the GC

Table 9 Cabling for other instruments in a 8890 Series GC system

Instrument 1 Instrument 2 Type of cable Part number

Mass Selective Detector Purge & trap, thermal Splitter (“Y”) cable for remote G1530-61200
desorber, or headspace start/stop, 1 male and 2 female
sampler connectors
Splitter (“H”) cable for APG remote, 2 35900-60800
male and 2 female connectors

GC / MS / Agilent data system / ALS

1. LAN cable
8121-0940 LAN switch or hub

1. LAN cable 1. LAN cable


8121-0940 8121-0940

MSD GC Computer

2. APG Remote Cable,


G1530-61200

Table 10 Cables for a typical GC/MSD or GC/MS system

Number Part number and description

1 G1530-61200, 2-m APG remote cable, 9-pin male/9-pin male

2 8121-0940, Cable, LAN, 25 foot

Additional cabling configurations


For additional cabling configurations, see Appendix B, “Cabling Diagrams and Remote
Start/Stop”.

Installation and First Startup 47


1 Installing the GC

Step 16 Vent ECD or uncombusted hydrogen to a


fume hood
If using a ECD, or if using hydrogen carrier gas that will be uncombusted, you must either
safely vent the exhaust or operate the GC inside a fume hood. For example, if using hydrogen
carrier gas the GC would vent uncombusted hydrogen from a thermal conductivity detector
(TCD) and from the inlet split vent and septum purge vent.
The ECD exhaust vents through a coiled tube. Connect tubing from the tube fitting at the end
of this tubing to an exhaust hood via a hole in the back panel.
H2
connections

ECD vent
tubing hole

For a TCD, you must supply vent tubing and fittings to connect to the detector exhaust tube on
the top of the detector. Route the tubing out the back of the GC, following the same path as for
the ECD vent tubing.
The other detectors (FID and FPD) combust any hydrogen carrier gas.

48 Installation and First Startup


1 Installing the GC

Step 17 Connect cryogenic cooling (if present)


Cryogenic cooling allows you to cool the oven or inlet, including cooling to setpoints below
ambient temperature. A solenoid valve controls the flow of coolant to the inlet or oven. The
oven can use either liquid carbon dioxide (CO2) or liquid nitrogen (N2) as a coolant. All inlets
except the multimode inlet must use the same coolant type as the oven. The multimode inlet
can use a different coolant than configured for the oven, and can also use compressed air as a
coolant.
CO2 and N2 coolants require different hardware on the GC. (You can use air cooling on a
multimode inlet, with either the CO2 or N2 solenoid valves and hardware.)
Flared or AN tubing fittings are commonly used to connect the liquid supply tubing to the cryo
coolant tank. Check with the supplier of the coolant before plumbing to be sure you have the
correct fittings.

Connecting liquid carbon dioxide


Do not use copper or thin-wall stainless steel tubing! Either presents an explosion hazard.
WAR N IN G

Do not use padded tanks for CO2 supplies. The cryogenic valve is not designed to handle the
C AU T I O N higher pressures padded tanks generate.

The tank must be equipped with an eductor tube (dip tube) that reaches to the bottom of the
tank, so that liquid (rather than gaseous) CO2 is drawn.

Materials needed
• 1/8-inch heavy-wall, stainless steel tubing

Procedure
1 Locate the inlet for liquid CO2 on the rear of the GC. Prepare enough tubing to reach from
the supply tank to this fitting. See Figure 13.

Installation and First Startup 49


1 Installing the GC

Cryo inlets

Figure 13. Location of cryogenic cooling valve

2 Connect the supply tubing to the liquid CO2 tank outlet with the fitting recommended by the
supplier.
3 Use a Swagelok fitting to connect the supply tubing to the cryogenic valve inlet.

Connecting liquid nitrogen


Materials needed
• 1/4-inch insulated copper tubing

Procedure
1 Position the nitrogen tank as close to the GC as possible to insure that liquid and not gas is
delivered to the inlet.
2 Locate the inlet for coolant on the rear of the GC. Prepare enough tubing to reach from the
supply tank to this outlet. See Figure 14.

50 Installation and First Startup


1 Installing the GC

Cryo inlets

Figure 14. N2 cryogenic cooling valve connections

3 Connect the supply tubing to the liquid N2 tank outlet with the fitting recommended by the
supplier.
4 Use a Swagelok fitting to connect the supply tubing to the cryogenic valve inlet.

Connecting air to the multimode inlet


The multimode inlet can also use compressed air cooling with the liquid N2 inlet cooling
option. Requirements for compressed air cooling:
• The compressed air should be free of particulate material, oil, and other contaminants.
These contaminants could clog the inlet's cryo valve and expansion orifice or impact the
proper operation of the GC.
• The required air supply pressure depends on the installed solenoid valve type. For a
multimode inlet with N2 cooling, set the air supply pressure to 138 to 276 kPa (20 and
40 psig).
While air supplied from tanks can meet these criteria, the consumption rate of air can be
80 L/min, varying based on supply pressure.

A noise reduction kit, G3510-67001, is available for users of compressed air cooling with a
NOTE multimode inlet.

Materials needed
Installation of a compressed air line to the inlet cryo coolant valve requires the hardware (and
appropriate fittings) noted below:
• Use 1/4-inch copper or stainless steel tubing for supply tubing to the N2 valve

Installation and First Startup 51


1 Installing the GC

Procedure
1 Locate the input fitting for inlet coolant on the rear of the GC. Prepare enough tubing to
reach from the supply to this outlet.
2 Connect the supply tubing to the air supply outlet with the fitting recommended by the
supplier.
3 Use a Swagelok fitting to connect the supply tubing to the cryogenic valve input fitting.

52 Installation and First Startup


1 Installing the GC

Step 18 Connect valve actuator air (if present)


Valves are driven by air actuators. Valves should have a dedicated air source; they cannot
share detector air supplies.

Do not share air between a detector and valves.


C AU T I O N

Valves can use nitrogen as an alternate supply. In this case, the nitrogen does not have to be
chromatographic grade but must be free from contaminants.
Valve actuator air is supplied through 1/4-inch plastic tubing. If your GC was ordered with
valves, the plastic tubing will already be attached to the actuators and will extend from the
back of the GC. Additional valves are shipped with a 1/4 to 1/8-inch reducing union to be used
in plumbing.

Route the tubing away from the oven exhaust. The hot air will melt the plastic tubing.
C AU T I O N

Turn off the air supply at the source. If needed, shorten the supplied plastic tubing using a
sharp knife. Connect the tubing to the air source using a 1/4-inch Swagelok nut and ferrules.
See Figure 15.

Hole for
actuator air
tubing

Figure 15. Valve actuator air tubing

Installation and First Startup 53


1 Installing the GC

Step 19 Configure Headspace Communications


The 7697 headspace sampler can be configured to communicate with the connected GC. This
feature requires a HS with firmware A.01.06 (or greater). With communications configured, the
HS knows GC method timings and programs, and can synchronize with the GC clock and
follow the GC instrument schedule.
To configure GC-HS communications:
1 Select Settings > Configuration > Headspace.
2 Use this page to enter details for, and control, the headspace sampler.
3 Select Apply. The entered changes are saved to the GC.
If communications fails, check the IP addresses. Verify that the GC's IP address is correct in
the headspace sampler, and that the headspace sampler's IP address is correct in the GC. Also
check that both instruments are turned on and connected to the LAN. Verify all LAN cable
connections.
After GC installation, complete HS configuration. Refer to the HS control software help and the
HS manuals for information on the configuration options.

54 Installation and First Startup


1 Installing the GC

Step 20 Configure the checkout column


You must configure the consumable items (such as the checkout column).
If your checkout column has a Smart ID Key, Insert the key into one of the six Smart ID key
slots on the front of the GC. Input which number column (1-6) the key corresponds to in the
dialog that appears.

Checkout column
The column length, inside diameter, and film thickness are on a metal tag attached to the
column.
1 Select Settings > Configuration > Columns > Column # to be configured and choose
Column Type.
2 In the Inlet connection field, choose the Inlet to select a gas pressure control device for
this end of the column. Selections include the installed GC inlets, and installed Aux and
PCM channels.

3 In the Length field, type the column length, in meters.


4 In the Diameter field, type the column inside diameter in microns.
5 In the Film thickness field, type the film thickness in microns. The column is now defined.
6 In the Outlet connection field, select a gas pressure control device for this end of the
column. Selections include the installed Aux and PCM channels, and detectors. When a
detector is selected, the outlet end of the column is controlled at 0 psig for the FID, TCD,
FPD, NPD, and ECD or vacuum for the MSD.

Installation and First Startup 55


1 Installing the GC

7 Select the Thermal zone. In most cases this will be GC oven, but you may have an MSD
transfer line heated by an auxiliary zone, valves in a separately-heated valve box or other
configurations.

8 Press Apply.
This completes configuration for a single capillary column. Also see the Operation manual for
more information about configuring columns.

56 Installation and First Startup


1 Installing the GC

Step 21 Install the checkout column


A capillary column was shipped with the GC to be used to confirm proper operation. Agilent
suggests that it be used only for that purpose.
Before use, the column must be conditioned to remove any contaminants.
1 Locate the installation instructions for the column, inlet, and detector you will use. Refer to
the Maintaining Your GC manual. See to the sections on your specific inlet and detector
types:
2 Install the column in the inlet.
3 Connect the free end of the column to the detector, as described in Maintaining Your GC.
4 Turn on the carrier gas.
5 If using a split/splitless or multimode inlet, perform an Inlet Leak Check. Select Diagnostics
> Diagnostic Test, select Inlet #, then select Leak & Restriction Test. Press Start Test to
begin the check. If the check fails, tighten connections.

Installation and First Startup 57


1 Installing the GC

6 Set the oven temperature and inlet flow conditions specified for conditioning the column.
Select Method to access current GC temperatures and flows.
• Set the oven temperature to 20 °C higher than the highest checkout method
temperature (do not exceed the column maximum temperature). For example, for FID
checkout set the oven temperature to 210 °C.
• Set the detector temperature to 20 °C higher than the checkout method temperature.
For example, for FID checkout set the detector temperature to 320 °C.
7 Turn the detector gases on. Light the flame, if appropriate.
8 Heat the detector to the temperature given in the bakeout instructions, and hold at
temperature for the time given in the instructions.

58 Installation and First Startup


1 Installing the GC

Step 22 Transfer the checkout sample to a


screw-top sample vial
1 The checkout sample is contained in sealed glass vials. Wrap a piece of cloth or a paper
towel around the vial to protect your fingers and snap the top off.

2 Use a pipette to transfer the sample to a 2-mL screw-top vial. (If using an ALS, use a vial
suitable for the ALS turret or tray, as applicable.)

Installation and First Startup 59


1 Installing the GC

Step 23 When the system stabilizes, run one


injection
Perform the checkout procedure as described in the Operation Manual.
1 Enter the parameters for the checkout procedure.
• If using an Agilent data system, use it to create a checkout method.
• If not using a data system, enter the setpoints using the GC touchscreen or the Browser
Interface.
2 When the GC is ready to begin a run, the Touchscreen status shows STATUS: NORMAL
READY (alternately, when the component of the GC is not ready to begin a run, the
touchscreen shows STATUS: NOT READY), make the injection and start the run.
For a manual injection, inject the sample and press Prep Run .

3 Evaluate results by comparing the chromatogram you generated with the one in the
checkout procedure. There should be a close resemblance.

60 Installation and First Startup


1 Installing the GC

Step 24 Prepare for the Next Analysis


After evaluating the GC under the checkout conditions, installation checkout is complete. The
next step is to prepare the GC for your next analysis. Be sure to cool the GC before making
changes.
1 Cool all heated zones to < 40 °C, and set safe gas flows. Place the GC in maintenance
mode: Maintenance > Instrument > Perform Maintenance > Maintenance Mode > Start
Maintenance and wait for the GC to become ready.
2 Turn off the power by pressing the On/Off switch.
3 Shut off all gas valves at the gas source.
4 If you are using cryogenic cooling, shut off the cryo coolant valve at the source.
5 When the GC is cool, do the following:
• Install the appropriate inlet hardware (can include septum, liner, liner-O-ring, inlet gold
seal, inserts, and so on).
• Install the appropriate detector hardware (wavelength filter for FPD+, jet for FID or NPD).
• Change to any alternate gas sources as needed for the new analysis.
• Install the desired column and condition it per the manufacturer’s recommendations.
• Configure the GC to match any hardware or gas type changes (columns, liners, carrier or
makeup gas types, and so on).
• Load or create the desired method.

Installation and First Startup 61


1 Installing the GC

62 Installation and First Startup


A Making Swagelok Connections
Making Swagelok Connections 64

Using a Swagelok Tee 67

The gas supply tubing is attached with Swagelok fittings. If you are not familiar with Swagelok
connections, review the following procedures.

Installation and First Startup 63


A Making Swagelok Connections

Making Swagelok Connections


Objective
To make a tubing connection that does not leak and that can be taken apart without damaging
the fitting.

Materials needed
• 1/8-inch (or 1/4-inch, if used) preconditioned copper tubing
• 1/8-inch (or 1/4-inch, if used) Swagelok nuts
• Front and back ferrules
• Two 7/16-inch (for 1/8-inch nuts) or 9/16-inch (for 1/4-inch nuts) wrenches

Procedure
1 Place a Swagelok nut, back ferrule, and front ferrule on the tubing as shown in Figure 16.

Front ferrule
Important!
Back ferrule
The narrow end of the
Nut back ferrule fits into
the rear of the front
ferrule.

Tubing

Figure 16. Swagelok nuts and ferrules

2 Push the tubing into the stainless steel fitting.


3 Make sure that the front ferrule is fully engaged. Slide the Swagelok nut over the ferrule and
thread it onto the plug.
4 Push the tube fully into the plug, then withdraw it approximately 1 to 2 mm. See Figure 17.

64 Installation and First Startup


A Making Swagelok Connections

Front Nut
ferrule
Insert
tubing fully

Back
ferrule

Withdraw tubing
1-2 mm

Tighten nut

Figure 17. Insert the tubing

5 Finger-tighten the nut.


6 Mark the nut with a pencil line. See Figure 18.

Pencil line

Figure 18. Marking the fitting

7 For 1/8-inch Swagelok fittings, use a pair of wrenches to tighten the fitting 3/4 of a turn.
See Figure 19.

Figure 19. Final tightening

8 Remove the plug from the fitting. To connect the tubing, with nut and ferrules, to another
fitting, finger-tighten the nut, then use a wrench to tighten it 3/4 (1/8-inch fittings) of a turn.

Installation and First Startup 65


A Making Swagelok Connections

9 Both correctly and incorrectly swaged connections are shown in Figure 20. Note that the
end of the tubing in a correctly swaged fitting is not crushed and does not interfere with the
action of the ferrules.

Figure 20. Completed fitting

66 Installation and First Startup


A Making Swagelok Connections

Using a Swagelok Tee


To supply gas from a single source to more than one input, use a Swagelok Tee.

Do not combine valve actuator air with flame ionization air. The valve action will cause major
NOTE upsets in the detector signal.

Materials needed:
• 1/8-inch preconditioned copper tubing
• Tubing cutter
• 1/8-inch Swagelok nuts and front and back ferrules
• 1/8-inch Swagelok Tee
• Two 7/16-inch wrenches
• 1/8-inch Swagelok cap (optional)
1 Cut the tubing where you want to install the Tee. Connect the tubing and Tee with a
Swagelok fitting. See Figure 21.

Cap

Tee fitting

Nut and
ferrules

Figure 21. Swagelok tee

2 Measure the distance from the Tee to the instrument fittings. Attach copper tubing to the
open Tee ends with Swagelok fittings.

Installation and First Startup 67


A Making Swagelok Connections

68 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

B Cabling Diagrams and Remote


Start/Stop
Using the Remote Start/Stop Cable 70

Multi-instrument Cabling Examples 73

Cable Diagrams 77

This section lists cabling requirements and connection diagrams that apply to less common or
specialized GC installations.

Installation and First Startup 69


B Cabling Diagrams and Remote Start/Stop

Using the Remote Start/Stop Cable


Remote start/stop is used to synchronize two or more instruments. For example, you might
connect an integrator and the GC so that the Start/Stop buttons on either instrument control
both of them. You can synchronize a maximum of ten instruments using Remote cables.

Connecting Agilent products


If connecting two Agilent products with Remote cables, the sending and receiving circuits will
be compatible—just plug in both ends of the cable.

Connecting non-Agilent products


If connecting to a non-Agilent product, the following paragraphs contain information you will
need to ensure compatibility.

APG Remote signal electrical specifications


The APG signals are a modified open collector type. The signal levels are generally TTL levels
(low voltage is logic zero, high voltage is logic one) but the open circuit voltage will be between
2.5 and 3.7 V. The typical voltage is 3 V. A voltage over 2.2 V will be interpreted as a high logic
state while a voltage below 0.4 V will be interpreted as a low logic state. These levels provide
some margin over the specifications of the devices used.
The pull-up resistance, connected to the open-circuit voltage, is in the range of about 1 kOhms
to 1.5 kOhms. For a logic-low state, for a single device on the bus, the minimum current you
must be able to sink is 3.3 mA. Since devices are connected in parallel, when you have multiple
devices this minimum current must be multiplied by the number of devices attached on the
bus. The maximum voltage for a low-input state is 0.4 V.
The bus is passively pulled high. Leakage current out of a port must be less than 0.2 mA to
keep the voltage from being pulled lower than 2.2 V. Higher leakage current may cause the
state to be interpreted as a low.
Over-voltage protection: APG Remote connections are clamped by a zener diode to 5.6 V.
Exceeding this voltage will damage the circuit (GC logic board).

APG Remote - Suggested drive circuits


A signal on the APG bus may be driven by another APG device or by one of the following
circuits:
• A relay, with one side connected to ground, when closed will set a logic-low state.
• An NPN transistor, with the emitter connected to ground and the collector connected to the
signal line will set a logic-low state if proper base current is supplied.
• An open-collector logic gate will perform this same function.
• A low-side drive IC will also work, but Darlington-type drivers should be avoided as they will
not meet the low-side voltage requirement of less than 0.4 V

70 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

APG Remote connector

1 Pin Function Logic


6
1 Digital ground
5 9
2 Prepare LOW true

3 Start LOW true (output)

4 Start relay

5 Start relay

6 Not used

7 Ready HIGH true (output)

8 Stop LOW true

9 Not used

APG Remote signal descriptions

Prepare (Low True) Request to prepare for analysis. Receiver is any module performing
pre-analysis activities. For example, shorting pin 2 to ground will put the GC into Prep Run
state. This is useful for Splitless Mode to prepare the inlet for injection or when using Gas
Saver. This function is not needed by Agilent autosampler systems.

Ready (High True) If the Ready line is high (> 2.2 VDC) then the system is ready for next
analysis. Receiver is any sequence controller.

Start (Low True) Request to start run/timetable. Receiver is any module performing
runtime-controlled activities. The 8890 Series GC requires a pulse duration of at least
500 micro-seconds to sense a start from an external device.

Start Relay (Contact Closure) A 120 millisecond contact closure used as an isolated output to
start another device that is not compatible or connected with APG Remote pin 3.

Stop (Low True) Request to reach system ready state as soon as possible (for example, stop
run, abort or finish, and stop injection). Receiver is any module performing runtime-controlled
activities. Normally this line is not connected, if the GC oven program is used to control the
method Stop time.

Installation and First Startup 71


B

72
Stop
Start

Ready
L
H
H
Prepare H
Waiting for Ready

H
L System Ready
Cabling Diagrams and Remote Start/Stop

Requeswt for Prepare


APG Remote timing diagram

Not Ready during Prep

H System Ready

Start Requested

Inject cycle started


L

Injection/Start

Run
L

Runtime elapsed/Start

Postrun
Waiting for Ready
H

System Ready

Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

Multi-instrument Cabling Examples


GC / ALS / Non-Agilent Data System

GC/ALS

1. APG Remote Cable, 2. External event cable,


G1530-60930 8 pin/spade lugs, G1530-60590

Number Part number and description

1 G1530-60930, General use APG remote cable, 9-pin male/spade lug (0.5m)

2 G1530-60590, External event cable, 8-pin/spade lugs

35900-60670 APG remote G1530-60590 External event


cable spade lug identification cable spade lug identification

Connector 1  Signal name Connector 2  Pin Color Signal


9 pin (male) spade lugs

1 GND Black 1 Yellow 24 V Out

2 Prepare White 2 Black 24 V Out 2

3 Start Red 3 Red Ground

4 Shut down Green 4 White Ground

5 Reserved Brown 5 Orange Contact 1

6 Power on Blue 6 Green Contact 1

7 Ready Orange 7 Brown Contact 2

8 Stop Yellow 8 Blue Contact 2

9 Start Request Violet 9

Installation and First Startup 73


B Cabling Diagrams and Remote Start/Stop

GC / 3395A/3396B Integrator / ALS

GC/ALS

1. APG Remote Cable, 2. Analog cable, 2-m, 6 pin,


03396-61010 G1530-60570

Number Part number and description

1 03396-61010, 2-m APG remote cable, 9-pin/15-pin

2 G1530-60570, 2-m Analog cable, 6-pin

GC / 3396C Integrator / ALS

GC/ALS

1. APG Remote Cable, 2. Analog cable, 2-m, 6 pin,


G1530-60930 G1530-60570

Number Part number and description

1 G1530-60930, 2-m APG remote cable, 9-pin male/9-pin male

2 G1530-60570, 2-m Analog cable, 6-pin

74 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

Example: Using a Y-Cable in a setup (GC/MSD/Data


System/Headspace Sampler)
1. LAN cable 8121-0940 LAN switch or hub

1. LAN cable 1. LAN cable 1. LAN cable


8121-0940 8121-0940 8121-0940

MSD GC/ALS HS Computer

2. APG Remote Y-Cable,


G1530-61200

Number Part number and description

1 8121-0940, Cable, LAN, 25 foot

2 G1530-61200, 2-m Y-cable, remote start/stop

Installation and First Startup 75


B Cabling Diagrams and Remote Start/Stop

GC / External Events (unspecified, non-Agilent


instrument)

1. External event cable,


8 pin/spade lugs,
G1530-60590
GC/ALS

Number Part number and description

1 G1530-60590, External events cable, 8-pin/spade lugs

Connector Signal name Maximum rating Wire color Corresponds to valve #

24 volt control output

1 24 volt output 1 150 mA output Yellow 5

2 24 volt output 2 150 mA output Black 6

3 Ground Red

4 Ground White

Relay contact closures (normally open)

5 Contact closure 1 48 V AC/DC, 250 mA Orange 7

6 Contact closure 1 Green 7

7 Contact closure 2 48 V AC/DC, 250 mA Brown or violet 8

8 Contact closure 2 Blue 8

76 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

Cable Diagrams
Analog signal cable, general use, G1530-60560
Connects GC signal outputs to non-Agilent products. Also used for the Analog Input Board
(AIB).
5 6

3 4 G1530-60560

1 2

Connector 1

Connector 2
The pin assignments for the general use analog out cable are listed in Table 11.

Table 11 Analog cable, general use, output connections

Connector 1 Connector 2, wire color Signal

1 Brown or violet Not used

2 White 0 to 1 V, 0 to 10 V (–)

3 Red Not used

4 Black 1 V (+)

6 Blue 10 V (+)

Shell Orange Ground

Installation and First Startup 77


B Cabling Diagrams and Remote Start/Stop

Agilent analog signal cable, G1530-60570


This cable connects an Analog out port to an external data system. Both 0 to 1 volt and
0 to 10 volts are provided. Connects both GC signal outputs to Agilent 3395B/3396C
integrators, and the 35900 A/D.

Figure 22. Analog output cable to an Agilent product

Remote start/stop cable, general use, 35900-60670

1
6
35900-60670
9
5

Connector 1

Connector 2

The pin assignments for the remote start/stop cable are listed in Table 12.

Table 12 Remote start/stop cable connections

Connector 1, 9-pin male Connector 2, wire color Signal

1 Black Digital ground

2 White Prepare (low tone)

3 Red Start (low tone)

4 Green Start relay (closed during


start)

5 Brown Start relay (closed during


start)

6 Blue Open circuit

7 Orange Ready (high true input)

8 Yellow Stop (low tone)

9 Violet Open circuit

78 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

Agilent APG remote start/stop cable, 03396-61010


Synchronizes the GC with an Agilent integrator. Additional cables may be used to add more
instruments (up to 10 total).

Figure 23. Remote start/stop cable, GC to Agilent integrator

Agilent APG remote start/stop cable, G1530-60930


Synchronizes the GC with another Agilent instrument. Additional cables may be used to add
more instruments (up to 10 total).

1 1
6 G1530-60930
9
5
2
5 5
9 9
6
1
1 6

Figure 24. Remote start/stop cable, GC to Agilent instrument

Installation and First Startup 79


B Cabling Diagrams and Remote Start/Stop

Agilent remote start/stop Y-cable, G1530-61200


Synchronizes the GC with another 2 Agilent instruments.

Figure 25. Remote start/stop cable, GC to Agilent instrument

BCD cable, G1530-60590


The BCD cable connector has eight passive inputs that sense total binary-coded decimal
levels. The pin assignments for this connector are listed in Table 13.

Table 13 BCD input connections

Pin Function Maximum rating

1 Relay 48 V AC/DC, 250 mA

2 Relay 48 V AC/DC, 250 mA

3 LS digit 0

4 LS digit 1

5 LS digit 2

6 LS digit 3

7 MS digit 0

8 Ground

Shield Chassis ground

When used for BCD input, apply label G1580-87100 to identify the cable for BCD use.

BCD cable, G1530-61100


The BCD cable connector has eight passive inputs that sense total binary-coded decimal
levels. The pin assignments for this connector are listed in Table 14.

Table 14 BCD cable connections

Connector 1 Pin Connector 2 Pin Ribbon Cable Wire Color

1 Brown

2 Red

80 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

Table 14 BCD cable connections (continued)

Connector 1 Pin Connector 2 Pin Ribbon Cable Wire Color

1 3 Orange

4 Yellow

5 Green

6 Blue

7 Violet

8 Gray

9 White

2, 8 10 Black

11 Brown

6 12 Red

13 Orange

5 14 Yellow

15 Green

4 16 Blue

7 17 Violet

3 18 Gray

19 White

20 Black

21 Brown

22 Red

23 Orange

24 Yellow

25 Green

26 Blue

Installation and First Startup 81


B Cabling Diagrams and Remote Start/Stop

External event cable, G1530-60590


Apply label
G1580-87200

6 7 8

3 4 5

1 2

Wire terminations
The external event cable has two passive relay contact closures with two 24-volt control
outputs. Devices connected to the passive contact closures must be connected to their own
power sources.
The pin assignments for this cable are listed in Table 15.

Table 15 External events cable

Connector 1 pin Signal name Maximum rating Connector 2, wire color Controlled by valve #

24 volts output

1 24 V output 1 150 mA Yellow 5

2 24 V output 1 150 mA Black 6

3 Ground Red

4 Ground White

Relay contact closures (normally open)

5 Closure 1 48 V AC/DC, 250 mA Orange 7

6 Closure 1 Green 7

7 Closure 2 48 V AC/DC, 250 mA Brown or violet 8

8 Closure 2 Blue 8

When used for external event control, apply label G1580-87200 to identify the cable for EVENT
use.

82 Installation and First Startup


B Cabling Diagrams and Remote Start/Stop

External valve cable, G1580-60710


Supplies power for certain valve applications.

2 6 8
V5
1

INTO THE BCD PORT.


CAUTION: DO NOT PLUG
EVENT
2 1 2
V6
1

Connector 1 pin Wire color Connector and pin Function

1 Yellow V5 pin 1 24 V, 150 mA max.

2 Black V6 pin 1 24 V, 150 mA max.

3 Red V5 pin 2 Ground

4 White V6 pin 2 Ground

Pulser module power supply cable, G1580-60730


Supplies power for a PDHID pulser module.

Installation and First Startup 83


B Cabling Diagrams and Remote Start/Stop

6 8 Connector 1

1 2

Connector 2 1 2

1 3
Connector 3

2 4

Connector 1 pin Wire color Connector and pin Function

1 Yellow

2 Black

3 Red

4 White Connector 3 pin 1* Ground

5 Orange Connector 2 pin 1 Contact closure 1, 48 V


AC/DC, 250 mA

6 Green Connector 3 pin 3 Contact closure 1

7 Brown

8 Blue

* Connector 3: Pin 1 is jumpered to pin 2. Pin 2 is jumpered to pin 4.

84 Installation and First Startup


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85 Installation and First Startup


www.agilent.com
Agilent Technologies, Inc. 2018
First edition, December 2018
*G3540-90013*
G3540-90013

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