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    Chap 5 Miscellaneous Test Methods

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    Diosa Juno
    This document outlines various miscellaneous test methods found in Chapter Five of a manual. It lists over 30 different methods for testing properties like water content, cyanide, sulfides, chlorides, and more. The methods can be used to test solid waste, wastewater, soils and other materials.

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    Chap 5 Miscellaneous Test Methods

    Uploaded by

    Diosa Juno
    5 views2 pages
    This document outlines various miscellaneous test methods found in Chapter Five of a manual. It lists over 30 different methods for testing properties like water content, cyanide, sulfides, chlorides, and more. The methods can be used to test solid waste, wastewater, soils and other materials.

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    EPA chap 5 Miscellaneous test methods

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    chap 5 Miscellaneous test methods

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    This document outlines various miscellaneous test methods found in Chapter Five of a manual. It lists over 30 different methods for testing properties like water content, cyanide, sulfides, chlorides, and more. The methods can be used to test solid waste, wastewater, soils and other materials.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    5 views2 pages

    Chap 5 Miscellaneous Test Methods

    Uploaded by

    Diosa Juno
    This document outlines various miscellaneous test methods found in Chapter Five of a manual. It lists over 30 different methods for testing properties like water content, cyanide, sulfides, chlorides, and more. The methods can be used to test solid waste, wastewater, soils and other materials.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

    CHAPTER FIVE

    MISCELLANEOUS TEST METHODS

    Prior to employing the methods in this chapter, analysts are advised to consult the
    disclaimer statement at the front of this manual and the information in Chapter Two for
    guidance on the allowed flexibility in the choice of apparatus, reagents, and supplies. In
    addition, unless specified in a regulation, the use of SW-846 methods is not mandatory in
    response to Federal testing requirements. The information contained in each procedure is
    provided by EPA as guidance to be used by the analyst and the regulated community in making
    judgements necessary to meet the data quality objectives or needs for the intended use of the
    data.

    The following methods are found in Chapter Five:

    Method 5050: Bomb Preparation Method for Solid Waste


    Method 9000: Determination of Water in Waste Materials by Karl Fischer
    Titration
    Method 9001: Determination of Water in Waste Materials by Quantitative
    Calcium Hydride Reaction
    Method 9010B: Total and Amenable Cyanide: Distillation
    Method 9012A: Total and Amenable Cyanide (Automated Colorimetric, with
    Off-line Distillation)
    Method 9013: Cyanide Extraction Procedure for Solids and Oils
    Method 9014: Titrimetric and Manual Spectrophotometric Determinative
    Methods for Cyanide
    Method 9020B: Total Organic Halides (TOX)
    Method 9021: Purgeable Organic Halides (POX)
    Method 9022: Total Organic Halides (TOX) by Neutron Activation Analysis
    Method 9023: Extractable Organic Halides (EOX) in Solids
    Method 9030B: Acid-Soluble and Acid-Insoluble Sulfides: Distillation
    Method 9031: Extractable Sulfides
    Method 9034: Titrimetric Procedure for Acid-Soluble and Acid-Insoluble
    Sulfides
    Method 9035: Sulfate (Colorimetric, Automated, Chloranilate)
    Method 9036: Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II)
    Method 9038: Sulfate (Turbidimetric)
    Method 9056A: Determination of Inorganic Anions by Ion Chromatography
    Method 9057: Determination of Chloride from HCl/Cl2 Emission Sampling
    Train (Methods 0050 and 0051) by Anion Chromatography
    Method 9060A: Total Organic Carbon
    Method 9065: Phenolics (Spectrophotometric, Manual 4-AAP with
    Distillation)
    Method 9066: Phenolics (Colorimetric, Automated 4-AAP with Distillation)
    Method 9067: Phenolics (Spectrophotometric, MBTH with Distillation)
    Method 9070A: n-Hexane Extractable Material (HEM) for Aqueous Samples

    FIVE - 1 Revision 5
    February 2007
    Method 9071B: n-Hexane Extractable Material (HEM) for Sludge, Sediment,
    and Solid Samples
    Method 9075: Test Method for Total Chlorine in New and Used Petroleum
    Products by X-Ray Fluorescence Spectrometry (XRF)
    Method 9076: Test Method for Total Chlorine in New and Used Petroleum
    Products by Oxidative Combustion and Microcoulometry
    Method 9077: Test Methods for Total Chlorine in New and Used Petroleum
    Products (Field Test Kit Methods)
    Method A: Fixed End Point Test Kit Method
    Method B: Reverse Titration Quantitative End Point Test Kit
    Method
    Method C: Direct Titration Quantitative End Point Test Kit
    Method
    Method 9131: Total Coliform: Multiple Tube Fermentation Technique
    Method 9132: Total Coliform: Membrane-Filter Technique
    Method 9210A: Potentiometric Determination of Nitrate in Aqueous Samples
    with an Ion-Selective Electrode
    Method 9211: Potentiometric Determination of Bromide in Aqueous Samples
    with Ion-Selective Electrode
    Method 9212: Potentiometric Determination of Chloride in Aqueous Samples
    with Ion-Selective Electrode
    Method 9213: Potentiometric Determination of Cyanide in Aqueous Samples
    and Distillates with Ion-Selective Electrode
    Method 9214: Potentiometric Determination of Fluoride in Aqueous Samples
    with Ion-Selective Electrode
    Method 9215: Potentiometric Determination of Sulfide in Aqueous Samples
    and Distillates with Ion-Selective Electrode
    Method 9216: Potentiometric Determination of Nitrate in Aqueous Samples
    with Ion-Selective Electrode
    Method 9250: Chloride (Colorimetric, Automated Ferricyanide AAI)
    Method 9251: Chloride (Colorimetric, Automated Ferricyanide AAII)
    Method 9253: Chloride (Titrimetric, Silver Nitrate)
    Method 9320: Radium-228

    FIVE - 2 Revision 5
    February 2007

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