Instruction Manual: Vacuum Dry Oven
Instruction Manual: Vacuum Dry Oven
Instruction Manual: Vacuum Dry Oven
Vacuum Constant
Temperature
Dryer
Vacuum Dry Oven Instruction Manual
VOS-210C
VOS-310C
This instruction manual is designed to use the product efficiently and safely with keeping its best performance.
Wrong handling is assumed to cause the possibility of the death or heavy injury of the user.
Warning
Wrong handling is assumed to cause the risk of injury of the operator or physical damages.
Caution
possible occurrence of risk in the course of use of the product, but the prediction of all and every kind of risk is extremely difficult. Namely, cautions
dure described in this manual, the safe operation and work are ensured. Be sure to pay utmost care during handling of the product to prevent accid
2. Warning Display on the Product
① ② ③
①
②
③
Thank you for purchasing our
product.
Introduction
•This instruction manual explains installation, operation,
troubleshooting, maintenance and inspection, and discarding Always read this manual before use to ensure
procedures for the products below: familiarization of the product.
•Vacuum constant-temperature dryer
•Vacuum Dry Oven;
•VOS-210C/VOS-310C
Table of contents
1. For safe operation 1
5.3.2 Temperature control alarm function 26
2. Product Summary
5.3.3 How to set Temp. Alarm 1
2.1 Intended use 2 Upper/Lower Limiter 26
2.2 Specification 2 5.3.4 How to set Temp. Alarm 2
2.3 Names of parts 3 Temperature Setting Upper/Lower Alarm 27
3. Names and Function of Operating Part 5.4 Setting mode operating method 28
3.1 Control panel 4 5 4-1 How to display setting mode28
3.2 Display part 5 5.4.2 PID channel 29
3.3 Constant-value operation and program run 6 5.4.3 Custom PID 29
3.4 Setting 8 5.4.4 How to use Auto-Tuning 30
3.5 Safety and alarm functions 9 5.4.5 Measured temperature correction function
31
4.Installation 5 4-6 Blackout recovery function 32
4.1 Installation environment 12 5.4.7 Optional features 33
4.2 Installation condition 12 5.4.8 Reset setting items 34
4.3 Utility connections 13 5.4.9 Lock operation keys 35
5. Operation 5 4-10 Adjust the display screen contrast 36
5.1 Preparation for operation 14
5.5 Vacuum operation method 37
5.1.1 Set shelf plates and connect to the vacuum
pump 14 5.6 Gas replacing operation method 38
5.1.2 Setting sample and container in the chamber 6. Causes of Trouble and Countermeasures 39
14 7. Maintenance and Inspection
5-1-3 Connect power plug 14
7.1 Leak breaker movement test 41
5.2 Operating method 15
7.2 Cleaning and care of the product
5.2.1 Set overheat protector 15
41 7-3 Consumable Parts 42
5.2.2 Setting, running and stopping constant-value
operation 16 8. Disposal of Product 42
5.2.3 Setting, running and stopping program run 18 9. Post-sale Service 43
5.3 Alarm function of temperature controller 25
5.3.1 How to display alarm screen on 10. List of Consumable and Replacing Components/Parts
the temperature controller 25 44
Product VOS-
Description of Package 210C 310C
1 Main body 1 1
2 Shelf plate 2 2
3 Instruction Manual 1 1
4 Warranty 1 1
1For safe operation
Pay due attention on the safety. The product may be extremely hot and is not of
an explosion-proof structure.
During operation, take care not to touch the top surface and the
upper portion of door because they become excessively hot.
During operation and for a certain period after operation, the observation window and the top and side of door
become extremely hot. Do not touch these portions to prevent burn.
• Side
1
2 Description of the Product
2.1 Application
NG This is the vacuum constant-temperature dryer that is
mpt to modify the product. Operate the unit for the specified purpose only. used for water removal of various samples and
materials
ock or a malfunction may result if the product is modified or used for any purposes other in the depressurized environment and for
than that specified.
drying and testing of various materials and parts in
the oxygen-free condition by filling the interior with
inactive gas.
Drying and testing in the absence of oxygen can be
performed by flowing inactivated gas inside the
chamber.
2.2 Specification
Product name Vacuum Constant Temperature Dryer (Vacuum Oven)
control 40 - 240ºC
Range of level of 1.01×105 to 1.33×102 Pa (760 to 1Torr)
vacuum in use
Accuracy of
temperature control*
±1.5ºC (at 240ºC)
Time to reach
temperature* About 80 minutes
Temperature controller Microcomputer PID control
Temperature sensor Pt 100Ω
Temperature
Sheet key input, digital display
Composition
setting/temperature display
Suction port Vacuum nozzle outer dia. 22 mm , Purge nozzle outer dia. 22 mm
*Unloaded at room temperature of 20ºC at normal pressure. The time to reach the temperature is the value of the can body
surface temperature in reduced pressure.
2
2.3 Names of parts
Observation window
Power cord
Handle
Door
*VOS-210C
does not have this
Purge nozzle
(Outer dia. 22mm)
3
3 Names and function of operating parts
3.1 Control panel
③ ② Panel key ⑤
① ⑧ ⑦ ⑥ ④
③ Indicator Temperature, time, set character and alarm detail are displayed.
This is valid only when the setting is displayed. Every push of a set value will add one value
⑤ ▲ key and holding down the value will make serial values.
If character setting is effective, the character is switched.
This is valid only when the setting is displayed. If a set value is numeric, every push reduces
⑥ ▼ key one and holding it down makes serial reductions.
If character setting is effective, the character is switched.
This switches a measured value to a set value and undertakes selection and confirmation of
⑦ Set key
a set item.When the alarm is output, the alarm display is cleared.
⑨ Contrast adjusting This key adjusts contrast. Insert a plus driver into the hole, turn the inner knob either left
or right to adjust to the position of giving good visibility of the display screen.
part
3.2 Display part (Main screen)
* This is reference for an explanation and is not different from the actual display screen.
② ③
① ④
⑤
⑥
⑦
⑩ ⑨
④ Time display The elapsed time is displayed while the timer is in operation during temperature control.
⑤ Status display The current control status and alarm are displayed.
Constant-value operation
Temperature
When a certain temperature is set and operation starts,
continuous operation is run at the set temperature.
Operation starts or stops with [Run/Stop] key. Set temperature
Time
Program run
✔ mark display
Time
(2) Auto Stop
t
Set time and start operation:
operation will be performed for the set time. The controls automatically Temperature
stop when the time has gone by.
Set temperature
It can be used in combination with Auto Start.
t1: The system runs for the set time once the measured value reaches
the set temperature.
t2: Press RUN/STOP key and the system runs for the set time. Time
t1
(3) 1Step
Set
temperature
T2
Time
(4) 2 Step t
Temperature
Set 2 temperatures and 2 times and set the number of loops.
Set temperature
Once the temperature control starts, temperature is controlled T2
at the set temperature T1 for t1 time.
t1 t2 t1 t2
Repeated
operation
3.4 Setting modes
Various values and optional features can be set.
*To change the value in the set mode, do so in the state of temperature control stopped.
Leak breaker Turned off and power disconnected. • Electricity leaks or overcurrent flows.
When the temperature inside the chamber • The set temperature of the overheat protector is low.
Overheat protector goes up more than the set temperature of • The temperature controller and/or SSR were out of order
the overheat protector, power is and the temperature inside the chamber
disconnected. went up more than the set temperature of the overheat
*When it returns to a temperature below the protector.
setting, recovery is done according to the
blackout recovery function.
Alarm functions
Names of alarms Alarm display and movement Cause of alarm movement and countermeasures
11
th e atures m t ting to
T
e limit may h overheat
h
te againstmove a e sample
A e
m SV. up u etc. (In the
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at "Set" greatl - Continuation o fan will
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limi e Wheneither u control prevent
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et not PID i the selection a
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Alarm th temper perfor . l In case of
mp rm i p
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Ala Co h u
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ol D i
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12
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w r t The
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T rature
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35ºC.
Watch Contro t Stop
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specifi r the
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13
4 Installation
Caution
Select the location with care.
Poor installation environment may accelerate deterioration of the product or may result in failure of demonstrating the functions and performance fully.
60 ㎝
Caution
This is a heavy product. Take utmost care during transport.
VOS-210C (about 40kg), VOS-310C (about 60kg)
20 ㎝ 20 ㎝
4.3 Connecting utilities
ning Warning
rm the voltage,
Always
phase,
connect
capacity,
to the
andoutlet
the type
with
ofearth
receptacle
terminal
of power
. supply.
onnection of powerWhen
supplyconnection
may causetofire or“outlet
the electricwithout
shock earth terminal” is inevitable, be sure to connect the earth wire of the earth adaptor to the ground, Otherwise, leakage can
Pay attention to the connection state of the earth adaptor and power plug. Inclined or insufficient insertion may cause overheat or fire.
Warning
Do not use the branching socket or table tap.
Burn-out of the cable or a fire may result from over current.
* Temporary set up
When you use an outlet without an earth
terminal, set an earth adaptor to the power
plug and be sure to connect the earth wire of
the adapter to the earth terminal.
* The earth adaptor is not included.
Check the
connection state
Connect to the
earth
* The earth adaptor is not included. When an outlet with an earth terminal is used
2-pole outletEarth adaptorPower plug (3-pole)
5 Operation
5.1 Preparation
5-1-1. Setting the shelf plate and connecting with the vacuum pump
Main body left side
(1) Set the shelf plate.
Evenly
Shelf plate
5.2 Operating method
aution Caution
not touch the hot parts
ring use and for a while after use. Stop using it if abnormality occurs.
Turn
observation window and upper and side parts of the door areoff
at the
highpower switch and
temperatures leakuse
during breaker (power
and for switch)
a while after immediately
use. if abnormality occurs and see the section Causes of Tro
ching any part of them may lead to burn.
Caution
5-2-1.Setting the overheat protector
Base point
Knob
Reset switch
Leak
breaker
Indicator Overheat
protector
Power switch
Purge valve
Vacuum valve
Setting, running and stopping
constant-value operation
Turn on the leak breaker.
The main screen displays after 5 seconds of the initial screen.
2) Operate [▲] and/or [▼] keys and input the set temperature.
Alarm
Run/Stop
Run Stop
MenuSet
Alarm
Run/Stop
Run Stop
MenuSet
Alarm
Run/Stop
Run Stop
MenuSet
*All counts are reset when power is restored and control either
resumes from the very beginning or stops according to the setting for
blackout recovery.
Alarm
the power plug from the outlet.
Run/Stop
If the system is not used for a long time, turn off the leak breaker and then remove
Run Stop
MenuSet
Setting, running and stopping program run
* Set this one while temperature control is terminated.
• Select 01 Program Run with [▲] or[ ▼] key and press "Set" key.
* No key operation for 30 seconds or longer will return to the main screen.
Alarm
Run/Stop
(2) Program run display screen
When each program run is set to be effective, Run
MenuSet Stop
a check (✔) is displayed on the checkbox in the left screen.
Checkbox
Alarm
Run/Stop
Run
MenuSet Stop
(3) Auto Start
Temperature control starts after a set time goes by.
1) How to set Auto Start
• Choose 01 Auto Start in the "Program Run" Program Run screen on
the previous page with [▲] or [▼] key by moving the cursor and press
“Set” key.
• The set temperature counts down after the set temperature T1 is reached.
• After the set time is counted down, control is provided at the set
temperature T2.
• 2 Step sets 2 times (t1 and t2) and 2 set temperatures (T1 and T2).
* T1: Set temperature used for control during the set time t1.
* T2: Set temperature used for control during the set time t2.
• Set the set temperature T2. • A time count value is displayed on the time display.
*T2 is the temperature to be controlled for the set time t2. • The current set temperature T1/T2 is displayed
Operate [▲] or [▼] key to select T2. on the set temperature display.
Press "Set" key to blink the value, enter a number * If the alarm sounds during counting, counting is
Operate [▲] or [▼] key to enter a value and press "Set" key suspended during the alarm.
to confirm the value.
3) During 2 Step control
• Press "Menu" key 3 times to return to the main screen. • Provide temperature control at the set temperature T1 and
count down the set time t1.
Alarm
Run/Stop
Run Stop
MenuSet
Alarm
Run/Stop
Run Stop
MenuSet
Checkbox
Alarm
Run/Stop
Run Stop
MenuSet
5-3-2. Alarm function of the temperature controller
• Two types of setting are available for the alarm of the temperature controller.
2 functions can be used at the same time.
• Control stop
The control is stopped w hen the measured
• Alarm display
1 01 Temp. Alarm1 Upper/Low er limiter temperature exceeds the upper and low er limit
A-0 (1H, 1L)
temperature.
• Alarm sound
While the checkbox is selected, press " Set" key to blink the checkbox,
operate [▲] or [▼] key to display ✔ mark.
Press "Set" key again to confirm the value.
*Upper limit (High) only or lower limit (Low) only or both can be set.
While the checkbox is selected, press " Set" key to blink the checkbox,
operate [▲] or [▼] key to display ✔ mark.
Press "Set" key again to confirm the value.
* Upper limit (High) only or lower limit (Low) only or both can be set.
Alarm
Run/Stop
Run Stop
MenuSet
Alarm
Run/Stop
Run Stop
MenuSet
Alarm
Run/Stop
Run Stop
MenuSet
31
5-4-2. PID channel
Select PID to be used for control. Two types of PID can be selected in this system.
* Do not make a change during control.
* They are set to default at factory shipment.
This should be chosen when a PID constant value calculated through auto-tuning or
2 Custom a PID constant value entered optionally in the Custom PID item is used.
* If Auto-Tuning starts, Custom is automatically chosen.
• Select 02 Customer PID on the Setting screen and press “Set” key.
• Operate [▲] or [▼] key to select the item you wish to change
and press "Set" key.
• While the value is blinking, operate [▲] or [▼] key to enter a value
and press “Set” to confirm the value.
32
2) Detail of Custom PID setting
This system employs PID control method for temperature control. Normally, there is no problem with the default PID,
but the precision of temperature control may get worse depending on the condition of use.
If this is the case, use either Auto-Tuning function or enter a PID value optionally.
This system employs PID control method for temperature control. Normally,
there is no problem with the default PID but the precision of temperature
control may get worse depending on the use condition. If this is the case,
try the Auto-Tuning function.
* Start auto-tuning when the temperature is stable below 20ºC from the
temperature you wish to control.
If you want to get better temperature control, adjust each PID constant Execution of auto-tuning automatically
value optionally. If overshoot occurs too often, it may be better if ARW is set switches to Custom PID.
at about 50%.
• Select the checkbox below the graph and press "Set" key to blink the checkbo x.
• Operate [▲] or [▼] key to display ✔ mark and press "Set" key to confirm it.
* The function becomes effective by displaying ✔ mark.
• Move to the number from the checkbox with [▲] or [▼] key and press
"Set" key to make it possible to enter a number.
• Operate [▲] or [▼] key to enter a value and press "Set" key to confirm
the value.
* The number can be entered in the range from -50.0ºC to +50.0ºC.
• Press "Set" key to blink the checkbox, operate [▲] or [▼] key to
display or hide ✔ mark.
• Press "Set" key to confirm. Set the blackout recovery function to be effective/not
effective by displaying or hiding ✔ mark in the
• One push of Menu key returns to the Settings item. checkbox.
2 pushes of "Menu" key return to the main screen.
When the blackout recovery function is not effective
-32-
5-4-7. Optional features
Optional function has two setting items.
• Buzzer effectiveness/non-effectiveness setting
• Display colors on screen reverse setting
* The icon on the main screen displays the setting status of buzzer.
• One push of “Menu” key returns to the Settings item. Reverse setting changing area for display
2 pushes of "Menu" key return to the main screen. colors on screen
An optionally set item can be reset to the factory shipment state. If this
operation is done, all entered values will be reset.
* It is recommended to take note of any important value or setting before
reset.
1) How to reset
• Select 07 Default Settings on the Setting screen and press "Set" key.
• Press “Set” key to select the checkbox and operate [▲] or [▼] key to
display ✔ mark.
• Once reset is over, the screen automatically return to the main screen.
nozzle
Purge
nozzle
Purge valve
Vacuum valve
(3) When drying is over, turn the vacuum valve clockwise to OPEN
close.
Then, turn the purge valve counterclockwise to open,
allowing the chamber inside to return to the atmospheric CLOSE
pressure.
×
Vacuum pump
Vacuum valve
Purge valve
(4) With the purge valve left open, turn the vacuum valve again
counterclockwise to open, allowing purge of air by the OPEN
vacuum pump for one minute.
CLOSE
* For the experiment with the sample placed under Vacuum pump (OFF)
depressurization, close the vacuum valve when the main
body has been drawn to a vacuum or gas purge is
Vacuum valve
completed. Then disconnect the piping between the main
body and the vacuum pump (return the suction port of the Purge valve
pump to atmosphere), turn OFF power supply to the
vacuum pump.
If power supply to the pump is turned OFF without
disconnecting the vacuum hose beforehand, oil of the pump
may backflow to the vacuum nozzle of the main body.
ry out gas replacement with the gas supply pressure of 19.6 kPa (0.2 kg/cm2) or less.
ment inside the chamber, high gas supply pressure may cause deformation of can body or damage to the observation window.
(4) Carry out gas replacement while opening the purge valve
gradually.
(5) After gas replacement, close the purge valve to put the
chamber interior to the airtight state.
For troubles other than those listed below, contact a shop from which you have purchased the product or our serv
6 Troubleshooting Guide
There is electric leakage. Stop the operation and contact the company
Overcurrent flow s. w here you purchased the product or the nearby
Earth leakage breaker is faulty. service center.
The earth leakage breaker does
Turn the knob of the overheat preventer to the
not turn on. right to change the setting temperature. Set the
It turns off immediately. Overheat prevention device is operating.
overheat preventer to a temperature that is 20 °
The set temperature of the overheat protector is
C higher than the set value that you w ant to set
low er than the inside temperature of the device.
to control the temperature inside the
compartment.
Even if the earth leakage The earth leakage breaker is faulty. Stop the operation and contact the company
breaker is turned on, nothing is w here you purchased the product or the nearby
displayed on the indicator. Temperature controller is faulty. service center.
Key operation is impossible. Key lock function is enabled. Please unlock according to P35
* In case of emergency stop w ith breaker.
Situation Cause Countermeasure
"F - x" alarm symbol on the Stop the operation and contact the company
Refer to P.9 "3-5 Safety and alarm functions" and
dialog display is displayed on w here you purchased the product or the nearby
check the cause of the alarm.
the screen and control stops. service center.
Caution
Carry out the earth leakage breaker operation test.
Test button
If the earth leakage breaker is used in the faulty state, electric shock may occur in case of electric leakage.
Carry out the operation test at least once a month.
Warning Caution
Never attempt to disassembly the product. Do not attempt cleaning or servicing while the product is hot.
Cleaning or servicing the product while it is still hot may cause burn.
t contains parts with high voltage applied or may become hot, and disassembly may cause an electrical shock or an injury.
Caution
Use a correct method and items for cleaning or caring the product.
terior or the inside directly, do not put any foreign materials and never use the cleanser, thinner, oil, kerosene, acid, and equivalent. Otherwise, the user may suffer electric shock o
Caution
Take care to remove dust from the outlet.
If the device is used with the plug inserted in the outlet for a long period of time, dust may accumulate in a gap between the socket and powe
(1) Turn the power switch (ELB) OFF and remove the power
plug off the outlet before maintenance work.
(2) Use a moistened and well wriggled soft cloth for cleaning.
Use mild detergent for stubborn dirt and completely wipe
remaining detergent after cleaning.
7.3 Consumables
The door packing (material: heat-resistant silicon) is a consumable.
If the required vacuum cannot be achieved because of swelling or
cracking of packing due to solvent, replace the packing.
8 Disposal of Products
Disposal of product or part must be done according to the specified disposal method.
VOS-210C Approx. 40kg 355 (W) x 406 (D) x 580 (H) (mm)
Request the disposal operator for
Main body
disposal.
VOS-310C Approx. 60kg 505 (W) x 545 (D) x 760 (H) (mm)
•*We ask you to discard packing materials after classifying them by material types.
9 After-sale Services
1. In case the product does not function satisfactorily, check
first by referring to the page on troubleshooting to see if 3. Repair during the guarantee period will be made
this is actually a trouble. according to the guarantee stipulations.
Warranty Provisions
1 The warranty period of your product is 12 months from the date of purchase.
2 We will repair or replace your product free of charge for troubles occurred in your product during proper usage in the
warranty period.
3 This warranty is limited to the product itself and shall not be construed to cover all and any consequential losses
(operating losses, various expenses, etc.) from malfunctions or troubles of the product.
4 The provisions of this warranty are valid only in Japan.
When you are going to indirectly export the product you purchased to a foreign country, the provisions shall be exempted
from application provided that a certification be issued that the product is not subject to the export control regulations
and, in such case, all liabilities in relation to the product shall be borne by the exporting party .
5 Repair shall be paid by the user even during the warranty period for the following cases.
a) The user did not return the customer card or made user registration at our HP within one month from the date of
purchase.
b) This warranty card was not presented or user registration could not be confirmed at the time of request for repair.
c) When the dealer name is not sealed on the warranty card or the date of the purchase is not indicated on it.
d) Malfunctions or damages caused by handling that is against cautions in the manual or labels on the product, or
transportation from the installation site after purchase, dropping during use, or shocks.
e) Malfunctions or damages caused by mishandling, unauthorized modification or repair by the user.
f) Malfunctions or damages caused by a fire, an earthquake, wind and flood, salt damage, lightening, or other Acts of
God or external factor including the power supply.
g) Degrading of performance or malfunctions resulted from consumption of consumable parts or replacement of
consumable parts.
6 Warranty conditions may differ depending on specific products. Check the warranty conditions stipulated in the warranty
space in the operation manual.
7 Ask your dealer or the nearest sales office for repair for malfunctions after the warranty period.
(In principle, the retention period of repair parts is five years after the end of production. )
8 Product warranty for products sold overseas by our overseas sales department shall be separately specified.
10 List of Consumable and Replacement parts/ Optional parts
Target Target
Code No Name Quantity Code No Name Quantity model
model
100800 Shelf plate 1 VOS-210C 100880 Door packing 1 VOS-210C
100810 Shelf plate 1 VOS-310C 100890 Door packing 1 VOS-310C
Quantit
Code No Name
y
100940 Rubber handle 1