Oils - Performed at All Locations: Test Method Units of Measure Req. Sample Rush Availability Notes

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The document lists various oil, lubricant and diesel fuel tests that can be performed along with required samples and availability. It also discusses modifications made to ASTM standard methods and rush availability timeframes.

The document lists various chemical, physical and performance tests for oils, lubricants and diesel fuels including acid number, viscosity, flash point, metals analysis and more.

Rush availability includes same day, next day and expedited testing. It provides timeframes for sample receipt and completion for different rush options.

COMPLETE TEST LISTS

HORIZON® develops and validates modifications to ASTM standard methods. Reasons for modification include: minimization of required sample and supplies, use of modern automated equipment, and less
variation in sample preparation and testing. The modifications reduce costs and in most cases improve throughput, which results in lower sample pricing and faster turnaround time for our customers.

OILS – Performed at All Locations


REQ. RUSH AVAILABILITY1 NOTES
UNITS OF
TEST METHOD SAMPLE

BOG
HOU

EDM

GUA

POZ
SLC
IND
MEASURE
VOLUME
Acid Number mod. ASTM D664 mg KOH/g 5 mL
Appearance Internal Method description 10 mL
Base Number mod. ASTM D4739 mg KOH/g 3 mL
Elemental Metals Analysis mod. ASTM D5185 ppm 2 mL
FTIR - Full Spectrum Scan FTIR graph 20 mL
FTIR - Full Spectrum Scan w/
FTIR graph w/ consult 20 mL
interpretation
Fuel Dilution % ASTM D7593 % 5 mL Diesel Engine and Gasoline Engine Lube Oils Only.
Glycol mod. ASTM D2982 pos/neg 8 mL
Soot % %
Nitration ASTM E2412 abs/0.1mm 40 mL
Oxidation abs/cm
Not suitable for dark or black samples (e.g. Used Diesel
Particle Count (Calibration: ISO 11171) ISO 4406 counts/mL 80 mL Engine Oils).

Particle Quantifier (Ferrous Density) Manufacturer no units 4 mL


i-pH mod. ASTM D7946 pH 5 mL
Strong Acid Number mod. ASTM D664 mg KOH/g 5 mL
Viscosity 2 mL or High water samples not suitable for 100°C analysis.
mod. ASTM D445 cSt
- 40°C and/or 100°C 10 mL Req’d sample volume location dependent
Viscosity Index 4 mL or Not available for high water samples (see above). Req’d
ASTM D2270 no units
(Requires Vis @40°C & 100°C) 20 mL sample volume location dependent
Water by Crackle (estimate) Internal Method % 2 mL
mod. ASTM
Water by Karl Fischer - Coulometric D6304C
% or ppm 10 mL
1.1.Rush Availability Key
Key Rush Type Time Frame
Received by 2pm local time – completed by 5pm local time
Same-Day Service
Received after 2pm local time – completed by noon local time the next business day
Next Day Service Completed by 5pm local time the next business day
Expedited Exception Sample will be moved next in line for testing, but no time guarantee for results
Testing performed at a different laboratory location. Same as Expedited Service
Outsourced Test Rush Service Unavailable

C-0027 rev. 40 Page 1 of 6 © 2021 Horizon


COMPLETE TEST LISTS

OILS/LUBRICANTS – Additional Testing


RUSH AVAILABILITY1
UNITS OF SAMPLE
TEST METHOD NOTES

BOG
HOU

EDM

GUA

POZ
SLC
IND
MEASURE REQD
4 Ball Wear Test (Oil) ASTM D5183 no units 200 mL
4 Ball Wear Test (Grease) ASTM D2266 no units 200 g
Acid Digestion ASTM D5198 Sample Prep 1-5 g
Acidity (as acetic acid) ASTM D1613 % 60 mL
Air Release ASTM D3427 minutes 250 mL
Aniline Point ASTM D611 Celsius 100 mL
Base Number by Perchloric Acid ASTM D2896 mg KOH/g 5 mL Suitable for New Lubricant analysis
Carbon Residue (Conradson) ASTM D189/IP13 % 200 mL
Chlorine ASTM D5384 ppm 20 mL Not suitable for severely water-contaminated samples
Cold Crank Simulator ASTM D5293 mPa·s 120 mL Suitable for SAE Multi-Grade Lubricants only.
Not suitable for solid samples or petroleum products
Color ASTM D6045 no units 50 mL
containing dye or having extreme fluorescence
Cone Penetration Unworked ASTM D217 mm 800 g Applicable to greases that are sufficiently hard to hold their
Cone Penetration Worked ASTM D217 mm 800 g shape
mod. ASTM
Contamination Dispersancy IC, MD, DP 10 mL
D7899
Copper Corrosion ASTM D130 no units 70 mL
Density ASTM D7777 g/mL 20 mL
Dielectric Strength ASTM D877 kV 450 mL
Ferrography - Analytical ASTM D7690 picture 2 mL
Some filters may not be suitable for analysis. Please
Filter Debris Analysis Internal Method no units 1 Filter
consult if unsure.
Fire Point Not available for gasoline products and some solvents.
ASTM D92 Celsius 200 mL
Flash Point – Cleveland Open Cup Please consult if unsure.

Foaming Tendency ASTM D892 mL 800 mL


Gravimetric Solids Internal Method Ppm 10 mL
Micro-Patch Internal Method picture 20 mL
mod. ASTM
MPC (Membrane Patch Colorimetry) no units 120 mL Intended for in-service turbine oils without dyes.
D7843
Pentane Insolubles (Coagulated) ASTM D893 % 35 mL
Pentane Insolubles (Uncoagulated) ASTM D893 % 35 mL
Photo Micrograph (Picture Only) Internal Method Picture 20 mL
Resistivity ASTM D1169 Ohms – cm 400 mL Applicable for new electrical insulating liquids
RPVOT ASTM D2272 minutes 200 mL Turbine oils or oils of similar composition
LSV (Ruler) ASTM D6971 % 4 mL Non-Zinc turbine Oil formulations only

C-0027 rev. 40 Page 2 of 6 © 2021 Horizon


COMPLETE TEST LISTS

OILS/LUBRICANTS – Additional Testing cont.


RUSH AVAILABILITY1
UNITS OF SAMPLE
TEST METHOD NOTES

BOG
HOU

EDM

GUA

POZ
SLC
IND
MEASURE REQD

Rust ASTM D665 pass/fail 1200 mL Intended for steam-turbine oils but may be used for other oils
Lubricants and Greases only, not intended for internal
Saponification Number ASTM D94 mg KOH/g 50 mL
combustion engine crankcase oils or used turbine oils
Not available for gasoline products and some solvents.
Seta Flash ASTM D3828 Celsius 50 mL
Please consult if unsure.
Specific Gravity ASTM D7777 no units 20 mL Result is a calculation of API Gravity
Lubricating Oils only, not intended for used engine oils or oils
Sulfated Ash ASTM D874 % 100 mL
containing lead
Sulfation ASTM E2412 Abs/0.1mm 10 mL
Sulfur in Oil Mod. ASTM D5185 % 2 mL
Toluene Insolubles (Coagulated) ASTM D893 % 35 mL
Toluene Insolubles (Uncoagulated) ASTM D893 % 35 mL
Viscosity (Brookfield) ASTM D2983 mPa·s 200 mL
Water Separability Characteristics ASTM D1401 mL 80 mL

1. Rush Availability Key:


Key Rush Type Time Frame
Received by 2pm local time – completed by 5pm local time
Same-Day Service
Received after 2pm local time – completed by noon local time the next business day
Next Day Service Completed by 5pm local time the next business day
Expedited Exception Sample will be moved next in line for testing, but no time guarantee for results
Testing performed at a different laboratory location. Same as Expedited Service
Outsourced Test Rush Service Unavailable

C-0027 rev. 40 Page 3 of 6 © 2021 Horizon


COMPLETE TEST LISTS

COOLANTS
RUSH AVAILABILITY1 NOTES
UNITS OF SAMPLE
TEST METHOD
MEASURE REQD

BOG
HOU

EDM

GUA

POZ
SLC
IND
Antifreeze % Internal Method %
- Ethylene or Propylene Glycol
2 mL Only applicable for Ethylene or Propylene
Boil Point Internal Method Fahrenheit
Glycol receiving Antifreeze Percent
Only applicable for Ethylene or Propylene
Freeze Point mod. ASTM D3321 Fahrenheit
Glycol receiving Antifreeze Percent
Bacteria, Fungi, Mold Manufacturer counts 60 mL
Only applicable for certain coolant
Carboxylic Acid Manufacturer pass/fail 10 mL
manufacturers
Density ASTM D7777 g/mL 20 mL

Elemental Metals Analysis by ICP mod. ASTM D6130 ppm 2 mL

HPLC
- Benzotriazole, Tolyltriazole, Mercaptobenzothiazole, Technical approval required for non-Engine
Internal Method ppm 20 mL
Benzoic Acid, Sebacic Acid, 2-Ethylhexanoic Acid, Octanoic Coolant samples.
Acid, P-Toluic Acid
Ion Chromatography Technical approval required for non-Engine
- Chloride, Sulfate, Nitrite, Nitrate, Phosphate, Glycolate, ASTM D5827 mg/L 5 mL
Coolant samples.
Acetate, Formate & Oxalate.
Nitrite Internal Method ppm 2 mL

pH Waters ASTM D1287 pH 20 mL

Reserve Alkalinity ASTM D1121 mL 20 mL


Result is a calculation of ICP and Nitrite
SCA Number Internal Method no units 8 mL
testing
Specific Gravity ASTM D7777 no units 20 mL Result is a calculation of API Gravity
Specific Conductance Meter Measurement µS/cm
60 mL
Total Dissolved Solids Meter Measurement mg/L
Result is a calculation of Elemental
Total Hardness Internal Method ppm 8 mL
Analysis
Visuals Subjective test performed under a Tru-
- color, oil, fuel, foam, magnetic precipitate, non-magnetic Internal Method description 25mL
Color light
precipitate, odor & foam.

1. Rush Availability Key:


Key Rush Type Time Frame
Received by 2pm local time – completed by 5pm local time
Same-Day Service
Received after 2pm local time – completed by noon local time the next business day
Next Day Service Completed by 5pm local time the next business day
Expedited Exception Sample will be moved next in line for testing, but no time guarantee for results
Testing performed at a different laboratory location. Same as Expedited Service
Outsourced Test Rush Service Unavailable
C-0027 rev. 40 Page 4 of 6 © 2021 Horizon
COMPLETE TEST LISTS

DIESEL FUEL
RUSH AVAILABILITY1
UNITS OF SAMPLE
TEST METHOD NOTES

BOG
HOU

EDM

GUA

POZ
SLC
IND
MEASURE REQD

Acid Number mod. ASTM D664 mg KOH/g 5 mL


Aerobic Bacteria Manufacturer counts 100 mL
API Gravity ASTM D7777 no units 20 mL
Aromatic Contents ASTM D6591 separate report 60 mL
Ash ASTM D482/IP4 % 50 mL
Bacteria, Fungi, Mold Manufacturer counts 60 mL
% Biodiesel (FAME) mod. EN14078 % 20 mL
BTU per gallon ASTM D4868 btu/gal 300 mL
BTU per pound ASTM D4868 btu/lb 300 mL
Carbon Residue (Conradson) ASTM D189/IP13 % 200 mL

Cetane Index ASTM D976 no units Result is a calculation of Distillation and API Gravity.
Predicted D86 results by 20mL
Micro-Distillation ASTM D7345
Celsius

Cloud Point ASTM D7689 Celsius 10 mL

Cold Filter Plug Point IP309/ASTM D6371 Celsius 100 mL


Copper Corrosion ASTM D130 no units 70 mL
Density ASTM D7777 g/mL 20 mL
Elemental Metals Analysis mod. ASTM D5185 ppm 2 mL
Not available for gasoline products and some solvents.
Flash Point - Closed Cup ASTM D3828 Celsius 20 mL
Please consult if unsure.
Lubricity ASTM D6079 µm 20 mL
Oxidation Stability ASTM D2274 % 700 mL
Particle Count (Calibration: ISO Not suitable for dark or black samples (e.g. Used Diesel
ISO 4406 counts/mL 80 mL
11171) Engine Oils).
Pour Point ASTM D7346 Celsius 10 mL
Specific Gravity ASTM D7777 no units 20 mL Result is a calculation of API Gravity
Sulfur ASTM D7220 ppm 50 mL
Thermal Stability mod. ASTM D6468 % 120 mL
Total Free Glycerin ASTM D6584 % 60 mL
Viscosity - 40°C mod. ASTM D445 cSt 2 mL Not available for 100°C analysis
Water by Karl Fischer -
mod. ASTM D6304C % or ppm 10 mL
Coulometric
Water & Sediment ASTM D2709 % 200 mL

C-0027 rev. 40 Page 5 of 6 © 2021 Horizon


COMPLETE TEST LISTS

GREASE
RUSH AVAILABILITY1
UNITS OF SAMPLE
TEST METHOD NOTES

BOG
HOU

EDM

GUA

POZ
SLC
IND
MEASURE REQD

Basic Grease Testing 2g


Color ASTM D7918 CIE color Requires Grease Sampler to do testing.
FTIR – Full Spectrum Scan FTIR Graph Individual tests are not available without doing all
tests.
Ferrous Debris Level ASTM D7918 ppm
Water by Crackle (estimate) Internal Method %
Advanced Grease Testing 2g Requires Grease Sampler to do testing.
Individual tests are not available without doing all
As Basic Grease Testing, plus: tests.
Die Extrusion
Consistency ASTM D7918
Index
Elemental Metals Analysis (ICP) mod. ASTM D5185 ppm
LSV (Ruler) ASTM D7918 %
Microbiological Activity Mod. ASTM D7463 pg ATP
Water by KF – Coulometric mod. ASTM D6304C ppm

Ferrous Wear Identification 2g Requires Grease Sampler to do testing.


Individual tests are not available without doing all
Ferrous Debris Level ASTM D7918 ppm tests.
Elemental Metals Analysis (ICP) mod. ASTM D5185 ppm NOT compatible with Basic and Advanced Grease
Ferrography - Analytical ASTM D7690 picture Testing above.

1. Rush Availability Key:


Key Rush Type Time Frame
Received by 2pm local time – completed by 5pm local time
Same-Day Service
Received after 2pm local time – completed by noon local time the next business day
Next Day Service Completed by 5pm local time the next business day
Expedited Exception Sample will be moved next in line for testing, but no time guarantee for results
Testing performed at a different laboratory location. Same as Expedited Service
Outsourced Test Rush Service Unavailable

C-0027 rev. 40 Page 6 of 6 © 2021 Horizon

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