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    Experiment No. 3 Preparations of Solutions: Precaution

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    Crizel Mae Enoviso
    1. The experiment involves preparing solutions of NaOH and HCl from solids and a more concentrated solution. Proper safety precautions like wearing eye protection and washing hands must be followed when handling the corrosive and toxic chemicals. 2. The procedure describes preparing 250 mL of 1 M NaOH solution from NaOH pellets and 100 mL of 3 M HCl solution from concentrated HCl. Volumetric flasks and equipment are used to accurately measure and dilute the chemicals to the desired concentrations. 3. Key steps include calculating amounts, adding the solid or concentrated solution to water, diluting to the mark, mixing, and transferring

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    Experiment No. 3 Preparations of Solutions: Precaution

    Uploaded by

    Crizel Mae Enoviso
    37 views3 pages
    1. The experiment involves preparing solutions of NaOH and HCl from solids and a more concentrated solution. Proper safety precautions like wearing eye protection and washing hands must be followed when handling the corrosive and toxic chemicals. 2. The procedure describes preparing 250 mL of 1 M NaOH solution from NaOH pellets and 100 mL of 3 M HCl solution from concentrated HCl. Volumetric flasks and equipment are used to accurately measure and dilute the chemicals to the desired concentrations. 3. Key steps include calculating amounts, adding the solid or concentrated solution to water, diluting to the mark, mixing, and transferring

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    Analytical Chemistry

    Original Title

    Analytical-Chemistry-Experiment-on-Solution-Preparation

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    1. The experiment involves preparing solutions of NaOH and HCl from solids and a more concentrated solution. Proper safety precautions like wearing eye protection and washing hands must be followed when handling the corrosive and toxic chemicals. 2. The procedure describes preparing 250 mL of 1 M NaOH solution from NaOH pellets and 100 mL of 3 M HCl solution from concentrated HCl. Volumetric flasks and equipment are used to accurately measure and dilute the chemicals to the desired concentrations. 3. Key steps include calculating amounts, adding the solid or concentrated solution to water, diluting to the mark, mixing, and transferring

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    37 views3 pages

    Experiment No. 3 Preparations of Solutions: Precaution

    Uploaded by

    Crizel Mae Enoviso
    1. The experiment involves preparing solutions of NaOH and HCl from solids and a more concentrated solution. Proper safety precautions like wearing eye protection and washing hands must be followed when handling the corrosive and toxic chemicals. 2. The procedure describes preparing 250 mL of 1 M NaOH solution from NaOH pellets and 100 mL of 3 M HCl solution from concentrated HCl. Volumetric flasks and equipment are used to accurately measure and dilute the chemicals to the desired concentrations. 3. Key steps include calculating amounts, adding the solid or concentrated solution to water, diluting to the mark, mixing, and transferring

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 3

    Experiment No.

    3
    PREPARATIONS OF SOLUTIONS

    In this experiment, solutions of NaOH and HCl will be prepared to illustrate the
    2 ways of solution preparation: from solids and from a more concentrated solution.

    Precaution:

    Students must wear safety eye protection while performing this experiment.
    Wash hands before touching the eyes and after completing the experiment.

    NaOH pellets are corrosive! Handle this solution very carefully, and avoid contact
    with your skin or clothes. If you do spill some, wash it off at once with copious amounts
    of water.

    Concentrated HCl is corrosive and has toxic vapors! Handle this acid very
    carefully, and avoid contact with your skin or clothes. If you do spill some, wash it off
    at once with water and soap.

    Materials:

    250-mL volumetric flask concentrated HCl 250-mL beaker


    NaOH pellets 100-mL volumetric flask pipette
    Graduated cylinder spatula droppers
    Watch glass Analytical balance

    Procedure:

    I. Preparation of Solutions from Solids 250 mL of 1.0 M NaOH solution

    1. Calculate the mass of NaOH pellets needed to prepare a solution with a


    concentration of 1.0 M. Show your calculations.
    2. Using a clean and dry 250-mL beaker, weigh the calculated mass of NaOH pellets
    using top-loading balance. (An analytical balance is not suitable in weighing
    NaOH pellets since it is hygroscopic).
    3. Add enough distilled water to dissolve the pellets and stir. The dissolution is
    exothermic, so cool the solution if necessary.
    4. When completely dissolved, transfer quantitatively into a 250-mL volumetric
    flask using distilled water to wash the beaker. Add enough distilled water to
    make a volume of about 200 mL. Cover and cool the flask and solution to room
    temperature.
    5. Bulk the solution to the mark with distilled water and cover. Mix the solution
    thoroughly by repeated shaking and inversion of flask.
    6. The prepared solution is a 1.0 M NaOH. Transfer the solution into a dry and
    clean plastic bottle and label properly.

    (NEVER store any solution in a volumetric flask as it is not a storage container.


    Never store NaOH or any basic solutions in glass containers as they slowly etch the
    glass.)

    100 mL of 3.0 M hydrochloric acid solution

    1. Calculate the volume of concentrated HCl needed to prepare a solution with a


    concentration of 3.0 M. Show your calculations.
    2. Pipette out the calculated volume of concentrated HCl solution into a 100-mL
    volumetric flask containing about 25-mL of distilled water. (Always add
    concentrated acid to water; never water to acid when diluting acid solutions.)
    3. Add enough distilled water to make a volume of about 90-mL. Swirl to mix, cover
    the flask and cool the solution to room temperature, if necessary.
    4. Bulk the solution to the mark with distilled water and cover. Mix the solution
    thoroughly by repeated shaking and inversion of the flask.
    5. The prepared solution is a 3.0 M HCl. Transfer the solution into a dry and clean
    reagent bottle and label properly.

    Notes:
    a. Never store any solution in a volumetric flask as it is not a storage container. Do
    not discard stock 3.0 M HCl, this will be used in FUTURE experiments.
    b. Never store NaOH or any basic solutions in glass containers. Do not discard
    stock 1.0 M NaOH, this will be used in FUTURE experiments.
    Report Sheet: Experiment 3

    Preparation of Solutions

    Experimental Purpose:

    Data Sheet:

    Calculations:

    QUESTIONS
    1. Define the terms “stock solution”, “aliquot”, and “dilution” and state the role
    played by each during the preparation of a solution.
    2. What is parallax error? What steps can be taken to minimize this type of error
    when using a volumetric device?
    3. Describe how you would prepare the following solutions:
    a. 100.00 mL of 1.00 M NaCl in water, beginning with solid sodium chloride.
    b. 250 mL of 1.0 M Na2SO4 in water, beginning with a 2.5 M sodium sulfate
    solution.
    c. 250 mL of 0.500 M HCl in water, beginning with 12 M HCl.
    4. It is something necessary during an analysis to convert from one unit of
    concentration to another. Show how you would convert between each of the
    following pairs of concentration units. State what additional information would
    be needed for each of these conversions. Confirm your approach by using
    dimensional analysis.
    a. Converting a concentration in g/L to molarity
    b. Converting a concentration in molarity to molality
    5. A doctor orders 100 mL of 2.0% (w/v) ibuprofen. If you have 8.0% (w/v) ibuprofen
    on hand, how many milliliters do you need?

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