CEB 3032 Chemical Engineering Lab III

May 2021

CEB 3032
CHEMICAL ENGINEERING LABORATORY III
MAY 2021
LABORATORY COURSE OUTLINE

1. GENERAL INFORMATION & COURSE ADMINISTRATION

CREDIT UNIT : 2 CREDIT HOURS (Core Engineering subject)

COORDINATOR
Room 05-03-22, Block 5
1. Serene Lock Sow Mun
[email protected]

Room 5-03-08, Block 5

2. Jalal Foroozesh
[email protected]

LABORATORY TECHNOLOGISTS

1. Azhar Bin Zainal Abidin [email protected]

2. Suleiman Hakimi Zainal Abidin [email protected] 03-01-09
3. Azriha Anuar [email protected] 04-02-17
4. M Shaharuddin Bin A Rahman [email protected] 05-00-10

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CEB 3032 Chemical Engineering Lab III
May 2021

LAB INSTRUCTORS (GA STUDENTS)

No Name Email
1 Obaid Ur Rehman [email protected]
2 Brandon Li Jian Ngiam [email protected]
3 Husnain Ali [email protected]
4 Masooma Nazar [email protected]
5 Aqeel Ahmad [email protected]
6 Naveen Sunder [email protected]
7 Rasel Ahmed [email protected]
8 Yaleeni Kanna Dasan [email protected]
9 Sie Ding Hao [email protected]
10 Wegik Dwi Prasetyo [email protected]
11 Muhammad Asyraf [email protected]
12 Vienoth Segar [email protected]
13 Usman Bello [email protected]
14 Khadija Asif [email protected]
15 Eileen Ng Li Shien [email protected]
16 Tahir Sultan [email protected]

Duties and responsibilities of the lab instructors (GA students):

• Conduct viva on experiment.
• Take note on the late comer(s) and deduct his/her marks by 50%.
• Evaluate the reports and give feedback on the content and what needs to be improved. E.g., report of
experiment in week 7 will be submitted by the students prior to the experiment in week 8.

2. COURSE LEARNING OUTCOME (CLO)

The objective of this laboratory is to extend the knowledge of chemical process dynamics, instrumentation and
control into practical work. The laboratory content will offer you the application of the fundamental concepts and
theory of the subjects as applied to the chemical engineering unit operations and everyday life.

COURSE SYNOPSIS:
1. This practical course requires several groups of ~5 students to perform experiments related to process
instrumentation, dynamics and control.

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CEB 3032 Chemical Engineering Lab III
May 2021
COURSE LEARNING OUTCOME:
At the end of this course, you should be able to:
1. Apply appropriate sensors, instrumentation and/or computing tools to measure physical quantities.
2. Device suitable procedures and implement them in order to characterize dynamic and control systems.
3. Analyze and interpret experimental data for writing and presenting technical reports.

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CEB 3032 Chemical Engineering Lab III May 2021

2. LABORATORY MODULE CONTENT, GA LIST & LAB TECHNOLOGIST

Monday Tuesday Friday Friday

Experiment Number & Title Location (8.00 – 12.00) (10.00 – 14.00) (8.00 – 12.00) (15.00 – 19.00)
EXP 1 - Temperature Control Simulation Obaid Ur Rehman Obaid Ur Rehman Husnain Ali Husnain Ali
EXP 2 - Cascade Control Simulation Brandon Li Jian Ngiam Brandon Li Jian Ngiam Brandon Li Jian Ngiam Brandon Li Jian Ngiam
EXP 3 - Heat Exchanger Simulation Husnain Ali Husnain Ali Husnain Ali Husnain Ali
EXP 4 - Control Valve Characteristic Virtual GA dependent on group GA dependent on group GA dependent on group GA dependent on group
EXP 5 - Flow Meter Measurement Virtual GA dependent on group GA dependent on group GA dependent on group GA dependent on group
EXP 6 - Level Transmitter Calibration Virtual GA dependent on group GA dependent on group GA dependent on group GA dependent on group
EXP 7 - pH, DO and Conductivity Measurement Virtual GA dependent on group GA dependent on group GA dependent on group GA dependent on group

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CEB 3032 Chemical Engineering Lab III May 2021

Experiment Number & Title Location Monday Tuesday Friday Friday

(8.00 – 12.00) (10.00 – 14.00) (8.00 – 12.00) (15.00 – 19.00)
a Virtual Vienoth Segar Vienoth Segar Vienoth Segar Vienoth Segar
b Virtual Aqeel Ahmad Aqeel Ahmad Aqeel Ahmad Aqeel Ahmad
c Virtual Naveen Sunder Naveen Sunder Naveen Sunder Naveen Sunder
d Virtual Usman Bello Usman Bello Rasel Ahmed Rasel Ahmed
e Virtual Yaleeni Kanna Dasan Yaleeni Kanna Dasan Yaleeni Kanna Dasan Yaleeni Kanna Dasan
f Virtual Sie Ding Hao Sie Ding Hao Sie Ding Hao Sie Ding Hao
g Virtual Masooma Nazar Masooma Nazar Masooma Nazar Masooma Nazar
h Virtual Wegik Dwi Prasetyo Wegik Dwi Prasetyo Wegik Dwi Prasetyo Wegik Dwi Prasetyo
i Virtual Husnain Ali Husnain Ali Husnain Ali Husnain Ali

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CEB 3032 Chemical Engineering Lab III May 2021

3. LABORATORY DELIVERY & SCHEDULING

Wk 1 Wk 2 Wk 3 Wk 4 Wk 5 Wk 6 Wk 7 Wk 8 Wk 9 Wk 10 Wk 11 Wk 12

EXP. SEQ. Monday 1ST 2ND 3RD 4TH 5TH 6TH 7TH
(8.00-12.00)
DATE OF EXP. 10 May 17 May 24 May 31 May 11 June 14 June 21 June 28 June 5 July 16 July 22 July

1 2 3 4a 5c 6e 7g

LAB III TEST, 22nd July 2021, 15.00

OPEN ENDED ASSIGNMENT DUE
G1
LAB SEMINAR, 10th May 2021,

OPEN ENDED PROJECT DUE

1 2 3 4b 5d 6f 7h
G2
GROUP 1-7

17.00 – 18.00
1 2 3 4c 5e 6g 7i
(MS Teams)

G3

NO LAB

-17.00
LAB III
1 2 3 4d 5f 6h 7a
G4
1 2 3 4e 5g 6i 7b
G5
1 2 3 4f 5h 6a 7c
G6
1 2 3 4g 5i 6b 7d
G7

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CEB 3032 Chemical Engineering Lab III May 2021

ACAD. WK. Wk 1 Wk 2 Wk 3 Wk 4 Wk 5 Wk 6 Wk 7 Wk 8 Wk 9 Wk 10 Wk 11 Wk 12

EXP. SEQ. Tuesday 1ST 2ND 3RD 4TH 5TH 6TH 7TH
(10.00-14.00)
DATE OF EXP. 10 May 18 May 25 May 1 June 11 June 15 June 22 June 29 June 6 July 16 July 22 July

1 2 3 4a 5c 6e 7g

LAB III TEST, 22nd July 2021, 15.00

OPEN ENDED ASSIGNMENT DUE
G8

LAB SEMINAR, 10th May 2021,

OPEN ENDED PROJECT DUE

1 2 3 4b 5d 6f 7h
G9
GROUP 8-14

1 2 3 4c 5e 6g 7i

17.00 – 18.00
(MS Teams)
G10

NO LAB

-17.00
LAB III
1 2 3 4d 5f 6h 7a
G11
1 2 3 4e 5g 6i 7b
G12
1 2 3 4f 5h 6a 7c
G13
1 2 3 4g 5i 6b 7d
G14

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CEB 3032 Chemical Engineering Lab III May 2021

ACAD. WK. Wk 1 Wk 2 Wk 3 Wk 4 Wk 5 Wk 6 Wk 7 Wk 8 Wk 9 Wk 10 Wk 11 Wk 12

EXP. SEQ. Friday 1ST 2ND 3RD 4TH 5TH 6TH 7TH
(8.00-12.00)
DATE OF EXP. 10 May 21 May 28 May 4 June 11 June 18 June 25 June 2 July 9 July 16 July 22 July

1 2 3 4a 5h 6f 7d
G15

LAB III TEST, 22nd July 2021, 15.00 -17.00

1 2 3 4b 5i 6g 7e

OPEN ENDED ASSIGNMENT DUE

G16

LAB SEMINAR, 10th May 2021,

OPEN ENDED PROJECT DUE

1 2 3 4c 5a 6h 7f
GROUP 15-23

G17
1 2 3 4d 5b 6i 7g

17.00 – 18.00
(MS Teams)
G18

NO LAB

LAB III
1 2 3 4e 5c 6a 7h
G19
1 2 3 4f 5d 6b 7i
G20
1 2 3 4g 5e 6c 7a
G21
1 2 3 4h 5f 6d 7b
G22
1 2 3 4i 5g 6e 7c
G23

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CEB 3032 Chemical Engineering Lab III May 2021

ACAD. WK. Wk 1 Wk 2 Wk 3 Wk 4 Wk 5 Wk 6 Wk 7 Wk 8 Wk 9 Wk 10 Wk 11 Wk 12

EXP. SEQ. Friday 1ST 2ND 3RD 4TH 5TH 6TH 7TH
(15.00-19.00)
DATE OF EXP. 10 May 21 May 28 May 4 June 11 June 18 June 25 June 2 July 9 July 16 July 22 July

1 2 3 4a 5h 6f 7d
G24

LAB III TEST, 22nd July 2021, 15.00 -17.00

1 2 3 4b 5i 6g 7e

OPEN ENDED ASSIGNMENT DUE

G25

LAB SEMINAR, 10th May 2021,

OPEN ENDED PROJECT DUE

1 2 3 4c 5a 6h 7f
GROUP 24-32

G26
1 2 3 4d 5b 6i 7g

17.00 – 18.00
(MS Teams)
G27

NO LAB

LAB III
1 2 3 4e 5c 6a 7h
G28
1 2 3 4f 5d 6b 7i
G29
1 2 3 4g 5e 6c 7a
G30
1 2 3 4h 5f 6d 7b
G31
1 2 3 4i 5g 6e 7c
G32

NOTE:
● Submit the report of the previous experiment to the corresponding lab instructor through email before your next session begins.

● Viva is conducted to evaluate student’s preparation and concepts underlying the theory of the laboratory session.

● DO NOT come late!!! 50% marks deduction on the VIVA will be applied to those individuals who come late!

● DO NOT come unprepared! GA students will conduct a VIVA, starting from the 1st virtual experiment (week 7) to check if each student understands what to do before preparing the report.

● Bold red numbers in light yellow box = group numbers

● Numbers in white box = experiment numbers with short report

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CEB 3032 Chemical Engineering Lab III May 2021

● Long report should be submitted for experiments in yellow (week 10)

● Some tutorials for process simulation are here: https://www.youtube.com/watch?v=Wf7wFTyKzUg&list=PLFK7DKgtefxsQ0uvwa5LU4o-SccbJzxI9&index=5

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CEB 3032 Chemical Engineering Lab III May 2021

4. GROUPING

Please refer to group list distributed in Ulearn.

5. LABORATORY ASSESSMENT

Assessment Task Mark Assessment Type

Lab reports (6 Short + 1 Long) 35% Group

Open ended assignment 5% Group

Open ended project 20% Group & Individual

Viva 10% Individual

Test 30% Individual

TOTAL 100%

6. REPORT SUBMISSION

a) List below illustrate the types of report and their submission criteria:

Physical laboratory session:

ONLY softcopy submission to respective GA. Late report is considered as No Report.

Virtual/ simulation laboratory session:

Only softcopy submission to respective GA. Late report is considered as No Report.

Lab report 1: Muhammad Asyraf ([email protected])

Lab report 2: Eileen Ng Li Shien ([email protected])
Lab report 3: Khadija Asif ([email protected])
Open Ended Assignment: Tahir Sultan ([email protected])
Lab report 4: Muhammad Asyraf ([email protected])
Lab report 5: Eileen Ng Li Shien ([email protected])
Lab report 6: Khadija Asif ([email protected])
Lab report 7: Tahir Sultan ([email protected])

b) The length and contents of the report: please refer to template uploaded in Ulearn.
c) Submit report & simulation files (for open ended assignment) on time. Late submission will not be marked.
d) Softcopy shall be submitted to emails of GA:
● Please ensure the report file size does not exceed 5 MB.
● The filing name format for reports and videos: YYYYMMDD-GXX-EXPXX.
Example: Group 1, Exp 1, Date 25/06/2021, the file name should be typed as:
20210625-G01-EXP01
• Incorrect naming is seen as No Report

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CEB 3032 Chemical Engineering Lab III May 2021
3. REFERENCES

1. Marlin, T., “Process Control, Designing Processes and Control Systems for Dynamic Performance, 2nd
Edition”. Link: http://pc-textbook.mcmaster.ca/
2. https://controlguru.com/
3. http://apmonitor.com/pdc/index.php/Main/ArduinoTemperatureControl
4. http://homepages.ed.ac.uk/jwp/control06/controlcourse/restricted/course/index.html

4. PROGRAM OUTCOMES

Investigate complex chemical engineering problems using research-based knowledge and

PO4 research methods including design of experiments, analysis and interpretation of data, and
synthesis of information to provide valid conclusions
Select and apply modern engineering and IT tools to evaluate complex chemical engineering
PO5 activities
Communicate clearly on complex chemical engineering activities with the engineering
PO9 community and society

Programe Outcomes (POs)

Course Learning Outcome
PO4 PO5 PO9

Apply appropriate sensors, instrumentation

CLO1 and/or computing tools to measure physical x
quantities.

Device suitable procedures and implement

CLO2 them in order to characterize dynamic and x
control systems.

Analyze and interpret experimental data for

CLO3 x
writing and presenting technical reports.

5. DO’s and DON’Ts

a) You must attend all lab sessions. In case of absentees, these rules apply:

Absent because of: What should you submit to the Coordinator?

● Illness / hospitalization. A valid Medical Certificate issued by registered Medical Doctor.

● UTP commitments Release letter from the Chairman, lecturer or authorized personnel.

● Family matters Letter from parents or responsible next-of-kin.

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CEB 3032 Chemical Engineering Lab III May 2021

You are required to inform the Lab Coordinator/Lab Technologist/ Lab

● Other emergencies/
Instructor. This needs to be supported by an authorized document that
unavoidable matters
has to be submitted later on.

b) Lab session is a GROUP EFFORT.

● If you are absent during the lab session, you cannot replace it. However, you have to be involved in
preparing the lab report with the group members to validate the mark on your part.
● Peer review will be considered for all reports during compilation of coursework marks.
● You must also attend the viva voce session accordingly (subjected to the arrangement with the Lab
Instructor).
● Without valid supporting document due to absenteeism, you will not be getting marks for any of the
lab assessments.
c) In case of lab falls on the public holiday, lab session will be replaced at other suitable time subjected to
availability.
d) In case of equipment breakdown, your experiment will be replaced with other available equipment.
However, cases below apply:
● If equipment breakdown happens after more than half of the experiment requirement, you must
proceed with the available results.
● If equipment breakdown happens less than half of the experiment requirement or before any results
obtained, the experiment must be replaced with other available experiment/equipment.

6. LAB SAFETY

a) Properly attired.
● You MUST wear your lab coat whenever you are in the lab.
● Other personal protective equipment (PPE, such as goggles, safety helmet, ear plugs, ear muff, etc)
will be provided accordingly.
● These clothing are not allowed in the laboratory:
a. National costumes (baju kurung, cheongsam, saree, traditional outfit, etc),
b. Jubah, skirts (short or long), sarongs, shorts.
c. Sandals, slippers and any uncovered shoes.
● For those who are wearing tudung or hijab, and with long hair, you are required to keep them neat.
● Comply with strict SOP and social distancing at all times.

b) The Lab Instructors and Lab Technologists have the authority to ask you to leave the lab if you do not adhere
to the safety regulations.
c) You ARE NOT ALLOWED TO PROCEED with your laboratory work if you fail to do that.
d) Abide to the safety signs in the lab.

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