RADLEYS Reactor-Ready-Lab-Reactors
RADLEYS Reactor-Ready-Lab-Reactors
RADLEYS Reactor-Ready-Lab-Reactors
Reactor-Ready™
Lab Reactors
Patented Design
Innovative, patented,
low cost, reaction work
stations for glass
vessels from
100 ml to 5 litres
-70˚C 230˚C
www.radleys.com
Reactor-Ready Du
o
Reactor-Ready Lab Reactor -70˚C 230˚C
250 ml
Single Jacket
Hose couplings
• quick release
• connect in seconds
• chemically resistant PEEK
A choice of
popular stirrer
paddles
Individual manifolds
• easy connection
• easy drain down
• reduces stress on
vessel sidearms
2 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Change to Reactor-Ready
It improves your chemistry by saving space, time and money
Reactor-Ready Duo
accepts two vessels and
allows reactions in
parallel or series
Simple stirrer alignment
• slide and glide
• set and lock
The beauty of Reactor-Ready is that this one reactor work station can replace many,
saving you money and fumehood space.
Features include
• Rapid vessel exchange with quick-release vessel clamp and hose couplings.
• Range of single and vacuum jacketed vessels from 100 ml to 5 litres.
• Range of process vessels to mimic larger scale plant or manufacturing reactors.
• Accepts all leading brands of overhead stirrer and allows easy, tool-free adjustment.
• Triple support stand features heavy duty stainless steel support rods for strength and stability.
• Self aligning stirrer coupling engages without the need for tools.
• Temperature range: -70 ºC to +230 ºC (jacket temperature)
• Innovative hose manifolds allow easy thermofluid drain down.
• Wide range of accessory glassware including condensers, dropping funnels etc.
• Optional software allows you to log and control stirrers, circulators, balances, pumps, temperature
sensors and other devices.
4 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Choice of PTFE stirring shafts
• Reactor-Ready is offered with a choice of PTFE stirring shafts: anchor, retreat curve
and turbine/propeller styles.
• PTFE anchor stirring shaft is included with all standard reaction vessel kits
• PTFE turbine stirring shaft is included with all process reaction vessel kits.
Commenting on their existing methods the Lead Scientist said, “We use round “The first time I changed vessels, it took about 5 minutes but now I can change in
bottom flasks, but temperature control via mantles or oil baths is poor. Alternatively, less than 2 minutes. That includes removing and attaching the heating fluid hoses.
when we use traditional jacketed reactor vessels, we need a different set up for Occasionally I lose a drop or two of heat transfer fluid but most times I lose none.
every scale change. Even changing a reactor of the same size takes ages.” The thing I like about the system is the control and speed. I get better control of
my reactions and I can vary my work or scale immediately”.
Reactor-Ready…
allows the stirrer motor
Quick-release PEEK coupling
4. If you need a thermoregulator, allows rapid exchange of vessels
hoses, hose without the use of tools. Operates
adapters, over the temperature range
thermofluid -70 ˚C to +230 ˚C
or accessory (jacket temperature).
glassware,
then select
from the
accessory list.
6 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Support system accepts Reactor-Ready core system
includes
all leading brands of overhead
stirrer and allows easy,
tool-free adjustment.
• Stand with base, support rods, bosses
and all clamps
• Glass reaction vessel lid
-70˚C 230˚C • Vessel FEP O-ring seal and PTFE collar
• HDPE drip tray
• Vessel-to-manifold insulated hoses with
quick-release connections
Wide range of accessory glassware • Lower inlet manifold + drain
including condensers, dropping funnels, • Upper outlet manifold
adapters, powder addition funnels,
+ vent
gas purge adapters and liquid Patented drop-in stirrer
inlet adapters etc. coupling engages easily • PTFE stirrer guide
without the need • Stainless steel drop-in
for tools. stirrer guide coupling
• Two stainless steel
vessel support
collars
• Locking rod for
PTFE stirrer guide provides excellent support rod
stirring and sealing performance.
bosses
An extended stirrer shaft support minimises
wobble even at high speeds.
Chemically resistant
PTFE stirrers. Accepts single jacketed and vacuum Reaction vessel kits make
jacketed vessels of 100 ml, 250 ml, ordering vessels simple and
more cost effective
500 ml, 1 litre, 2 litre, 3 litre and 5 litre.
Reactor-Ready Video
catch any spills and
can accommodate
the contents of Visit www.radleys.com
a 5 litre vessel
to watch the demo
and jacket.
Vessels
• 100 ml to 5 litres
• combine different volumes Patented stirrer coupling
• vacuum jacketed option • drop in
• process and standard • no tools
geometry • no fuss
Hose couplings
• quick release
• connect in seconds
Thermofluid manifolds • chemically resistant PEEK
• choice of two manifold kits
• single circulator manifolds
• double circulator manifolds
Strong framework
• heavy duty base
• solid s/steel support rods
• large drip tray
8 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Why Reactor-Ready Duo?
All the benefits of Reactor-Ready with two vessels in parallel or series
Features include
• Rapid exchange of both vessels independently, with quick-release vessel clamp and hose couplings.
• Choice of manifold kits allow two vessels to run from a single thermoregulator or two separate thermoregulators.
• System accepts two overhead stirrers which can be operated and moved independently.
Applications
• Parallel synthesis or reaction optimisation: use the same or different size vessels and vary stirring
speed, stirrer shape and temperature between vessels as appropriate.
• Two stage reaction: transfer reactant from one vessel to the other using vacuum or a pump.
• Single reaction vessel: using the second vessel as either a receiving or feed vessel
(where reagents can be pre-heated or pre-cooled prior to addition).
• Use optional AVA Software to control fluid transfer between vessels.
Similar vessels with Different vessels with Single vessel with
double circulator manifold kit double circulator manifold kit double circulator manifold kit
Features include
Duo core.
10 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Hei-Torque overhead stirrers
The powerful Hei-Torque range can accomplish the most
demanding mixing tasks whilst providing the highest safety
Stirrer models include
• Powerful stirring from 10 to 2000 rpm (Max. recommended speed with Reactor-Ready is 500 rpm).
• Available with basic (Value) or advanced (Precision) features, and a choice of up to 40, 200
or 400 Ncm torque.
• Intuitive control panel for easy operation, safe start and stop to avoid accidental start-up.
• New features for Precision range: set speed limit, adjustable acceleration, set a torque limit.
• New unique Quick-chuck for immediate and convenient ‘one-hand’ impellor changes, without tools.
Hei-Torque Hei-Torque Hei-Torque Hei-Torque Hei-Torque
Core Value 200 Value 400 Precision 200 Precision 400
Power rating, motor input/output (W) 105/75 120/80 150/90 120/80 150/90
Number of gears 1 1 2 1 2
Speed range (rpm) 20 to 2000 10 to 2000 10 to 400 and 200 to 2000 10 to 2000 10 to 400 and 200 to 2000
Speed indicator digital monochrome 2” digital monochrome 2.4” digital monochrome 2.4” digital colour 3.2” digital colour 3.2”
Speed control electronic electronic electronic electronic electronic
Torque, maximum (Ncm) 40 200 400 200 400
Torque indicator (Ncm) symbol symbol symbol precise value precise value
Overheat protection automatic cut-out automatic cut-out automatic cut-out automatic cut-out automatic cut-out
Viscosity up to (mPa s) 10,000 100,000 250,000 100,000 250,000
Stirring cap. H2O max. (L) 25 50 100 50 100
Shaft diameter, max. (mm) 10.5 10.5 10.5 10.5 10.5
Dimensions (W x H x D) (mm) 70 x 281.5 x 195 86 x 350 x 247 93 x 350 x 247 86 x 350 x 247 93 x 350 x 247
Weight (kg) 2.3 5.1 5.3 5.1 5.3
Set speed limit, Torque limit, Adjustable acceleration - - - Yes Yes
Analogue/digital interface - - - USB and RS232 USB and RS232
Thermoregulators/circulators
For Reactor-Ready and Reactor-Ready Duo the maximum speed is 500 rpm for continuous use for 800 rpm for short periods.
Heating Cooling
Temperature
Description power power Application Examples
range ˚C Huber Unistat 405
(kW) at 0 ˚C (kW)
Huber 250 ml Cool to -10 ºC in <1 hr, then heat to 130 ºC in <30 mins
-45 ˚C to 200 ˚C 2.0 0.38
Ministat 230 1 Litre Control at 0 ºC, then heat to 100 ºC in 20 mins
Huber 500 ml Cool to -20 ºC in approx 30 mins, then heat to 150 ºC in <30 mins
-40 ˚C to 200 ˚C 1.5 0.45
Petite Fleur 1 Litre Heat to 150 ºC, then cool to 0 ºC at > 2.5 K/min
Huber 1 Litre Cool to -30 ºC in <1 hr, then heat to 180 ºC in <1 hr
-45 ˚C to 250 ˚C 3.0 0.7
Unistat Tango 2 Litre Heat to 180 ºC, then cool to 20 ºC in approx 1 hr
Huber 2 Litre Cool to -20 ºC in <30 mins, then heat to 100 ºC in <30 mins
-45 ˚C to 250 ˚C 3.0 1.0
Unistat 405 5 Litre Control at 20 ºC, then cool to -20 ºC in approx 70 mins
The above applications are intended as a guide to the relative performance of each Huber thermoregulator with a range of vessel sizes and are not a prediction of actual Huber Petite Fleur - Baby Tango
performance. To achieve optimum performance the use of vacuum jacketed vessels is recommended for below ambient temperature applications. For comprehensive advice
on thermoregulator selection please contact your local Radleys distributor.
Features include
• Precision engineered borosilicate glass vessels can be used with Reactor-Ready and Reactor-Ready Duo.
• DN100 ground and polished flat flange combines with the FEP-encapsulated O-ring and our unique
self centering PTFE collar to offer a leak-tight seal between the vessel and lid.
• Convenient and cost-effective vessel kits include stirrer, temperature probe and adapter.
1000 ml single 1000 ml vacuum 2000 ml single 2000 ml vacuum 5000 ml single 5000 ml vacuum
jacketed vessel jacketed vessel jacketed vessel jacketed vessel jacketed vessel jacketed vessel
1000 ml single jacketed 1000 ml vacuum jacketed 2000 ml single jacketed 2000 ml vacuum jacketed 5000 ml single jacketed 5000 ml vacuum jacketed
process vessel process vessel process vessel process vessel process vessel process vessel
12 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Reaction vessel kits
Reaction vessel kits make ordering vessels and accessories simple and much more cost effective
Boss head
3 Pronged clamp
Condenser Condenser Condenser Dropping funnel PTFE hose Liquid additions Glass cone Reducing Right angle Enlarging
liebig, B29 double surface, B29 jacket coil, B29 equalising arm, B24 adapter, B19 adapter, B24 stopper, B29 adapter, B29 adapter, B29 adapter, B29
Other styles
and sizes of
glassware are
available, please
see full listing.
Reflux divider head Reflux divider head Valved liquid Gas purge Oil bubbler, Solid additions Swan neck
B29 + GL18 B29 + GL18 + temp- inlet adapter, B24 adapter, B24 B24 Funnel, B34 Adapter, B24
+ PTFE fitting probe port B14
14 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Huber Thermoregulators (Circulators) Glass DN100 Vessel Lid
HB2016.0005.01 Ministat 240 Pilot ONE Controller RR136000 5 Neck Glass Lid - 1 x B19, 2 x B24, 1 x B29, 1 x B34
HB1030.0001.01 Petite Fleur Pilot ONE Controller Includes Rodaviss sealing caps
HB1030.0001.01ET Petite Fleur with 4 Litre Expansion Tank
HB1000.0037.01 Unistat Tango Pilot ONE Controller PTFE DN100 Vessel Lids
RR136100 5 Neck PTFE Lid with 2 Blanked Ports. 1 x B19, 2 x B24, 1 x B29, 1 x B34
HB1002.0045.01 Unistat 405 Pilot ONE Controller Includes Rodaviss sealing caps
HB1001.0041.01 Unistat 705 Pilot ONE Controller (230V or 400V)
Thermoregulator Hoses, Adapters and Thermofluid RR136110 7 Neck PTFE Lid with 7 Threaded Ports. 2 x ¼” NPT, 5 x ¾” NPT
PTFE inserts not included - select from below
Insulated Hose with PTFE Inner
HB9325 M24x1.5 Insulated Hose NW12 100cm -60°C to +260°C PTFE Rodaviss Sockets, Compression Fittings and Blanking Plugs for PTFE Lids
HB9326 M24x1.5 Insulated Hose NW12 150cm -60°C to +260°C RR136300 Rodaviss B19 Socket Adapter (¾” NPT)
HB9327 M24x1.5 Insulated Hose NW12 200cm -60°C to +260°C RR136301 Rodaviss B24 Socket Adapter (¾” NPT)
HB9328 M24x1.5 Insulated Hose NW12 300cm -60°C to +260°C RR136302 Rodaviss B29 Socket Adapter (¾” NPT)
Insulated Hose with Metal Inner RR136303 Rodaviss B34 Socket Adapter (¾” NPT)
HB9274 M24x1.5 Insulated Hose NW12 100cm -100°C to +350°C RR136304 Rodaviss B45 Socket Adapter (¾” NPT)
HB9275 M24x1.5 Insulated Hose NW12 150cm -100°C to +350°C RR136314 3mm Bore Compression Fitting ¼" NPT
HB9276 M24x1.5 Insulated Hose NW12 200cm -100°C to +350°C RR136315 6mm Bore Compression Fitting ¼" NPT
RR136316 8mm Bore Compression Fitting ¾" NPT
HB9277 M24x1.5 Insulated Hose NW12 300cm -100°C to +350°C RR136317 12mm Bore Compression Fitting ¾" NPT
Adapters RR136318 14mm Bore Compression Fitting ¾" NPT
HB6724 M24x1.5 Female to M16x1 Male Adapter RR136319 16mm Bore Compression Fitting ¾" NPT
HB6945 M24x1.5 Male to M16x1 Female Adapter RR136320 19mm Bore Compression Fitting ¾" NPT
HB6723 M24x1.5 Female to M30x1.5 Male Adapter RR136327 PTFE Blanking Plug ¼" NPT
HB6195 M16x1 90° Adapter RR136328 PTFE Blanking Plug ¾" NPT
HB9256 M24x1.5 90° Adapter
HB6089 M16x1 Nut Standard Reaction Vessels Only
RR130250 250ml Single Jacketed Vessel
HB12634 M24x1.5 Nut RR130255 250ml Vacuum Jacketed Vessel
HB6086 M16x1 Hose Connector NW8 RR130500 500ml Single Jacketed Vessel
HB9471 M24x1.5 Hose Connector NW12 RR130550 500ml Vacuum Jacketed Vessel
HB6091 M16x1 Isolating Ball Valve -20°C…+140°C (max. 6 bar at +140°C) RR131000 1000ml Single Jacketed Vessel
HB9236 M24x1.5 Isolating Ball Valve -10°C…+180°C (max. 6 bar at +180°C) RR131050 1000ml Vacuum Jacketed Vessel
Thermofluid RR132000 2000ml Single Jacketed Vessel
HB6161 SilOil M20.195/235.20, 5 Litre -20°C to +195°C/235°C RR132050 2000ml Vacuum Jacketed Vessel
HB6162 SilOil M20.195/235.20, 10 Litre -20°C to +195°C/235°C RR133000 3000ml Single Jacketed Vessel
HB6163 SilOil M40.165/220.10, 5 Litre -40°C to +165°C/220°C RR133050 3000ml Vacuum Jacketed Vessel
RR135000 5000ml Single Jacketed Vessel
HB6164 SilOil M40.165/220.10, 10 Litre -40°C to +165°C/220°C RR135050 5000ml Vacuum Jacketed Vessel
HB6165 SilOil M60.115/200.05, 5 Litre -60°C to +115°C/200°C
HB6166 SilOil M60.115/200.05, 10 Litre -60°C to +115°C/200°C PTFE Stirrer Shafts (for Standard Vessels)
HB6479 DW-Therm M90.200.02, 10 Litre -90°C to +200°C (Unistats only) RR150250 Anchor PTFE Stirrer Shaft - 250ml vessels
RR150255 Retreat Curve PTFE Stirrer Shaft - 250ml vessels
Glassware Accessories RR150260 Turbine PTFE Stirrer Shaft - 250ml vessels
RR139005 Condenser Liebig 250mm B29 + GL14 + fittings RR150500 Anchor PTFE Stirrer Shaft - 500ml vessels
RR139007 Condenser Double Surface 200mm B29 + GL14 + fittings RR150505 Retreat Curve PTFE Stirrer Shaft - 500ml vessels
RR139009 Condenser Jacket Coil Rodaviss B29 + GL14 + fittings RR150510 Turbine PTFE Stirrer Shaft - 500ml vessels
RR139011 Right Angle Adapter B29 + GL14 + PTFE fittings RR151000 Anchor PTFE Stirrer Shaft - 1000ml vessels
RR139013 50ml Graduated Dropping Funnel Equalising Arm B24 RR151005 Retreat Curve PTFE Stirrer Shaft - 1000ml vessels
RR151010 Turbine PTFE Stirrer Shaft - 1000ml vessels
RR139015 100ml Graduated Dropping Funnel Equalising Arm B24 RR152000 Anchor PTFE Stirrer Shaft - 2000ml vessels
RR139017 250ml Graduated Dropping Funnel Equalising Arm B24 RR152005 Retreat Curve PTFE Stirrer Shaft - 2000ml vessels
RR139019 500ml Graduated Dropping Funnel Equalising Arm B24 RR152010 Turbine PTFE Stirrer Shaft - 2000ml vessels
RR139021 1000ml Graduated Dropping Funnel Equalising Arm B24 RR153000 Anchor PTFE Stirrer Shaft - 3000ml vessels
RR139023 Swan Neck Adapter Angled B24 to Vertical B24 RR153005 Retreat Curve PTFE Stirrer Shaft - 3000ml vessels
RR139025 Gas Purge Adapter B24 + GL14 + fittings RR153010 Turbine PTFE Stirrer Shaft - 3000ml vessels
RR139027 Glass Cone Stopper B19 RR155000 Anchor PTFE Stirrer Shaft - 5000ml vessels
RR139029 Glass Cone Stopper B24 RR155005 Retreat Curve PTFE Stirrer Shaft - 5000ml vessels
RR139031 Glass Cone Stopper B29 RR155010 Turbine PTFE Stirrer Shaft - 5000ml vessels
RR139033 Glass Cone Stopper B34 Process Reaction Vessels Only
RR139035 Enlarging Adapter B24 to B29 RR130102 100ml Single Jacketed Process Vessel
RR139037 Enlarging Adapter B29 to B34 RR130152 100ml Vacuum Jacketed Process Vessel
RR139039 Reducing Adapter B24 to B19 RR130252 250ml Single Jacketed Process Vessel
RR139041 Reducing Adapter B29 to B19 RR130257 250ml Vacuum Jacketed Process Vessel
RR139043 Reducing Adapter B29 to B24 RR130502 500ml Single Jacketed Process Vessel
RR139045 Reducing Adapter B34 to B19 RR130552 500ml Vacuum Jacketed Process Vessel
RR139047 Reducing Adapter B34 to B24 RR131002 1000ml Single Jacketed Process Vessel
RR139049 Reducing Adapter B34 to B29 RR131052 1000ml Vacuum Jacketed Process Vessel
RR132002 2000ml Single Jacketed Process Vessel
RR139051 Oil Bubbler Type 1 B24 + GL14 + fittings RR132052 2000ml Vacuum Jacketed Process Vessel
RR139053 Solid Additions Funnel B34 (with extended tube) RR133002 3000ml Single Jacketed Process Vessel
RR139057 Valved Liquid Inlet Adapter B24 to GL14 RR133052 3000ml Vacuum Jacketed Process Vessel
RR139063 PTFE Hose Adapter B19 for 12mm ID Tubing RR135002 5000ml Single Jacketed Process Vessel
RR139067 Boss Head RR135052 5000ml Vacuum Jacketed Process Vessel
RR139069 3-Prong Clamp
RR139079 PTFE Flexible Bellows B24 PTFE Stirrer Shafts (for Process Vessels)
RR139081 PTFE Flexible Bellows B29 RR150102 Anchor PTFE Stirrer Shaft - 100ml Process Vessels
RR150107 Retreat Curve PTFE Stirrer Shaft - 100ml Process Vessels
RR139083 PTFE Flexible Bellows B34 RR150112 Turbine PTFE Stirrer Shaft - 100ml Process Vessels
RR139150 Reflux Divider Head B29 + GL18 + PTFE Fitting RR150252 Anchor PTFE Stirrer Shaft - 250ml Process Vessels
RR139152 Reflux Divider Head B29 + GL18 + Temp Probe Port B14 RR150257 Retreat Curve PTFE Stirrer Shaft - 250ml Process Vessels
RR139190 Reflux Divider Kit RR150262 Turbine PTFE Stirrer Shaft - 250ml Process Vessels
RR139192 Reflux Divider Kit with Vapour Temp Kit RR150502 Anchor PTFE Stirrer Shaft - 500ml Process Vessels
RR139154 250ml Receiver Flask 2 x B24 Socket, + B24 Cone and Tap RR150507 Retreat Curve PTFE Stirrer Shaft - 500ml Process Vessels
RR139324 500ml Receiver Flask 3 x B24 Socket, + B24 Cone and Tap RR150512 Turbine PTFE Stirrer Shaft - 500ml Process Vessels
RR139326 1000ml Receiver Flask 3 x B24 Socket, + B24 Cone and Tap RR151002 Anchor PTFE Stirrer Shaft - 1000ml Process Vessels
RR151007 Retreat Curve PTFE Stirrer Shaft - 1000ml Process Vessels
PTFE Pt100 Temperature Probes and Adapters RR151012 Turbine PTFE Stirrer Shaft - 1000ml Process Vessels
RR140250 Probe 8mm with LEMO Plug - 100ml, 250ml + 500ml Vessels RR152002 Anchor PTFE Stirrer Shaft - 2000ml Process Vessels
RR141000 Probe 9mm with LEMO Plug - 1000ml, 2000ml + 3000ml Vessels RR152007 Retreat Curve PTFE Stirrer Shaft - 2000ml Process Vessels
RR152012 Turbine PTFE Stirrer Shaft - 2000ml Process Vessels
RR145000 Probe 9mm with LEMO Plug - 5000ml Vessel RR153002 Anchor PTFE Stirrer Shaft - 3000ml Process Vessels
RR140010 PTFE Temperature Probe Adapter - 8mm RR153007 Retreat Curve PTFE Stirrer Shaft - 3000ml Process Vessels
RR140015 PTFE Temperature Probe Adapter - 9mm RR153012 Turbine PTFE Stirrer Shaft - 3000ml Process Vessels
RR155002 Anchor PTFE Stirrer Shaft - 5000ml Process Vessels
Reaction Vessel Support Collar RR155007 Retreat Curve PTFE Stirrer Shaft - 5000ml Process Vessels
RR121048 Vessel Support Collar RR155012 Turbine PTFE Stirrer Shaft - 5000ml Process Vessels
We have been manufacturing scientific glassware and laboratory instruments for over 50 years and
our customers include leading blue-chip industrial and academic research facilities around the world. Shire Hill, Saffron Walden,
Our areas of expertise are focused on equipment for chemical synthesis, process development, Essex, CB11 3AZ. United Kingdom.
t: +44 1799 513320
work-up and evaporation.
f: +44 1799 513283
Visit www.radleys.com to see our full range of chemistry productivity tools. e: [email protected]