RADLEYS Reactor-Ready-Lab-Reactors

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Improving the productivity of your chemistry

innovations for chemistry

Reactor-Ready™
Lab Reactors
Patented Design

Innovative, patented,
low cost, reaction work
stations for glass
vessels from
100 ml to 5 litres

-70˚C 230˚C

www.radleys.com
Reactor-Ready Du
o
Reactor-Ready Lab Reactor -70˚C 230˚C

Replace multiple reaction set-ups with a single universal


system that accepts vessels from 100 ml to 5 litres Unique vessel clamp
• self centering
• quick release
A single reaction system • change vessels in minutes
that accepts a range of 5 Litre Single Jacket

different vessel sizes


with Support Collar
2 Litre
Vacuum Jacket
1 Litre
Vacuum Jacket
500 ml
Vacuum Jacket

250 ml
Single Jacket

Hose couplings
• quick release
• connect in seconds
• chemically resistant PEEK

A choice of
popular stirrer
paddles

PTFE Anchor PTFE Retreat PTFE Turbine


Stirrer Curve Stirrer or Propeller Stirrer

Convenient vessel kits


make buying vessels
and accessories easy
and cost effective

Individual manifolds
• easy connection
• easy drain down
• reduces stress on
vessel sidearms

2 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Change to Reactor-Ready
It improves your chemistry by saving space, time and money

Reactor-Ready Duo
accepts two vessels and
allows reactions in
parallel or series
Simple stirrer alignment
• slide and glide
• set and lock

Patented stirrer coupling


• drop in
• no tools
• no fuss
Optional AVA
Control Software
allows you to log and
control stirrers, circulators,
Standard vessels balances, pumps,
temperature sensors
• 250 ml to 5 litres
and other devices
• vacuum jacketed option

Process vessels Data Hub

• mimic plant scale geometry


• 100 ml to 5 litres
• vacuum jacketed option

Accepts all leading brands


of overhead stirrer
NEW

Compatible with all leading


brands of circulator or
thermoregulator

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 3


Reactor-Ready
Swap reaction vessels in minutes, NOT hours
Reactor-Ready is designed as a universal reactor
work station that can be used for different vessel sizes
and different experiments. Reactor-Ready can easily and
quickly be configured to suit the chemistry and scale you need for each project.

The beauty of Reactor-Ready is that this one reactor work station can replace many,
saving you money and fumehood space.

Features include
• Rapid vessel exchange with quick-release vessel clamp and hose couplings.
• Range of single and vacuum jacketed vessels from 100 ml to 5 litres.
• Range of process vessels to mimic larger scale plant or manufacturing reactors.
• Accepts all leading brands of overhead stirrer and allows easy, tool-free adjustment.
• Triple support stand features heavy duty stainless steel support rods for strength and stability.
• Self aligning stirrer coupling engages without the need for tools.
• Temperature range: -70 ºC to +230 ºC (jacket temperature)
• Innovative hose manifolds allow easy thermofluid drain down.
• Wide range of accessory glassware including condensers, dropping funnels etc.
• Optional software allows you to log and control stirrers, circulators, balances, pumps, temperature
sensors and other devices.

Patented vessel clamp allows rapid vessel exchange without tools


• Unique clamp design allows vessel to be supported and clamped by a single operator in less than a minute.
• Use the same clamp to hold all vessel sizes; plus the vessels remain supported even when the clamp is unlocked.

Vessel support collar aids vessel loading


• Reactor-Ready uses an innovative support collar fitted to the neck of each vessel, which allows the vessels to be swapped
Stainless steel vessel in and out of the Reactor-Ready core like a cartridge.
support collar
• The stainless steel collar locks securely into the support plate on the framework and allows the vessel to remain supported,
even when not clamped.
• Vessel exchange is tool free and can easily be undertaken
by one person.

Unique self aligning stirrer coupling saves


time when changing vessels
• Patented drop-in stirrer coupling engages easily without
the need for tools.
• Simply lower the stirrer coupling to engage with the
stirrer guide below.
• The stainless steel stirrer coupling will fit in any standard
stirrer chuck (for 10mm diameter)
• Powerful stirring up to 500 rpm, or 800 rpm for short
periods (subject to motor selected).

4 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Choice of PTFE stirring shafts
• Reactor-Ready is offered with a choice of PTFE stirring shafts: anchor, retreat curve
and turbine/propeller styles.
• PTFE anchor stirring shaft is included with all standard reaction vessel kits
• PTFE turbine stirring shaft is included with all process reaction vessel kits.

I-beam support allows the stirring motor to be positioned with ease


• I-beam allows the stirrer motor to be raised or lowered without needing to remount the stirrer.
• Adjustable safety stop collars located below the I-beam allow the user to lower the stirrer
motor to a set position for ease of operation and safety. PTFE anchor PTFE retreat PTFE turbine/
• Reactor-Ready accepts all leading brands of motor or air-powered overhead stirrer with stirrer curve stirrer propeller stirrer
support rods up to 16 mm in diameter.

PTFE Stirrer Guide


• The Reactor-Ready’s PTFE stirrer guide screws directly on to the glass lid and features
a unique extended support which minimises wobble even at high speeds. PTFE stirrer
• The stirrer guide is chemically inert, gas-tight and suitable for work under vacuum. guide provides
whip-free agitation

Quick release PEEK hose couplings


• Operates over the temperature range -70 ˚C to +230 ˚C (jacket temperature).
• Quick-release, screwthread design allows rapid exchange of vessels without the use of tools.
• Simply tighten by hand for a leak-tight seal.
• PEEK with Viton O-rings ensures all wetted parts are chemically resistant.
• Lightweight, metal-free design prevents chipping and minimises strain on the glass fitting.
• All hoses have a 12 mm ID, maximising thermofluid flow and heating/cooling performance.
• Low thermal conductivity of PEEK reduces frosting when cooling.

Hose manifolds allow easy thermofluid drain down


• The inlet and outlet hoses from the Reactor-Ready vessel connect to manifolds attached to
the support rod. These manifolds serve two important functions:
1. Support the hoses running from the vessel, thereby eliminating stress on the glass sidearms.
2. Allows thermofluid drain-down, which provides a quick and clean method of removing the
thermofluid from the vessel jacket when changing vessels.
• By opening the venting valve on the (upper) outlet manifold, thermofluid drains from the vessel
back to the thermoregulator under gravity.
• Opening the drain tap on the (lower) inlet manifold allows drainage to an external reservoir.

Case study: Accelerating process optimisation in a busy chemical development lab


Researchers at a leading US pharmaceutical company invested in Reactor-Ready “So I liked Reactor-Ready the minute I saw how easy it was to change reactors.
for use in their chemical development lab. The process R&D group, specialising in Reactor-Ready does it all. I get one stand which fits all sizes up to 5 litres. I get
small molecule research, are using Reactor-Ready for optimising new or existing overhead stirring on all scales. I get vacuum jacketed vessels, which provide
chemistry, identifying and eliminating impurities, and screening process variables excellent temperature control with minimum heat loss, which is a real advantage
for transfer to kilo-labs, pilot plant and manufacturing sites. at low temperatures, and I get the ability to rapidly change out my reactors.”

Commenting on their existing methods the Lead Scientist said, “We use round “The first time I changed vessels, it took about 5 minutes but now I can change in
bottom flasks, but temperature control via mantles or oil baths is poor. Alternatively, less than 2 minutes. That includes removing and attaching the heating fluid hoses.
when we use traditional jacketed reactor vessels, we need a different set up for Occasionally I lose a drop or two of heat transfer fluid but most times I lose none.
every scale change. Even changing a reactor of the same size takes ages.” The thing I like about the system is the control and speed. I get better control of
my reactions and I can vary my work or scale immediately”.

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 5


How to order Reactor-Ready in detail Stirrer support I-beam

Reactor-Ready…
allows the stirrer motor

It is the attention to detail and wealth


to be easily raised
and lowered.
1. Select the of innovative features that makes
Reactor-Ready so much better
Reactor-Ready
core.

Precision ground lid and vessel


flanges combine with PTFE collar
and FEP-encapsulated O-ring
to offer superior sealing
performance.

Vessel clamp support allows easy


2. Choose the vessel kit or kits vertical repositioning of the vessel
you require by whilst maintaining the stirrer
selecting the coupling alignment.
vessel volume
and style.

Venting stopcock on the outlet manifold


allows quick and easy draining of the
thermofluid during vessel exchange.

3. Select the overhead stirrer


you need.
Vessel-to-manifold hoses are
supported by the manifolds
and frame, eliminating stress
on the vessel.

Quick-release PEEK coupling
4. If you need a thermoregulator, allows rapid exchange of vessels
hoses, hose without the use of tools. Operates
adapters, over the temperature range
thermofluid -70 ˚C to +230 ˚C
or accessory (jacket temperature).
glassware,
then select
from the
accessory list.

5. If you need automation add the


AVA Control Software
and data hub.
Thermofluid may be drained back to the thermoregulator
or decanted via a fluid drain tap on the inlet manifold.

Heavy-duty base plate with levelling feet


ensures that the Reactor-Ready support
stand is secure and stable.

6 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Support system accepts Reactor-Ready core system
includes
all leading brands of overhead
stirrer and allows easy,
tool-free adjustment.
• Stand with base, support rods, bosses
and all clamps
• Glass reaction vessel lid
-70˚C 230˚C • Vessel FEP O-ring seal and PTFE collar
• HDPE drip tray
• Vessel-to-manifold insulated hoses with
quick-release connections
Wide range of accessory glassware • Lower inlet manifold + drain
including condensers, dropping funnels, • Upper outlet manifold
adapters, powder addition funnels,
+ vent
gas purge adapters and liquid Patented drop-in stirrer
inlet adapters etc. coupling engages easily • PTFE stirrer guide
without the need • Stainless steel drop-in
for tools. stirrer guide coupling
• Two stainless steel
vessel support
collars
• Locking rod for
PTFE stirrer guide provides excellent support rod
stirring and sealing performance.
bosses
An extended stirrer shaft support minimises
wobble even at high speeds.

Reaction vessels are held by a


novel quick-release clamp. No tools
are required to exchange vessels.

Chemically resistant
PTFE stirrers. Accepts single jacketed and vacuum Reaction vessel kits make
jacketed vessels of 100 ml, 250 ml, ordering vessels simple and
more cost effective
500 ml, 1 litre, 2 litre, 3 litre and 5 litre.

These cost effective vessel kits include the


vessel and accessories you need to get
started. The Pt100 probe and PTFE stirrer
Innovative triple support stand
included in each kit are matched to the
features heavy duty stainless steel
support rods for maximum strength, vessel size. Each vessel kit includes:
stability and to minimise vibration.
• Reaction vessel with PTFE stopcock
• Sidearm couplings
• Pt100 PTFE temperature
probe with LEMO
Zero dead space PTFE bottom outlet valve is connector
designed to minimise leaking or weeping across • PTFE temperature
the full temperature range (-70 ºC to +230 ºC). Probe adapter
Large 15 mm bore minimises sample hold-up
• PTFE stirrer
and is ideal for slurries.

HDPE drip tray will

Reactor-Ready Video
catch any spills and
can accommodate
the contents of Visit www.radleys.com
a 5 litre vessel
to watch the demo
and jacket.

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 7


Reactor-Ready Duo
Supports two glass reaction vessels of different or same volume
from 100 ml to 5 litres
Reactor-Ready Duo shares the same unique features as Reactor-Ready, except
that it supports two separate jacketed glass reaction vessels. The system can
be configured to operate with a single thermoregulator controlling the temperature
of both vessels simultaneously, or with two thermoregulators
controlling the temperature of each
vessel independently.

Unique vessel clamp


• supports two vessels Simple stirrer alignment
• change vessels independently • set and lock
• change vessels in minutes • independent stirring
for each vessel

Vessels
• 100 ml to 5 litres
• combine different volumes Patented stirrer coupling
• vacuum jacketed option • drop in
• process and standard • no tools
geometry • no fuss

Hose couplings
• quick release
• connect in seconds
Thermofluid manifolds • chemically resistant PEEK
• choice of two manifold kits
• single circulator manifolds
• double circulator manifolds

Strong framework
• heavy duty base
• solid s/steel support rods
• large drip tray

8 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Why Reactor-Ready Duo?
All the benefits of Reactor-Ready with two vessels in parallel or series
Features include
• Rapid exchange of both vessels independently, with quick-release vessel clamp and hose couplings.
• Choice of manifold kits allow two vessels to run from a single thermoregulator or two separate thermoregulators.
• System accepts two overhead stirrers which can be operated and moved independently.

Applications
• Parallel synthesis or reaction optimisation: use the same or different size vessels and vary stirring
speed, stirrer shape and temperature between vessels as appropriate.
• Two stage reaction: transfer reactant from one vessel to the other using vacuum or a pump.
• Single reaction vessel: using the second vessel as either a receiving or feed vessel
(where reagents can be pre-heated or pre-cooled prior to addition).
• Use optional AVA Software to control fluid transfer between vessels.
Similar vessels with Different vessels with Single vessel with
double circulator manifold kit double circulator manifold kit double circulator manifold kit

Similar vessels with Different vessels with Single vessel with


single circulator manifold Kit single circulator manifold Kit Single circulator manifold Kit

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 9


How to order Reactor-Ready Duo core system
Reactor-Ready Duo…
Easy-to-order Reactor-Ready Duo core system includes all the
1. Select the framework components required for operation
Reactor-Ready

Features include
Duo core.

• Robust heavy-duty framework features solid stainless


steel support rods.
• Two separate quick release clamps support each
of the vessels independently.
• Large drip tray will retain vessel contents.
• Manifold and hose kits must be ordered separately.
2. Choose
manifold
Core system (RR121300) includes
& hose • Stand with base, support rods, bosses and all clamps
kit for • 2 x glass reaction vessel lids
one or • 2 x vessel FEP O-ring seals and PTFE centering collars
two circulators. • 2 x PTFE stirrer guides and couplings
• HDPE drip tray
• 2 x stainless steel stirrer
3. Choose the drop-in couplings
vessel kits • 2 x stainless steel vessel
you need. support collars
• locking rod for support
rod bosses

Reactor-Ready Duo manifolds and hoses


4. Select the overhead stirrers.
A choice of manifold kits for use with one or two thermoregulators
Double thermoregulator manifold and hose kit (RR121310)
This double thermoregulator kit is designed to work with two
separate thermoregulators controlling the temperature of each
vessel independently. With this set-up both vessels can operate
at different temperatures. This is the recommended kit.
• R/H upper return manifold with vent valve
5. If you need a thermoregulator, • L/H upper return manifold with vent valve
hoses, hose
• R/H lower supply manifold with drain valve
adapters,
thermofluid • L/H lower supply manifold with drain valve
or accessory • 4 x quick-release insulated hoses, 60 cm
glassware, • 4 x sealing caps for hoses
then select
from the
accessory list. Single circulator manifold and hose kit (RR121305)
This single circulator kit is designed to work with one thermoregulator
6. If you need automation, add the controlling the temperature of both vessels simultaneously. With this
AVA Software set-up both vessels would operate at the same temperature. The
and data hub. manifolds are supplied with blanking plugs should
you wish to run only one vessel.
• central upper return manifold with vent valve
• central lower supply manifold with drain valve
• 4 x quick-release insulated hoses, 70 cm
• 4 x sealing caps for hoses
• 2 x stainless steel blanking plugs

10 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Hei-Torque overhead stirrers
The powerful Hei-Torque range can accomplish the most
demanding mixing tasks whilst providing the highest safety
Stirrer models include
• Powerful stirring from 10 to 2000 rpm (Max. recommended speed with Reactor-Ready is 500 rpm).
• Available with basic (Value) or advanced (Precision) features, and a choice of up to 40, 200
or 400 Ncm torque.
• Intuitive control panel for easy operation, safe start and stop to avoid accidental start-up.
• New features for Precision range: set speed limit, adjustable acceleration, set a torque limit.
• New unique Quick-chuck for immediate and convenient ‘one-hand’ impellor changes, without tools.
Hei-Torque Hei-Torque Hei-Torque Hei-Torque Hei-Torque
Core Value 200 Value 400 Precision 200 Precision 400
Power rating, motor input/output (W) 105/75 120/80 150/90 120/80 150/90
Number of gears 1 1 2 1 2
Speed range (rpm) 20 to 2000 10 to 2000 10 to 400 and 200 to 2000 10 to 2000 10 to 400 and 200 to 2000
Speed indicator digital monochrome 2” digital monochrome 2.4” digital monochrome 2.4” digital colour 3.2” digital colour 3.2”
Speed control electronic electronic electronic electronic electronic
Torque, maximum (Ncm) 40 200 400 200 400
Torque indicator (Ncm) symbol symbol symbol precise value precise value
Overheat protection automatic cut-out automatic cut-out automatic cut-out automatic cut-out automatic cut-out
Viscosity up to (mPa s) 10,000 100,000 250,000 100,000 250,000
Stirring cap. H2O max. (L) 25 50 100 50 100
Shaft diameter, max. (mm) 10.5 10.5 10.5 10.5 10.5
Dimensions (W x H x D) (mm) 70 x 281.5 x 195 86 x 350 x 247 93 x 350 x 247 86 x 350 x 247 93 x 350 x 247
Weight (kg) 2.3 5.1 5.3 5.1 5.3
Set speed limit, Torque limit, Adjustable acceleration - - - Yes Yes
Analogue/digital interface - - - USB and RS232 USB and RS232

Thermoregulators/circulators
For Reactor-Ready and Reactor-Ready Duo the maximum speed is 500 rpm for continuous use for 800 rpm for short periods.

Which thermoregulator should you choose?


• Radleys are a Huber distribution and service partner, so we recommend the Huber range of thermo-
regulators, circulators, chillers and waterbaths. However, Reactor-Ready is compatible with all leading
brands of thermoregulator including Julabo, Lauda, Polyscience, Haake and many others.
• Also available are a range of hoses, adapters, temperature probes and thermofluid for all applications.

Heating Cooling
Temperature
Description power power Application Examples
range ˚C Huber Unistat 405
(kW) at 0 ˚C (kW)

Huber 250 ml Cool to -10 ºC in <1 hr, then heat to 130 ºC in <30 mins
-45 ˚C to 200 ˚C 2.0 0.38
Ministat 230 1 Litre Control at 0 ºC, then heat to 100 ºC in 20 mins

Huber 500 ml Cool to -20 ºC in approx 30 mins, then heat to 150 ºC in <30 mins
-40 ˚C to 200 ˚C 1.5 0.45
Petite Fleur 1 Litre Heat to 150 ºC, then cool to 0 ºC at > 2.5 K/min

Huber 1 Litre Cool to -30 ºC in <1 hr, then heat to 180 ºC in <1 hr
-45 ˚C to 250 ˚C 3.0 0.7
Unistat Tango 2 Litre Heat to 180 ºC, then cool to 20 ºC in approx 1 hr

Huber 2 Litre Cool to -20 ºC in <30 mins, then heat to 100 ºC in <30 mins
-45 ˚C to 250 ˚C 3.0 1.0
Unistat 405 5 Litre Control at 20 ºC, then cool to -20 ºC in approx 70 mins

Huber 1 Litre Control at 20 ºC, then cool to -50 ºC in 40 mins


-75 ˚C to 250 ˚C 3.0 0.65
Unistat 705 5 Litre Cool to -40 ºC at approx 1 K/min, then heat to 150 ºC in <1 hr

The above applications are intended as a guide to the relative performance of each Huber thermoregulator with a range of vessel sizes and are not a prediction of actual Huber Petite Fleur - Baby Tango
performance. To achieve optimum performance the use of vacuum jacketed vessels is recommended for below ambient temperature applications. For comprehensive advice
on thermoregulator selection please contact your local Radleys distributor.

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 11


Reaction vessels
Single jacketed, vacuum jacketed and process styles

Features include
• Precision engineered borosilicate glass vessels can be used with Reactor-Ready and Reactor-Ready Duo.
• DN100 ground and polished flat flange combines with the FEP-encapsulated O-ring and our unique
self centering PTFE collar to offer a leak-tight seal between the vessel and lid.
• Convenient and cost-effective vessel kits include stirrer, temperature probe and adapter.

Vessels feature zero dead space PTFE bottom outlet valve


• Exclusive stopcock design prevents over-tightening that can cause glass breakage.
• Piston design allows quick and safe removal, eliminating the cleaning and assembly problems associated
with other stopcock styles.
• Glass-filled PTFE piston minimises leaking or weeping across the full temperature range (-70 ºC to +230 ºC)
• Interchangeable between vessels with a full range of replacement parts and FEP O-rings.
• The large 15 mm bore minimises sample hold-up and is ideal for slurries (25 mm available on request).

Glass vessel lids


• DN100 5 neck glass lid fits all vessel sizes.
• DN100 lid with 5 x Rodaviss, grease-free, safety joints. B24 centre, B34, B29, B24 and B19 side joints.
• Rodaviss glass sockets will accept any glassware with traditional A, B or C length conical cones. PTFE vessel lids
• DN100 7 neck PTFE lids fit all vessel sizes.
• More robust and less likely to break than glass.
Standard Vessels • Ideal for use with analytical probes.
• Lids accept a range of removable Rodaviss
250 ml single 250 ml vacuum 500 ml single 500 ml vacuum sockets and compression fittings.
jacketed vessel Jacketed vessel jacketed vessel jacketed vessel
• Rodaviss PTFE sockets will accept any glassware
with traditional A, B or C length conical cones.

1000 ml single 1000 ml vacuum 2000 ml single 2000 ml vacuum 5000 ml single 5000 ml vacuum
jacketed vessel jacketed vessel jacketed vessel jacketed vessel jacketed vessel jacketed vessel

Process Vessels - mimic the geometry of plant scale reactors


Feature a 1.25 to 1 ratio of internal height to internal diameter, with dish-shaped bottom.
100 ml single jacketed 100 ml vacuum jacketed 250 ml single jacketed 250 ml vacuum jacketed 500 ml single jacketed 500 ml vacuum jacketed
process vessel process vessel process vessel process vessel process vessel process vessel

1000 ml single jacketed 1000 ml vacuum jacketed 2000 ml single jacketed 2000 ml vacuum jacketed 5000 ml single jacketed 5000 ml vacuum jacketed
process vessel process vessel process vessel process vessel process vessel process vessel

Note: 3 litre vessels not shown

12 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Reaction vessel kits
Reaction vessel kits make ordering vessels and accessories simple and much more cost effective

Standard reaction vessel kits Process reaction vessel kits


These cost effective vessel kits include the Process vessel kits include a Pt100
vessel and accessories you need to get temperature probe and turbine stirrer
started. The Pt100 probe and anchor matched to the vessel size.
stirrer included in each kit are matched Each vessel kit includes:
to the vessel size. Each vessel kit includes:
• Reaction vessel
• Reaction vessel • PTFE turbine
• PTFE anchor stirrer stirrer
• Sidearm couplings • Sidearm
• Pt100 PTFE couplings
temperature probe • Pt100 PTFE
with LEMO Connector temperature probe
• PTFE temperature with LEMO connector
Probe adapter • PTFE temperature probe
adapter

Glassware and accessories


Wide choice of standard glassware to suit your application
Glassware features Rodaviss joints and is compatible with Reactor-Ready lids

Boss head

3 Pronged clamp

Condenser Condenser Condenser Dropping funnel PTFE hose Liquid additions Glass cone Reducing Right angle Enlarging
liebig, B29 double surface, B29 jacket coil, B29 equalising arm, B24 adapter, B19 adapter, B24 stopper, B29 adapter, B29 adapter, B29 adapter, B29

Other styles
and sizes of
glassware are
available, please
see full listing.

Reflux divider head Reflux divider head Valved liquid Gas purge Oil bubbler, Solid additions Swan neck
B29 + GL18 B29 + GL18 + temp- inlet adapter, B24 adapter, B24 B24 Funnel, B34 Adapter, B24
+ PTFE fitting probe port B14

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 13


How to order Reactor-Ready How to order Reactor-Ready Duo
1. Select the Reactor-Ready core: RR121000. 1. Select the Reactor-Ready Duo core: RR121300.
2. Choose the vessel kit or kits you require by selecting the vessel volume and style. 2. Choose manifold and hose kit for one or two circulators.
3. Select the overhead stirrer you require. 3. Choose the vessel kit or kits you require by selecting the vessel volume and style.
4. If you need a thermoregulator, hoses, hose adapters, thermofluid or accessory 4. Select the overhead stirrers you require.
glassware, then select from the accessory list opposite. 5. If you need a thermoregulator, hoses, hose adapters, thermofluid or accessory
5. If you need automation, add the AVA Software and Data Hub. glassware, then select from the accessory list opposite.
6. If you need automation, add the AVA Control Software and Data Hub.
Reactor-Ready core system
RR121000 Reactor-Ready core system includes: Reactor-Ready Duo core system
• Stand with base, drip tray, support rods, bosses and all clamps RR121300 Reactor-Ready Duo core system includes:
• Vessel to framework insulated hoses with quick-release connections • Duo stand with base, drip tray, support rods, bosses and all clamps
• Upper and lower drain-down manifolds • 2 x PTFE stirrer guides and drop-in couplings
• PTFE stirrer guide and drop-in coupling • 2 x Glass reaction vessel lids with Rodaviss sealing caps
• Glass reaction vessel lid with Rodaviss sealing caps • 2 x Vessel FEP O-ring seal and PTFE centering collars
• Vessel FEP O-ring seal and PTFE centering collar • 2 x Stainless steel vessel support collars
• 2 x Stainless steel vessel support collars
Important: Hoses to connect the Reactor-Ready Duo framework to your thermoregulator
Important: Hoses to connect the Reactor-Ready framework to your thermoregulator are are NOT included. You will require hoses with an M24x1.5 female connection or
NOT included. You will require hoses with an M24x1.5 female connection or appropriate appropriate adapters. See opposite for hoses, adapters and suitable thermoregulators.
adapters. See opposite for hoses, adapters and suitable thermoregulators.
Double Circulator Manifold and Hose Kit
RR121310 Double Circulator Manifold and Hose Kit includes:
• R/H Upper Return Manifold with Vent Valve
Standard Reaction Vessel Kits • L/H Upper Return Manifold with Vent Valve
Kits include: standard vessel, PTFE anchor stirrer paddle, PTFE Pt100 temp probe • R/H Lower Supply Manifold with Drain Valve
(with LEMO plug for connection to the thermoregulator) and PTFE temp probe adapter. • L/H Lower Supply Manifold with Drain Valve
• 4 x Quick-Release Insulated Hoses, 60cm
RR120010 250ml Single Jacketed Vessel Kit
• 4 x Sealing Caps for Hoses
RR120015 250ml Vacuum Jacketed Vessel Kit
RR120020 500ml Single Jacketed Vessel Kit
Single Circulator Manifold and Hose Kit
RR120025 500ml Vacuum Jacketed Vessel Kit
RR121305 Single Circulator Manifold and Hose Kit includes:
RR120030 1000ml Single Jacketed Vessel Kit
• Central Upper Return Manifold with Vent Valve
RR120035 1000ml Vacuum Jacketed Vessel Kit
• Central Lower Supply Manifold with Drain Valve
RR120040 2000ml Single Jacketed Vessel Kit
• 4 x Quick-Release Insulated Hoses, 70cm
RR120045 2000ml Vacuum Jacketed Vessel Kit
• 4 x Sealing Caps for Hoses
RR120042 3000ml Single Jacketed Vessel Kit
Kit includes • 4 x Stainless Steel Blanking Plugs
RR120047 3000ml Vacuum Jacketed Vessel Kit
Anchor Stirrer
RR120050 5000ml Single Jacketed Vessel Kit
RR120055 5000ml Vacuum Jacketed Vessel Kit
Hei-Torque Overhead Stirrers .
Process Reaction Vessel Kits 501-60410-00 Hei-Torque Core
Kits include: process vessel, PTFE turbine stirrer paddle, PTFE Pt100 temp probe 501-62010-00 Hei-Torque 200 Value
(with LEMO plug for connection to the thermoregulator) and PTFE temp probe adapter. 501-62020-00 Hei-Torque 200 Precision (USB/RS232)
501-64010-00 Hei Torque 400 Value
RR120105 100ml Single Jacketed Process Vessel Kit 501-64020-00 Hei-Torque 400 Precision (USB/RS232)
RR120107 100ml Vacuum Jacketed Process Vessel Kit
RR120110 250ml Single Jacketed Process Vessel Kit
RR120115 250ml Vacuum Jacketed Process Vessel Kit
RR120120 500ml Single Jacketed Process Vessel Kit General Maintenance Accessories
RR120125 500ml Vacuum Jacketed Process Vessel Kit RR121150 Reactor-Ready Maintenance Kit (includes items listed below)
RR120130 1000ml Single Jacketed Process Vessel Kit RR121027 Oil Wipe for Support Rods, Pack 10
RR120135 1000ml Vacuum Jacketed Process Vessel Kit RR121063 Stirrer Guide Bearing Seal B24 10mm
RR120140 2000ml Single Jacketed Process Vessel Kit RR121064 Stirrer Guide Ferrule and Shaft Seal B24 10mm
RR120145 2000ml Vacuum Jacketed Process Vessel Kit RR121071 23mm Viton O-Rings for Quick Release Hose Coupling, Pack 2
RR120142 3000ml Single Jacketed Process Vessel Kit Kit includes RR121072 28mm Viton O-Rings for Quick Release Hose Coupling, Pack 2
RR120147 3000ml Vacuum Jacketed Process Vessel Kit Turbine Stirrer RR121090 FEP Encapsulated Silicone Vessel O-Ring
RR120150 5000ml Single Jacketed Process Vessel Kit RR166100 Replacement 15mm Piston Top O-Ring
RR120155 5000ml Vacuum Jacketed Process Vessel Kit RR166102 Replacement 15mm Piston Middle O-Ring

Reactor-Ready Duo reaction vessel compatibility guide


The following combinations of reaction vessel sizes can be used in the Reactor-Ready Duo.
100ml 250 ml 500 ml 1000 ml 2000 ml 3000 ml 5000 ml 100ml 250 ml 500 ml 1000 ml 2000 ml 3000 ml 5000 ml
Standard Vessel, Single Jacketed Standard Vessel, Vacuum Jacketed
250 ml n/a       250 ml n/a      
500 ml n/a       500 ml n/a      
1000 ml n/a       1000 ml n/a      
2000 ml n/a       2000 ml n/a      
5000 ml n/a       5000 ml n/a     n/a n/a
Process Vessel, Single Jacketed Process Vessel, Vacuum Jacketed
100 ml        100 ml       
250 ml        250 ml       
500 ml        500 ml       
1000 ml        1000 ml      n/a n/a
2000 ml        2000 ml      n/a n/a
3000 ml        3000 ml       
5000 ml      n/a n/a 5000 ml    n/a n/a n/a n/a

14 Radleys Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom
Huber Thermoregulators (Circulators) Glass DN100 Vessel Lid
HB2016.0005.01 Ministat 240 Pilot ONE Controller RR136000 5 Neck Glass Lid - 1 x B19, 2 x B24, 1 x B29, 1 x B34
HB1030.0001.01 Petite Fleur Pilot ONE Controller Includes Rodaviss sealing caps
HB1030.0001.01ET Petite Fleur with 4 Litre Expansion Tank
HB1000.0037.01 Unistat Tango Pilot ONE Controller PTFE DN100 Vessel Lids
RR136100 5 Neck PTFE Lid with 2 Blanked Ports. 1 x B19, 2 x B24, 1 x B29, 1 x B34
HB1002.0045.01 Unistat 405 Pilot ONE Controller Includes Rodaviss sealing caps
HB1001.0041.01 Unistat 705 Pilot ONE Controller (230V or 400V)
Thermoregulator Hoses, Adapters and Thermofluid RR136110 7 Neck PTFE Lid with 7 Threaded Ports. 2 x ¼” NPT, 5 x ¾” NPT
PTFE inserts not included - select from below
Insulated Hose with PTFE Inner
HB9325 M24x1.5 Insulated Hose NW12 100cm -60°C to +260°C PTFE Rodaviss Sockets, Compression Fittings and Blanking Plugs for PTFE Lids
HB9326 M24x1.5 Insulated Hose NW12 150cm -60°C to +260°C RR136300 Rodaviss B19 Socket Adapter (¾” NPT)
HB9327 M24x1.5 Insulated Hose NW12 200cm -60°C to +260°C RR136301 Rodaviss B24 Socket Adapter (¾” NPT)
HB9328 M24x1.5 Insulated Hose NW12 300cm -60°C to +260°C RR136302 Rodaviss B29 Socket Adapter (¾” NPT)
Insulated Hose with Metal Inner RR136303 Rodaviss B34 Socket Adapter (¾” NPT)
HB9274 M24x1.5 Insulated Hose NW12 100cm -100°C to +350°C RR136304 Rodaviss B45 Socket Adapter (¾” NPT)
HB9275 M24x1.5 Insulated Hose NW12 150cm -100°C to +350°C RR136314 3mm Bore Compression Fitting ¼" NPT
HB9276 M24x1.5 Insulated Hose NW12 200cm -100°C to +350°C RR136315 6mm Bore Compression Fitting ¼" NPT
RR136316 8mm Bore Compression Fitting ¾" NPT
HB9277 M24x1.5 Insulated Hose NW12 300cm -100°C to +350°C RR136317 12mm Bore Compression Fitting ¾" NPT
Adapters RR136318 14mm Bore Compression Fitting ¾" NPT
HB6724 M24x1.5 Female to M16x1 Male Adapter RR136319 16mm Bore Compression Fitting ¾" NPT
HB6945 M24x1.5 Male to M16x1 Female Adapter RR136320 19mm Bore Compression Fitting ¾" NPT
HB6723 M24x1.5 Female to M30x1.5 Male Adapter RR136327 PTFE Blanking Plug ¼" NPT
HB6195 M16x1 90° Adapter RR136328 PTFE Blanking Plug ¾" NPT
HB9256 M24x1.5 90° Adapter
HB6089 M16x1 Nut Standard Reaction Vessels Only
RR130250 250ml Single Jacketed Vessel
HB12634 M24x1.5 Nut RR130255 250ml Vacuum Jacketed Vessel
HB6086 M16x1 Hose Connector NW8 RR130500 500ml Single Jacketed Vessel
HB9471 M24x1.5 Hose Connector NW12 RR130550 500ml Vacuum Jacketed Vessel
HB6091 M16x1 Isolating Ball Valve -20°C…+140°C (max. 6 bar at +140°C) RR131000 1000ml Single Jacketed Vessel
HB9236 M24x1.5 Isolating Ball Valve -10°C…+180°C (max. 6 bar at +180°C) RR131050 1000ml Vacuum Jacketed Vessel
Thermofluid RR132000 2000ml Single Jacketed Vessel
HB6161 SilOil M20.195/235.20, 5 Litre -20°C to +195°C/235°C RR132050 2000ml Vacuum Jacketed Vessel
HB6162 SilOil M20.195/235.20, 10 Litre -20°C to +195°C/235°C RR133000 3000ml Single Jacketed Vessel
HB6163 SilOil M40.165/220.10, 5 Litre -40°C to +165°C/220°C RR133050 3000ml Vacuum Jacketed Vessel
RR135000 5000ml Single Jacketed Vessel
HB6164 SilOil M40.165/220.10, 10 Litre -40°C to +165°C/220°C RR135050 5000ml Vacuum Jacketed Vessel
HB6165 SilOil M60.115/200.05, 5 Litre -60°C to +115°C/200°C
HB6166 SilOil M60.115/200.05, 10 Litre -60°C to +115°C/200°C PTFE Stirrer Shafts (for Standard Vessels)
HB6479 DW-Therm M90.200.02, 10 Litre -90°C to +200°C (Unistats only) RR150250 Anchor PTFE Stirrer Shaft - 250ml vessels
RR150255 Retreat Curve PTFE Stirrer Shaft - 250ml vessels
Glassware Accessories RR150260 Turbine PTFE Stirrer Shaft - 250ml vessels
RR139005 Condenser Liebig 250mm B29 + GL14 + fittings RR150500 Anchor PTFE Stirrer Shaft - 500ml vessels
RR139007 Condenser Double Surface 200mm B29 + GL14 + fittings RR150505 Retreat Curve PTFE Stirrer Shaft - 500ml vessels
RR139009 Condenser Jacket Coil Rodaviss B29 + GL14 + fittings RR150510 Turbine PTFE Stirrer Shaft - 500ml vessels
RR139011 Right Angle Adapter B29 + GL14 + PTFE fittings RR151000 Anchor PTFE Stirrer Shaft - 1000ml vessels
RR139013 50ml Graduated Dropping Funnel Equalising Arm B24 RR151005 Retreat Curve PTFE Stirrer Shaft - 1000ml vessels
RR151010 Turbine PTFE Stirrer Shaft - 1000ml vessels
RR139015 100ml Graduated Dropping Funnel Equalising Arm B24 RR152000 Anchor PTFE Stirrer Shaft - 2000ml vessels
RR139017 250ml Graduated Dropping Funnel Equalising Arm B24 RR152005 Retreat Curve PTFE Stirrer Shaft - 2000ml vessels
RR139019 500ml Graduated Dropping Funnel Equalising Arm B24 RR152010 Turbine PTFE Stirrer Shaft - 2000ml vessels
RR139021 1000ml Graduated Dropping Funnel Equalising Arm B24 RR153000 Anchor PTFE Stirrer Shaft - 3000ml vessels
RR139023 Swan Neck Adapter Angled B24 to Vertical B24 RR153005 Retreat Curve PTFE Stirrer Shaft - 3000ml vessels
RR139025 Gas Purge Adapter B24 + GL14 + fittings RR153010 Turbine PTFE Stirrer Shaft - 3000ml vessels
RR139027 Glass Cone Stopper B19 RR155000 Anchor PTFE Stirrer Shaft - 5000ml vessels
RR139029 Glass Cone Stopper B24 RR155005 Retreat Curve PTFE Stirrer Shaft - 5000ml vessels
RR139031 Glass Cone Stopper B29 RR155010 Turbine PTFE Stirrer Shaft - 5000ml vessels
RR139033 Glass Cone Stopper B34 Process Reaction Vessels Only
RR139035 Enlarging Adapter B24 to B29 RR130102 100ml Single Jacketed Process Vessel
RR139037 Enlarging Adapter B29 to B34 RR130152 100ml Vacuum Jacketed Process Vessel
RR139039 Reducing Adapter B24 to B19 RR130252 250ml Single Jacketed Process Vessel
RR139041 Reducing Adapter B29 to B19 RR130257 250ml Vacuum Jacketed Process Vessel
RR139043 Reducing Adapter B29 to B24 RR130502 500ml Single Jacketed Process Vessel
RR139045 Reducing Adapter B34 to B19 RR130552 500ml Vacuum Jacketed Process Vessel
RR139047 Reducing Adapter B34 to B24 RR131002 1000ml Single Jacketed Process Vessel
RR139049 Reducing Adapter B34 to B29 RR131052 1000ml Vacuum Jacketed Process Vessel
RR132002 2000ml Single Jacketed Process Vessel
RR139051 Oil Bubbler Type 1 B24 + GL14 + fittings RR132052 2000ml Vacuum Jacketed Process Vessel
RR139053 Solid Additions Funnel B34 (with extended tube) RR133002 3000ml Single Jacketed Process Vessel
RR139057 Valved Liquid Inlet Adapter B24 to GL14 RR133052 3000ml Vacuum Jacketed Process Vessel
RR139063 PTFE Hose Adapter B19 for 12mm ID Tubing RR135002 5000ml Single Jacketed Process Vessel
RR139067 Boss Head RR135052 5000ml Vacuum Jacketed Process Vessel
RR139069 3-Prong Clamp
RR139079 PTFE Flexible Bellows B24 PTFE Stirrer Shafts (for Process Vessels)
RR139081 PTFE Flexible Bellows B29 RR150102 Anchor PTFE Stirrer Shaft - 100ml Process Vessels
RR150107 Retreat Curve PTFE Stirrer Shaft - 100ml Process Vessels
RR139083 PTFE Flexible Bellows B34 RR150112 Turbine PTFE Stirrer Shaft - 100ml Process Vessels
RR139150 Reflux Divider Head B29 + GL18 + PTFE Fitting RR150252 Anchor PTFE Stirrer Shaft - 250ml Process Vessels
RR139152 Reflux Divider Head B29 + GL18 + Temp Probe Port B14 RR150257 Retreat Curve PTFE Stirrer Shaft - 250ml Process Vessels
RR139190 Reflux Divider Kit RR150262 Turbine PTFE Stirrer Shaft - 250ml Process Vessels
RR139192 Reflux Divider Kit with Vapour Temp Kit RR150502 Anchor PTFE Stirrer Shaft - 500ml Process Vessels
RR139154 250ml Receiver Flask 2 x B24 Socket, + B24 Cone and Tap RR150507 Retreat Curve PTFE Stirrer Shaft - 500ml Process Vessels
RR139324 500ml Receiver Flask 3 x B24 Socket, + B24 Cone and Tap RR150512 Turbine PTFE Stirrer Shaft - 500ml Process Vessels
RR139326 1000ml Receiver Flask 3 x B24 Socket, + B24 Cone and Tap RR151002 Anchor PTFE Stirrer Shaft - 1000ml Process Vessels
RR151007 Retreat Curve PTFE Stirrer Shaft - 1000ml Process Vessels
PTFE Pt100 Temperature Probes and Adapters RR151012 Turbine PTFE Stirrer Shaft - 1000ml Process Vessels
RR140250 Probe 8mm with LEMO Plug - 100ml, 250ml + 500ml Vessels RR152002 Anchor PTFE Stirrer Shaft - 2000ml Process Vessels
RR141000 Probe 9mm with LEMO Plug - 1000ml, 2000ml + 3000ml Vessels RR152007 Retreat Curve PTFE Stirrer Shaft - 2000ml Process Vessels
RR152012 Turbine PTFE Stirrer Shaft - 2000ml Process Vessels
RR145000 Probe 9mm with LEMO Plug - 5000ml Vessel RR153002 Anchor PTFE Stirrer Shaft - 3000ml Process Vessels
RR140010 PTFE Temperature Probe Adapter - 8mm RR153007 Retreat Curve PTFE Stirrer Shaft - 3000ml Process Vessels
RR140015 PTFE Temperature Probe Adapter - 9mm RR153012 Turbine PTFE Stirrer Shaft - 3000ml Process Vessels
RR155002 Anchor PTFE Stirrer Shaft - 5000ml Process Vessels
Reaction Vessel Support Collar RR155007 Retreat Curve PTFE Stirrer Shaft - 5000ml Process Vessels
RR121048 Vessel Support Collar RR155012 Turbine PTFE Stirrer Shaft - 5000ml Process Vessels

t: +44 1799 513320 f: +44 1799 513283 e: [email protected] www.radleys.com 15


AVA Lab Control Software - take control of your chemistry
Control multi-device jacketed reaction system
Multi-device reactions
• Control up to 4 reaction systems with up to 16 devices on one screen
• Create complex experiments with any number of steps in series or in parallel
• Pre-program multi-step recipe, with the flexibility to make and track on-the-fly adjustments
• Interlink devices and set feedback/control loops, end-point conditions and safety limits

No more manual data logging or manual errors


• Automatically record reaction parameters and log what you do, as you do it
• Repeat experiments accurately for reproducible and consistent results
• Create reports in a few clicks or export data as a CSV file for further analysis
• Share results between users to improve research and collaboration
Safe unattended chemistry
• Automate cooling during exothermic events
• Link devices such as balances and pumps for controlled, unattended reagent additions
• Define safety overrides and cut-off conditions
• Configure audio and visual alarms
Level 4
Data Hub
Data Hub Specifications
Using the Data Hub, AVA can control and log multiple
• 4 x RS232 ports
3rd party devices with RS232 serial interface.
• 2 x Pt100 temperature sensor ports
with LEMO connection
• 1 x Ethernet port
• 2 x Ethernet cables

AVA Software Kit includes:


• AVA Software Control and log reaction systems
with multiple devices
• Laptop controller
Pt100 Temp. RS232 • 4 Port data hub
Sensor Ports Serial Ports • 1 year AVA Care Support Control a variety of devices
AVA software includes a library of
AVA Care Support pre-configured driver files allowing
• Free support for 1st year easy integration with a wide range of
• Free priority email and telephone support 3rd party devices.
• Free set up and application support
• Free software updates during support period, keeping software current Radleys also provide a ‘New Driver
Configuration Service’ if required.
Download and try the software for FREE
Learn how AVA software works - try before you buy Download
• Simulate control of devices Free AVA
• Set up apparatus and control experimental Schedules Demo
m
• Share setups and schedules with other AVA users www.radleys.co
• Analyse results and create reports for real or simulated data
• Find out more about AVA Level 1-3 on our website

World leaders in innovative productivity tools for chemists


Radleys provides innovative chemistry equipment for safer, cleaner, greener and more productive
chemical research.

We have been manufacturing scientific glassware and laboratory instruments for over 50 years and
our customers include leading blue-chip industrial and academic research facilities around the world. Shire Hill, Saffron Walden,
Our areas of expertise are focused on equipment for chemical synthesis, process development, Essex, CB11 3AZ. United Kingdom.
t: +44 1799 513320
work-up and evaporation.
f: +44 1799 513283
Visit www.radleys.com to see our full range of chemistry productivity tools. e: [email protected]

© Radleys (R.B.Radley & Co Ltd) 2019

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