Lab Turbidity
Lab Turbidity
Lab Turbidity
This experiment consisted of measuring the turbidities of a variety of samples using the
nephelometer .These recorded turbidities were then analyzed and a reasonable explanation
for each value is made.
INTRODUCTION
Turbidity is the cloudiness or haziness of a fluid caused by large numbers of
individual particles that are generally invisible to the naked eye, similar to
smoke in air. The measurement of turbidity is a key test of water quality.
Turbidity is a measurement of how cloudy water appears. Technically, it is a
measure of how much light passes
through water, and it is caused by suspended solid particles that scatter
light. These particles may be microscopic plankton, stirred up sediment or
organic materials, eroded soil, clay, silt, sand, industrial waste, or sewage.
Bottom sediment may be stirred up by such actions as waves or currents,
bottom-feeding fish, people swimming, or wading, or storm runoff.
Clear water may appear cleaner than turbid water, but it is not necessarily
healthier. Water may be clear because it
has too little dissolved oxygen, too much acidity or too many contaminants
to support aquatic life. Water that is turbid
from plankton has both the food and oxygen to support fish and plant life.
However, high turbidity may be a symptom of
other water quality problems.
Experimental procedures
A. Jackson Turbidimeter
1. Place a clean Jackson turbidimeter tube in the receptacle on the stand.
Place a
candle in the device and insure that the spring in the candle holder is
released
and keeping the top of the candle at a distance of 7.6 cm below the bottom
of the
tube. If the water is relatively clean use the longer tube, otherwise use the
shorter
tube.
2. Add a small amount of well-mixed sample to the tube and light the candle.
Be
sure to add a small amount of sample BEFORE lighting the candle to prevent
cracking the tube.
3. Add well-mixed sample to the tube until the light field becomes uniform.
Note the
reading from the side of the calibrated tube.
4. Empty the tube. Extinguish the flame. Mix the sample again, add a few mL
to the
tube and light the candle. Then add ¾ of the volume of sample added in Step
3.
Then add sample slowly until a uniform light field is observed. Record the
reading
B. Nephelometer
1. Select a standard that compares with the turbidity of the sample. Turn on
the unit
and select the range corresponding to the standard. Insert the standard and
replace the cover. Adjust the calibration knob to provide the correct reading
on
the meter. Remove the standard.
2. Fill the sample tube about ¾ full of well-mixed sample and wipe the
outside of the
tube with Kimwipes if any spillage occurred. Insert the tube and replace the
cover. If the reading is offscale, switch the range of the meter until the
reading is
on scale. Record the reading and report it as NTU.
3. If the sample reading is significantly outside of the range in which the
meter was
calibrated, repeat the exercise calibrating with a standard in the appropriate
range.
Results
Turbidity:
The following data was collected during this experiment:
SAMPLE TURBIDITY(NTU)
Drinking water 1.2
Distilled water 0.8
coffee 78
CaCO3 Error(too high)
Sugar dissolved In water 55(should be between 0-1)
Sand + water 47.3
Soil + water 149
Silt + water 293
DISCUSSION AND CONCLUSION
A direct measurement of suspended solids is not usually performed on
samples from natural bodies of water or on potable water supplies. The
nature of the solids in these waters and the secondary effects they produce
are more important than the actual quantity. For such waters a test for
turbidity is commonly used.
Sand and water mixture gave less turbidity than that of silt and water which
is logical. Silt is a much smaller particle than sand and thus more surface
area for pollutants to settle exist leading to higher turbidity. On the other
hand, comparing coarse soil and fine sand we see that coarse soil and water
had a higher turbidity of 149, this result seems illogical because coarse soil
has a larger grain size than the fine sand, yet this result may be due to the
fact that coarse particles have more bumps and irregularities resulting in a
larger surface area. As for distilled and drinking water, the results obtained
are also logical and acceptable. Calcium carbonate gave an error implying
that the sample has a very high turbidity that cannot be measured using the
Nephelometer .To find the turbidity of this sample we should dilute it by a
known ratio, measure the turbidity of the diluted sample and deduce the
original’s turbidity.On the other hand, the cold coffee sample gave a turbidity
of 78NTU which is larger than that of water . When Coffee cools, its
solubility decreases and the coffee precipitates out to become a suspension,
and then cause that turbidity we found.
From our experiment we conclude that absorption and scattering and thus
turbidity are influenced by both size and surface characteristics of the
suspended material, and that turbidity is not a direct quantitative
measurement of suspended solids .For example a small pebble in a glass of
water would produce virtually no turbidity .If this pebble were crushed into a
thousand particles of colloidal size,a measurable turbidity would result even
though the mass of solids is still the same.
APPENDIX
1.decribed above
-Air bubbles inside the sample that can be only extracted through de-airing.
-The coffee and sugar samples are cold thus solubility is reduced and some
particles will settle leading to increased turbidity.
References
-Environmental engineering Peavey Row
http://www.water-research.net/index.php/stream-water-quality-importance-of-
total-suspended-solids-turbidity