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    Instrumentation Methods15-16 PDF

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    Tom Jerry
    This document outlines a course on instrumentation methods for chemical analysis. The course aims to teach students to classify instrumental techniques, select appropriate spectroscopy instruments to analyze samples, distinguish techniques like atomic absorption spectrometry and infrared spectrometry, and select chromatographic instrumentation to test samples. The course covers topics like absorption and emission spectroscopy, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas chromatography, high performance liquid chromatography, and chromatography principles.

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    Instrumentation Methods15-16 PDF

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    Tom Jerry
    95 views3 pages
    This document outlines a course on instrumentation methods for chemical analysis. The course aims to teach students to classify instrumental techniques, select appropriate spectroscopy instruments to analyze samples, distinguish techniques like atomic absorption spectrometry and infrared spectrometry, and select chromatographic instrumentation to test samples. The course covers topics like absorption and emission spectroscopy, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas chromatography, high performance liquid chromatography, and chromatography principles.

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    This document outlines a course on instrumentation methods for chemical analysis. The course aims to teach students to classify instrumental techniques, select appropriate spectroscopy instruments to analyze samples, distinguish techniques like atomic absorption spectrometry and infrared spectrometry, and select chromatographic instrumentation to test samples. The course covers topics like absorption and emission spectroscopy, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas chromatography, high performance liquid chromatography, and chromatography principles.

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    © All Rights Reserved
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    95 views3 pages

    Instrumentation Methods15-16 PDF

    Uploaded by

    Tom Jerry
    This document outlines a course on instrumentation methods for chemical analysis. The course aims to teach students to classify instrumental techniques, select appropriate spectroscopy instruments to analyze samples, distinguish techniques like atomic absorption spectrometry and infrared spectrometry, and select chromatographic instrumentation to test samples. The course covers topics like absorption and emission spectroscopy, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas chromatography, high performance liquid chromatography, and chromatography principles.

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    of 3

    20 Chemical Engineering

    INSTRUMENTATION METHODS FOR


    CHEMICAL ANALYSIS
    (Professional Elective-II)

    COURSE CODE:15CH1125 L T P C
    3 0 0 3
    COURSE OUTCOMES:
    At the end of the course the student shall be able to
    CO 1 Classify the instrumental techniques and interpret the signals.
    CO 2 Select the spectroscopy instruments and analyze the given
    sample.
    CO 3 Distinguish the Atomic Absorption Spectrometry and Infrared
    spectrometry.
    CO 4 Select the chromatographic instrumentation and test a given
    sample for project work.
    CO 5 Classify the chromatographic methods; identify the column
    efficiency and resolution.
    UNIT-I (10 LECTURES)
    AN INTRODUCTION TO INSTRUMENTAL METHODS:
    Terms Associated With Chemical Analysis, Classification Of
    Instrumental Techniques, A Review Of The Important Considerations
    In Analytical Methods, Basic Functions of Instrumentation, Important
    Considerations in Evaluating an Instrumental Method.
    MEASUREMENTS, SIGNALS AND DATA:
    Introduction, Signal-to-Noise Ratio, Sensitivity and Detection
    Methods, Source of Noise, Hardware Techniques for Signal-to-Noise
    Enhancement, Software Techniques for Signal-to-Noise Enhancement,
    Evaluation of Results, Accuracy and Instrument Calibration,
    Chemometrics.

    G V P College of Engineering (Autonomous) 2016


    Chemical Engineering 21

    UNIT-II (10 LECTURES)


    AN INTRODUCTION TO ABSORPTION AND EMISSION
    SPECTROSCOPY:
    The Nature of Electromagnetic Radiation, The Electromagnetic
    Spectrum, Atomic Energy Levels, Molecular Electronic Energy Levels,
    Vibrational Energy Levels, Raman Effect, Lasers, Nuclear Spin
    Behaviour, Electron Spin Behaviour.
    ULTRAVIOLET AND VISIBLE SPECTROMETRY-
    INSTRUMENTATION:
    Radiation Sources, Wave Length Selection, Cells and Sampling
    Devices, Detectors, Instruments for Absorption Photometry.
    ULTRAVIOLET AND VISIBLE ABSORPTION METHODS:
    Fundamental Laws of Photometry, Spectrophotometric Accuracy,
    Photometric Precision, Quantitative Methodology, Differential or
    Expanded-Scale Spectroscopy.
    UNIT-III (10 LECTURES)
    FLAME EMISSION AND ATOMIC ABSORPTION SPECTROSCOPY:
    Introduction, Instrumentation for Flame Spectrometric Methods, Flame
    Emission Spectrometry, Atomic Absorption Spectrometry, Interference
    Associated with Flame and Furnaces, Applications, Comparison of
    FES and AAS.
    INFRARED SPECTROMETRY:
    Correlation of Infrared Spectra with Molecular Structure,
    Instrumentation, Sample Handling.
    UNIT-IV (10 LECTURES)
    MASS SPECTROMETRY:
    Sample Flow in a Mass Spectrometer, Inlet Sample System, Ionization
    Methods in Mass Spectrometry, Mass Analyzers, Ion-Collection
    System, Vacuum System, Isotope- Ratio Spectrometry, Correlation
    of Mass Spectra With Molecular Structure.
    GAS CHROMATOGRAPHY:
    Gas Chromatographs, Derivative Formation, Gas Chromatographic
    Columns, Liquid Phases and Column Selection, Detectors for Gas
    G V P College of Engineering (Autonomous) 2016
    22 Chemical Engineering

    Chromatography.
    HIGH PERFORMANCE LIQUID CHROMATOGRAPHY:
    HPLC Instrumentation, Mobile-Phase Delivery System, Sample
    Introduction, Separation Columns, Detectors.
    X RAY DIFFRACTION:
    General Principles, Braggs equation, Laue photographic method,
    Rotating crystal method, Oscillating crystal method, Powder method,
    Interpretation of the Diffraction pattern, Applications of XRD.
    UNIT-V (10 LECTURES)
    CHROMATOGRAPHY: GENERAL PRINCIPLES:
    Classification of Chromatographic Methods, Chromatographic
    Behaviour of Solutes, Column Efficiency and Resolution, Column
    Processes and Band Broadening, Time of Analysis and Resolution,
    Quantitative Determinations.
    TEXT BOOKS:
    1. Willard,H.H, Merritt,L.L, Dean,J.A, and Settle, F.A,
    “Instrumental methods of analysis” CBS Publishers &
    Distributors, 7 Ed, 1986.
    REFERENCES:
    1. Srivastava. A.K. and. Jain, P.C, “Instrumental Approach to
    Chemical Analysis”, 4th Edition , S Chand and Company
    Ltd, New Delhi, 2012.
    2. Chatwal. G.R., Anand, Sham K., “Instrumental Methods of
    Chemical Analysis” 5th Edition, Himalaya Publishing House,
    2005.

    pqr

    G V P College of Engineering (Autonomous) 2016

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