Plant Operating Manual
Plant Operating Manual
Plant Operating Manual
For
Manufacturer
Specialty Process Equipment Corporation
6400 Hawes Road, Houston, TX 77396
Tel: 281-812-SPEC Fax: 281-852-SPEC
www.spec-pro.com
SPEC Job No. 08002
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PREFACE
THIS MANUAL SHOULD BE READ AND THOROUGHLY UNDERSTOOD BY THE
OPERATOR PRIOR TO ATTEMPTING TO OPERATE OR SERVICE THIS EQUIPMENT.
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Table of Contents
1 Purpose
2 Scope
3 General
4 Operating Philosophy
5 Instrumentation & Control Philosophy
6 Operating Guidelines
7 Health, Safety & Environment
8.1 Introduction
8.2 Process Description
8.3 Instrumentation
8.4 Start Up & Operation
8.5 Shut Down
9.1 Introduction
9.2 Process Description
9.3 Equipment Specifications
9.4 Instrumentation
9.5 Start Up
9.6 Shut Down
9.7 Pumps Startup
10.1 Introduction
10.2 Equipment Specifications
10.3 Instrumentation
10.4 Start Up
10.5 Shut Down
10.6 Trouble Shooting
10.7 Safety Precautions
11.1 Introduction
11.2 Equipment Specifications
11.3 Circulation Start Up
11.4 Shut Down
11.5 Trouble Shooting
12. Incinerator
12.1 Introduction
12.2 Start Up
12.3 Shut Down
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13. Instrument Air Package
13.1 Introduction
13.2 Instrumentation
13.3 Start Up
13.4 Shut Down
14.1 Introduction
14.2 Start Up
14.3 Shut Down
15.1 Introduction
15.2 Operating Limits
15.3 Start Up
15.4 Shut Down
16.1 Introduction
16.2 Instrumentation
17.1 Start up
17.2 Shut down
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1. PURPOSE
The purpose of this document is to provide guidelines to the operating staff for safe operation of the plant and the
associate equipment during Normal Operation, Emergency Operation or isolation for maintenance. Procedure
should be established to assure continued system integrity. The purpose is to follow safe operating practices,
identify potential hazards when the process is subjected to all known conditions. This would eliminate to greater
extent human error. Adverse consequences due to human factor related errors could result in personnel injury,
damage to equipment or environment.
2. SCOPE
This SOP applies to all activities of production, processing of gas, handling and treatment of produced water,
commissioning and decommissioning of line or equipment, chemicals used for processing and the employee
exposed to these chemical hazards, personnel protective equipment required to handle the chemicals.
3. GENERAL
Undesirable events could result in personnel injury, pollution or facility damage. Safety devices and procedures
should be used to prevent the propagation of undesirable events. The release of hydrocarbon is a factor in
virtually all threats to safety. Major objective of the safety system should be to prevent the release of hydrocarbon
from the process and to minimize the adverse effects.
Process facility is designed for safe operation in accordance to good engineering practice. However all safety
procedures should be strictly adhered to and followed.
Process safety system generally has two levels of protection to prevent or minimize the effects of equipment
failure. These two levels of safety are independent of and in addition to the control devices used in normal
process operation.
Process operation is a coordinated affair and information is necessary before attempting to start or commission
the equipment. Moreover proper sequence of operation should be followed.
Rule Of Thumb: If in doubt, never operate. Confirm and verify before attempting to start any operation.
4. OPERATING PHILOSOPHY
Controls are partly pneumatic and partly PLC based for equipment such as Amine, Gas dehydration and Metering
skid. Alarms are in the Control Room operation is manual and largely depends on the operator’s ability and
judgment. Aim of the process operation is to run the plant safely with minimum downtime, maximum
productivity and following the HSE policy of no accidents, no harm to people, and no damage to environment.
Universally human error is the primary cause of concern in process operation that could lead to loss of
containment such as abnormal release of hydrocarbon to the atmosphere and this could be reduced to greater
extent by imparting proper training, providing adequate controls and guidelines.
First level of Safety is the individual equipment alarms followed by shutdown due to process parameters upset.
Operator has to respond immediately and take corrective action. Equipment or vessel cannot be shut down from
control room.
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Ultimate level of Safety is the Emergency Shut Down (ESD). Total flow (IN and OUT) Gas is stopped. Blow
down valves open to depressurize.
There are ESD push buttons in the Control Room and Process area. However ESD should be activated by Shift In
charge / Lead Operator judging the criticality of the situation.
In case of spurious ESD, the plant is allowed to depressurize. The cause for the ESD is investigated/determined
with the help of I & E and upon getting the green signal, plant is re-started.
Controls are local and pneumatic; Alarms are digitally transmitted to Control Room. Timely response to act on
receiving the alarm could prevent unit shutdown.
Safer Plant design and instrumentation can prevent or minimize exposure of operator to hazards and should be
able to control/mitigate conditions arising from normal or abnormal operations.
Protective systems are the devices and controls which make a primary contribution to preventing, controlling or
mitigating abnormal condition and prevent hydrocarbon loss of containment.
Devices to prevent equipment design limits being exceeded (especially pressure ratings)
Haseeb Gas facility has manually adjusted controls for setting the basic process variables. Operators are
required to routinely survey and monitor the operations of all equipment.
6. OPERATING GUIDELINES
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Never ignite the burners of heating components unless they are thoroughly purged.
Know your plant thoroughly; it’s operating parameters and limitations.
If in doubt, do not operate. Seek advice.
Plan your major activities in daylight.
Ensure good house keeping.
Use proper PPE while handling/ filling chemicals (corrosion inhibitor). Avoid prolonged contact with crude
oil/Condensate (if any).
Non operational work require permit to work, working at height require safety harness, and venting and draining
require precaution against static charge.
Proper operation of the unit will result in efficient operation and reduce environmental excursions.
8.1 INTRODUCTION
The theory of separation depends on gravity settlement and density difference between the three phases (oil,
water & gas). The produced fluid stream, coming either directly from the producing well or from free water
knock-out vessel, enters the separator or hits the inlet diverter, where the initial bulk separation of the gas and
liquid takes place due to the change in momentum as shown in figure.
The mist extractor does further separation of the liquid and gas. Using the bucket and weir system separates the
oil and water. For proper separation to be achieved, proper retention time and surge volumes must be accounted
for using the varying differences. After oil & water the weir is fixed such that its level is set slightly below the
level of the oil bucket. This allows the oil to be collected in the oil bucket and water to flow under the bucket and
over the weir into the water compartments.
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8.2 PROCESS DESCRIPTION
Process Stream from the Haseeb well # 01 enters the separator from the upper side of the shell. This fluid
impinges on the deflector plate. Gas is released and travels through mesh across the upper zone and then through
a mist eliminator (demister pad) and exits from the top.
Liquid (oil and water) leaves from the bottom. A weir plate separates the oil/Condensate and water phase.
8.3 INSTRUMENTATION
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Shutdown Separator
Valve
8.4 START UP
9.1 INTRODUCTION
The most widely used for sweetening of natural gas are aqueous solutions of alkanolamines. They are generally
used for bulk removal of CO2 and H2S. A liquid physical solvent can be added to the amine to improve
selectivity.
The acid gas is fed into a scrubber to remove entrained water and liquid hydrocarbons. The gas enters the bottom
of absorption tower which is either a tray (for high flow rates). The sweet gas exits at the top of tower.
The regenerated amine (lean amine) enters at the top of this tower and the two streams are contacted counter
currently. In this tower, CO2 and H2S are absorbed with the chemical reaction into the amine phase.
The exit amine solution, loaded with CO2 and H2S, is called rich amine. This stream is flashed, filtered, and then
fed to the top of a stripper to recover the amine, and acid gases (CO2 and H2S) are stripped and exit at the top of
the tower. The refluxed water helps in steam stripping the rich amine solution. The regenerated amine (lean
amine) is recycled back to the top of the absorption tower.
Haseeb Well gas which is processed at SPEC Gas Processing Facility contains about 3 to 4 mole % Carbon
dioxide and 400 ppm H2S. Sales gas agreement dictates that CO2 content not to exceed 2 %, H2S 0.2 grain per
100 scf and total sulphur not more than 3.0 grain per 100 scf. This excess CO2 & H2S in the gas stream is
reduced by treating with Methyl Diethanol Amine in which CO2 and H2S is selectively absorbed. The Amine is
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then regenerated by stripping off CO2 and H2S in stripper column; CO2 and H2S are sent to incinerator instead
of releasing to atmosphere.
In the MDEA unit, the sour gas enters the absorber at the bottom and flows counter currently to MDEA solution.
The liquid entering at the top, the lean solution, passes down through the bubble cap trays absorbing H2S & CO2
from the gas stream thus producing sweet gas that exits the top. While rich solution (rich in acid gases) exits the
bottom of the tower.
The rich MDEA is regenerated for reuse in a closed system. It is flashed at low pressure in the flash drum thus
reducing its pressure to favor stripping. Preheated solution from lean/rich heat exchanger is fed to the top of the
stripper where heat is continuously supplied through a thermo siphon re-boiler. Low pressure and high
temperature help to strip out acid gases along with some entrained amine vapors which are then cooled in
overhead Amine reflux exchanger and returned to reflux accumulator beneath the stripper. Acid gases from the
accumulator are sent to Incinerator for burning. Lean MDEA is drawn from Reboiler bottom, and returned to the
contactor through lean/rich heat exchanger. This completes the cycle.
9.4 INSTRUMENTATION
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TAG
1. PSV-1100 Safety Relief Valve Safety Relief Valve Inlet Filter Separator
17. LC-1102 Level Controller Maintains the level of Rich Amine in Amine
Absorber
18. LCV-1102 Level Control Valve Controls the Level of Rich Amine in Amine
Absorber
19. LSH-1101 Level Switch High Sends alarming signals to PCS if Rich
Amine level is high from its normal level.
20. LSLL-1101 Level Switch Low Sends alarming signals to PCS if Rich
Low Amine level is very Low from its normal level.
21. PSDV-1100 Process Shutdown Shutdown valve at Amine absorber outlet
Valve
22. PI-1102 Pressure Indicator Indicates pressure at Amine Absorber Inlet
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A ,Set at 1100PSIG
28. PSV-1201 Safety Relief Valve Safety Relief Valve at Lean Amine Charge pump
B ,Set at 1100PSIG
29. TI-1200 Temperature Indicator Indicate temperature at Amine flash Tank
32. LC-1200 Level Control Valve Level controller at Amine flash tank
,Pneumatically control LCV-1300
33. PSV-1202 Safety Relief Valve Safety Relief Valve at Amine Flash Tank ,Set at
150PSIG
34. PCV-1200 Pressure Control Regulate back pressure at Amine Flash Tank inlet
Valve
35. PCV-1202 Pressure Control Regulate pressure at Amine Flash Tank Inlet
Valve
36. PSV-1300 Safety Relief Valve Safety Relief Valve at Amine Filter Outlet
40. PDI-1300 Differential Pressure Indicates differential pressure across Amine filter
Indicator
41. PSV-1301 Safety Relief Valve Safety Relief Valve at charcoal Filter Outlet
42. PSV-1302 Safety Relief Valve Safety Relief Valve at outlet of Lean Amine
Exchanger
43. TI-1303 Temperature Indicator Indicate temperature at lean amine exchanger outlet
44. LCV-1300 Level Control Valve Controls amine Level at inlet of Amine Stripper
45. PDI-1301 Differential Pressure Indicates differential pressure across Charcoal filter
Indicator
46. TI-1301 Temperature Indicator Indicates temperature at booster
pumps outlet
47. TI-1304 Temperature Indicator Indicates temperature at inlet of
exchanger coming from charcoal filter
48. TI-1306 Temperature Indicator Indicate temperature at line from
Amine Exchanger to Amine Stripper
49. PI-1400 Pressure Indicator Indicate pressure at inlet of amine
reflux exchanger
50. TI-1400 Temperature Indicator Indicate temperature at inlet of amine
reflux exchanger
51. TI-1401 Temperature Indicator Indicate pressure at outlet of amine reflux exchanger
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55. LSL-1400 Level Switch Low Send alarming signal to PLC if amine
level is low in the amine stripper
56. LG-1400 Level Gauge Level Indication in Amine stripper
57. PSV-1400 Pressure safety valve Ensure that pressure is not exceed
then 50psig at line from Amine
Reboiler to Amine stripper
58. PI-1402 Pressure Indicator Indicate pressure at reflux pump A Outlet
60. LCV-1400 Level control valve Control the level of amine in Amine Stripper
61. PCV-1401 Pressure control valve Pressure Regulator at fuel gas supply ,set at 10 PSIG
Fully open suction & discharge v/v of P-610 A/B and also open recycle valve
Open discharge PI bleeder to remove entrapped air
Start the pump
Gradually close recycle v/v to maintain flow (at FIT-1200) and check pressure at PI
Check for any abnormal sound, motor temperature, ampere and vibration
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Remove and discard the used cartridges and install new ones
Examine the shell gasket for deterioration. If it is warned replace it
Place spring seal assemblies and seal plate. Make sure that individual seal plates are positioned in the top
end of each cartridge and tighten down knob
Place the head. Be sure the edge of the head is aligned with the bottom flange. Position the cover clamp.
Replace the T- Bolt and tighten the clamp nut. A gap of about ½” should remain between clamp
ends.
Close drain valve
Open inlet valve slowly. Allow to vent to remain open until a steady stream of liquid comes out the vent
hole. Install vent plug. Check for leaks.
Filter is now ready for operation
10.1 INTRODUCTION
In Glycol Dehydration process, a liquid desiccant dehydrator serves to absorb water vapor from the gas
stream. Glycol, the principal agent in this process, has a chemical affinity for water. This means that,
when in contact with a stream of natural gas that contains water, glycol will serve to 'steal' the water out
of the gas stream.
The saturated TEG is circulated through a regeneration loop consisting of a flash drum, reboiler and
circulation pumps before reintroducing to the gas.
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10.2.1 GLYCOL DRAIN TANK
Reboiler Size 72” I.D * 20’ Fire Tube Size 18” * 16’
Operating Pressure 1 psig Operating Temperature 400 0F
MAWP int/ext 1 / 1.11 psig Design Pressure Atmospheric
0
Design temp. -20/500 F Capacity 4230 Gallons.
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Max Stroke / minute 28 Design pressure 1500Psig
10.3 INSTRUMENTATION
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S.NO INSTRUMENT DESCRIPTION FUNCTION
TAG
1. LSLL-1600 Level Switch Low Low Sends alarming signals to PLC if liquid level is
very Low in Glycol Contractor Scrubber from its
normal level
2. LG-1601 Level Gauge Glycol level indication in Glycol Contractor
13. DPI-1701/1702 Differential Pressure Differential Pressure Indication across Sock filter
Indicator
14. PSV-1700/1701 Pressure Safety Valve Ensures that the system is not over Pressured. Set
at 150 PSIG.
15. LG-1700 Level Gauge Glycol level indication in glycol Reboiler
17. TCV-1700 Temperature Control Regulate Temperature. Obtains signal from TC-
Valve 1700
18. TI- Temperature Indicates the Temperature at different points in
1700/1701/1702 Indicator Glycol Reboiler
19. BSL-1700 Burner Safety Low To detect the main burner flame.
10.4.2 HEATING
Gradually reduce flow of gas to the contactor but keep the system pressurized
Shutdown the reboiler burner
Gradually reduce the TEG unit pressure
Stop circulation of TEG
Depressurize TEG UNIT gradually
Drain the TEG level unit wise to the main TEG drain tank
10.6 TROUBLESHOOTING
10.6.1 OXIDATION
Oxygen enters the system with the incoming gas, through unblanketed tanks or through pump packing glands.
The Glycol will oxidize readily in the presence of oxygen and form corrosive organic acids. The primary acid
formed is formic acid although some acetic acid is also found to be present in oxidized glycols.
To prevent oxidation, tanks have been gas blanketed to keep air out of the system.
Oxidation inhibitors such as hydrazine can also be used to prevent corrosion.
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Excessive heat, a result of one of the following conditions, will decompose the glycol and form corrosive
compounds.
A reboiler temperature above the glycol decomposition level.
A high heat flux rate, usually caused by trying to operate the unit above the design capacity.
Localized overheating, caused by deposits of salt or tarry compounds on the reboiler fire tubes or poor flame
direction on the fire tubes.
Low acute chronic toxicity, skin and mucous irritation, TEG can produce irritation when in contact with
skin.
Before hand over of any equipment proper depressurization, flushing and electrical isolation to be done for
safety of personnel working on it.
Refer MSDS (material safety data sheets)
Personnel protective equipments should be used.
11 HEAT MEDIUM
11.1 INTRODUCTION
Alkyl Benzene Oil is used as heat medium for Amine reboiler and Sour water system. It is heated in helical coil
heater and pumped to the respective units.
11.3START UP
After the system is filled and the heater expansion tank is about ¼ full, allow the circulating pump to
circulate and manually bleed off any air at high points and water at any low points.
When air and water pockets are bled off, the hot oil level in the expansion tank should be approximately ¼
full. (This is normal cold fluid level)
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Heat medium fluid level should be sufficient in V-190 and there is oil level visible in the expansion tank
sight glass
Prepare line up of heat medium to amine reboiler and sour water stripper, keep pump discharge valve close
Prepare fuel gas supply line up to burner
Set regulator on fuel gas supply to expansion tank minimum 35 psig
Turn on the pump, prime if needed then slowly open the discharge valve if pressure drops then reprime the
pump.
Start the burner when cold circulation becomes stable
Allow burner to light and visually check flame pattern
As oil temperature rises and approaches set point, check to see that burner control switch shuts off burner
properly
11.4SHUT DOWN
11.5 TROUBLESHOOTING
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11.5.5 HEATER RUNNING BUT SMOKING
Black smoke – low fire: Too much fuel, increase air by opening bottom air damper on burner housing
Black smoke – high fire: Too much fuel, increase air by opening top air damper on burner housing
White smoke – low fire: Too much air, decrease air by closing bottom air damper on burner housing
White smoke – high fire: Too much air, decrease air by closing top air damper on burner housing
12 INCINERATOR
12.1 INTRODUCTION
12.1.1 WHAT IS INCINERATION?
Incineration is a that involves the combustion of waste at high temperatures. Incineration and other high
temperature waste treatment systems are described as "thermal treatment". Incineration of waste materials
converts the waste into heat, gases and particulates of combustion, and a smaller amount of solid residue (ash).
The gaseous and particulate emissions are dispersed of in the atmosphere.
12.2 START UP
12.2.1 PRE CHECKS
All isolating valves are closed
All logics should be reset.
Direction off all motors checked
All instruments should be in service
There should be no water level in V-1310, drain if any
Utilities (power, inst air, fuel gas) should be available
12.2.2 START UP
Open B-1300 inlet & outlet valves, Start B-1300 and purge I-1300
Now open PSDV-4300 and slowly pressurize the fuel gas circuit
Now ignite burner & increase temperature @ 50deg C /hour.
When temperature is increased to 500 ºF, we can now introduce sour gases to I-1300
Check level in fuel knock out pot after regular intervals and drain if any
Open all manual valves and PSDV-4302 and slowly introduce acid gases to I-1300
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Divert the acid gases to flare by opening the BDV-4300 and closing the PSDV-4302 downstream isolating
v/v gradually
After diverting, slowly bring down I-1300 stack temperature by reducing fuel gas flow
When temperature reduce to 475 F stop burner
Close PSDV-4300, and close all isolation valves
Check and drain V-1310
13.1 INTRODUCTION
The Instrument Air Package is designed to provide a reliable supply of clean, dry, oil free compressed air to the
pneumatic control system components.
The Instrument Air Package is designed to provide a reliable supply of clean, dry, oil free compressed air to the
pneumatic control system components. Air is compressed in the rotary screw compressor after which it moves to
the wet air receiver where wet particles are removed and a stream of dry air is supplied to utility air distribution
while a second stream is moved to the desiccant air dryer and dry air receiver. Clean and dry air is after passing
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from dry air receiver is supplied to instrument air distribution from where it is used in pneumatic control system
components.
13.2 INSTRUMENTATION
3. LG-4000 Level Gauge Indicates the level in the wet air receiver.
4. PSV-4000 Pressure Safety Valve Ensures that the wet air receiver is not over
pressure. Set at 200 PSIG.
5. LG-4000 Level Gauge Indicates the level in the dry air receiver.
6. PI-4003/4004 Pressure Indicator Indicates the pressure in the dessicant air dryer.
7. PI-4001/4002 Pressure Indicator Indicates the pressure at dessicant air dryer outlet.
8. PSV-4001/4002 Pressure Safety Valve Ensures that the dessicant air dryer is not over
pressure. Set at 200 PSIG.
9. UY-4000/UY-4001 Solenoid Valve Solenoid valve to switch between desiccants after
specific time duration
10. PI-4005 Pressure Indicator Indicates the pressure in the dry air receiver.
11. TI-4001 Temperature Indicator Indicates the Temperature in dry air receiver.
12. PI-4006 Pressure Indicator Indicates the pressure of the instrument air.
13. PSLL-4000 Pressure Switch Low Maintains the instrument air from low pressure
Low through sending alarming signals to PLC. Set at
80 PSIG
14. PSV-4003 Pressure Safety Valve Ensures that the dry air receiver is not over
pressure. Set at 200 PSIG.
15. PCV-4000 Pressure Control Control the pressure at dry air receiver outlet. Set
Valve at 100 PSIG.
13.3 START UP
All jobs are completed and work permits have been returned
All the instrumentation is in service
Check the main power breaker is on
Line up the compressor
Start the compressor
Check for any abnormal sound etc.
Check for auto cut in and cut off function of the compressor
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13.4 SHUT DOWN
14.1 INTRODUCTION
The flare system includes headers from all PSVs, PCVs and BDVs relief. A pilot for flare is available from the
main flare line. Flare system consist of a Flare Knock Out Drum V-130 having one pneumatic pump P-2100, Fuel
Gas supply and a continuous flare purge arrangement.
14.2 START UP
1.1 INTRODUCTION
Fuel gas to utilities is taken from the dry gas d/s of Glycol Contactor.
Utility Fuel Gas conditioning Vessel is V-180. High pressure gas is let down to 300 psig by a Regulator PCV-
4100 and pressure is again letdown to 100 psig with PCV-4101 before gas enters into the scrubber. Any liquid
condensation and entrainment is knocked off in the scrubber. The gas outlet is from the top of the scrubber,
passes through filter separator F-156 to knock out entrained liquid and goes to the distribution header.
Following utilities are fed from the fuel gas header:
Gas Generators
Pilot to the Flare
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Purge Gas to Flare Knock Out Drum
Blanketing gas to Amine, Sour water, Heat medium and glycol units
Fuel Gas To Reboiler (Regeneration Skid)
Fuel Gas to Heat medium, incinerator and glycol reboiler.
15.3 START UP
16 METERING SKID
16.1 INTRODUCTION
The Gas Metering Skid is designed to measure 60MMSCFD of natural gas at a pressure of 1200 PSIG. The
primary measurement elements are parallel orifice meters which meet AGA3 standard. Flow tantalization is by
three-pen chart recorder. In metering skid Gas Chromatograph is installed to take gas composition and then
transfer this data to Flow Computer for BTU and other Flow Calculations.
16.2 INSTRUMENTATION
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S.NO INSTRUMENT DESCRIPTION FUNCTION
TAG
1. BDV-2001 Blow Down Valve Depressurize plant in case of any emergency.
17 O
VE 2. TI-2000 Temperature Indicator Indicates temperature at metering skid Inlet
R
17.1 START UP
Check the SSSV pressure before its opening, if the pressure of SSSV is less than operating pressure; make
up the pressure hydraulically up to 7000 psi.
Check main Well head Control panel is in service according to its securities
Line up the X-MASS tree as follows
Open SSSV and SSV from the panel
Open Master valve, and then open the wing valve
Open the main flow isolation valve
Inform shift I/C at plant before opening the well
It is also important here to mention that if the well has been shut for long duration then in order to observe
any changes; log bottom hole pressure and well head shut in pressure on hourly basis
Always open well in burning pit for some time as there are chances of sludgy material coming out during off
loading of well. Observe for a couple of hours minimum.
Manager process/Process Engineer ensure that well is flowing smoothly in the burning pit i.e. no surges
observed
Gradually divert the well flow to plant by closing burning pit valve slowly
Divert well to plant at adjustable choke gradually from 8/64” up to 16/64 or 20/64 “ adj
Switch over the well from 20/64 adj to 20/64” fix choke for smooth operation of the well avoiding any back
pressure.
Process Engineer and S/I personally check and ensure the complete line up of the plant according to the
valve check list and equipment check list.
Install the chart at separator FPTR and at the custody transfer point(also zero check the FPTRs)
When the pressure of the fuel gas reaches up to 100 psi
Check the line up for the fuel gas for generator, and all the burners
Start the Gas Genset after its complete line up and levels of radiator water ,and lube oil
Start instrument air comp. Make up system pressure to 145 psi
Start the cooling water circulation
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Check all the instruments are working properly
Check all drain and vent valves are in close position
Purge the whole plant with nitrogen if available otherwise purging will be carried out with the sour gas
section wise up to the flare system; maintain the plant pressure up to 100 psi.
Gradually increase separator pressure up to 990 psi with the help of U/S PCV -600.
Gradually increase plant pressure up to 300 psi. Check for any leaks by foam leak test.
Repeat this step at 500 psi and at 700 psi
Finally pressurize the plant up to operating pressure i.e. 900 psi by gradually decreasing the flare
Now control and maintain this pressure by plant U/S PCV-600. Minimize flare so that minimum gas is
flared which is very important.
During plant pressurizing from 0-900psi; Shift in charge check all the securities related to the other
equipment.
After complete line up of Amine and TEG unit, once again check and ensure all valve positions of both units
Check and ensure that all vent and drain valves are in close position.
Start Amine unit circulation and establish level in Amine absorber, Flash tank and Reboiler.
Prepare heat medium line up of Amine reboiler and sour water system.
Start heat medium circulation pump and ignite the burner.
Gradually increase the temperature up to 350-400 0F.
Gradually increase reboiler temperature up to 240 to 250 F so that an equilibrium is attained b/w reboiler
outlet vapors and stripper column.
Start Incinerator (If needed)
Start TEG circulation and ignite the burner.
Gradually increase TEG temperature up to 380 F
Keep close monitoring of all levels and controls
When both the units TEG and Amine becomes smooth conduct the lab analysis for MDEA and TEG
For MDEA; conduct sample analysis for lean and rich amine for its color, appearance, strength, CO2 grains
per gallon, H2S grains /gallon and check for black particles if any.
For TEG; conduct sample analysis for specific gravity at 60 F, IBP, FBP, and check for its color.
After complete lab analysis Process Engineer and Shift In charge check and ensure that all the results are
within the limits..
Closely monitor GC analysis report (auto calibration) in control room
As Sweet Gas comes within Sales Gas Specifications, gradually divert it to SSGC by closing BDV by pass
v/v.
Periodically check and calculate flow on Sales Gas FPTR and check flow temperature and pressure on
FLOW BOSS as well
Co-ordinate with SSGC personnel for injection of Sales Gas to SSGC main header.
Log Sales Gas parameters.
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Complete this procedure of well shut in within 20 minutes
At the same time, gradually reduce temp of heat medium. Reduce temperatures of TEG and Amine to 150F.
Stop heat medium and TEG burners.
Stop Sales Gas to SSGC only when back pressure from SSGC header is observed
Close main isolation PCV-600 U/S Production Separator and PLANT OUTLET PCV-2000 at metering
station.
When Plant pressure reaches at 550 psig, depressurize all units slowly by opening their valves to main flare
header through BDV bypass valve.
When the pressure reaches up to 250-300 psi, drain liquids retained in the respective units to their unit wise
drains. S/I to check personally that each and every unit and line is properly and completely drained.
Stop heat medium circulation pump.
Stop the Amine charge pump followed by booster pump and TEG circulation pumps.
Stop the cooling water circulation.
S/I again check and ensure that all plant units have been completely depressurized & drained.
Isolate all units like separator, Amine unit, TEG unit, Incinerator, sour water system, hot oil system
Isolate fuel gas header and keep monitoring fuel gas pressure
Keep checking Generator load
When the plant and fuel gas pressure reaches to 40-50 psi, start Diesel Genset and Stop GAS Genset
Depressurize all the units up to 0 psi.
Isolate flare from main header and sale gas BDV bypass.
Wait for the flare to be lit off
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