Astm D 746 PDF

Designation: D 746 – 07
Standard Test Method for

Brittleness Temperature of Plastics and Elastomers by
Impact1
This standard is issued under the fixed designation D 746; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope* Point of Flexible Polymers and Coated Fabrics

1.1 This test method covers the determination of the tem- E 1 Specification for ASTM Liquid-in-Glass Thermometers
perature at which plastics and elastomers exhibit brittle failure E 77 Test Method for Inspection and Verification of Ther-
under specified impact conditions. Two routine inspection and mometers
acceptance procedures are also provided. E 608/E 608M Specification for Mineral-Insulated, Metal-
Sheathed Base Metal Thermocouples
NOTE 1—When testing rubbers for impact brittleness use Test Methods E 1137/E 1137M Specification for Industrial Platinum Re-
D 2137.
sistance Thermometers
1.2 The values stated in SI units are to be regarded as the 2.2 ISO Standard:
standard. ISO 974 (E) Plastics—Determination of the Brittleness
1.3 Due to the potential safety and environmental hazards Temperature by Impact3
associated with mercury-filled thermometers, the use of alter- 2.3 ASTM Adjuncts:
native temperature measuring devices (such as thermocouples Detailed Drawing of a Typical Clamp4
and RTDs) is encouraged.
1.4 This standard does not purport to address all of the 3. Terminology
safety concerns, if any, associated with its use. It is the 3.1 General—The definitions of plastics used in this test
responsibility of the user of this standard to establish appro- method are in accordance with Test Method D 883 unless
priate safety and health practices and determine the applica- otherwise specified.
bility of regulatory limitations prior to use. 3.2 brittleness temperature—that temperature, estimated
NOTE 2—This test method and ISO 974 (E) are technically equivalent statistically, at which 50 % of the specimens would probably
when using the Type B fixture and the Type III specimen, however, the fail.
minimum number of specimens that are required to be tested is signifi-
cantly different when using this test method. The ISO method requires that 4. Summary of Test Method
a minimum of 100 specimens be tested. 4.1 To determine the brittleness temperature, specimens are
secured to a specimen holder with a torque wrench. The
2. Referenced Documents
specimen holder is immersed in a bath containing a heat-
2.1 ASTM Standards: 2 transfer medium that is cooled. The specimens are struck at a
D 618 Practice for Conditioning Plastics for Testing specified linear speed and then examined. The brittleness
D 832 Practice for Rubber Conditioning For Low Tempera- temperature is defined as the temperature at which 50 % of the
ture Testing specimens fail.
D 883 Terminology Relating to Plastics
D 2137 Test Methods for Rubber Property—Brittleness 5. Significance and Use
5.1 This test method establishes the temperature at which
50 % of the specimens tested fail when subjected to the
1
This test method is under the jurisdiction of ASTM Committee D20 on Plastics conditions specified herein. The test provides for the evaluation
and is the direct responsibility of Subcommittee D20.30 on Thermal Proper-
ties.30.07).
Current edition approved March 1, 2007. Published March 2007. Originally
3
approved in 1943. Last previous edition approved in 2004 as D 746 - 04. ISO Standards Handbook 21, Vol 1. ISO Standards are available from
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York,
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM NY 10036.
4
Standards volume information, refer to the standard’s Document Summary page on A detailed drawing of a typical clamp may be obtained from ASTM Headquar-
the ASTM website. ters. Order Adjunct : ADJD0746.
*A Summary of Changes section appears at the end of this standard.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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Copyright ASTM International 1

Provided by IHS under license with ASTM Licensee=Federal Highway Administration /5962542001
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D 746 – 07
of long-time effects such as crystallization, or those effects that ing impact. The clearance between the outside of the striking
are introduced by low-temperature incompatibility of plasticiz- edge and the clamp shall be 2.0 6 0.1 mm at impact. These
ers in the material under test. Plastics and elastomers are used dimensional requirements of the striking edge and clamping
in many applications requiring low-temperature flexing with or device are illustrated in Fig. 3. Fig. 4 shows a typical clamp.
without impact. Use data obtained by this method to predict the Details of the specimen clamp are given in Fig. 5.
behavior of plastic and elastomeric materials at low tempera- 6.3 Torque Wrench, 0 to 8.5 N · m.
tures only in applications in which the conditions of deforma- NOTE 3—Because of the difference in geometry of the specimen
tion are similar to those specified in this test method. This test clamps, test results obtained when using the Type A specimen clamp and
method has been found useful for specification purposes, but striking member may not correlate with those results obtained when using
does not necessarily measure the lowest temperature at which the Type B apparatus.
the material is suitable for use. 6.4 Temperature-Measurement System—The temperature of
the heat-transfer medium shall be determined with a tempera-
6. Apparatus ture measuring device (for example, thermocouple, resistance
6.1 Type A: thermometer, or liquid-in-glass thermometer) having a suitable
6.1.1 Specimen Clamp and Striking Member—Design the range for the temperatures at which the determinations are to
specimen clamp to hold the specimen or specimens as a be made. The temperature-measuring device and the related
cantilever beam. Each individual specimen shall be firmly and readout equipment shall be accurate to at least 60.5°C. The
securely held in a separate clamp. The striking edge shall move temperature-measuring device shall be located as close to the
relative to the specimens at a linear speed of 2000 6 200 mm/s specimens as possible. Thermocouples shall conform to the
at impact and during at least the following 6.4 mm of travel. In requirements of Specification E 608/E 608M. Resistance tem-
order to maintain this speed on some instruments, it is perature devices shall comply with the requirements of Speci-
necessary to reduce the number of specimens tested at one fication E 1137/E 1137M. Liquid-in-glass thermometers, are
time. The distance between the center line of the striking edge described in Specification E 1. Use the thermometer appropri-
and the clamp shall be 7.87 6 0.25 mm at impact. The striking ate for the temperature range and accuracy required, and
edge shall have a radius of 1.6 6 0.1 mm. The striking arm and calibrate it for the appropriate immersion depth in accordance
specimen clamp shall have a clearance of 6.35 6 0.25 mm at with Test Method E 77.
and immediately following impact. These dimensional require- 6.5 Heat-Transfer Medium— Use any liquid heat transfer
ments are illustrated in Fig. 1. Fig. 2 shows a typical clamp.4 medium that remains fluid at the test temperature and does not
Use free-fitting clamping screws, 10-32 National Fine Thread. appreciably affect the material being tested. Measurement of
6.2 Type B: selected physical properties prior to and after 15-min exposure
6.2.1 Specimen Clamp and Striking Member—Design the at the highest temperature used will provide an indication of
specimen clamp to hold the specimen or specimens as a the inertness of a plastic to the heat transfer medium.
cantilever beam. Each individual specimen shall be firmly and 6.5.1 Where a flammable or toxic solvent is used as the
securely held in a separate clamp. The striking edge shall move cooling medium, follow customary precautions when handling
relative to the specimens at a linear speed of 2000 6 200 mm/s such materials. Methanol is the recommended heat transfer
at impact and during at least the following 5.0 mm of travel. In medium for rubber.
order to maintain this speed on some instruments, it is
NOTE 4—The following materials have been found suitable for use at
necessary to reduce the number of specimens tested at one
the indicated temperatures. When silicone oil is used, moisture from the
time. The radius of the lower jaw of the clamp shall be air will condense on the surface of the oil, causing slush to form. If slush
4.0 6 0.1 mm. The striking edge shall have a radius of collects on the temperature-measuring device as ice, it will affect
1.6 6 0.1 mm. The striking edge and specimen clamp shall temperature measurement. When this occurs, remove the ice from the
have a clearance of 3.6 6 0.1 mm at and immediately follow- temperature-measuring device.
Material Temperature, °C
5-mm2/s viscosity silicone oil −60
2
2-mm /s viscosity silicone oil −76
Methyl alcohol −90
6.6 Temperature Control—Suitable means (automatic or

manual) shall be provided for controlling the temperature of
the heat-transfer medium to within 60.5°C of the desired
value. Powdered solid carbon dioxide (dry ice) and liquid
nitrogen are recommended for lowering the temperature, and
an electric immersion heater for raising the temperature.
6.7 Tank, insulated.
6.8 Stirrer, to provide thorough circulation of the heat
transfer medium.
FIG. 1 Dimensional Requirements Between Specimen Clamp and NOTE 5—Suitable apparatus is commercially available from several
Striking Edge (Type A) suppliers. The striking member may be motor-driven, solenoid-operated,
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D 746 – 07
FIG. 2 Typical Clamp (Type A)
7.2 Type II (for Fixture Type A):

7.2.1 Geometry (Modified T-50 Specimen)—This type of
specimen shall be T-shaped, as illustrated in Fig. 6. When using
this type of specimen, clamp it so that the entire tab is inside
the jaws for a minimum distance of 3.18 mm.
7.2.2 Preparation— Specimens shall be 1.91 6 0.13 mm
thick. Specimens shall be die-punched, cut by hand using a
razor blade or other sharp tool, or cut by an automatic machine
from flat sheet, or prepared by injection molding.
7.3 Type III (for Fixture Type B):
7.3.1 Geometry—This type of specimen shall be
NOTE—Dimensions are in millimetres. 20.0 6 0.25 mm long by 2.5 6 0.05 mm wide and 1.6 6 0.1
FIG. 3 Dimensional Details of Striking Edge and Clamping mm thick as illustrated in Fig. 6.
Device, Type B (Positioning of Unnotched Test Specimen) 7.3.2 Preparation—Specimens shall be die-punched, cut by
hand using a razor blade or other sharp tool, or cut by an
automatic machine from flat sheet, or prepared by injection
molding.
7.4 Test results will vary according to molding conditions
and methods of specimen preparation. It is essential that
preparation methods produce uniform specimens. The pre-
ferred method of preparation is to use an automatic cutting
FIG. 4 Assembled Clamp with Test Specimens, Type B machine, however specimens that are punched using an arbor
press or hydraulically operated press are also acceptable. No
gravity-actuated, or spring-loaded. Equip the motor-driven tester with a matter which preparation method is employed, the specimen
safety interlock to prevent striker arm motion when the cover is open. edges shall be free of all flash. Specimens that are damaged in
any way shall be discarded. If specimens are to be die punched,
7. Test Specimen sharp dies must be used in the preparation of specimens for this
7.1 Type I (for Fixture Type A): test if reliable results are to be achieved. Careful maintenance
7.1.1 Geometry—This type of specimen shall be of die cutting edges is of extreme importance and is obtained
6.35 6 0.51 mm wide by 31.75 6 6.35 mm long as illustrated by daily lightly honing and touching up the cutting edges with
in Fig. 6. jewelers’ hard Arkansas honing stones. The condition of the
7.1.2 Preparation—Specimens shall be 1.91 6 0.13 mm die is judged by investigating the rupture point on any series of
thick. Specimens shall be die-punched, cut by hand using a broken specimens. When broken specimens are removed from
razor blade or other sharp tool, or cut by an automatic machine the clamps of the testing machine it is advantageous to pile
from flat sheet, or prepared by injection molding. these specimens and note if there is any tendency to break at or
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D 746 – 07
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NOTE—Dimensions are in millimetres.
FIG. 5 Details of One Form of Clamp Meeting the Requirements of 6.2
FIG. 6 Specimen Geometry
near the same portion of each specimen. Rupture points dull, nicked, or bent at that particular position, or that some
consistently at the same place are the indication that the die is other defect is present.

D 746 – 07
8. Conditioning impact and examined for cracks at the bend. Record the
8.1 Conditioning— Condition the test specimens at number of failures and the temperature at which they were
23 6 2°C and 50 6 5 % relative humidity for not less than 40 tested.
h prior to the test in accordance with Procedure A of Practice 9.7 Increase or decrease the temperature of the bath in
D 618 for those tests where conditioning is required. In cases uniform increments of 2 or 5°C and repeat the procedure until
of disagreement, the tolerances shall be 61°C and 62 % the lowest temperature at which none of the specimens fail and
relative humidity. the highest temperature at which all of the specimens fail is
8.2 Where long-time effects such as crystallization, incom- determined. A minimum of four tests shall be conducted in that
patibility, and so forth, of materials are to be studied, condition temperature range. New specimens are to be used for each test.
the test specimens in accordance with Practice D 832.
10. Routine Inspection and Acceptance
9. Procedure 10.1 Procedure A— For routine inspection of materials
9.1 In establishing the brittleness temperature of a material, received from an approved supplier, it shall be satisfactory to
it is recommended that the test be started at a temperature at accept lots on the basis of testing a minimum of ten specimens
which 50 % failure is expected. Test a minimum of ten at a specified temperature as stated in the relevant material
specimens at this temperature. If all of the specimens fail, specifications. Not more than five shall fail (see Section 9).
increase the temperature of the bath by 10°C and repeat the test 10.2 Procedure B— It shall be satisfactory to accept elas-
using new specimens. If none of the specimens fail, decrease tomeric composition on a basis of testing five specimens at a
the bath temperature by 10°C and repeat the test using new specified temperature, as stated in the relevant material speci-
specimens. If the approximate brittleness temperature is not fications. None shall fail.
known, select the start temperature arbitrarily.
9.2 Prior to beginning a test, prepare the bath and bring the 11. Calculation
apparatus to the desired starting temperature. If the bath is 11.1 Standard Method— Using the number of specimens
cooled using dry ice, place a suitable amount of powdered dry that failed, calculate the percentage of failures at each tem-
ice in the insulated tank and slowly add the heat-transfer perature. Calculate the brittleness temperature of the material
medium until the tank is filled to a level 30 to 50 mm from the as follows:
top. If the apparatus is equipped with a liquid nitrogen or CO2
Tb 5 T h 1 DT[~S/100! 2 ~1/2!#
cooling system and automatic temperature control, follow
instructions provided by the manufacturer of the instrument for where:
preparing and operating the bath. T b = brittleness temperature, °C,
9.3 Mount the test specimens firmly in the clamping device. Th = highest temperature at which failure of all the speci-
Secure the specimens with a torque wrench. To avoid excessive mens occurs (proper algebraic sign must be used),
deformation of the specimens, use a torque suitable for the °C,
material being tested. DT = temperature increment, °C, and
S = sum of the percentage of breaks at each temperature
NOTE 6—It is recommended that a clamping torque of 0.56 6 0.01
N · m (5 6 0.1 lb · in.) be used to mount the samples. If slippage of the
(from a temperature corresponding to no breaks
specimens in the clamp occurs, increase the torque the minimum amount down to and including Th). Derivations of the above
necessary to eliminate the slippage. formula are contained in other references.7,8
9.4 Mount the clamping device in the testing apparatus and NOTE 7—Example: The following example illustrates application of
lower the clamping device into the heat-transfer medium. If dry this formula:
ice is being used as a coolant, maintain constant temperature by Material—Plasticized poly(vinyl chloride)
the judicious addition of small quantities of dry ice. If the Number of Specimens Tested at Each Temperature—Ten.
apparatus is equipped with a liquid nitrogen or CO2 cooling At −30°C, 0 failed
system and automatic temperature control, follow the manu-
At −32°C, 2 failed
facturer’s instructions for setting and maintaining temperature.
9.5 After waiting for 3 6 0.5 min, record the temperature
and deliver a single impact to the specimens.
9.6 Remove the clamping device from the testing apparatus
and remove the individual specimens from the clamping At −40°C, 10 failed
device. Allow the specimens to warm up prior to being bent for At −42°C, 10 failed
inspection of cracks by leaving the specimens at room tem-
perature for 1 min or by placing them in lukewarm water for 10 Then: Th = −40°C
to 15 s. Examine each specimen to determine whether or not it DT = 2
has failed. Failure is defined as the division of a specimen into S = 0 + 20 + 30 + 60 + 80 + 100 = 290
two or more completely separated pieces or as any crack in the Since: Tb = Th + DT[(S/100) − (1/2)]
specimen which is visible to the unaided eye. Where a Then: Tb = −40 + 4.8 = −35.2°C
specimen has not completely separated, it shall be bent to an
angle of 90° in the same direction as the bend caused by the Brittleness temperature, reported as −35°C.
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D 746 – 07
11.2 Alternative Graphic Method—The value reported by 12.1.5 Torque used to secure the specimens,
this graphic method is essentially the same as that calculated by 12.1.6 Brittleness temperature to the nearest 1°C,
the standard method described in 11.1, but is obtained without 12.1.7 Type of test apparatus and heat-transfer medium
determining either the highest temperature at which all speci- used,
mens fail or the lowest at which all pass the test. When testing 12.1.8 Method of calculation, and
materials that possess a wide temperature range of brittleness 12.1.9 Date of test.
transition, the graphic method also requires the testing of fewer 12.2 For routine inspection and acceptance testing only, the
sets of samples to determine the brittleness temperature. Select following shall be recorded instead of 12.1.6 and 12.1.8:
sets of ten specimens each in which both failures and nonfail- 12.2.1 Number of specimens tested,
ures occur at four or more temperatures. Choose temperatures 12.2.2 Temperature of test, and
above and below the estimated 50 % failure point. Plot the data 12.2.3 Number of failures.
on probability graph paper with temperature on the linear scale 5
and percent failure on the probability scale. Select the tem- 13. Precision and Bias
perature scale so that it represents a minimum of two divisions TABLE 1 Precision and Bias Data
for each degree. Draw the best fitting straight line through Materials Average Sr SR r R
these points. The temperature indicated at the intersection of #1 Injection Molded PP −8.5 0.67 1.90 1.89 5.33
the data line with the 50 % probability line shall be reported as #2 Injection Molded PP −31.9 1.11 4.33 3.11 12.12
#3 Die Cut PE −35.1 2.22 9.03 6.22 25.28
the brittleness temperature, T b. Where there is a question of
conformance to the relevant material specification, the value
obtained according to 11.1 shall be accepted as the Tb value.
13.1 Precision— Table 1 is based on a round-robin test
NOTE 8—The graphic method applied to the data from the example in conducted in 1997 involving three materials and nine labora-
Note 7 is shown in Fig. 7. The brittleness temperature, Tb, estimated to the tories. Each laboratory made two determinations on each
nearest degree is −35°C. material. This study has been submitted to ASTM to be filed as
12. Report a research report.
13.1.1 Sr is the within-laboratory standard deviation of the
12.1 Report the following information:
average; r = 2.8 Sr. (See 13.1.3 for application of r.)
12.1.1 Reference to this test method,
13.1.2 SR is the between-laboratory standard deviation of
12.1.2 Complete identification of the material tested, includ-
the average; R = 2.8 SR. (See 13.1.4 for application of R.)
ing type, source, manufacturer’s code designation, form in
13.1.3 Repeatability— In comparing two test results for the
which supplied, and previous history,
same material, obtained by the same operator using the same
12.1.3 Specimen type, dimensions, and method of prepara-
equipment on the same day, those test results are to be judged
tion,
not equivalent if they differ by more than the r value for the
12.1.4 Specimen conditioning methods, if any, including
material and condition.
time elapsed since molding or annealing,
13.1.4 Reproducibility— In comparing two test results for
the same material, obtained by different operators using differ-
ent equipment on different days, those test results are to be
judged not equivalent if they differ by more than the R value
for the material and condition. (This applies between different
laboratories or between different equipment within the same
laboratory.)
13.1.5 Any judgement in accordance with 13.1.3 and 13.1.4
will have an approximate 95 % (0.95) probability of being
correct.
13.2 Bias—There are no recognized standards on which to
base an estimate of bias for this test method.
14. Keywords
14.1 brittle failure; brittleness temperature; elastomer; im-
pact plastics
FIG. 7 Graphic Method for Determining the Tb Brittleness 5

Supporting data have been filed at ASTM International Headquarters and may
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Temperature be obtained by requesting Research Report RR: D20–1228.

D 746 – 07
APPENDIXES
(Nonmandatory Information)
X1. STRIKER MECHANISM VELOCITY CALIBRATION FOR THE SOLENOID-ACTUATED BRITTLENESS TESTER
X1.1 Calibration is accomplished by measuring the height,

h, to which a steel ball, suspended on the striker mechanism of
the tester, rises after the striker has had its upward motion
halted by contact with a mechanical stop. The ball is acceler-
ated in such a manner that the law governing a freely falling
body applies. The velocity, v, of the striker is readily calculated
from the following expression:
v5=2gh
X1.2 Securing Ball Support—Remove either one of the

nuts that fasten the striking bar guide rods to the solenoid
armature yoke. Place the small hole of the ball support (Fig.
X1.1) over the guide rod and replace and secure the nut.
FIG. X1.2 Rubber Bumper
X1.3 Adjusting Stroke of Striker—Remove the metal guard
from around the solenoid. Spread open the rubber bumper (Fig. upward flight of the ball is independent of the mass of the ball.
X1.2) and insert it around the armature. Replace the solenoid However, if the mass is too large, the motion of the striker bar
guard. Insert a typical rubber or plastic specimen into the will be impeded.) Clamp a glass or clear plastic tube with a
specimen holder of the tester. Raise the striking mechanism by minimum inside diameter of 25.4 mm in a vertical position
hand until the end of the stroke is reached. It is essential that, directly over the ball. The tube contains a scale divided into
with the striking mechanism raised to its maximum height, the 5-mm intervals. Align the zero position on the scale with the
striker bar of the tester be in contact with the specimen but that top of the ball when the ball is at the top of the stroke of the
the bar not be in the plane of the specimen. If the striker bar is striker mechanism.
not in contact with the specimen, the rubber bumper must be
removed and replaced by a thinner bumper. Conversely, if the X1.5 Measurement and Calculation—With the tester
striker bar moves into the plane of the specimen, the bumper equipped as described above and devoid of test specimens and
must be replaced by a thicker one. immersion medium, fire the solenoid and read the ball height to
the closest 5 mm. Make at least five measurements. Average all
X1.4 Placement of Ball and Measuring Tube—Place a results and convert the average to metres. Determine the striker
19-mm diameter steel ball on the ball holder. (In theory, the velocity, v, from the following equation:
v 5 =2gh
where:
v = velocity, m/s,
g = 9.8 m/s2, and
h = average ball height, m.
NOTE X1.1—Calibration measurements are to be made with the tester
supported on a nonresilient surface, such as a laboratory bench or concrete
floor. Resilient mountings tend to absorb some of the striker energy
FIG. X1.1 Ball Support causing low ball height values.
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D 746 – 07
X2. STRIKER MECHANISM VELOCITY CALIBRATION FOR THE SOLENOID-ACTUATED BRITTLENESS TESTER
DURING ACTUAL TESTING
X2.1 With the tester equipped with ball support, ball, and X2.3.1 Using the procedure of Appendix X1, the striker
measuring tube (see Appendix X1), but without the rubber velocity at point of impact of a tester devoid of test specimens
bumper (tester in normal operating condition) and devoid of and immersion medium was found to be 1.9 m/s. This velocity
test specimens and immersion medium, fire the solenoid and is within the specified limits of 5.1.1.
read the ball height to the closest 5 mm. Make ten measure- X2.3.2 Using the procedure of X2.1, with the tester devoid
ments. From the lowest and highest ball height readings, of test specimens and immersion medium, the range of striker
determine the range in striker velocity, using the equation in velocity at the top of the stroke was found to be 2.5 to 2.7 m/s.
X1.5. This range is termed “range of velocity at the top of the This range becomes the acceptable range for this series of tests.
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stroke.” The acceptable ranges shall be established each time the striker
X2.2 With the tester equipped as described in X2.1, but also velocity at point of impact is determined (see Appendix X1).
with test specimen(s) and immersion medium, conduct the X2.3.3 Using the procedure of X2.2, with the tester con-
brittleness test as outlined in Section 9. Read the ball height taining a test specimen(s) and immersion medium, the velocity
each time the solenoid is fired. Convert the ball height to at the top of the stroke during the first solenoid firing was found
velocity as shown in X1.5. If the velocity lies within the to be 2.5 m/s. This velocity was within the acceptable range
predetermined range of velocity at the top of the stroke, the test and the test was valid.
shall be considered valid. If the speed lies outside of the X2.3.4 The velocity at the top of the stroke during the
predetermined range, the test shall be invalid and shall not be second and third solenoid firings were found to be 2.4 and 2.3
reported. If successive tests are found to be invalid, adjust- m/s, respectively. These velocities are outside of the acceptable
ments shall be made to bring the velocity at the top of the range and both tests are invalid.
stroke within the acceptable, predetermined range. This is
X2.3.5 Adjustments were made to increase the velocity at
accomplished by reducing the number of specimens tested per
the top of the stroke, using the procedures given in X2.2.
impact or by changing from Type A to Type B specimens.
X2.3.6 The speeds at the top of the stroke during the fourth
X2.3 The following example typifies the entire velocity and all subsequent solenoid firings were found to lie between
calibration procedure for solenoid-actuated testers: 2.5 and 2.7 m/s. The results of all these tests were valid.
SUMMARY OF CHANGES
Committee D20 has identified the location of selected changes to this standard since the last issue (D 746 - 04)
that may impact the use of this standard. (March 1, 2007)
(1) Added 1.3. (3) Moved Note 5 into the Apparatus section.
(2) Revised standard references in 2.1 and deleted date refer- (4) Revised 6.4 and deleted old Note 5.
ences for the ISO standard in 2.2. (5) Revised example calculation in 11.1.

D 746 – 07
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Designation: D 746 – 07

Standard Test Method for

1. Scope* Point of Flexible Polymers and Coated Fabrics

*A Summary of Changes section appears at the end of this standard.

Copyright ASTM International 1

6.6 Temperature Control—Suitable means (automatic or

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FIG. 2 Typical Clamp (Type A)

7.2 Type II (for Fixture Type A):

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FIG. 6 Specimen Geometry

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FIG. 7 Graphic Method for Determining the Tb Brittleness 5

Temperature be obtained by requesting Research Report RR: D20–1228.

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X1.1 Calibration is accomplished by measuring the height,

X1.2 Securing Ball Support—Remove either one of the

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