Kwame Nkrumah University of Science and Technology Department of Petroleum Engineering Petroleum Engineering Lab Pete

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KWAME NKRUMAH UNIVERSITY OF SCIENCE AND TECHNOLOGY

DEPARTMENT OF PETROLEUM ENGINEERING

PETROLEUM ENGINEERING LAB PETE (375)

FLUID PROPERTIES LAB

NAME: ANTHONY AMEYAW DAMOAH ADJEI

INDEX: 6910516

EXPERIMENT NO: 3

DEMONSTRATOR: EMMANUEL APPIAH DANKWAH


TILE: THE EFFECT OF TEMPERATURE ON VISCOSITY IN FLUIDS

TABLE OF CONTENTS
AIMS AND OBJECTIVES .................................................................................. 3

INTRODUCTION .............................................. Error! Bookmark not defined.

APPARATUS ....................................................................................................... 3

PROCEDURE ....................................................................................................... 4

OBSERVATIONS AND DATA .......................................................................4-6

TABLE OF RESULTS…………………………………………………………..6

DISCUSSIONS .................................................................................................. 10

ERROR ANALYSIS............................................................................................. 7

PRECAUTIONS ................................................................................................... 7

CONCLUSIONS ................................................................................................... 8

REFERENCES...................................................................................................... 8
AIMS AND OBJECTIVES

1. To examine the effect of viscosity on fluids

INTRODUCTION

This experiment talks about the viscosity of fluids. Viscosity is a


quantitative measure of a fluid’s resistance to flow. Viscosity is an important
physical property that controls the flow of fluids through porous media and pipes.
Viscosity affects the flow of fluids. High viscous fluids would take a long time to
flow and low viscous fluids would take a shorter time to flow from one point to
another.

Viscosity of fluids are affected by two main factors. They are temperature
and pressure. An increase in temperature would cause a decrease in viscosity.
When the temperature of a fluid is increased, the molecules gain more kinetic
energy and move apart. This increases the bond length and in turn decreases the
bond strength. Therefore, the viscosity is decreased.

An increase in pressure would cause an increase in viscosity and vice versa.


When the pressure of a fluid is increased, the volume is decreased and this would
bring the molecules together, thereby decreasing the bond length and hence,
increases the bond strength.

APPARATUS

1. Viscometer
2. Water bath
3. Pycnometer
4. Stop watch
5. Mass Balance
MATERIALS
1. Lube 2. Diesel
PROCEDURE

1. The lube and Diesel was weighed on a mass balance and their masses were
recorded.
2. The volume of the pycnometer was noticed and recorded.
3. The mass of the empty pycnometer was weighed and recorded.
4. The empty pycnometer was filled with lube and weighed with a mass balance
and its mass was recorded.
5. Another pycnometer was filled Diesel and weighed with a mass balance and
its mass was recorded.
6. The reservoir of two different viscometers was filled with lube and Diesel.
7. The viscometers are put into a water bath and heated to 100 and 40 degree
Celsius for a period of time.
8. The fluid was then sucked into the bulb A and the sucker was released for the
fluid to flow pass the mark and the time taken was recorded.

OBSERVATIONS AND DATA

LUBE

Volume of pycnometer = 10.223 cm3

Mass of empty pycnometer = 16.132g

Mass of filled pycnometer = 24.782g

Density=mass/volume= 0.846g/cm^3
Viscometer serial number= 350371P

Constant at 40 degree Celsius= 0.4705mm^2/s^2

Constant at 100 degree Celsius= 0.4683 mm^2/s^2

Efflux time after 10 minutes at 40 degree Celsius = 12.13s

Efflux time after 15 minutes at 100 degree Celsius= 4.61s

Kinematic viscosity=efflux time x constant

Kinematic viscosity at 40 degree Celsius

= 12.13*0.4705*10^(-6)=5.70*10^(-6)m^2/s

Absolute viscosity at 40 degree Celsius

=v*p=5.70*10^(-6)*846=4.822*10^(-3) N-s/m2

Kinematic viscosity at 100 degree Celsius

=4.61*0.4683*10^(-6)=2.159*10^(-6)m^2/s

Absolute viscosity at 100 degree Celsius

=v*p=2.159*10^(-6)*846=1.826*10^(-3)N-s/m^2

DIESEL

Volume of empty pycnometer = 9.838 cm3

Mass of empty pycnometer = 16.916g

Mass of filled pycnometer = 25.068 g

Viscometer Serial number= 200412S

Constant at 40 degree Celsius= 0.1092mm^2/s^2

Constant at 100 degree Celsius= 0.1088mm^2/s^2

Efflux time after 10 minutes at 40 degree Celsius= 31.19s


Efflux time after 15 minutes at 100 degree Celsius= 12.20s

Density = 8.152/9.838=0.829g/cm3

Kinematic viscosity at 40 degree Celsius

= 31.9*0.1092*10^ (-6) =3.484*10^ (-6) m^2/s

Absolute viscosity at 40 degree Celsius

=v*p= 3.484*10^(-6)*829=2.89*10^(-3)N-s/m^2

Kinematic viscosity at 100 degree Celsius

=12.20*0.1088*10^(-6)=1.327*10^(-6)m^2/s

Absolute viscosity at 100 degree Celsius

=v*p=1.327*10^(-6)*829=1.1*10^(-3)N-s/m^2

TABLE OF RESULTS

Table for the determination of density

Volume of Mass of Mass of Mass of Density


empty empty filled fluid g/cm3
pycnometer / pycnometer pycnometer /g
cm3 /g /g
Lube 10.223 16.132 24.782 8.65 0.846
Diesel 9.838 16.916 25.068 8.152 0.829

Table for the determination of efflux time

Fluid Temperature / degree Efflux time / seconds


Celsius
Lube 40 12.13
100 4.61
Diesel 40 31.19
100 12.20

DISCUSSIONS

In the experiment, the fluids were heated to 100 degree Celsius and 40
degree Celsius. From the experiment, it could be seen that the efflux time of the
fluids at 100 degree Celsius is lower than that of 40 degree Celsius. This is
observed because at 100 degree Celsius, the molecules gained more kinetic
energy than molecules of the fluids at 40 degree Celsius. The fluid molecules at
100 degree Celsius moved farther apart thereby reducing the bond strength and
this caused a decrease in viscosity. When the viscosity of a fluid is decreased, it
takes it a relatively smaller time to flow.

The efflux time of diesel at 40 degree Celsius was higher than that of the
lube because the diesel is more viscous than lube and that was why it took it a
relatively more time to flow to reach the mark.

From the density table, it could be observed that lube had a density greater
than that of diesel.

ERROR OF ANALYSIS

1. Some of the fluids were lost when heated.


2. Errors due to parallax were made when ensuring that the meniscus of the
fluid was on the mark

PRECAUTIONS

1. It was ensured the mass balance was zeroed before weighing the
pycnometer.
2. It was ensured that the filled pycnometer was wiped of excess fluids around
it so that they do not add to the mass of the pycnometer.
3. It was ensured that the fluid samples were not contaminated.
4. It was ensured two different viscometer were used for the two diesels

CONCLUSIONS

From the experiment, it can be concluded that viscosity is dependent on


temperature and that an increase in temperature would cause a decrease in
viscosity. Also, it can be concluded that a lube is denser than diesel.

REFERENCES

1. Amyx, J.M., Bass, D.M., Whiting, R., 1960. Petroleum Reservoir


Engineering — Physical Properties. McGraw-Hill, pp 459-461.
2. Beggs, H.D., Robinson, J.R., 1975. Estimating the viscosity of crude oil
systems. J. Pet. Technol. 27 (9), pp 1140–1141.
3. Craft, B., Hawkins, M., 1959. Applied Petroleum Reservoir Engineering.
Prentice-Hall, Englewood Cliffs, pp 115-118.

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