This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles

for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Designation: C117 17

Standard Test Method for

Materials Finer than 75-m (No. 200) Sieve in Mineral
Aggregates by Washing1
This standard is issued under the fixed designation C117; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon () indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.

1. Scope* 2. Referenced Documents

1.1 This test method covers the determination of the amount 2.1 ASTM Standards:2
of material finer than a 75-m (No. 200) sieve in aggregate by C136 Test Method for Sieve Analysis of Fine and Coarse
washing. Clay particles and other aggregate particles that are Aggregates
dispersed by the wash water, as well as water-soluble materials, C670 Practice for Preparing Precision and Bias Statements
will be removed from the aggregate during the test. for Test Methods for Construction Materials
C702 Practice for Reducing Samples of Aggregate to Testing
1.2 Two procedures are included, one using only water for
Size
the washing operation, and the other including a wetting agent
D75 Practice for Sampling Aggregates
to assist the loosening of the material finer than the 75-m (No.
E11 Specification for Woven Wire Test Sieve Cloth and Test
200) sieve from the coarser material. Unless otherwise
Sieves
specified, Procedure A (water only) shall be used.
2.2 AASHTO Standard:
1.3 The values stated in SI units are to be regarded as the T11 Method of Test for Amount of Material Finer than
standard. No other units of measurement are included in this 0.075-mm Sieve in Aggregate3
standard.
1.4 The text of this standard references notes and footnotes 3. Summary of Test Method
which provide explanatory material. These notes and footnotes 3.1 A sample of the aggregate is washed in a prescribed
(excluding those in tables and figures) shall not be considered manner, using either plain water or water containing a wetting
as requirements of the standard. agent, as specified. The decanted wash water, containing
1.5 This standard does not purport to address all of the suspended and dissolved material, is passed through a 75-m
safety concerns, if any, associated with its use. It is the (No. 200) sieve. The loss in mass resulting from the wash
responsibility of the user of this standard to establish appro- treatment is calculated as mass percent of the original sample
priate safety and health practices and determine the applica- and is reported as the percentage of material finer than a 75-m
bility of regulatory limitations prior to use. (No. 200) sieve by washing.
1.6 This international standard was developed in accor- 4. Significance and Use
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the 4.1 Material finer than the 75-m (No. 200) sieve can be
Development of International Standards, Guides and Recom- separated from larger particles much more efficiently and
mendations issued by the World Trade Organization Technical completely by wet sieving than through the use of dry sieving.
Barriers to Trade (TBT) Committee. Therefore, when accurate determinations of material finer than
75 m in fine or coarse aggregate are desired, this test method

1 2
This test method is under the jurisdiction of ASTM Committee C09 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Concrete and Concrete Aggregatesand is the direct responsibility of Subcommittee contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
C09.20 on Aggregates. Standards volume information, refer to the standards Document Summary page on
Current edition approved Aug. 1, 2017. Published August 2017. Originally the ASTM website.
3
approved in 1935. Last previous edition approved in 2013 as C117 13. DOI: Available from American Association of State Highway and Transportation
10.1520/C0117-17. Officials (AASHTO), 444 N. Capitol St., NW, Suite 249, Washington, DC 20001.

*A Summary of Changes section appears at the end of this standard

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 C117 17
is used on the sample prior to dry sieving in accordance with
Test Method C136. The results of this test method are included A
Based on sieve sizes meeting Specification E11.
in the calculation in Test Method C136, and the total amount of
material finer than 75 m by washing, plus that obtained by dry 7. Selection of Procedure
sieving the same sample, is reported with the results of Test 7.1 Procedure A shall be used, unless otherwise specified by
Method C136. Usually, the additional amount of material finer the Specification with which the test results are to be
than 75 m obtained in the dry sieving process is a small compared, or when directed by the agency for which the work
amount. If it is large, the efficiency of the washing operation is performed.
should be checked. It could also be an indication of degrada-
tion of the aggregate. 8. Procedure AWashing with Plain Water
4.2 Plain water is adequate to separate the material finer 8.1 Dry the test sample in the oven to constant mass at a
than 75 m from the coarser material with most aggregates. In temperature of 110 6 5C. Determine the mass to the nearest
some cases, the finer material is adhering to the larger particles, 0.1 % of the mass of the test sample.
such as some clay coatings and coatings on aggregates that
have been extracted from bituminous mixtures. In these cases, 8.2 If the applicable specification requires that the amount
the fine material will be separated more readily with a wetting passing the 75-m (No. 200) sieve shall be determined on a
agent in the water. portion of the sample passing a sieve smaller than the nominal
maximum size of the aggregate, separate the sample on the
5. Apparatus and Materials designated sieve and determine the mass of the material
passing the designated sieve to 0.1 % of the mass of this
5.1 BalanceA balance or scale readable and accurate to
portion of the test sample. Use this mass as the original dry
0.1 g or 0.1 % of the test load, whichever is greater, at any
mass of the test sample in 10.1.
point within the range of use.
NOTE 2Some specifications for aggregates with a nominal maximum
5.2 SievesA nest of two sieves, the lower being a 75-m size of 50 mm or greater, for example, provide a limit for material passing
(No. 200) sieve and the upper a 1.18-mm (No. 16) sieve, both the 75-m (No. 200) sieve determined on that portion of the sample
conforming to the requirements of Specification E11. passing the 25.0-mm sieve. Such procedures are necessary since it is
impractical to wash samples of the size required when the same test
5.3 ContainerA pan or vessel of a size sufficient to sample is to be used for sieve analysis by Test Method C136.
contain the sample covered with water and to permit vigorous
agitation without loss of any part of the sample or water. 8.3 After drying and determining the mass, place the test
sample in the container and add sufficient water to cover it. No
5.4 OvenAn oven of sufficient size, capable of maintain- detergent, dispersing agent, or other substance shall be added
ing a uniform temperature of 110 6 5C. to the water. Agitate the sample with sufficient vigor to result
5.5 Wetting AgentAny dispersing agent, such as liquid in complete separation of all particles finer than the 75-m (No.
dishwashing detergents, that will promote separation of the fine 200) sieve from the coarser particles, and to bring the fine
materials. material into suspension. Immediately pour the wash water

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containing the suspended and dissolved solids over the nested
NOTE 1The use of a mechanical apparatus to perform the washing
operation is not precluded, provided the results are consistent with those sieves, arranged with the coarser sieve on top. Take care to
obtained using manual operations. The use of some mechanical washing avoid, as much as feasible, the decantation of coarser particles
equipment with some samples may cause degradation of the sample. of the sample.
6. Sampling 8.4 Add a second charge of water to the sample in the
container, agitate, and decant as before. Repeat this operation
6.1 Sample the aggregate in accordance with Practice D75. until the wash water is clear.
If the same test sample is to be tested for sieve analysis
according to Test Method C136, comply with the applicable NOTE 3If mechanical washing equipment is used, the charging of
requirements of that test method. water, agitating, and decanting may be a continuous operation.

6.2 Thoroughly mix the sample of aggregate to be tested 8.5 Return all material retained on the nested sieves by
and reduce the quantity to an amount suitable for testing using flushing to the washed sample. Dry the washed aggregate in the
the applicable methods described in Practice C702. If the same oven to constant mass at a temperature of 110 6 5C and
test sample is to be tested according to Test Method C136, the determine the mass to the nearest 0.1 % of the original mass of
minimum mass shall be as described in the applicable sections the sample.
of that method. Otherwise, the mass of the test sample, after NOTE 4Following the washing of the sample and flushing any
drying, shall conform with the following: material retained on the 75-m (No. 200) sieve back into the container, no
water should be decanted from the container except through the 75-m
Nominal Maximum SizeA Minimum Mass, g
sieve, to avoid loss of material. Excess water from flushing should be
4.75 mm (No. 4) or smaller 300
evaporated from the sample in the drying process.
Greater than 4.75 mm (No. 4) 1000
to 9.5 mm (38 in.) 9. Procedure BWashing Using Wetting Agent
Greater than 9.5 mm (38 in.) 2500
to 19.0 mm (34 in.) 9.1 Prepare the sample in the same manner as for Procedure
Greater than 19.0 mm (34 in.) 5000 A.

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 C117 17
9.2 After drying and determining the mass, place the test TABLE 1 Precision
sample in the container. Add sufficient water to cover the Standard
Acceptable Range
sample, and add wetting agent to the water (Note 5). Agitate of two Results
Deviation (1s)A , %
(d2s)A , %
the sample with sufficient vigor to result in complete separation
Coarse AggregateB
of all particles finer than the 75-m (No. 200) sieve from the Single-Operator Precision 0.10 0.28
coarser particles, and to bring the fine material into suspension. Multilaboratory Precision 0.22 0.62
Immediately pour the wash water containing the suspended and Fine AggregateC
Single-Operator Precision 0.15 0.43
dissolved solids over the nested sieves, arranged with the Multilaboratory Precision 0.29 0.82
coarser sieve on top. Take care to avoid, as much as feasible, A
These numbers represent the (1s) and (d2s) limits as described in Practice
the decantation of coarser particles of the sample. C670.
B
Precision estimates are based on aggregates having a nominal maximum size of
NOTE 5There should be enough wetting agent to produce a small 19.0 mm (14 in.) with less than 1.5% finer than the 75-m (No. 200) sieve.
amount of suds when the sample is agitated. The quantity will depend on C
Precision estimates are based on fine aggregates having 1.0 to 3.0% finer than
the hardness of the water and the quality of the detergent. Excessive suds the 75-m (No. 200) sieve.
may overflow the sieves and carry some material with them.
9.3 Add a second charge of water (without wetting agent) to Amount of Material Finer than 0.075-mm Sieve in Aggregate3
the sample in the container, agitate, and decant as before. required, while Test Method C117 prohibited, the use of a
Repeat this operation until the wash water is clear. wetting agent. The data are based on the analyses of more than
9.4 Complete the test as for Procedure A. 100 paired test results from 40 to 100 laboratories.
12.1.1 The precision values for fine aggregate in Table 1 are
10. Calculation based on nominal 500-g test samples. Revision of this test
10.1 Calculate the amount of material passing a 75-m (No. method in 1994 permits the fine aggregate test sample size to
200) sieve by washing as follows: be 300 g minimum. Analysis of results of testing of 300-g and
A 5 @ ~ B 2 C ! /B # 3 100 (1) 500-g test samples from Aggregate Proficiency Test Samples
99 and 100 (Samples 99 and 100 were essentially identical)
where: produced the precision values in Table 2, which indicates only
A = percentage of material finer than a 75-m (No. 200) minor differences due to test sample size.
sieve by washing, NOTE 6The values for fine aggregate in Table 1 will be revised to
B = original dry mass of sample, g, and reflect the 300-g test sample size when a sufficient number of Aggregate
C = dry mass of sample after washing, g. Proficiency Tests have been conducted using that sample size to provide
reliable data.
11. Report 12.2 BiasSince there is no accepted reference material
11.1 Report the following information: suitable for determining the bias for the procedure in this test
11.1.1 Report the percentage of material finer than the method, no statement on bias is made.
75-m (No. 200) sieve by washing to the nearest 0.1 %, except
13. Keywords
if the result is 10 % or more, report the percentage to the
nearest whole number. 13.1 aggregate; coarse aggregate; fine aggregate; grading;
11.1.2 Include a statement as to which procedure was used. loss by washing; 75 m (No. 200) sieve; size analysis

12. Precision and Bias TABLE 2 Precision Data for 300-g and 500-g Test Samples
Within Between
12.1 PrecisionThe estimates of precision of this test Fine Aggregate Proficiency Sample
Laboratory Laboratory
method listed in Table 1 are based on results from the Test Result
Sample No. of
Average 1s d2s 1s d2s
AASHTO Materials Reference Laboratory Proficiency Sample Size Labs
AASHTO T11/ASTM 500 g 270 1.23 0.08 0.24 0.23 0.66
Program, with testing conducted by this test method and C117
AASHTO Method T 11T11Method of Test for Amount of Total material 300 g 264 1.20 0.10 0.29 0.24 0.68
Material Finer than 0.075-mm Sieve in Aggregate3. The passing the 75m
(No. 200) sieve by
significant differences between the methods at the time the data washing (%)
were acquired is that Method T 11T11Method of Test for

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 C117 17
SUMMARY OF CHANGES

Committee C09 has identified the location of selected changes to this standard since the last issue (C117 13)
that may impact the use of this standard. (Approved Aug. 1, 2017.)

(1) Added new 1.4 and renumbered subsequent sections ac-

cordingly.

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