Manual SMART Turbo
Manual SMART Turbo
Manual SMART Turbo
Corporation
CEM Corporation
P.O. Box 200
Matthews, North Carolina 28106-0200
(704) 821-7015
e-mail: [email protected]
MANUFACTURED IN THE
UNITED STATES OF AMERICA
This instrument complies with United States Code of Federal Regulations (CFR) Title
21, Part 1030 for microwave leakage. A verification report is on file.
This instrument complies with United States Code of Federal Regulations (CFR) Title
47, Federal Communications Commission (FCC) Part 18 Industrial, Scientific and
Medical (ISM) Equipment emissions requirements. A verification report is on file.
600141
Rev. 7
NOTICE
Do not tamper with the safety interlocks. The SMART Turbo System is equipped with three safety
interlocks
which prevent the instrument from producing microwave power if the cover is open.
Do not place any object between the microwave cavity and the cover or allow soil or cleaner residue to
accumulate on sealing surfaces.
Do not operate the instrument if it is damaged. It is particularly important that the instrument cover close
properly and that there is no damage to the cover (bent), hinges and latch (broken or loosened), or
sealing
surfaces.
The instrument should not be placed close to any electrical device susceptible to EMI. It is suggested
that the
user post a sign warning pacemaker wearers that a microwave device is in operation.
If the instrument is suspected of inducing EMI, the cover should be carefully inspected. A microwave
leakage
measurement should be performed as outlined in the Troubleshooting, Maintenance and Service
section of this
manual. Leakage measured above the legal limit of 5 mW/cm2 should be reported to the CEM Service
Department.
This instrument utilizes high voltages and microwave radiation. Instrument service and repair should
be performed only by those trained in repair and maintenance of high voltage and microwave power
systems.
If the SMART Turbo System is used in a manner not specified by CEM Corporation, protection provided
by the system may be impaired.
ii
Table of Contents
Introduction ............................................................................................................................................................................. 1
System Installation .................................................................................................................................................................. 2
Instrument Description ............................................................................................................................................................ 6
Sample Analysis...................................................................................................................................................................... 9
Sampling ............................................................................................................................................................................. 9
Preparation.......................................................................................................................................................................... 10
Weight ................................................................................................................................................................................. 11
Holders ................................................................................................................................................................................ 11
Application........................................................................................................................................................................... 12
Method Information ............................................................................................................................................................. 16
Bias Identification ................................................................................................................................................................ 16
Determining Ash/COH for Processed Meats ....................................................................................................................... 18
Ash Content of Meats .......................................................................................................................................................... 19
Methods Development ............................................................................................................................................................ 22
Quick Test ............................................................................................................................................................................... 23
Set Time .................................................................................................................................................................................. 29
Edit/Create Method ................................................................................................................................................................. 35
Edit Method ............................................................................................................................................................................. 37
Moisture/Solids Standard ..................................................................................................................................................... 38
Moisture/Solids Wastewater TSS ...................................................................................................................................... 44
Moisture/Solids Wastewater TSS/TVSS ........................................................................................................................... 51
Moisture/Solids Dilution ........................................................................................................................................................ 58
Moisture/Solids Syringe Weigh Internal Balance............................................................................................................... 66
Moisture/Solids Syringe Weigh External Balance ............................................................................................................. 73
Moisture/Solids Ash ............................................................................................................................................................. 80
Moisture/Fat or Moisture/Fat/Protein Standard .................................................................................................................... 86
Moisture/Fat or Moisture/Fat/Protein Dilutions ..................................................................................................................... 96
Moisture/Fat or Moisture/Fat/Protein Constant Weight Modified ....................................................................................... 109
Load Method ........................................................................................................................................................................... 120
Setup....................................................................................................................................................................................... 121
Print ........................................................................................................................................................................................ 135
Statistics .................................................................................................................................................................................. 137
Maintenance, Troubleshooting and Service ............................................................................................................................ 143
Cleaning Recommendations ............................................................................................................................................... 143
Routine Maintenance .......................................................................................................................................................... 143
Special Tools and Kits ......................................................................................................................................................... 143
Troubleshooting .................................................................................................................................................................. 144
Error Messages ................................................................................................................................................................... 146
Monitor Sample Kit Test .......................................................................................................................................................... 147
Microwave Leakage Measurement ......................................................................................................................................... 148
IntelliTemp Calibration ............................................................................................................................................................ 149
IntelliTemp Verification ............................................................................................................................................................ 150
Component Replacement ....................................................................................................................................................... 153
Service and Repair.................................................................................................................................................................. 154
Specifications .......................................................................................................................................................................... 156
Warranty ................................................................................................................................................................................. 157
iii
iv
Introduction
The CEM SMART Turbo Moisture/Solids Analyzer is designed to provide a rapid moisture/solids analysis on a
broad range of products. The patented weighing technology provides continuous weighing of the sample during
the drying process. The system determines the precise time the sample is dry, and the moisture or solids content
of the sample is then automatically calculated based on weight loss.
Microwave energy is used to dry the samples. Polar compounds such as water, polar organic solvents such as
alcohols or ketones, and ions in the solution will absorb microwave energy and volatilize. Once water and/or other
solvents have volatilized, the remaining solid material does not usually absorb microwave energy and will remain
relatively cool. Thus, the weight loss is due only to the volatile solvents present in the sample. Moisture is used
throughout this manual to refer to any volatile substance for which the system can measure weight loss after
drying the sample.
The SMART Turbo delivers 150 - 300 watts of microwave energy when programmed for 100 percent power.
Voltage of the incoming electrical service is measured and the microwave power is adjusted by the power control
system in order to normalize the power and provide repeatable power conditions. Magnetron power is
automatically adjusted to deliver appropriate wattage to the instrument cavity. The magnetron fan remains on for
15 minutes after the end of the specified drying time to cool the instrument.
System components consist of a microwave drying chamber, an electronic balance, a 1/4 VGA black and white
screen, an infrared temperature controller, a microprocessor and an internal impact printer. The Octawave
cavity is designed to effectively deliver the microwave energy directly to the sample to achieve rapid test times.
The 50 gram four-place analytical balance has a 0.1 mg sensitivity. Infrared temperature measurement permits
automatic adjustment of microwave power based on user defined temperature setpoint. The microprocessor
controls and monitors system operations, automatically calculates sample results and enables interface with
external printers, external balances and/or computers.
The system is equipped with three safety interlock switches to monitor the mating of the cavity cover and floor and
one safety interlock switch to monitor the cavity cover latch. A flame detector with an infrared feedback
automatically turns off the microwave power if excessive burning is detected. If the system is used in a manner
not specified by CEM Corporation, these protection devices may be impaired.
The SMART Turbo software is user friendly and easy to operate. It is capable of storing up to 100 methods and
300 test results, and is multilingual (English, German, Spanish, French and Italian).
System Installation
1. Following the instructions provided in the packing carton, carefully remove the SMART Turbo from its
shipping carton and place it on a vibration-free workbench or laboratory table in a location that:
a. provides at least 8 in (20 cm) open space on each side and 6 in. (15 cm) open space in the rear of
the instrument for ventilation.
c. provides a temperature range of 41 F (5 C) to 104 F (40 C) and a humidity range of 10-85 percent
relative humidity.
e. allows the instrument to be connected to a dedicated, grounded 120 or 240 VAC outlet. The SMART
Turbo should be operated on a stabilized, constant voltage AC power supply. To operate properly,
the voltage must be within 10% of the specified level.
4. Remove the tape from the instrument cover. Inspect the top cover for proper alignment. The cover must
open and close freely with no binding or restriction of movement.
WARNING
AVERTISSEMENT
5. If the instrument has been damaged in shipping, contact the freight carrier to report the damage and to
file a damage report. Contact the CEM Service Department or the nearest subsidiary or distributor (page
4) to request service information.
6. Verify that all accessories illustrated and listed in Figure 1 are included.
7. Lift the instrument cover. Install the balance stem into the balance stem retainer in the opening of the
cavity floor, ensuring that the balance stem is firmly seated. Install the balance pan onto the stem.
Note: If the balance stem requires removal, lift the stem straight up from its installed position. Moving the balance
stem from side to side can cause damage to the balance assembly.
8. Using a voltage meter, measure the voltage of the dedicated power outlet to verify voltage (120 VAC, 60
Hz or 220/240 VAC, 50 Hz).
9. Facing the back of the instrument, use a small screwdriver to pry the dual voltage supply from the power
module.
10. Install the voltage slide switch in the proper direction for the measured voltage (120V, 60Hz or 220/240V,
50Hz).
Glass Fiber
Sample Pads
Reorder par
t # 200150
Figure 1. Accessories
11. Based on the voltage selected in step 9, install the proper fuses in the dual voltage supply 10 AMP (60
Hz) or 5 AMP (50 Hz).
12. Install the dual voltage supply with the appropriate fuses and with the proper voltage aligned with the
arrow on the power module.
14. Plug the power cord into the power cord receptacle in the rear of the instrument and into a grounded,
dedicated electrical outlet. Note: If using external components such as a printer, computer or balance,
install these components as outlined in this manual.
15. Position the power switch located in the rear of the instrument above the power cord receptacle in the
on position.
16. Using a small flat blade screwdriver, remove the printer cover. Install the roll of printer paper on the paper
holder (supplied in the accessories kit) and install the paper holder in the instrument. Position the end of
3
the paper for proper feeding. Install the printer cover. Press PRINT. Press the operation key below
FORM FEED to advance the paper. If the paper does not advance, ensure that it is positioned correctly to
engage the form feed.
CAUTION
Permit the SMART Turbo to warm up (power switch on, microwaves not being produced) for at
least 45 minutes prior to operation. If the instrument is switched off for an extended period of time
(weekend, holidays, etc.), ensure that warmup time is permitted prior to use.
Mise en garde
17. Refer to the Maintenance, Troubleshooting And Service section of this manual and perform the
MONITOR Test at least five times.
Note: CEM Corporation recommends that the power cord be connected to an AC power outlet and the power
switch remains in the on position at all times. After 15 minutes of idle time, the SMART Turbo assumes a
sleep mode.
CEM Corporation
Service Department
P.O. Box 200
3100 Smith Farm Road
Matthews, NC 28104 -5044 USA
Within the continental United States
Telephone: (800) 726-5551
Fax: (704) 821-4368
email: [email protected]
Outside the United States
Telephone: (704) 821-7015
Fax: (704) 821-4368
email: [email protected]
Italian Subsidiary
CEM S.r.l.
Via DellArtigianato, 6/8
24055 Cologno al Serio (Bg)
Italy
Tel: (39) 35-896224
Fax: (39) 35-891661
email: [email protected]
Instrument Description
Display displays menu choices, instructional messages and analysis results on a 1/4 VGA black and white
screen
Keyboard controls operation of the SMART Turbo. Temperature, time, or other numeric data may be entered
with the numeric keys as requested on the display.
Cavity decreases test times due to its patented compact Octawave design.
Air Shield prevents air flow within the microwave cavity from affecting weight measurements.
Enter Press to store entered parameters and data in the computer memory.
Ready Press to initiate current method for a test or to reset method for next test.
Start/Pause Press to begin or pause sample analysis. Microwave heating begins when the Start/Pause button
is pressed unless the cavity cover is open. Operation will continue through the analysis unless the Start/Pause
button is pressed to interrupt the analysis or the operation key indicating Stop Test is pressed.
Tare Press to tare or zero the weight of the sample pads prior to sample analysis.
0 - 9 Press to select items from menus such as the Main Menu, setup screens, etc. and to select values for
parameters such as time and power.
Operation Keys Press to select specific operation options such as Stop Test, Print, Main Menu, Prev.
Page, etc.
Power Cord Receptacle receives the female end of the power cord.
PC Port permits connection and communication with a personal computer for data storage, etc.
External Balance Port permits connection and communication with an external balance for specific
applications.
Sample Analysis
Proper sample preparation and testing are critical to obtaining accuracy and precision. Each sample has a
specific characteristic composition; therefore, each sample may require an individual method of analysis.
However, guidelines can be established for analysis of general sample types.
Preparation As with any chemical analysis, a homogeneous sample is critical to obtaining precision and
accuracy.
Weight A consistent sample size helps ensure precision and accuracy. Most CEM applications specify a
sample size of 2-5 grams, emphasizing the importance of a homogeneous sample.
Holders Absorbent pads to which a sample can be applied are used for most analyses. Glass fiber pads
are recommended because glass fibers do not absorb microwaves. Other holders include Teflon coated
glass fiber mesh and a drying basket.
Application Most samples should be spread smoothly, avoiding lumps, peaks or any uneven areas.
Sample spread must be consistent.
Drying Time The drying time is determined by the type of sample and its microwave absorbency.
Constant weight drying permits drying of a sample until a constant weight is achieved. Set time drying
permits the control of the sample analysis by entering a specified time and power level.
Infrared Temperature The infrared temperature measurement may be used to operate at temperatures
used in standard or vacuum oven procedures.
Microwave Power The power necessary to dry a sample is determined by sample composition. A
sample should be tested at the highest possible power without burning or degradation of the sample.
Sampling
Proper sampling of a product or process is critical in achieving proper moisture/solids analysis. A representative
sample is required to ensure that the test results are representative of the entire batch or lot of material.
Many standard procedures such as AOAC, USDA and ASTM methods reference sampling techniques. It is
extremely important to follow techniques outlined in these procedures for a particular sample type.
Proper handling and storage of the sample prior to analysis is also critical in achieving accurate and
representative results. Samples should not be exposed to the air for long intervals prior to analysis. Proper
storage also ensures that no moisture is lost.
Preparation
Sample preparation is critical to achieving precise and accurate test results. The sample should be properly
prepared to achieve repeatable moisture results between duplicate analyses of the same sample. Sample
preparation is a physical or modification of the sample. Physical modification may be as simple as stirring or
shaking the sample to ensure homogeneity or more complex such as particle size reduction, dilution or
deaeration.
The objective is to create a homogeneous sample and to improve the correlation of the test method to standard
methods. Some products, such as a beef emulsion or comminuted poultry, may require no additional preparation.
Other materials will require particle size reduction, dilution or dearation prior to testing. Samples should be kept
cool and in sealed containers to prevent loss of moisture. If repeatable results cannot be obtained on the same
sample, re-blend the sample to improve the homogeneity and repeat tests. Sample preparation methods include:
2. Particle Size Reduction Many products require particle size reduction prior to being applied to the
glass fiber pad. Reduction, based on product sample, can be accomplished with a meat grinder, either an
industrial or consumer grade food processor, a coffee mill or a cheese grater. The meat grinder is the
best choice for all meat products. USDA procedure specifies three to four passes through a 1/8 or 5/64
blade with mixing between grinds. A USDA inspector or outside laboratory can make recommendations.
An industrial grade food processor is a good alternative for grinding meat products. A consumer grade
food processor is ideal for grinding frozen potatoes, breaded products, or dry snack foods such as
cookies, crackers, and chips. A coffee mill can be used to grind or mix dry snack foods. A cheese grater
can be used to grate small quantities of hard cheese samples or soap.
3. Dilution Products with a high carbohydrate content are strong microwave absorbers and have a
tendency to burn. These samples may require either a water or salt dilution.
a. Water Dilution A specified amount of sample is diluted with a specified amount of water and mixed
in a blender. Typical samples include doughs, cheese powders, corn syrups, dried meat bases and
sauces. An external balance and a blender are required for this procedure.
b. Salt Dilution A specified amount of salt is added to the product sample prior to analysis. Typical
samples include frozen potatoes and frozen breaded products. This procedure requires a Teflon
basket and dry table salt (sodium chloride).
i. Line a Teflon basket (CEM p.n. 200090) with two square glass fiber pads.
ii. Place the lined basket on the balance of the Moisture/Solids Analyzer. Press Tare.
iv. Place the product sample on top of the salt. Press Start to record the initial weight.
v. Press Stop.
10
4. Deaeration Frozen dairy and imitation dairy products must be deaerated to remove the excess air
in order to provide reproducible test results. This procedure requires a 125 mL Erlenmeyer flask, a 1
liter beaker, a magnetic stirrer, a 11/2 x 3/8 magnetic stirring bar, and a #5 rubber stopper.
ii. Place a 11/2 x 3/8 magnetic stirring bar in the flask. Using a #5 rubber stopper, loosely cap the
flask.
iii. Place flask in a 1 liter beaker containing 250 mL of water which has been heated to 70C.
iv. Place beaker with flask on a magnetic stirrer. Mix for 5 - 7 minutes.
v. Cool sample to ambient temperature and thoroughly mix sample prior to testing.
Weight
Sample weight can be very critical to the final test result. As with most analytical procedures, a consistent sample
size helps ensure precision and accuracy. Sample sizes can vary, based on type of sample, from 1 gram on the
low end (high percent solids level) to 10-15 grams on the high end (very low percent solids level). Test
procedures documented by CEM and included in this manual are for specific sample types and suggested sample
size. Sample size should remain within the weight guidelines. CEM has determined that the suggested sample
size results in the most consistent drying and test results. Heavier sample weights may cause sample degradation
or burning, resulting in high moisture results. Lower sample weights may result in under-drying of the sample.
Holders
Sample holders should be transparent to microwave energy.
CEM Square Sample Pad The square pad is the most commonly used sample holder. Typically, two (2)
pads are used with the sample sandwiched between the pads. For heat sensitive samples, only one pad
is recommended to minimize heat buildup. For low solids samples, three or four pads are used for
absorption.
CEM Round Sample Pad The round pad is used as a collection pad for fat extraction.
Sample Pads CEM glass fiber pads are designed to provide optimum conditions for rapid, thorough
and repeatable drying. CEM Corporation follows strict specifications in the manufacture of sample
pads. Specifications include low moisture content and optimum absorbency, density, porosity, and
strength for microwave drying.
Moisture Content Excessive moisture in sample pads will cause moisture or solids values to be
incorrect. Controlling the moisture ensures that residual moisture is maintained to very close
tolerances.
Absorbency The pad material must be absorbent enough to form a wick for a liquid sample and
to be a sample holder for more viscous type samples.
Density The sample medium must have uniform density to guarantee that the moisture will
volatilize rapidly and evenly, without causing residual heating.
Porosity Correct porosity of the pad material ensures maximum surface area for liquid samples
in order to increase volatilization of moisture. Correct porosity helps prevent sample degradation or
burning.
11
Strength The tensile strength of the medium has a direct effect on the ability of the sample pad
to withstand the stress imposed during sample application.
Teflon Coated Glass Fiber Mesh The mesh is used as a holder for fiber samples or as a spacer
between multiple sheets of paper samples.
Drying Basket The basket is made of Teflon coated glass fiber mesh. It is typically lined with two square
pads. It is used to hold large samples and for salt dilutions.
Application
The viscosity of the sample plays an important role in determining how the sample is spread onto the pad for
analysis. If a sample is thin, it can be pipetted onto the pad and can be tested at high power levels. A thin sample
spread over a large area permits moisture to evaporate rapidly with little residual heat buildup. Glass fiber pads
may be stacked for increased absorbency.
High viscosity samples (samples that do not flow well) require a different technique. If the sample can be easily
spread across the glass fiber pad, no dilution is required. A thick sample will tend to puddle and form a crust,
sometimes trapping volatiles within the bubble. Overheating or burning can also occur on thick samples. If
repeatable results cannot be obtained by spreading the sample, a dilution may be necessary. The sample must
be soluble in the diluting agent, and the diluting agent must be a microwave absorber.
To generate the appropriate amount of heat and achieve optimum moisture results, different types of samples
must be spread to different thicknesses over different areas of the glass fiber sample pad. As a general guideline,
the sample will generate heat in direct proportion to the thickness of the sample layer on the pad. A sample
spread too thickly can cause sample burning; a sample spread too thinly can cause insufficient drying. The
prepared sample should be applied to a glass fiber sample pad. Once the sample is properly applied to the
sample pad, it should be covered with a second glass fiber pad to ensure heat retention and to eliminate
splattering.
Liquid samples should be pipetted onto the pad. Solid samples should be spread onto a pad placed on the edge
of a clean, flat surface, such as a countertop. The spatula should be held level with the pad when spreading the
sample to ensure a smooth, uniform application of sample to the pad surface.
If the sample is an organic solvent-based liquid, special handling is required. Equipment and method modification
may be required. CEM recommends using the SMART Turbo Exhaust Kit when analyzing solvent based samples.
Non-polar organic solvents do not absorb microwave energy; therefore, samples containing this type of solvent
will not dry unless they are mixed with a diluent which absorbs microwave energy and has a higher boiling point
than the non-polar solvent.
If the sample is a polar organic solvent-based liquid, samples will absorb microwave energy and dry as readily as
a water-based liquid. If the organic solvent is an alcohol, a ketone, or an ester, samples should be tested with
water-based techniques.
Some base resins are microwave absorbers. Polyester is a known base resin that is an absorber of microwaves.
Titanium dioxide and calcium carbonate have also been found to be microwave absorbent. If these materials are
present in a sample, usually enough heat is generated to remove most high boiling non-polar solvents and any
other volatiles. Oils become very hot when placed in the microwave field. Some metal based samples can be
tested. If carbon black is present in a sample, it will heat very quickly and possibly burn even at low power levels.
It is recommended that CEM Corporation or a local distributor be consulted prior to testing any solvent-based
sample.
12
If the sample is in a paste, semi-solid, or crumb form or a raw or skeletal meat product such as fresh pork, ground
beef, or chicken, place the sample on the end of a spatula and spread it across one end of the pad. Then spread
the sample to a uniform thickness covering approximately 90% of the pad surface area.
13
If the sample contains bound water such as an all-meat emulsion, cooked all-meat sausage, sausage with
extenders, semi-dry sausage, or ham, place the sample on the end of the spatula and apply the sample to the
middle of the pad. Then spread the sample around the pad in a circle to generate thermal heat.
If the sample is a heat sensitive sample such as a water-based or solvent-based liquid, use a pipette to dispense
the sample onto the pad(s). Sample size should be 2-5 grams, based on solid content of the sample 2-3 grams
for high solids samples, 4-5 grams for samples containing less than 15 percent solids. Samples containing less
than two percent solids may require as much as 10 grams for analysis. Large quantity samples should be pipetted
onto the pads in a thin even layer. Additional glass fiber pads may be used for increased absorbency. A sufficient
number of pads should be used to ensure that liquid samples do not drip onto the floor of the instrument cavity.
14
If the sample is a water-based liquid or solvent-based chemical, use a pipette to puddle the sample onto the
pad(s). Cover the sample with an additional pad. A sufficient number of pads should be used to ensure that liquid
samples do not drip onto the floor of the instrument cavity.
Method Information
Most water-based samples should achieve constant weight settings in 1 - 3 minutes.
The microwave power and temperature settings should be appropriate to the sample. The standard oven or
vacuum oven temperature recommended in a reference method for the sample should be followed. If no
reference method is available, a starting temperature of 100 C should be programmed. Because the power level
in the instrument is adjusted based on temperature feedback, most samples can be dried using a 100% power
level setting. If a sample contains a strong microwave absorber such as carbohydrates, the power level will likely
need to be adjusted. In most instances, a 10% power change will be sufficient to prevent overheating.
During the initial testing of a new sample, the weight display should be monitored to ensure that the sample does
not ignite and that a stable weight reading is displayed. Sharp declines in weight indicate excessive sample
heating. If ignition occurs, the flame detection sensor will abort the analysis.
Samples that are strong absorbers of microwave energy should be diluted or tested at reduced power levels.
These products usually contain simple carbohydrates or tightly held moisture that will not readily escape, causing
overheating and/or burning and non-reproducible results. These samples should be tested at a low power.
Examples of heat sensitive samples include powders, paper fibers, candy and black liquor.
Bias Identification
Most samples can be analyzed for percent moisture content with a CEM drying method, and results will compare
precisely with the standard test method. Occasionally, however, all volatiles in a particular sample cannot be
removed with microwave power. Different spread techniques can be used to eliminate the need for a moisture
bias in most samples. Sometimes browning of the sample in the same manner as in the air oven will also produce
test results comparable to the standard test.
If microwave moisture test results are repeatable, but not comparable to the standard test results, a bias can be
identified. With most samples, the bias will amount to only a few tenths of a percent. To determine a moisture
bias, prepare a sample for testing, ensuring that the sample is homogeneous. Test this sample by both a standard
method and the CEM microwave method. Perform at least ten tests by each method to check repeatability, then
figure an average of the ten results. Subtract the average of the microwave test results from the average of the
standard test results. Enter the resulting number (moisture bias) into the CEM moisture/solids instrument.
Corrected moisture test results will be displayed and printed. If the difference in the average test results is a
negative number, the power level should be reduced and the tests should be repeated.
15
Some meat and poultry products, whether raw or cooked, show a fat bias when analyzed with the CEM
instruments. Less fat is extracted by a short solvent extraction than by the longer ether extraction of the traditional
Soxhlet technique. The bias will be a constant for a given product and should be considered when generating
data.
Cooked sausage (i.e. wieners, bolognas, etc. with extenders) and other cooked products tend to bind fat in the
carbohydrate/protein structure of the cooked product and will generally yield a lower fat value when extracted in
the CEM instrument than when extracted with the Soxhlet.
For proper determination and use of biases, results from the CEM instrument should be compared with the results
from traditional long or standard methods used by USDA laboratories for compliance testing. Standard methods
consist of an air oven (four hours, 125C) for moisture and Soxhlet (four hour ether extraction) for fat. USDA
recommends correlation of rapid fat and moisture methods with these long methods.
USDA Processed Products Inspection Division encourages the use of rapid methods for fat and moisture analysis
to assist in better process control and compliance. USDA recommends periodic back-up analysis (one in every 10
- 20 analyses) by standard long methods when rapid methods are used in approved Total and Partial QC
(TQC/PQC) Programs. Backup checks can be performed less frequently as laboratories gain confidence in the
established biases. CEM Corporation also recommends a Quality Assurance Program for establishing and
maintaining biases and to ensure USDA compliance.
Prior to establishing a fat bias for the Fat Analysis System, a laboratory should be confident of obtaining the best
possible results for moisture, since precision of the fat results will depend on the moisture results. Moisture results
should have repeatability between duplicate analyses of the same sample and a mean or average moisture
values that are close to the values being generated on the same samples by standard oven. To obtain the best
possible results for moisture, and thus for fat, there are three factors to consider: 1) sample preparation, 2)
sample application technique and 3) power and time parameters.
After establishing moisture repeatability and achieving moisture results as close to standard long methods as
possible, use the following procedure to identify fat biases for different product categories.
1. Select three or more samples (approximately two pounds each) from different lots of the same product.
2. Prepare each sample according to standard procedures (3 - 4 passes through a 5/64 blade, with mixing
between grinds, or equivalent).
3. Divide each ground sample in half and package and label sub-samples in two separate, air-tight
containers.
4. Analyze one set of the sub-samples (from step 3) in duplicate by standard long methods oven for
moisture, Soxhlet for fat. If facilities and/or personnel are not available for these tests, use an
independent laboratory. Request raw data (individual tests) from the laboratory, not the mean or
average value.
5. After obtaining the results from the standard long methods, analyze the other set of subsamples in the
CEM Moisture/Solids Analyzer for moisture only. Adjust power and spread technique until acceptable
moisture repeatability is achieved.
6. After obtaining acceptable moisture repeatability, use the Fat Analysis System and perform 3 - 5 moisture
and fat analyses for each sample. As with moisture, fat results should be repeatable. To obtain optimum
fat results, use a sufficient redry time. Two minutes is typical, although some samples may require more
time. The sample weight should be stable (<0.2 mg weight change in the last five seconds). An
insufficient redry time will yield artificially low fat results since the true dry, extracted weight will not be
reached.
7. Subtract values obtained from the SMART Turbo System from Soxhlet values. Average the differences to
identify the average bias for a specific product or product group.
Sample ABC
Average Soxhlet fatxxxx xx
- Average CEM fatxxxx xx
= Biasxxxx xx
8. The bias should be relatively less than 2.0% and must be added to the fat results from the SMART Turbo
System to produce results that correlate closely with official methods. Repeat this process on a regular
basis to confirm that the bias is consistent. Raw meats and blends will produce smaller biases than
cooked products with extenders.
For samples that contain salt, sugar, spice, cure or other added components, ash/carbohydrate (COH) values
must be determined by analysis. For purposes of calculating the protein by difference, the specific amount of each
component (salt, spice, bone, etc.) is not important, only the total amount.
To determine ash/COH values for finished products or blends with sugar, salt, spice, etc., use the following
procedure:
1. Collect and prepare three (3) samples from different lots of the same product. Store the samples in
airtight containers until tested.
2. Analyze the 3 samples in duplicate for fat and moisture in the SMART Turbo or SMART Trac Rapid
Analysis System and for protein using a long method such as Kjeldahl or a much shorter method in the
CEM Sprint System. If necessary, an independent laboratory can provide this analysis.
3. Average the results of the duplicate analyses for each sample, then total the % Protein + % Fat + %
Moisture for each sample.
4. Subtract the sum from 100% to get an Ash/Carbohydrate factor. For example, if the composition of a
sample is:
Moisture 52.54%
Fat 28.36%
Protein 11.25%
Total 92.15%
5. Calculate an average of the the ash/COH values for each of the 3 samples and program that factor into
the SMART Turbo.
Check samples periodically to verify the ash/COH values. Variations in the amount of added constituents (salt,
sugar, spice, extenders, etc.) can cause the ash/COH factor to vary.
17
The following values are estimates since composition may vary due to individual differences in the the meat
sources, seasonal variations, processing, etc.
18
19
Methods Development
The CEM Applications Laboratory has developed procedures for various types of samples. These procedures
include parameters (program, power, time, sample preparation, etc.) needed to program the SMART Turbo and
analyze samples in the SMART Turbo and SMART Trac. CEM sample analysis procedures can be requested
from the CEM Applications Laboratory.
If a procedure for a particular sample is not included in the applications list, review all information in this chapter
relating to sample preparation, sample spread technique, time and power parameters, redry time, and bias
identification to develop an application method. If necessary, call the CEM Applications Laboratory for additional
information and assistance (800) 726-3331 (inside the U.S.) or (704) 821-7015 (outside the U.S.) or email
[email protected].
2. If the sample has high solids content (approximately 75% solids), begin testing with a low sample weight
(1 - 2 grams).
4. Observe weight change closely. The weight should steadily decline. If weight is erratic (1 mg), the test
should be stopped because the sample is probably burning. Reduce the power to 50% and perform the
test again. If the sample continues to burn, continue testing the sample, reducing the power by 5 percent
each time until the sample does not burn.
6. Perform multiple sample tests with determined power and time. Results should be within 0.2%.
7. For fat content results, the re-dry power setting should be no higher than the power setting used to
remove moisture.
20
Quick Test
CEM Main Menu
Quick Test permits entry of parameters for a one-time analysis or method
development. The Quick Test method permits two sample analysis procedures - 1. QUICK TEST
2. EDIT/CREATE METHOD
Constant Weight and Set Time. 3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
Constant Weight
Quick Test
Constant weight permits the operator to dry a sample until a constant weight is
1. POWER: 0%
achieved. Dryness is specified by defining a maximum acceptable weight loss over 2. DELTA WEIGHT: 0.0 mg
a specified time interval. During the specified time, when the weight loss is equal to 3. DELTA TIME: 0 secs
or less than that which was specified, the analysis stops and results are calculated. 4. MAX TIME: 10 mins
5. MAX TEMP: 110 C
6. MIN WT RANGE: 2.00 g
1. With the CEM Main Menu displayed, press 1 to activate Quick Test. 7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
4. Press ENTER.
1. POWER: XXX%
2. DELTA WEIGHT: 0.0 mg
5. Press 2 to select and enter delta weight. 3. DELTA TIME: 0 secs
4. MAX TIME: 10 mins
5. MAX TEMP: 110 C
6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
Note: To edit any of the parameters, press the numeric key of the parameter to be
Quick Test
edited and use the numeric keys to enter the new parameter. Then, press ENTER.
6. Using the numeric keys, enter the delta weight (.1 - .9). Normally a weight loss 1. POWER: XXX%
2. DELTA WEIGHT: 0.0 mg
differential of 0.2 - 0.5 mg is used. 3. DELTA TIME: 0 secs
4. MAX TIME: 10 mins
5. MAX TEMP: 110 C
7. Press ENTER. 6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
21
Set NEXT
Time PAGE
Note: Maximum run time is the amount of time the instrument will operate prior to
Quick Test
shutdown if a constant weight has not been reached. A maximum run time must be
entered or the program will be invalid. If the instrument shuts down due to maximum
run time, parameters should be adjusted prior to repeating the analysis. 1. POWER: XXX%
2. DELTA WEIGHT: X.X mg
3. DELTA TIME: XX secs
11. Press 4 to select and enter maximum run time. If using the default value of 10 4. MAX TIME: 10 mins
5. MAX TEMP: 110 C
minutes, omit step 12. 6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
12. Using the numeric keys, enter the maximum run time (1 - 60 minutes).
Input max time, press ENTER.
13. Press ENTER. Entry: 10
Set NEXT
Time PAGE
14. Press 5 to select and enter maximum temperature. If using the default value of
Quick Test
110C, omit step 15.
15. Using the numeric keys, enter the maximum temperature (0 - 300 C) of the 1. POWER: XXX%
2. DELTA WEIGHT: X.X mg
instrument during the analysis. 3. DELTA TIME: XX secs
4. MAX TIME: 1XX mins
5. MAX TEMP: 110 C
16. Press ENTER. 6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
17. Press 6 to enter a minimum weight range. If using the default minimum weight
Quick Test
range of 2.00 g, omit step 18.
18. Using the numeric keys, enter the minimum weight range of the sample 1. POWER: XXX%
2. DELTA WEIGHT: X.X mg
(0 - 50 g). 3. DELTA TIME: XX secs
4. MAX TIME: XX mins
5. MAX TEMP: XXX C
19. Press ENTER. 6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
22
20. Press 7 to enter a maximum weight range. If using the default maximum
Quick Test
weight range of 4.00 g, omit step 21.
21. Using the numeric keys, enter the maximum weight range of the sample 1. POWER: XXX%
2. DELTA WEIGHT: X.X mg
(0 - 50 g). 3. DELTA TIME: XX secs
4. MAX TIME: XX mins
5. MAX TEMP: XXX C
22. Press ENTER. 6. MIN WT RANGE: X.XX g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
Note: Weight compensation is designed for use with samples having a buoyancy
Quick Test
effect created by heat. It should be used (turned on) for samples, such as milk,
margarine, condiments, etc., which have a higher temperature when the final weight
is calculated than at the beginning of the test. 1. POWER: XXX%
2. DELTA WEIGHT: X.X mg
3. DELTA TIME: XX secs
23. Press 8 to toggle weight compensation on or off. 4. MAX TIME: XX mins
5. MAX TEMP: XXX C
6. MIN WT RANGE: X.XX g
7. MAX WT RANGE: X.XX g
8. WT COMPENSATION: ON
Set NEXT
Time PAGE
Note: To edit any of the parameters, press the numeric key of the parameter to be
edited and use the numeric keys to enter the new parameter. Then, press ENTER.
Set PREV
Time PAGE
Note: The Quick Test screen appears indicating the power, temperature and time.
Quick Test
Note: Press the operation key below EDIT to return to the Quick Test parameter
screen to edit method parameters. Power: XXX%
Temp: XX.X
Time: XX:XX
27. If Autotrack is turned off, a sample identification is required. Press the operation
Wt: X.XXXXg
key below ID.
Place pads on balance and
Press TARE.
ID EDIT
23
28. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
29. Press READY to return to the Quick Test screen.
30. Lift the top cover of the SMART Turbo. Place two glass fiber sample pads on Press READY to continue.
the balance pan. Close the top cover.
31. Press TARE.
Quick Test
Wt: X.XXXXg
ID EDIT
32. Wait for the instrument to tare the weight of the sample pads. The Quick Test
screen will reappear when the tare function is complete.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
Quick Test
the sample pads has been tared.
Sample ID: XXXXXX
33. Lift the instrument cover. Apply the sample in a thin, even layer to one of the Power: XXX%
Temp: XX.X
sample pads. Quickly and gently place the sample pads back on the balance Time: XX:XX
pan. Close the top cover. T
Wt: X.XXXXg
ID EDIT
24
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . .
As the analysis begins, the flashing microwave indicators in the balance icon appear
Quick Test
and the time begins counting upward. The sample weight decreases as the
moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp: XX.X
Time: XX:XX
Moisture: XX.XX%
Wt: X.XXXXg
SMART STOP
SOLIDS Trac TEST
During the drying time, the operation key below SOLIDS or MOISTURE may be
Quick Test
pressed to display % solids or % moisture.
Sample ID: XXXXXX
Power: XXX%
Temp: XX.X
Time: XX:XX
SOLIDS: XX.XX%
Wt: X.XXXXg
SMART STOP
MOISTURE Trac TEST
When the weight loss is equal to or less than the selected parameter, five short
Data Results
beeps will be heard, and the Data Results screen will appear, displaying either the
% moisture or % solids as selected. The results will automatically print if the print
option is selected.
Note: Press READY to analyze additional samples using the same method. XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the
internal printer.
Press READY to continue.
34. Press the operation key below DATA to display the analysis data.
MAIN FORM
MENU FEED DATA PRINT
25
35. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
36. Press the operation key below PREV PAGE to return to the Data Results Fanal Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
37. Press the operation key below PRINT to print the analysis results either on the
internal printer or an external printer, if installed.
Note: Press READY to analyze additional samples using the same method.
Press READY to continue.
MAIN PREV
MENU PAGE
38. Press the operation key below MAIN MENU to return to the CEM Main Menu
Data Results
screen.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
26
Set time permits the operator to control the sample analysis by entering a specified
1. QUICK TEST
analysis time and power level. At the end of the specified time, the percent 2. EDIT/CREATE METHOD
solids and/or moisture of the sample is calculated and displayed. 3. LOAD METHOD
4. SETUP
5. PRINT
1. With the CEM Main Menu displayed, press 1 to activate Quick Test. 6. STATISTICS
1. POWER: 0%
2. DELTA WEIGHT: 0.0 mg
3. DELTA TIME: 0 secs
4. MAX TIME: 10 mins
5. MAX TEMP: 110 C
6. MIN WT RANGE: 2.00 g
7. MAX WT RANGE: 4.00 g
8. WT COMPENSATION: ON
Set
Time
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
5. Press ENTER.
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
27
7. Using the numeric keys, enter the run time (1 sec. - 99 min. 59 sec.).
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
8. Press ENTER. 3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
9. Press 3 to select and enter maximum temperature. If using the default value of
Quick Test
110C, omit step 10.
1. POWER: 0%
10. Using the numeric keys, enter the maximum temperature (0 - 300 C) of the 2. RUN TIME: 00:00 min:sec
instrument during the analysis. 3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
11. Press ENTER. 6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
12. Press 4 to enter a minimum weight range. If using the default minimum weight
Quick Test
range of 2.00 g, omit step 13.
1. POWER: 0%
13. Using the numeric keys, enter the minimum weight range of the sample (0 - 50 2. RUN TIME: 00:00 min:sec
g). 3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
14. Press ENTER. 6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
15. Press 5 to enter a maximum weight range. If using the default maximum
Quick Test
weight range of 4.00 g, omit step 16.
1. POWER: 0%
16. Using the numeric keys, enter the maximum weight range of the sample (0 - 50 2. RUN TIME: 00:00 min:sec
g). 3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
17. Press ENTER. 6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
28
Note: Weight compensation is designed for use with samples having a buoyancy
Quick Test
effect created by heat. It should be used (turned on) for samples, such as milk,
margarine, condiments, etc., which have a higher temperature when the final weight
1. POWER: 0%
is calculated than at the beginning of the test. 2. RUN TIME: 00:00 min:sec
3. MAX TEMP: 110 C
18. Press 6 to toggle Weight Compensation on or off. 4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
6. WT COMPENSATION: ON
19. Press 7 to toggle TURBO on or off. 7. TURBO: ON
Note: To edit any of the parameters, press the numeric key of the parameter to be Press item number to select.
edited and use the numeric keys to enter the new parameter. Then, press ENTER.
CONSTANT
WEIGHT
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
3. MAX TEMP: 110 C
4. MIN WT RANGE: 2.00 g
5. MAX WT RANGE: 4.00 g
6. WT COMPENSATION: ON
7. TURBO: ON
CONSTANT
WEIGHT
Note: The Quick Test screen appears indicating the power, temperature and time.
Quick Test
Note: Press the operation key below EDIT to return to the Quick Test parameter
screen to edit method parameters. Power: XXX%
Temp: XX.X
Time: XX:XX
ID EDIT
22. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
22. Press READY to return to the Quick Test screen.
29
24. Lift the top cover of the SMART Turbo. Place two glass fiber sample pads on
Quick Test
the balance pan. Close the top cover.
Sample ID: XXXXXX
25. Press TARE. Power: XXX%
Temp: XX.X
Time: XX:XX
Wt: X.XXXXg
ID EDIT
26. Wait for the instrument to zero the weight of the sample pads. The Quick Test
screen will reappear when the tare function is complete.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
Quick Test
the sample pads has been tared.
Sample ID: XXXXXX
27. Lift the top cover. Remove the sample pads from the balance pan. Apply the Power: XXX%
Temp: XX.X
appropriate amount of sample in a thin, even layer to one of the sample pads. Time: XX:XX
Quickly and gently place the sample pads back on the balance pan. Close the T
top cover.
Wt: X.XXXXg
28. Press START.
Place sample and pads on
balance and press START.
ID EDIT
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
30
As the analysis begins, the flashing microwave indicators in the balance icon appear
Quick Test
and the time begins counting down. The sample weight decreases as the moisture
is removed. Sample ID: XXXXXX
Power: XXX%
Temp: XX.X
During the drying time, the operation key below SOLIDS or MOISTURE may be Time: XX:XX
pressed to display % solids or % moisture.
Moisture: XX.XX%
Wt: X.XXXXg
Note: Press the operation key below STOP TEST to stop the method test.
STOP
SOLIDS TEST
When the drying time is complete, five short beeps will be heard, and the Data
Quick Test
Results screen will appear, displaying either the % moisture or % solids as selected.
The results will automatically be printed if that option is selected. Sample ID: XXXXXX
Power: XXX%
Temp: XX.X
Note: Press READY to analyze additional samples using the same method. Time: XX:XX
SOLIDS: XX.XX%
Wt: X.XXXXg
STOP
MOISTURE TEST
Note: Press the operation key below FORM FEED to advance blank paper from the
Data Results
internal printer.
29. Press the operation key below DATA to display the analysis data.
XX.XX%M
MAIN FORM
MENU FEED DATA PRINT
30. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
31
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
31. Press the operation key below PREV PAGE to return to the Data Results Fanal Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
MAIN PREV
MENU PAGE
32. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
33. Press the operation key below MAIN MENU to return to the CEM Main Menu
screen. CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
32
Edit/Create Method
The SMART Turbo permits a variety of analysis programs, based on sample type.
Dilution The sample is diluted, and a dilution factor is used for the diluted sample result; therefore, an accurate
moisture/solids value for the undiluted sample is obtained. An interfaced external balance is required. The dilution
program should be used with samples that burn easily, viscous samples or samples which dry unevenly.
Syringe Weigh Syringe Weigh is utilized when the moisture/solids instrument cannot accurately record the
initial sample weight due to rapid evaporation. The rapid evaporation can be caused by the sample being warmer
than room temperature or containing a solvent that evaporates quickly. The instrument internal balance or an
interfaced external balance can be used to calculate the weight of the syringe.
Ash The moisture/solids instrument performs a standard analysis on the sample. The sample is then
transferred into an ashing furnace. The ashed sample is returned to the moisture/solids instrument for calculation
of the ash content.
Wastewater Total Suspended Solids (TSS) A filter is utilized for samples with low solids concentration. The
instrument dries and weighs the solids obtained on a tared filter from the filtration of a known volume of sample
which is manually entered into the system.
Wastewater Total Volatile Suspended Solids (TSS/TVSS) The moisture/solids instrument performs a
standard analysis on the sample. The dried sample is then transferred to an ashing furnace. The ashed sample is
returned to the moisture/solids instrument for weighing of the ashed sample. Total Suspended Solids and Total
Volatile Suspended Solids are calculated.
Moisture/Fat Modified The fat is extracted from one sample while another sample is dried for moisture
analysis, permitting analysis of fat content of samples in which initial drying may bind the fat molecules.
33
Methods can be created in the following modes in either constant weight or set time:
Moisture/Solids
Standard
Wastewater
Dilution
Syringe Weigh
Ash
Moisture/Fat
Standard
Dilution
Modified Fat
Moisture/Fat/Protein
Standard
Dilution
Modified Fat
CEM Corporation has preprogrammed several methods into the SMART Turbo which can be used as
programmed or edited for a specific sample. Preprogrammed methods include:
Latex
Water Based Chemical
Meat (Raw)
Cheese
Milk
Tomato Paste
Butter
Mayonnaise
Eggs
Salad Dressing
Pet Food
Yogurt
Meat (Processed)
To use a CEM preprogrammed method, refer to the Load Method section of this manual. To Edit a
preprogrammed method, refer to the Edit Method section of this manual.
34
Edit Method
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. MONITOR
5. ICE CREAM
6. SALAD DRESSING
7. LATEX
8. WATER BASED CHEMICAL
Note: If the method to be edited is not displayed on the screen, press the operation Press item number to select.
key below NEXT PAGE to access additional methods. Continue to press the NEXT
operation key below NEXT PAGE until the desired method is displayed. PAGE
3. Refer to the CREATE METHOD section of this manual for specific instructions
for entering method information to edit desired modes and/or parameters.
CAUTION
35
Moisture/Solids - Standard
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. MONITOR
5. ICE CREAM
6. SALAD DRESSING
7. LATEX
8. WATER BASED CHEMICAL
NEXT
PAGE
3. Using the operation keys below the arrows, select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the method name utilizes numbers only, use the numeric keypad to enter Space Delete
the numbers for the name.
Highlight choice, press ENTER.
5. Continue using the operation keys to select each letter or number of the method
name. Press ENTER after each selection until the entire method name is
selected. Press READY to continue.
6. Press READY.
36
MAIN PREV
MENU PAGE
10. Press the appropriate number for the type test to be performed.
Moisture/Solids Analysis
1. STANDARD TEST
2. WASTEWATE4R
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
11. Press 1 to select Standard Test.
Moisture/Solids Analysis
1. POWER: 0%
2. DELTA WEIGHT: 0.0 mg
3. DELTA TIME: 0 secs
4. MAX TIME: 10 mins
5. BIAS; 0.00%
6. MAX TEMP: 110 C
12. Press the numbers (1 - 5 Constant Weight or 1 - 4 Set Time) and enter the
Standard Test
appropriate method parameters. C
O
N 1. POWER: 0/5
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. DELTA WEIGHT: 0.0 mg
entering method parameters for Constant Weight and Set Time. T 3. DELTA TIME: 0 secs
A 4. MAX TIME: 10 mins
N 5. BIAS: 0.00%
13. Press the operation key below NEXT PAGE to access additional method 6. MAX TEMP: 110 C
T
parameters.
W
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
37
Standard Test
1. POWER: 0/5
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
14. Press the numbers (1 - 6) and enter the appropriate method parameters.
Standard Test
Note: Weight compensation is designed for use with samples having a buoyancy
1. RESULT RANGE: MOISTURE
effect created by heat. It should be used (turned on) for samples, such as milk, 2. MIN RESULT: X.XX%
margarine, condiments, etc., which have a higher temperature when the final weight 3. MAX RESULT: XX.XX%
4. MIN WT RANGE: X.XX g
is calculated than at the beginning of the test. 5. MAX WT RANGE: X.XX g
6. WT COMPENSATION: ON
15. After the final method parameter is entered, press READY to begin the analysis.
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature and time.
XXXXXXXX
16. If Autotrack is turned off, a method identification name or number is required.
Press the operation key below ID. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID
17. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
18. Press READY to return to the method screen.
38
19. Lift the top cover of the SMART Turbo Place two glass fiber sample pads on the
XXXXXXXX
balance pan. Close the top cover.
Wt: X.XXXXg
ID SOLIDS
21.. Wait for the instrument to tare the weight of the sample pads. The method test
screen will reappear when the tare function is complete.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
XXXXXXXX
the sample pads has been tared.
22. Lift the instrument cover. Apply the sample in a thin, even layer to one of the Power: XXX%
Temp (XXX): XX.X
sample pads. Quickly and gently place the sample pads back on the balance Time: XX:XX
pan. Close the top cover. T
23. Press START.
Wt: X.XXXXg
ID
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
39
As the analysis begins, the flashing microwave indicators in the balance icon appear
XXXXXXXX
and the time begins counting (up for Constant Weight or down for Set Time). The
sample weight decreases as the moisture is removed.
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Moisture: XX.XX%
Wt: X.XXXXg
STOP
SOLIDS TEST
During the drying time, the operation key below SOLIDS or MOISTURE may be
XXXXXXXX
pressed to display % solids or % moisture.
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
SOLIDS: XX.XX%
Wt: X.XXXXg
SMART STOP
MOISTURE TRAC TEST
When the weight loss is equal to or less than the selected parameter, five short
Data Results
beeps will be heard, and the Data Results screen will appear, displaying either the
% moisture or % solids as selected. The results will automatically be printed if that
option is selected.
Note: Press READY to analyze additional samples using the same method. XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the
internal printer.
Press READY to continue.
24. Press the operation key below DATA to display the analysis data.
MAIN FORM
MENU FEED DATA PRINT
25. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
40
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
26. Press the operation key below PREV PAGE to return to the Data Results Fanal Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
MAIN PREV
MENU PAGE
27. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Moisture: XX.XX%
Solids: XX.XX%
28. Press the operation key below MAIN MENU to end the analysis and return to Dry Time: XX:XX
the CEM Main Menu screen.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
41
It is recommended that a minimum of 250 mL of liquid be filtered to achieve a representative level of solids after
drying. For very low levels of TSS (50 100 mg/liter) the volume will need to be increased to 500 or 1000 mL.
Recommended Equipment:
1 liter graduated cylinder
Whatman glass microfiber filters or equivalent
7 11 cm Buchner funner
2000 mL filtering flask with side arm
Vacuum pump, aspirator or other vacuum source
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows, select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the method name utilizes numbers only, use the numeric keypad to enter Space Delete
the numbers for the name.
Highlight choice, press ENTER.
5. Continue using the operation keys below the arrows to select each letter or
number of the method name. Press ENTER after each selection until the entire
method name is selected. Press READY to continue.
6. Press READY.
42
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
11. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter the
WasteWater
appropriate method parameters. C
O
N 1. POWER: 0%
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. DELTA WEIGHT: 0.0 mg
entering method parameters for Constant Weight and Set Time. T 3. DELTA TIME: 0 secs
A 4. MAX TIME: 10 mins
N 5. BIAS: 0.00%
12. Press the operation key below NEXT PAGE to access additional method 6. MAX TEMP: 110 C
T
parameters.
W
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
WasteWater
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
43
14. Press the numbers (2 - 8) and enter the appropriate method parameters.
1. OPTION: TSS
2. VOLUME: XXX mL
15. Press READY to begin the method analysis. 3. RESULT RANGE; MOISTURE
4. MIN RESULT: XX.XX%
5. MAX RESULT: XX.XX%
6. MIN WT RANGE: X.XX g
7. MAX WT RANGE: X.XX g
8. WT COMPENSATION: ON
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature and time.
XXXXXXXX
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Volume: XXX
Sample: X
Wt: X.XXXXg
ID
16. If Autotrack is turned off, a sample identification name or number is required.
SAMPLE ID:
Press the operation key below ID.
0123456789AB
CDEFGHIJKLMN
17. Using the operation keys below the arrows, position the cursor on (select) the OPQRSTUVWXYZ
first number or letter of the sample identification. Press ENTER. Continue to Space Delete
position the cursor on each letter or number and press ENTER until the
identification is complete. Highlight choice, press ENTER.
Note: If using an identification number only, use the numeric keys to enter the
number. Press READY to continue.
Wt: X.XXXXg
ID VOLUME SAMPLE
44
20. Using the numeric keys, enter the number of samples to be analyzed.
XXXXXXXX
21. Press ENTER. Sample ID: Sample XX
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Volume: XXX
Sample: X
Wt: X.XXXXg
ID VOLUME SAMPLE
Wt: X.XXXXg
ID VOLUME SAMPLE
23. Lift the instrument cover. Place filter #1 on the balance pan. Close the
TSS Multiple Tare
instrument cover.
Note: Press the operation key below ABORT to abort the analysis.
Place filter 1 on
balance and press TARE.
ABORT
25. Wait for the instrument to tare the weight of filter #1.
TARING BALANCE . . .
45
26. Lift the instrument cover. Remove filter #1 from the balance pan. Place filter #2
TSS Multiple Tare
on the balance pan. Close the instrument cover.
Place filter 2 on
balance and press TARE.
ABORT
27. Wait for the instrument to tare the weight of filter #2.
28. Continue the tare process until the filters for the total number of samples to be
analyzed have been tared.
Note: Filters must be kept in the order in which they are tared for proper sample
analysis. TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
XXXXXXXX
the sample pads has been tared.
Sample ID: Sample XX
29. Place the first tared filter in the funnel. With the vacuum source operating, pour Power: XXX%
Temp (XXX): XX.X
the sample into the funnel. When all the sample has been filtered, remove the Time: XX:XX
T
filter from the funnel. Volume: XXX
Sample: X Processing: X
30. Lift the instrument cover. Place the wet filter on the balance pan. Close the Wt: X.XXXXg
cover.
Place sample 1 on balance and
31. Press START. press START.
ID VOLUME SAMPLE
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
46
As the analysis begins, the flashing microwave indicators in the balance icon appear
XXXXXXXX
and the time begins counting (up for Constant Weight or down for Set Time).
Sample ID: XXXXXX
During the drying time, the operation key below SOLIDS or MOISTURE may be Power: XXX%
Temp (XXX): XX.X
pressed to display % solids or % moisture. Time: XX:XX
Note: Press the operation key below STOP TEST to abort the analysis. Moisture: XX.XX%
Wt: X.XXXXg
STOP
SOLIDS TEST
When the drying time is complete, five short beeps will be heard, and the Data
Data Results
Results screen will appear, displaying either the % moisture or % solids as selected.
The results will automatically be printed if that option is selected.
Note: Press READY to analyze additional samples using the same method.
XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the MG/Liter TSS
internal printer.
32. Press the operation key below DATA to display the analysis data.
Press READY to continue.
MAIN FORM
MENU FEED DATA PRINT
33. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
MG/Liter TSS: X
Sample: X
Volume: XXX
47
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
34. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
35. Press the operation key below Print to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Moisture: XX.XX%
Solids: XX.XX%
36. Press the operation key below MAIN MENU to end the analysis and return to Dry Time: XX:XX
the CEM Main Menu screen.
MG/Liter TSS: X
Sample: X
Sample: X
48
It is recommended that a minimum of 250 mL of liquid be filtered to achieve a representative level of solids after
drying. For very low levels of TVSS (50 100 mg/liter) the volume will need to be increased to 500 or 1000 mL.
Recommended Equipment:
1 liter graduated cylinder
Whatman glass microfiber filters or equivalent
7 11 cm Buchner funner
2000 mL filtering flask with side arm
Vacuum pump, aspirator or other vacuum source
CEM MAS-7000 Microwave Muffle Furnace or other ashing furnace
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows, select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the method name utilizes numbers only, use the numeric keypad to enter Space Delete
the numbers for the name.
Highlight choice, press ENTER.
5. Continue using the operation keys below the arrows to select each letter or
number of the method name. Press ENTER after each selection until the entire
method name is selected. Press READY to continue.
6. Press READY.
49
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
10. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter the
WasteWater
appropriate method parameters. C
O
N 1. POWER: 0/0
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. DELTA WEIGHT: 0.0 mg
entering method parameters for Constant Weight and Set Time. T 3. DELTA TIME: 0 secs
A 4. MAX TIME: 10 mins
N 5. BIAS: 0.00%
11. Press the operation key below NEXT PAGE to access additional method 6. MAX TEMP: 110 C
T
parameters.
W
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
WasteWater
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
13. Press the numbers (2 - 8) and enter the appropriate method parameters.
1. OPTION: TSS/TVSS
2. VOLUME: XXX mL
3. RESULT RANGE; MOISTURE
4. MIN RESULT: X.XX%
14. Press READY to begin the analysis. 5. MAX RESULT: XX.XX%
6. MIN WT RANGE: X.XX g
7. MAX WT RANGE: X.XX g
8. WT COMPENSATION: ON
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature, volume
XXXXXXXX
and time.
Power: XXX%
Temp (XXX): XX.X
Note: Press the operation key below VOLUME to edit or enter a sample volume. Time: XX:XX
Volume: XXX
Sample: X
15. If Autotrack is turned off, a sample identification name or number is required.
Press the operation key below ID.
Wt: X.XXXXg
ID VOLUME REWEIGH
16. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number
Highlight choice, press ENTER.
17. Press READY to return to the test screen.
18. Lift the instrument cover. Place the filter on the balance pan. Close the
XXXXXXXX
instrument cover.
Sample ID: Sample XX
19. Press TARE. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Volume: XXX
Sample: X
Wt: X.XXXXg
ID VOLUME SAMPLE
51
20. Wait for the instrument to tare the weight of the filter.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
XXXXXXXX
the sample pads has been tared.
Sample ID: Sample XX
21. Place filter in the funnel. With the vacuum source operating, pour the sample Power: XXX%
Temp (XXX): XX.X
into the funnel. When all the sample has been filtered, remove the filter from the Time: XX:XX
funnel. Volume: XXX T
22. Lift the instrument cover. Place the wet filter on the balance pan. Close the Wt: X.XXXXg
cover.
Place sample and filter on
23. Press START. balance and press START.
ID VOLUME REWEIGH
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
As the analysis begins, the flashing microwave indicators in the balance icon appear
XXXXXXXX
and the time begins counting (up for Constant Weight or down for Set Time).
Sample ID: XXXXXX
During the drying time, the operation key below SOLIDS or MOISTURE may be Power: XXX%
Temp (XXX): XX.X
pressed to display % solids or % moisture. Time: XX:XX
Note: Press the operation key below STOP TEST to abort the analysis. Moisture: XX.XX%
Wt: X.XXXXg
When the drying time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying either the % moisture or % solids as selected.
STOP
SOLIDS TEST
52
24. To ash the dried sample, fold the filter; place it in an ashing crucible; and place
Data Results
the crucible in the ashing furnace. Ash the sample by the defined method.
XX.XX%M
MG/Liter
MAIN FORM
MENU FEED DATA
26. Press the operation key below REWEIGH.
XXXXXXXX
Note: Press the operation key below VOLUME to edit the sample volume.
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Volume: XXX
Wt: X.XXXXg
ID VOLUME REWEIGH
27. Press the numerical key to select the proper sample to be reweighed.
Select Sample ID
1. XXXX
2. XXXXXX
3. XXXX
4. XXXX
5. XXXXXX
28. Lift the instrument cover. Place the ashed sample on the balance pan. Close
XXXXXXXX
the instrument cover.
Sample ID: Sample XX
29. Press START. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Volume: XXX T
Note: To reweigh additional samples, press READY and follow the steps outlined
above. Wt: X.XXXXg
ID VOLUME REWEIGH
53
The instrument reweighs the ashed sample and calculates the data results.
REWEIGHING SAMPLE. . .
30. Press the operation key below DATA to display the analysis data.
Data Results
XX.XX%M
MG/Liter TVSS
MAIN FORM
MENU FEED DATA PRINT
31. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
MG/Liter TSS: X
MG/Liter TVSS: X
Volume: XXX
The Sample Weight Data screen displays the initial weight, the final weight, the
Sample Weight Data
differential weight and the end weight.
Initial Wt: XX.XXXXg
32. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
PREV
PAGE
54
33. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to continue analysis using the same method. Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
34. Press the operation key below MAIN MENU to end the analysis and return to
MG/Liter TSS: X
the CEM Main Menu screen. MG/Liter TVSS: X
Volume: XXX
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
55
Moisture/Solids Dilution
This procedure is used for viscous samples or samples that dry unevenly. The dilution is accomplished by using a
volatile diluents such as water, methyl ethyl ketone or methyl isobutyl ketone. The diluent must be miscible with
the sample. Using an external balance connected to the SMART Turbo, the system performs calculations to
correct the dilution.
Recommended equipment:
External Balance
1. Refer to the SETUP section of this manual to ensure that the applicable
CEM Main Menu
external balance is selected.
1. QUICK TEST
2. With the CEM Main Menu displayed, press 2 to activate the Edit/Create 2. EDIT/CREATE METHOD
Method screen. 3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
4. Using the operation keys below the arrows select the first letter or number
METHOD NAME:
of the method name.
0123456789AB
5. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
6. Continue using the operation keys to select each letter or number of the Space Delete
method name. Press ENTER after each selection until the entire method
name is selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to
enter the numbers for the name. Press READY to continue.
7. Press READY.
56
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
12. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter
Dilution
the appropriate method parameters. C
O
N 1. POWER: 0/0
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. RUN TIME: 00:00 min:sec
entering method parameters for Constant Weight and Set Time. T 3. BIAS: 0.00%
A 4. MAX TEMP: 110 C
N
13. Press the operation key below NEXT PAGE to access additional
T
method parameters.
W
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
Dilution
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
57
14. Press the numbers (1 - 6) and enter the appropriate method parameters.
Dilution
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature, time
XXXXXXXX
and ratio.
Power: XXX%
Note: Press the operation key below SOLIDS to display the solids data rather Temp (XXX): XX.X
Time: XX:XX
than the moisture data on the screen. Ratio: XX.XXXX
ID RATIO DILUTION
17. Using the operation keys below the arrows, position the cursor on (select)
SAMPLE ID:
the first number or letter of the sample identification. Press ENTER.
Continue to position the cursor on each letter or number and press ENTER
0123456789AB
until the identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
18. Press READY to return to the method test screen.
Note: If sample and diluent are weighed on a balance not connected to the
XXXXXXXX
SMART Turbo, press the operation key below RATIO to enter the dilution ratio.
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Ratio: XX.XXXX
Wt: X.XXXXg
ID RATIO DILUTION
58
ID RATIO DILUTION
22. Place an empty container suitable for the sample and diluent on the
Dilution (Ext)
external balance. Wait for the weight to stabilize.
ABORT
24. Wait for the SMART Turbo to tare the weight of the container.
TARING BALANCE . . .
25. Place the sample in the container on the external balance pan.
Dilution (Ext)
Note: Press the operation key below ABORT to end the dilution analysis. Add sample to container
and press READY.
ABORT
59
READING BALANCE . . .
28. Add the diluent to the sample in the container on the external balance pan.
Dilution (Ext)
ABORT
The instrument reads and records the weight of the sample and diluent.
READING BALANCE . . .
The instrument displays the weight of the sample, the weight of the sample and
Dilution (Ext)
diluent, and the dilution ratio.
60
32. Lift the cover of the SMART Turbo. Place two glass fiber sample pads on
XXXXXXXX
the balance pan. Close the instrument cover.
Power: XXX%
33. Press TARE. Temp (XXX): XX.X
Time: XX:XX
Ratio: XX.XXXX
Wt: X.XXXXg
ID RATIO DILUTION
34. Wait for the instrument to tare the weight of the sample pads.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the
XXXXXXXX
weight of the sample pads has been tared.
Sample ID: Sample XX
35. Lift the instrument cover. Apply the sample in a thin, even layer to one of Power: XXX%
Temp (XXX): XX.X
the sample pads. Quickly and gently place the sample pads back on the Time: XX:XX
balance pan. Close the top cover. Ratio: X.XXXX T
The instrument reads and records the initial weight of the sample prior to
beginning the analysis.
READING BALANCE . . .
61
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting (up for Constant Weight or down for Set
Time). The sample weight decreases as the moisture is removed.
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Ratio: XX.XXXX
During the drying time, the operation key below SOLIDS or MOISTURE may be Moisture: XX.XX%
pressed to display % solids or % moisture.
Wt: X.XXXXg
STOP
SOLIDS TEST
When the weight loss is equal to or less than the selected parameter, five short
Data Results
beeps will be heard, and the Data Results screen will appear, displaying either
the % moisture or % solids as selected. The results will automatically be printed
if that option is selected.
Note: Press READY to analyze additional samples using the same method. XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the
internal printer.
Press READY to continue.
37. Press the operation key below DATA to display the analysis data.
MAIN FORM
MENU FEED DATA PRINT
38. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and
Sample Weight Data
the differential weight.
Initial Wt: XX.XXXXg
39. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
PREV
PAGE
62
40. Press the operation key below PRINT to print the analysis results either on
Data Results
the internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Dry Time: XX:XX
Moisture: XX.XX%
41. Press the operation key below MAIN MENU to end the analysis and return Solids: XX.XX%
to the CEM Main Menu screen.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
63
This procedure is used for samples that, due to rapid evaporation, cannot achieve a stable initial weight with the
standard moisture/solids application. The instrument internal balance calculates the weight of the syringe.
Recommended equipment
Syringe or Pipette
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows select the first letter or number
METHOD NAME:
of the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
5. Continue using the operation keys to select each letter or number of the Space Delete
method name. Press ENTER after each selection until the entire method
name is selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to
enter the numbers for the name. Press READY to continue.
6. Press READY.
64
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
11. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter
Syringe Weigh
the appropriate method parameters. C
O
N 1. POWER: 0%
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. DELTA WEIGHT: 0.0 mg
entering method parameters for Constant Weight and Set Time. T 3. DELTA TIME: 0 secs
A 4. MAX TIME: 10 mins
N 5. BIAS: 0.00%
12. Press the operation key below NEXT PAGE to access additional 6. MAX TEMP: 110 C
T
method parameters.
W
E
I Press item number to select.
G
H
MAIN PREV NEXT
T MENU PAGE PAGE
Syringe Weigh
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select.
65
13. Press the numbers (1 - 6) and enter the appropriate method parameters.
Syringe Weigh
MAIN PREV
MENU PAGE
Note: The test screen appears indicating the power, temperature, and time.
XXXXXXXX
15. If Autotrack is off and a method identification name or number is required,
press the operation key below ID. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID
16. Using the operation keys below the arrows, position the cursor on (select)
SAMPLE ID:
the first number or letter of the sample identification. Press ENTER.
Continue to position the cursor on each letter or number and press
0123456789AB
ENTER until the identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
17. Press READY to return to the test screen.
18. Lift the cover of the SMART Turbo. Place two glass fiber sample pads on
XXXXXXXX
the balance pan. Close the instrument cover.
Wt: X.XXXXg
ID
66
20. Wait for the instrument to tare the weight of the sample pads.
TARING BALANCE . . .
21. Lift the instrument cover. Remove the sample pads from the balance pan.
Syringe Weigh (Int)
Place the syringe containing the sample on the balance pan. Close the
instrument cover.
Note: Press the operation key below Abort to end the analysis. Remove sample pads. Place
filled syringe in on balance
and press READY.
ABORT
Note: Press the operation key below Abort to end the analysis.
WEIGHING BALANCE . . .
Note: Press the operation key below Abort to end the analysis.
Syringe Weigh (Int)
23. Lift the instrument cover. Remove the syringe from the balance pan.
24. Dispense the sample from the syringe on the tared sample pads.
25. Place the empty syringe back on the balance pan. Close the instrument Remove sample on pads.
cover. Place syringe back on
Balance and press READY.
ABORT
67
REWEIGHING BALANCE . . .
27. Lift the instrument cover. Remove the syringe from the balance pan.
Syringe Weigh (Int)
ABORT
29. Place the sample pads with the sample on the balance pan. Close the
XXXXXXXX
instrument cover.
Sample ID: Sample XX
30. Press START. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
T
Wt: X.XXXXg
ID
The instrument reads and records the initial weight of the sample prior to
beginning the analysis.
READING BALANCE . . .
68
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting (up for Constant Weight or down for Set
Time). The sample weight decreases as the moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
During the drying time, the operation key below SOLIDS or MOISTURE may be Time: XX:XX
pressed to display % solids or % moisture.
Moisture: XX.XX%
Wt: X.XXXXg
Note: Press the operation key below STOP TEST to end the analysis.
STOP
SOLIDS TEST
When the weight loss is equal to or less than the selected parameter, five short
XXXXXXXX
beeps will be heard, and the Data Results screen will appear, displaying either
the % moisture or % solids as selected. The results will automatically be printed
if that option is selected.
Note: Press READY to analyze additional samples using the same method. XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the
internal printer.
Press READY to continue.
31. Press the operation key below DATA to display the analysis data.
MAIN FORM
MENU FEED DATA PRINT
32. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and
Sample Weight Data
the differential weight.
Initial Wt: XX.XXXXg
33. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
PREV
PAGE
69
34. Press the operation key below PRINT to print the analysis results either on
Data Results
the internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Dry Time: XX:XX
Moisture: XX.XX%
35. Press the operation key below MAIN MENU to end the analysis and return Solids: XX.XX%
to the CEM Main Menu screen.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
70
This procedure is used for samples that, due to rapid evaporation, cannot achieve a stable initial weight with the
standard moisture/solids application. An external balance connected to the SMART Turbo calculates the weight
of the syringe.
Recommended Equipment
External Balance
Syringe or Pipette
1. Refer to the Setup section of this manual to ensure that the applicable external
CEM Main Menu
balance is selected.
1. QUICK TEST
2. With the CEM Main Menu displayed, press 2 to activate the Edit/Create Method 2. EDIT/CREATE METHOD
screen. 3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
4. Using the operation keys below the arrows select the first letter or number of the
METHOD NAME:
method name.
0123456789AB
5. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
6. Continue using the operation keys to select each letter or number of the method Space Delete
name. Press ENTER after each selection until the entire method name is
selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to enter the
numbers for the name. Press READY to continue.
7. Press READY.
71
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
12. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter the
Syringe Weigh
appropriate method parameters. C
O
N 1. POWER: 0%
Note: Refer to the QUICK TEST section of this manual for instructions for S 2. DELTA WEIGHT: 0.0 mg
entering method parameters for Constant Weight and Set Time. T 3. DELTA TIME: 0 secs
A 4. MAX TIME: 10 mins
N 5. BIAS: 0.00%
13. Press the operation key below NEXT PAGE to access additional method 6. MAX TEMP: 110 C
T
parameters.
W
E
I Press item number to select.
G
H
MAIN PREV NEXT
T MENU PAGE PAGE
Syringe Weigh
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
72
14. Press the numbers (1 - 6) and enter the appropriate method parameters.
Syringe Weigh
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature, and time.
XXXXXXXX
16. If Autotrack is turned off and a method identification name or number is required,
press the operation key below ID. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
EXTERNAL
ID SYRINGE
17. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
18. Press READY to return to the test screen.
19. Press the operation key below EXTERNAL SYRINGE to engage the external
XXXXXXXX
balance and activate the external balance syringe weigh menu.
Note: If External Balance does not appear on the screen as an option, return to the Power: XXX%
Temp (XXX): XX.X
Main Menu screen; press 4 - Setup; press 1 System Options; press 4 - Time: XX:XX
External Balance; then press the applicable number to select an external balance.
Wt: X.XXXXg
EXTERNAL
ID SYRINGE
73
20. Lift the cover of the SMART Turbo. Place two glass fiber sample pads on the
Syringe Weigh (Ext)
balance pan. Close the instrument cover. Press TARE.
ABORT
21. Wait for the instrument to tare the weight of the sample pads.
TARING BALANCE . . .
22. Ensure that the balance pan of the external balance is free of any weight. Press
Syringe Weigh (Ext)
TARE on the SMART Turbo.
ABORT
TARING BALANCE . . .
74
24. Place the syringe filled with sample on the external balance pan.
Syringe Weigh (Ext)
Note: Press the operation key below ABORT to end the analysis.
ABORT
READING BALANCE . . .
26. Lift the SMART Turbo cover. Remove the pads from the balance pan.
Syringe Weigh (Ext)
28. Dispense the sample from the syringe on the tared sample pads.
Dispense sample on pads. Place
29. Place the empty syringe back on the external balance pan. empty syringe on external
balance and press READY.
ABORT
READING BALANCE . . .
75
32. Place the sample pads with the sample on the balance pan. Close the
XXXXXXXX
instrument cover.
Sample ID: Sample XX
33. Press START. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Ratio: X.XXXX
T
Wt: X.XXXXg
EXTERNAL
ID SYRINGE
As the analysis begins, the flashing microwave indicators in the balance icon appear
XXXXXXXX
and the time begins counting (up for Constant Weight or down for Set Time). The
sample weight decreases as the moisture is removed.
Power: XXX%
Temp (XXX): XX.X
During the drying time, the operation key below SOLIDS or MOISTURE may be Time: XX:XX
pressed to display % solids or % moisture. Ratio: XX.XXXX
Moisture: XX.XX%
Note: Press the operation key below STOP TEST to end the analysis.
Wt: X.XXXXg
STOP
SOLIDS TEST
When the weight loss is equal to or less than the selected parameter, five short
XXXXXXXX
beeps will be heard, and the Data Results screen will appear, displaying either the %
moisture or % solids as selected.
Note: Press READY to analyze additional samples using the same method.
XX.XX%M
Note: Press the operation key below FORM FEED to advance paper from the
internal printer.
34. Press the operation key below DATA to display the analysis data.
Press READY to continue.
MAIN FORM
MENU FEED DATA
76
35. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
Solids: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
36. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
PREV
PAGE
37. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Dry Time: XX:XX
Moisture: XX.XX%
38. Press the operation key below MAIN MENU to end the analysis and return to the Solids: XX.XX%
CEM Main Menu screen.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
77
Moisture/Solids - Ash
This procedure is used to determine the ash and volatile solids content of a sample.
Recommended Equipment
CEM Phoenix Microwave Muffle Furnace or other ashing furnace.
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows select the first letter or number of the
METHOD NAME:
method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
5. Continue using the operation keys to select each letter or number of the method Space Delete
name. Press ENTER after each selection until the entire method name is
selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to enter
the numbers for the name. Press READY to continue.
6. Press READY.
78
MAIN PREV
MENU PAGE
1. STANDARD TEST
2. WASTEWATER
3. DILUTION
4. SYRINGE WEIGH
5. ASH
MAIN PREV
MENU PAGE
11. Press the numbers (1 - 6 Constant Weight or 1 - 4 Set Time) and enter the
Syringe Weigh
appropriate method parameters. C
O
N 1. POWER: 0%
S 2. DELTA WEIGHT: 0.0 mg
Note: Refer to the QUICK TEST section of this manual for instructions for T 3. DELTA TIME: 0 secs
4. MAX TIME: 10 mins
entering method parameters for Constant Weight and Set Time. A
5. BIAS: 0.00%
N
6. MAX TEMP: 110 C
T
12. Press the operation key below NEXT PAGE to access additional method
parameters. W
E
I Press item number to select.
G
H
MAIN PREV NEXT
T MENU PAGE PAGE
Syringe Weigh
1. POWER: 0%
2. RUN TIME: 00:00 min:sec
S 3. BIAS: 0.00%
E 4. MAX TEMP: 110 C
T
T
I
M
E Press item number to select or
NEXT PAGE for more menu items.
79
13. Press the numbers (1 - 6) and enter the appropriate method parameters.
Syringe Weigh
MAIN PREV
MENU PAGE
Note: The method test screen appears indicating the power, temperature, and time.
XXXXXXXX
15. If Autotrack is turned off and a method identification name or number is
required, press the operation key below ID. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID REWEIGH
16. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
17. Press READY to return to the test screen.
18. Lift the cover of the SMART Turbo. Place two glass fiber sample pads on the
XXXXXXXX
balance pan. Close the instrument cover.
SAMPLE ID: XXX
19. Press TARE. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID REWEIGH
80
20. Wait for the instrument to tare the weight of the sample pads.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight of
XXXXXXXX
the sample pads has been tared.
Sample ID: Sample XX
21. Lift the instrument cover. Apply the sample in a thin, even layer to one of the Power: XXX%
Temp (XXX): XX.X
sample pads. Quickly and gently place the sample pads back on the balance Time: XX:XX
pan. Close the instrument cover. Ratio: X.XXXX T
ID REWEIGH
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
As the analysis begins, the flashing microwave indicators in the balance icon appear
XXXXXXXX
and the time begins counting (up for Constant Weight or down for Set Time).
Sample ID: XXXXXX
During the drying time, the operation key below SOLIDS or MOISTURE may be Power: XXX%
Temp (XXX): XX.X
pressed to display % solids or % moisture. Time: XX:XX
Note: Press the operation key below STOP TEST to abort the analysis. Moisture: XX.XX%
Wt: X.XXXXg
When the drying time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying either the % moisture or % solids as selected.
STOP
SOLIDS TEST
81
23. To ash the dried sample, fold the pads; place them in an ashing crucible; and
Data Results
place the crucible in the ashing furnace. Ash the sample by the defined method.
XX.XX%M
MAIN FORM
MENU FEED DATA
25. Press the operation key below REWEIGH.
XXXXXXXX
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID REWEIGH
26. Press the numerical key to select the proper sample to be reweighed.
Select Sample ID
1. XXXX
2. XXXXXX
3. XXXX
4. XXXX
5. XXXXXX
27. Lift the instrument cover. Place the ashed sample on the balance pan. Close
XXXXXXXX
the instrument cover.
Sample ID: XXXXXX
28. Press START. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Note: To reweigh additional samples, press READY and follow the steps outlined
above.
Wt: X.XXXXg
ID REWEIGH
82
The instrument reweighs the ashed sample and calculates the data results.
29. Press the operation key below DATA to display the analysis data.
REWEIGHING BALANCE . . .
30. Press the operation key below SAMPLE WEIGHTS to view sample weight
Data Results
information.
XX.XX%M
% ASH
MAIN FORM
MENU FEED DATA PRINT
The Sample Weight Data screen displays the initial weight, the final weight, the
Sample Weight Data
differential weight and the end weight.
Initial Wt: XX.XXXXg
31. Press the operation key below PREV PAGE to return to the Data Results Final Wt: XX.XXXXg
screen. Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
PREV
PAGE
32. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to continue analysis using the same method. Dry Time: XX:XX
Moisture: XX.XX%
33. Press the operation key below MAIN MENU to end the analysis and return to Solids: XX.XX%
the CEM Main Menu screen.
Ash:
83
Moisture/Fat Standard
Moisture/Fat/Protein - Standard
This procedure is used to determine the moisture/fat and/or moisture/fat/protein content of a sample.
Recommended Equipment
CEM SMART Trac I or SMART Trac II
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
5. Continue using the operation keys to select each letter or number of the Space Delete
method name. Press ENTER after each selection until the entire method name
is selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to enter
the numbers for the name. Press READY to continue.
6. Press READY.
84
MAIN PREV
MENU PAGE
1. STANDARD
2. DILUTIONS
3. MODIFIED FAT
MAIN PREV
MENU PAGE
11. Press the numbers (1 - 7 Constant Weight or 1 - 5 Set Time) and enter the
Standard Moisture/Fat
appropriate method parameters. C
O
N Moisture Parameters
Note: Refer to the QUICK TEST section of this manual for instructions for S
entering method parameters for Constant Weight and Set Time. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
12. Press the operation key below NEXT PAGE to access additional method 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
parameters.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
Standard Moisture/Fat
Moisture Parameters
S 1. POWER: 0%
E 2. DRY TIME: 00:00 min:sec
T 3. BIAS: +0.00t
4. MIN RESUSLT: 0.00%
T 5. MAX RESULT: 100.00%
I
M
E Press item number to select or
NEXT PAGE for more menu items.
85
13. Press the numbers (1 - 7 Constant Weight) and enter the appropriate
Standard Moisture/Fat
method parameters. C
O
N Moisture Parameters
Note: Press the operation key below PREV PAGE to return to the moisture S
parameters screen. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
14. Press the operation key below NEXT PAGE to access additional method 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
parameters.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
Note: Press the operation key below PREV PAGE to return to the fat E
I Press item number to select or
parameters screen NEXT PAGE for more menu items.
G
H
MAIN PREV NEXT
T MENU PAGE PAGE
15. Press the numbers 1 4 and enter the appropriate method parameters.
Moisture/Fat
MAIN PREV
MENU PAGE
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID REWEIGH
18. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number and press ENTER.
Highlight choice, press ENTER.
19. Press READY to continue.
86
20. Lift the cover of the SMART Turbo. Place one round and two square glass fiber
XXXXXXXX
sample pads on the balance pan (round pad on bottom). Close the instrument
cover.
Power: XXX%
Temp (XXX): XX.X
21. Press TARE. Time: XX:XX
Wt: X.XXXXg
ID REDRY
22. Wait for the instrument to tare the weight of the sample pads. The method test
screen will reappear when the tare function is complete.
TARING BALANCE . . .
Note: The T in the lower left corner of the balance icon indicates that the weight
XXXXXXXX
of the sample pads has been tared.
23. Lift the instrument cover. Remove the square pads from the sample pan. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
24. Apply sample in a thin, even layer to one of the square sample pads and cover T
the sample with the second pad.
Wt: X.XXXXg
25. With the round pad still on the balance pan, quickly place the square sample
pads back on the balance pan. Close the instrument cover. Place sample and pads on
balance and press START.
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
87
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting (up for Constant Weight or down for Set
Time. The sample weight decreases as the moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
Note: Press the operation key below STOP TEST to end the analysis. Time: XX:XX
During the drying time, the operation key below SOLIDS may be pressed to display
% solids or
% moisture. Moisture: XX.XX
Wt: X.XXXXg
ID REWEIGH
When the drying time is complete, five short beeps will be heard, and the Data
Data Results
Results screen will appear, displaying either the % moisture or % solids as
selected.
27. Press READY to redry sample or to analyze additional samples.
XX.XX%M
MAIN FORM
MENU FEED DATA PRINT
28. Remove and place one sheet of Trac Film on the platform of the Trac Sation.
29. Lift the cover of the SMART Turbo and remove the pads from the balance pan.
30. Place the two square pads and dried sample in the center of the Trac Film.
88
31. Prepare the sample pads. Fold the left corner of the film and pads as illustrated. Fold the right
corner of the film and pads as illustrated. Fold the right corner. Pull the lower edge of the film and
sample pads toward the top and begin to roll them into a tube.
Note: For samples that are rigid after drying and more difficult to roll into a cylinder, prepare the pads as
illustrated.
89
32. Position the wrapped tube sample into the Trac tube. Carefully press the sample into the bottom of the tube
with the Trac Station press. The sample should be pressed firmly to ensure that the sample is positioned in the
appropriate analysis area.
Note: The Trac Station has a mark to verify the height of the sample in the tube.
33. Place the Trac tube with the pressed sample pads into the sample area of the SMART Trac magnet.
The SMART Trac II analyzes and records the total proton activity of fat present in the sample. The SMART Turbo
then analyzes the data and calculates and displays the fat results.
90
Note: Additional samples can be dried prior to redry of samples. Samples must be
XXXXXXXX
kept in proper order for redrying.
Wt: X.XXXXg
ID REDRY
37. Using the numeric key(s), press the number of the sample to be redried.
Select Sample ID
1. XXXX
2. XXXXXX
3. XXXX
4. XXXX
5. XXXXXX
38. Lift the cover of the SMART Turbo. Place the round pad with the extracted
XXXXXXXX
sample on the balance pan. Close the instrument cover.
Wt: X.XXXXg
ID REDRY
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting down. The sample weight decreases as the
moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
Note: Press the operation key below STOP TEST to end the analysis. Redry: XX:XX
When the drying time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying the % fat.
Fat: XX.XX
Wt: X.XXXXg
STOP
TEST
91
Note: Press the operation key below FORM FEED to advance paper from the
XXXXXXXX
internal printer.
40. Press the operation key below DATA to display the analysis data.
XX.XX%F
MAIN FORM
MENU FEED DATA PRINT
41. Press the operation key below SAMPLE WEIGHTS to display the weight data.
Data Results
Note: If performing a moisture/fat/protein analysis, the data results screen will also
Data Results
provide the % protein of the sample.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
Final Wt: XX.XXXXg
Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
M Bias: X.XX%
F Bias: X.XX%
PREV
PAGE
92
PREV
PAGE
42. Press the operation key below PREV PAGE to return to the Data Results
Data Results
screen.
Sample ID: XXXXXXXX
43. Press the operation key below PRINT to print the analysis results either on the Dry Time: XX:XX
internal printer or an external printer, if installed. Moisture: XX.XX%
Note: Press READY to analyze additional samples using the same method.
Redry Time: XX:XX
44. Press the operation key below MAIN MENU to end the analysis and return to Fat: XX.XX%
the CEM Main Menu screen. Protein: X.XX%
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
93
This procedure requires the CEM SMART Trac. Refer to the SMART Trac/SMART Trac II Operation Manual for
operating instructions for the applicable system.
Some types of samples require dilution prior to extraction of the fat. This procedure combines the dilution and the
fat analysis procedures.
Recommended Equipment
External Balance
Fat Extraction System
Note: Refer to the Setup section of this manual to ensure that the applicable external balance is selected.
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
5. Continue using the operation keys to select each letter or number of the Space Delete
method name. Press ENTER after each selection until the entire method name
is selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to enter
the numbers for the name. Press READY to continue.
6. Press READY.
94
MAIN PREV
MENU PAGE
1. STANDARD
2. DILUTIONS
3. MODIFIED FAT
MAIN PREV
MENU PAGE
11. Press the numbers (1 - 7 Constant Weight or 1 - 4 Set Time) and enter
Dilution Moisture/Fat
the appropriate method parameters. C
O
N Moisture Parameters
Note: Refer to the QUICK TEST section of this manual for instructions for S
entering method parameters for Constant Weight and Set Time. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
12. Press the operation key below NEXT PAGE to access the fat method 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
parameters screen.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
Dilution Moisture/Fat
Moisture Parameters
S 1. POWER: 0%
E 2. DRY TIME: 00:00 min:sec
T 3. BIAS: +0.00t
4. MIN RESULT: 0.00%
T 5. MAX RESULT: 100.00%
I
M
E Press item number to select or
NEXT PAGE for more menu items.
95
13. Press the numbers (1 - 7 Constant Weight or 1 -5 Set Time) and enter
Dilution Moisture/Fat
the appropriate method fat parameters. C
O
N Moisture Parameters
Note: Refer to the QUICK TEST section of this manual for instructions for S
entering method parameters for Constant Weight and Set Time. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
14. Press the operation key below NEXT PAGE to access additional method 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
parameters.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
Dilution Moisture/Fat
S Moisture Parameters
E 1. MAX TEMP: XXX C
T 2. MIN WT RANGE;: X.XXg
3. MAX WT RANGE: X.XXg
4. WT COMPENSATION: ON
T
I
M Press READY TO RUN TEST
E
MAIN PREV
MENU PAGE
15. Press the numbers (1 - 4) and enter the appropriate method parameters.
Dilution Moisture/Fat
MAIN PREV
MENU PAGE
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Ratio: 1.0000
Wt: X.XXXXg
ID RATIO DILUTION
96
18. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number
Highlight choice, press ENTER.
19. Press READY to return to the method screen.
Note: If the sample and diluent are to be weighed on a balance not connected to
XXXXXXXX
the SMART Turbo, press the operation key below RATIO to enter the dilution ratio.
Note: The applicable external balance must be selected in Setup procedures to Power: XXX%
Temp (XXX): XX.X
perform a moisture/fat or moisture/fat/protein dilution analysis. Time: XX:XX
Ratio: 1.0000
Wt: X.XXXXg
ID RATIO DILUTION
20. Using the numeric keys, enter the dilution ratio.
XXXXXXXX
Note: The dilution ratio is the ratio between the amount of sample and the amount
of diluent. The internal dilution ratio is calculated as the sample weight after the Power: XXX%
Temp (XXX): XX.X
diluent is added divided by the initial sample weight. Time: XX:XX
Ratio: 1.0000
21. Press ENTER.
Wt: X.XXXXg
22. Press the operation key below DILUTION to engage the external balance and
activate the dilution menu.
Input ratio, press ENTER.
Entry: 1.0000
ID RATIO DILUTION
23. Place an empty container suitable for the sample and diluent on the external
Dilution Moisture/Fat
balance. Wait for the weight to stabilize.
ABORT
97
25. Wait for the instrument to tare the weight of the container.
TARING BALANCE . . .
26. Place the sample in the container on the external balance pan.
Dilution Moisture/Fat
ABORT
READING BALANCE . . .
27. Add the diluent to the sample in the container on the external balance pan.
Dilution Moisture/Fat
ABORT
98
The instrument reads and records the weight of the sample and diluents.
READING BALANCE . . .
The instrument displays the weight of the sample, the weight of the sample and
Dilution Moisture/Fat (Ext)
diluent, and the dilution ratio.
31. Lift the cover of the SMART Turbo. Place one round and two square glass
XXXXXXXX
fiber sample pads on the balance pan (round pad on bottom). Close the
instrument cover. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
32. Press TARE. Ratio: X.XXXX
Wt: X.XXXXg
ID RATIO DILUTION
33. Wait for the instrument to tare the weight of the sample pads.
TARING BALANCE . . .
99
Note: The T in the lower left corner of the balance icon indicates that the weight
XXXXXXXX
of the sample pads has been tared.
34. Lift the instrument cover. Remove the square sample pads from the balance Power: XXX%
Temp (XXX): XX.X
pan. Time: XX:XX
Ratio: X.XXXX T
35. Apply the diluted sample in a thin, even layer to one of the square sample
pads and cover the sample with the other square sample pad. Wt: X.XXXXg
36. With the round pad still on the balance pan, quickly and gently place the Place sample and pads on
sample pads back on the balance pan. Close the instrument cover. balance and press START.
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting (up for Constant Weight or down for Set
Time). The sample weight decreases as the moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
During the drying time, the operation key below SOLIDS or MOISTURE may be Redry: XX:XX
pressed to display % solids or % moisture.
When the weight loss is equal to or less than the selected parameter, five short
beeps will be heard, and the Data Results screen will appear, displaying either the Moisture: XX.XX%
% moisture or % solids as selected. Wt: X.XXXXg
STOP
SOLIDS TEST
Note: Press the operation key below FORM FEED to advance paper from the
XXXXXXXX
internal printer.
37. Press READY to redry the sample or to analyze additional samples using the
same method.
XX.XX%M
MAIN FORM
MENU FEED DATA PRINT
100
38. Lift the cover of the SMART Turbo. Remove the pads from the balance pan.
XXXXXXXX
Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
Ratio: X.XXXX
Wt: X.XXXXg
ID REDRY
39. Remove and place one sheet of Trac Film on the platform of the Trac Station.
40. Place the two square pads and dried sample in the center of the Trac Film.
101
41. Prepare the sample pads. Fold the left corner of the film and pads as illustrated. Fold the right
corner of the film and pads as illustrated. Fold the right corner. Pull the lower edge of the film and
sample pads toward the top and begin to roll them into a tube.
Note: For samples that are rigid after drying and more difficult to roll into a cylinder, prepare the pads as
illustrated.
102
42. Position the wrapped tube sample into the Trac tube. Carefully press the sample into the bottom of the tube
with the Trac Station press. The sample should be pressed firmly to ensure that the sample is positioned in the
appropriate analysis area.
Note: The Trac Station has a mark to verify the height of the sample in the tube.
43. Place the Trac tube with the pressed sample pads into the sample area of the SMART Trac magnet.
The SMART Trac II analyzes and records the total proton activity of fat present in the sample. The SMART Turbo
then analyzes the data and calculates and displays the fat results.
103
46. Press the Run/Stop button on the extractor to start the extraction cycle. When
Select Sample ID
the extraction is complete, a beep tone will sound, and the light in the
Run/Stop button will flash. While the extractor cup is still in the inverted
1. XXXX XXXX
position, unlatch the lid and remove the round sample pad on which the 2. XXXX XX
chopped square pads and extracted and dried sample have been deposited. 3. XXXXXXX
4. XXXX
Latch the cup lid. The extractor cup will automatically rotate 180 degrees to 5. XXXXXX
the upright position.
Note: To dry additional samples, place the sample pads on the balance and press
XXXXXXXX
TARE.
Power: XXX%
47. Press the operation key below REDRY. Temp (XXX): XX.X
Time: XX:XX
Ratio: X.XXXX
48. Using the numeric key(s), press the number of the sample to be redried.
49. Lift the cover of the SMART Turbo. Place the round pad with the extracted
Wt: X.XXXXg
sample on the balance pan. Close the instrument cover.
Place pads on balance and press
50. Press START. TARE pr press START to redry.
ID REDRY
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting down. The sample weight decreases as the
moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
Note: Press the operation key below STOP TEST to end the analysis. Redry: XX:XX
When the drying time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying the % fat.
Moisture: XX.XX%
Wt: X.XXXXg
STOP
SOLIDS TEST
104
Note: Press the operation key below FORM FEED to advance paper from the
XXXXXXXX
internal printer.
51. Press the operation key below DATA to display the analysis data.
XX.XX%F
MAIN FORM
MENU FEED DATA PRINT
52. Press the operation key below SAMPLE WEIGHTS to display the weight data.
Data Results
Note: If performing a moisture/fat/protein analysis, the data results screen will also
Data Results
provide the % protein of the sample.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight.
Initial Wt: XX.XXXXg
Final Wt: XX.XXXXg
Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
M Bias: X.XX%
F Bias: X.XX%
MAIN PREV
MENU PAGE
105
MAIN PREV
MENU PAGE
53. Press the operation key below PREV PAGE to return to the Data Results
Data Results
screen.
Sample ID: XXXXXXXX
54. Press the operation key below PRINT to print the analysis results either on the Dry Time: XX:XX
internal printer or an external printer, if installed. Moisture: XX.XX%
Note: Press READY to analyze additional samples using the same method.
Redry Time: XX:XX
55. Press the operation key below MAIN MENU to end the analysis and return to Fat: XX.XX%
the CEM Main Menu screen.
Press READY to continue.
106
This procedure requires the CEM Fat Extraction System. Refer to the SMART Trac/SMART Trac II Operation
Manual for operating instructions for the applicable system.
With the modified moisture/fat or moisture/fat/protein procedure, the fat is extracted from one sample while
another sample is dried for moisture analysis. This procedure permits determination of fat content of samples in
which initial drying of the sample may bind the fat molecules in the sample matrix.
Recommended Equipment
Fat Extraction System
Note: Refer to the Setup section of this manual to ensure that the applicable external balance is selected.
1. With the CEM Main Menu displayed, press 2 to activate the Edit/Create
CEM Main Menu
Method screen.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
3. Using the operation keys below the arrows select the first letter or number of
METHOD NAME:
the method name.
0123456789AB
4. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
5. Continue using the operation keys to select each letter or number of the Space Delete
method name. Press ENTER after each selection until the entire method
name is selected (16 characters maximum). Highlight choice, press ENTER.
Note: If the method name utilizes numbers only, use the numeric keypad to enter
the numbers for the name. Press READY to continue.
6. Press READY.
107
MAIN PREV
MENU PAGE
1. STANDARD
2. DILUTIONS
3. MODIFIED FAT
MAIN PREV
MENU PAGE
Note: Press the operation key below PREV PAGE to return to the
Modified Moisture/Fat
moisture/fat mode screen. C
O
N Moisture Parameters
11. Press the numbers (1 - 7 Constant Weight or 1 - 5 Set Time) and enter S
the appropriate method parameters. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
Note: Refer to the QUICK TEST section of this manual for instructions for 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
entering method parameters for Constant Weight and Set Time.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
12. Press the operation key below NEXT PAGE to access the fat method E
I Press item number to select or
parameters screen. NEXT PAGE for more menu items.
G
H
MAIN PREV NEXT
T MENU PAGE PAGE
Modified Moisture/Fat
Moisture Parameters
S 1. POWER: 0%
E 2. DRY TIME: 00:00 min:sec
T 3. BIAS: +0.00t
4. MIN RESULT: 0.00%
T 5. MAX RESULT: 100.00%
I
M
E Press item number to select or
NEXT PAGE for more menu items.
108
13. Press the numbers (1 - 7 Constant Weight or 1 -5 Set Time) and enter
Modified Moisture/Fat
the appropriate method fat parameters. C
O
N Moisture Parameters
Note: Refer to the QUICK TEST section of this manual for instructions for S
entering method parameters for Constant Weight and Set Time. T 1. POWER: 0%
A 2. DELTA WEIGHT: 0.0 mg
N 3. DELTA TIME: 0 secs
14. Press the operation key below NEXT PAGE to access additional method 4. MAX TIME: 10 mins
T 5. BIAS: 0.00%
parameters.
6. MIN RESULT: 0.00%
W 7. MAX RESULT: 100.00%
E
I Press item number to select or
G NEXT PAGE for more menu items.
H
MAIN PREV NEXT
T MENU PAGE PAGE
Modified Moisture/Fat
S Moisture Parameters
E 1. POWER: 0%
T 2. DRY TIME: 00:00 min:sec
3. BIAS: +0.00t
4. MIN RESUSLT: 0.00%
T 5. MAX RESULT: 100.00%
I
M
E Press item number to select or
NEXT PAGE for more menu items.
15. Press the numbers (1 - 4) and enter the appropriate method parameters.
Modified Moisture/Fat
MAIN PREV
MENU PAGE
Wt: X.XXXXg
ID REDRY
109
18. Using the operation keys below the arrows, position the cursor on (select) the
SAMPLE ID:
first number or letter of the sample identification. Press ENTER. Continue to
position the cursor on each letter or number and press ENTER until the
0123456789AB
identification is complete. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If using an identification number only, use the numeric keys to enter the Space Delete
number.
Highlight choice, press ENTER.
19. Press READY to return to the method test screen.
20. Lift the cover of the SMART Turbo. Place one round and two square glass
XXXXXXXX
fiber sample pads on the balance pan (round pad on bottom). Close the
instrument cover. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
21. Press TARE.
Wt: X.XXXXg
ID REDRY
22. Wait for the instrument to tare the weight of the pads.
TARING BALANCE . . .
23. Lift the cover of the SMART Turbo. Remove the square sample pads from the
Modified Moisture/Fat
balance pan.
24. Apply the sample in a thin, even layer to one of the square sample pads and
cover the sample with the other square pad.
ABORT
110
The SMART Turbo weighs and records the initial weight of the sample.
WEIGHING BALANCE . . .
27. Lift the cover of the SMART Turbo and remove the pads from the balance pan.
28. Remove and place one sheet of Trac Film on the platform of the Trac Station.
29. Place the two square pads and dried sample in the center of the Trac Film.
111
30. Prepare the sample pads. Fold the left corner of the film and pads as illustrated. Fold the right
corner of the film and pads as illustrated. Fold the right corner. Pull the lower edge of the film and
sample pads toward the top and begin to roll them into a tube.
Note: For samples that are rigid after drying and more difficult to roll into a cylinder, prepare the pads as
illustrated.
112
31. Position the wrapped tube sample into the Trac tube. Carefully press the sample into the bottom of the tube
with the Trac Station press. The sample should be pressed firmly to ensure that the sample is positioned in the
appropriate analysis area.
Note: The Trac Station has a mark to verify the height of the sample in the tube.
32. Place the Trac tube with the pressed sample pads into the sample area of the SMART Trac magnet.
The SMART Trac II analyzes and records the total proton activity of fat present in the sample. The SMART Turbo
then analyzes the data and calculates and displays the fat results.
35. The SMART Trac II analyzes and records the total proton activity of fat present in the sample. The SMART
Turbo then analyzes the data and calculates and displays the fat results.
113
36. Wait for the SMART Turbo to tare the weight of the sample pads.
TARING BALANCE . . .
37. Lift the cover of the SMART Turbo. Remove the square sample pads from the
Modified Moisture/Fat
balance pan.
38. Apply the sample in a thin, even layer to one of the square sample pads and
cover the sample with the other square pad.
Note: The T in the lower left corner of the balance icon indicates that the weight
XXXXXXXX
of the sample pads has been tared.
Sample ID: XXXXXXXX
41. Press START. Power: XXX%
Temp (XXX): XX.X
Time: XX:XX
T
Wt: X.XXXXg
ID REDRY
The instrument reads and records the initial weight of the sample prior to beginning
the analysis.
READING BALANCE . . .
114
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the time begins counting (up for Constant Weight or down for Set
Time). The sample weight decreases as the moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
During the drying time, the operation key below SOLIDS or MOISTURE may be Dry Time: XX:XX
pressed to display % solids or % moisture.
When the weight loss is equal to or less than the selected parameter, five short
beeps will be heard, and the Data Results screen will appear, displaying either the Solids: XX.XX%
% moisture or % solids as selected. Wt: X.XXXXg
Note: Press the operation key below FORM FEED to advance paper from the
STOP
internal printer. MOISTURE TEST
44. When the extraction of sample no. 1 is complete, the extractor cup will be XX.XX%M
inverted, a beep tone will sound, and the light in the Run/Stop button will flash.
While the extractor cup is still in the inverted position, unlatch the lid and
remove the round sample pad on which the chopped square pads and
extracted sample have been deposited. Latch the cup lid. The extractor cup
Press READY to continue.
will automatically rotate 180 degrees to the upright position.
MAIN FORM
MENU FEED DATA PRINT
45. Place the pad with the extracted sample no. 1 on the balance pan of the
XXXXXXXX
SMART Turbo. Close and latch the instrument cover.
Power: XXX%
46. Press the operation key below REDRY. Temp (XXX): XX.X
Time: XX:XX
Wt: X.XXXXg
ID REDRY
47. Using the numeric key(s), press the applicable number of the sample to be
Select Sample ID
redried.
1. XXXX XXXX
2. XXXX XX
3. XXXXXXX
4. XXXX
5. XXXXXX
115
Wt: X.XXXXg
ID REDRY
As the analysis begins, the flashing microwave indicators in the balance icon
XXXXXXXX
appear and the redry time begins counting down. The sample weight decreases as
the moisture is removed. Sample ID: XXXXXX
Power: XXX%
Temp (XXX): XX.X
Note: Press the operation key below STOP TEST to end the analysis. Redry: XX:XX
When the redry time is complete, five short beeps will be heard, and the Data
Results screen will appear, displaying the % fat.
Fat: XX.XX
Wt: X.XXXXg
STOP
TEST
Note: Press the operation key below FORM FEED to advance paper from the
XXXXXXXX
internal printer.
49. Press the operation key below DATA to display the analysis data.
Note: The SMART Turbo will store the final weight of the fat extracted sample. XX.XX%F
Based on the weight of sample no. 1 prior to extraction, the weight prior to redry,
and the final weight after redry plus the weights of sample no. 2 prior to and
following the drying process, the instrument will compute and display fat, and if
applicable, protein analysis results.
Press READY to continue.
MAIN FORM
MENU FEED DATA PRINT
50. Press the operation key below SAMPLE WEIGHTS to display the weight data.
Data Results
116
Note: If performing a moisture/fat/protein analysis, the data results screen will also
Data Results
provide the % protein of the sample.
Sample ID: XXXXXXXX
Dry Time: XX:XX
Moisture: XX.XX%
The Sample Weight Data screen displays the initial weight, the final weight and the
Sample Weight Data
differential weight
Initial Wt: XX.XXXXg
Final Wt: XX.XXXXg
Diff Wt: XX.XXXXg
End Wt: XX.XXXXg
M Bias: X.XX%
F Bias: X.XX%
MAIN PREV
MENU PAGE
52. Press the operation key below PRINT to print the analysis results either on the
Data Results
internal printer or an external printer, if installed.
Sample ID: XXXXXXXX
Note: Press READY to analyze additional samples using the same method. Dry Time: XX:XX
Moisture: XX.XX%
53. Press the operation key below MAIN MENU to end the analysis and return to
the CEM Main Menu screen.
Redry Time: XX:XX
Fat: XX.XX%
117
Load Method
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. NEW METHOD
2. TEMP VERIFY
3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
When the CEM Main Menu returns to the screen, the selected method will be
CEM Main Menu
displayed.
1. QUICK TEST
3. Press READY to display the initial screen of the selected method. 2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
118
Setup
Setup procedures include system parameters such as date/time, printer functions,
CEM Main Menu
utilities, calibration, system password, etc.
1. QUICK TEST
1. With the CEM Main Menu displayed, press 4 to activate Setup. 2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
The Key Beeper is an audible beep after each key stroke and can be turned on
or off.
119
Predry time is a set time for the instrument to activate microwave energy, once the
System Options
TARE key is pressed, to dry the sample pads prior to taring the weight of the pads.
1. PREDRY: 0
13. Press 1 to select and enter a predry time.
14. Using the numeric keys, enter the preheat time (0 - 60 seconds).
16. Press the operation key below prev page to return to the System Options
Input time, press ENTER.
screen. Entry: 00
MAIN PREV
MENU PAGE
17. Press the operation key below PREV PAGE to return to the Setup screen.
System Options
1. AUTOTRACT ID: ON
2. AUTO PRINT: RESULTS
3. AUTO START: OFF
4. EXTERNAL BALANCE: NONE
5. LANGUAGE: ENGLISH
6. KEY BEEPER: ON
7. HEATER TEMP: 42
8. BAR GRAPH: ON
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATION
8. SECURITY
NEXT
PAGE
120
The System Information screen is for information purposes only. This screen System Information
provides the system software version, the PIC software version, the electrical line
frequency, the type of internal and external balance, etc. UNIT SN: XXXXXX
SOFTWARE VER: XXXXX
PIC SOFTWARE VER: X.XX
19. Press the operation key below PREV PAGE to return to the Setup screen. LINE FREQAUENCY: XX Hz
INTERNAL BALANCE: XXXXXXXX
EXTERNAL BALANCE: XXXXXX
BAL CALIBRATION XXXXXX
IR CALBRATION XXXXXX
PRINTER: INTERNAL
MAG TIME: XXXXX:XX
SYSTEM TIME: XXXXX:XX
COVER COUNT: XXX.X
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
21. Press 1 to toggle and select the Internal printer or an external printer.
Printer
1. PRINTER: INTERNAL
Note: If an external printer is selected, the following screen will appear.
MAIN PREV
MENU PAGE
22. Press 1 to toggle and select the applicable external printer IBM, Epson,
Printer
Citizens, or Canon Bubble.
1. PRINTER: XXX
23. Press 2 to toggle and select the applicable printer pitch 10, 12 or 17 cpi. 2. PITCH: XX cpi
3. QUALITY: XXXXX
24. If applicable, press 3 to toggle and select the quality of print Draft or NLQ
(Near Letter Quality).
25. Press the operation key below PREV PAGE to return to the Setup screen.
Press item number to select.
MAIN PREV
MENU PAGE
121
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
27. Press 1 to toggle and select the applicable baud rate for the communication
COM Port
port 1200, 2400, 4800, or 9600.
1. BAUD: XXX
28. Press 2 to toggle and select the applicable data bits 7 or 8. 2. DATA: XX cpi
3. STOP: XXXXX
29. Press 3 to toggle and select the applicable stop bit(s) 1 or 2. 4. PARITY: NONE
30. Press 4 to toggle and select the applicable parity None, Even, or
Odd.
Press item number to select.
31. Press the operation key below PREV PAGE to return to the Setup screen.
MAIN PREV
MENU PAGE
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
33. Press the operation key(s) below the up and down arrows to adjust the
Contrast
instrument screen to the desired level.
************************************
34. Press the operation key below PREV PAGE to return to the Setup screen. 1 2 3 4 5 6 7 8 901234567890
ABCDEFGHIJKLMNOPQRST
A b c d e f g h ij kl m n op qr st
************************************
MAIN PREV
MENU PAGE
122
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
36. Press 1 to toggle and select the desired date format MM/DD/YYYY or
Clock
DD/MM/YYYY.
1. DATE FORMAT: MM/DD/YYYY
37. Press 2 to enter the appropriate date. 2. DATE: XX/XX/XXXX
3. TIME FORMAT: XX HOUR
4. TIME: 00:00
MAIN PREV
MENU PAGE
38. Using the numeric keypad, enter the date based on the selected date format.
Clock
MAIN PREV
MENU PAGE
43. Press the operation key below PREV PAGE to return to the Setup screen.
1. DATE FORMAT: MM/DD/YYYY
2. DATE: XX/XX/XXXX
3. TIME FORMAT: XX HOUR
4. TIME: 00:00
MAIN PREV
MENU PAGE
123
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
ABORT
47. Wait for the instrument to tare the weight of the balance pan.
. . .TARING BALANCE . . .
124
48. Lift the instrument cover. Place either a 10 gram or 50 gram weight. Close the
Calibrate Balance
instrument cover.
ABORT
Note: Wait for the instrument to calibrate the balance with the applicable weight.
Wait . . .
Calibration Complete.
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATE BALANCE
8. SECURITY
NEXT
PAGE
125
Mise en garde
MAIN PREV
MENU PAGE
Afin dviter dtre incapable dentrer un nouveau programme ou modifier
un paramtre, sassurer de documenter ou dinscrire tout mot-de-passe
actif pour le retrouver.
53. Using the operation keys below the arrows, select the first letter or number of
ENTER PASSWORD:
the password.
0123456789AB
54. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the password utilizes numbers only, use the numeric keys to enter the Space Delete
numbers for the password.
Highlight choice, press ENTER.
55. Continue using the operation keys to select each letter or number of the
password. Press ENTER after each selection until the entire password is
selected. Press READY to continue.
57. Using the operation keys below the arrows, select each letter or number of the
RE-ENTER PASSWORD:
password and press ENTER after each selection to re-enter the password.
0123456789AB
58. Press READY to activate the selected password. CDEFGHIJKLMN
OPQRSTUVWXYZ
Space Delete
PASSWORD ACTIVATED
126
1. ACTIVATE PASSWORD
2. DEACTIVATE PASSWORD
3. CHANGE PASSWORD
MAIN PREV
MENU PAGE
61. Using the operation keys below the arrows, select the first letter or number of
ENTER PASSWORD:
the password to be deactivated.
0123456789AB
62. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the password utilizes numbers only, use the numeric keypad to enter the Space Delete
numbers for the password.
Highlight choice, press ENTER.
63. Continue using the operation keys to select each letter or number of the
password. Press ENTER after each selection until the entire password is
selected. Press READY to continue.
PASSWORD DEACTIVATED
PRESS ANY KEY TO CONTINUE
1. ACTIVATE PASSWORD
2. DEACTIVATE PASSWORD
3. CHANGE PASSWORD
MAIN PREV
MENU PAGE
127
67. Using the operation keys below the arrows, select the first letter or number of
OLD PASSWORD:
the old password.
0123456789AB
68. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the password utilizes numbers only, use the numeric keypad to enter the Space Delete
numbers for the password.
Highlight choice, press ENTER.
69. Continue using the operation keys below the arrows to select each letter or
number of the old password. Press ENTER after each selection until the entire
password is selected. Press READY to continue.
71. Using the operation keys below the arrows, select the first letter or number of
NEW PASSWORD:
the new password.
0123456789AB
72. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the password utilizes numbers only, use the numeric keypad to enter the Space Delete
numbers for the password.
Highlight choice, press ENTER.
73. Continue using the operation keys to select each letter or number of the new
password. Press ENTER after each selection until the entire password is
selected. Press READY to continue.
75. Using the operation keys below the arrows, select each letter or number to re-
RE-ENTER PASSWORD:
enter the password and press ENTER after each selection.
0123456789AB
76. Press READY to activate the selected password. CDEFGHIJKLMN
OPQRSTUVWXYZ
Space Delete
128
78. Press the operation key below PREV PAGE to return to the Setup screen.
Security
1. ACTIVATE PASSWORD
2. DEACTIVATE PASSWORD
3. CHANGE PASSWORD
MAIN PREV
MENU PAGE
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATION
8. SECURITY
NEXT
PAGE
MAIN PREV
MENU PAGE
81. Using the operation keys below the arrow, select the first letter or number of
COMPANY NAME:
the company name.
0123456789AB
82. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
Note: If the company name utilizes numbers only, use the numeric keypad to enter Space Delete
the numbers for the company name.
Highlight choice, press ENTER.
83. Continue using the operation keys to select each letter or number of the
company name. Press ENTER after each selection until the entire name is
selected. Press READY to continue.
129
1. COMPANY NAME
2. DELETE METHOD
3. SERIAL OPTIONS
4. UNIT SN
5. CALIBRATE Intelli-Temp
MAIN PREV
MENU PAGE
Note: If necessary, press the operation key below NEXT PAGE to locate the
1. XXXXXXXXXX
method to be deleted. 2. XXXXXX
3. XXXX
4. XXXXXXX
5. XXXXXXXX
6. XXXXXX
MAIN PREV
MENU PAGE
87. Press the operation key below Yes to delete the method or No to cancel
Delete Method
the deletion process.
YES NO
1. XXXXXXXXXX
2. XXXXXX
3. XXXX
4. XXXXXXX
5. XXXXXXXX
6. XXXXXX
MAIN PREV
MENU PAGE
130
1. COMPANY NAME
2. DELETE METHOD
3. SERIAL OPTIONS
4. UNIT SN
5. CALIBRATE Intelli-Temp
MAIN PREV
MENU PAGE
Note: The Serial Options screens are for use when connecting the SMART Turbo
SERIAL DATA OPTIONS
to a PC. If the instrument is connected to a PC, the Results Data in the first
options screen should set on PC. The additional information presented in the
1. RESULTS/DATA: OFF
Serial Options screens should be turned on or off based on methods being 2. TIME STAMP: ON
performed and the data desired to be sent to the PC. 3. COMPANY NAME: ON
4. METHOD NAME: ON
5. SAMPLE ID: ON
90. Press the applicable number(s) to turn the data results on or off. 6. RUN MODE: ON
7. RUN OPTION: ON
8. % DRY POWER: ON
91. Press the operation key below NEXT PAGE to access additional serial data
options.
Press item number to select or
NEXT PAGE for more menu items
92. Press the applicable number(s) to turn the data results on or off.
SERIAL DATA OPTIONS
93. Press the operation key below NEXT PAGE to access additional serial data
1. %REDRY POWER: OFF
options. 2. DRY TIME: ON
3. REDRY TIME: ON
4. % MOISTURE: ON
5. % SOLIDS: ON
6. % FAT: ON
7. % PROTEIN: ON
8. % MAX TEMP: ON
94. Press the applicable number(s) to turn the data results on or off.
SERIAL DATA OPTIONS
95. Press the operation key below NEXT PAGE to access additional serial data
1. % MOISTURE BIAS: ON
options. 2. % FAT BIAS: ON
3. % ASH + CARB: ON
96. Press the operation key below MAIN MENU to return to the CEM Main Menu. 4. INITIAL WEIGHT: ON
5. FINAL WEIGHT: ON
6. END WEIGHT: ON
7. DIFF WEIGHT: ON
8. INIT LIQUID VOL: ON
131
97. Press the applicable number(s) to turn the data results on or off.
SERIAL DATA OPTIONS
98. Press the operation key below NEXT PAGE to access additional serial data
1. DILUTION RATIO: ON
options. 2. TSS/TVSS RESULTS: ON
3. DELTA WEIGHT: ON
99. Press the operation key below PREV PAGE to return to the Setup screen. 4. DELTA TIME: ON
5. FAT DELTA WEIGHT: ON
6. FAT DELTA TIME: ON
7. % ASH: ON
Note: If the instrument, due to component failure, etc., cold starts, the instrument
1. COMPANY NAME
serial number will be erased from the instrument software. The serial number can 2. DELETE METHOD
be found on the instrument nameplate on the back of the instrument and reentered 3. SERIAL OPTIONS
4. UNIT SN
into the software. 5. CALIBRATE Intelli-Temp
MAIN PREV
MENU PAGE
101. Using the operation keys below the arrows, select the first letter of the serial
UNIT SN:
number.
0123456789AB
102. Press ENTER. CDEFGHIJKLMN
OPQRSTUVWXYZ
103. Continue using the operation keys to select each letter and number of the Space Delete
serial number. Press ENTER after each seletion until the entire serial number
is selected. Highlight choice, press ENTER.
Note: The SMART Turbo is completely factory calibrated. Calibration of the Intelli-
1. COMPANY NAME
Temp is not necessary prior to system use. Calibration is recommended only for 2. DELETE METHOD
verification of system operation or if a problem with calibration is suspected. Refer 3. SERIAL OPTIONS
4. UNIT SN
to the Maintenance, Troubleshooting and Service section of this manual for 5. CALIBRATE Intelli-Temp
calibration procedures.
MAIN PREV
MENU PAGE
132
FORM
FEED
3. Using the numeric key(s), enter the number of the sample for which results
Select Sample ID
are to be printed.
1. SAMPLE XX
Note: Press the operation key below NEXT PAGE for additional samples. 2. SAMPLE XX
3. SAMPLE XX
4. SAMPLE XX
5. SAMPLE XX
6. SAMPLE XX
7. SAMPLE XX
8. SAMPLE XX
FORM
FEED
133
5. Using the numeric key(s), enter the number of the sample for which results
Select Sample ID
are to be viewed.
1. SAMPLE XX
Note: Press the operation key below NEXT PAGE for additional samples. 2. SAMPLE XX
3. SAMPLE XX
4. SAMPLE XX
5. SAMPLE XX
6. SAMPLE XX
7. SAMPLE XX
8. SAMPLE XX
The analysis results for the selected sample appear on the screen.
XXXXXXXX
Note: Press the operation key below FORM FEED to advance paper from the
internal printer. Press the operation key below DATA to view the Data Results
screen. Press the operation key below Print to print the results information.
XX.XX%M
MAIN FORM
MENU FEED DATA PRINT
6. Press 3 to print a method.
Print
FORM
FEED
Note: Press the operation key below NEXT PAGE to access additional methods, if
1. TEMP VERIFY
applicable. 2. POWER TEST
3. STD SOLUTION
4. LATEX
Once the method is selected, the printer prints the method information. 5. WATER BASED CHEM
6. MEAT RAW
Note: Press the operation key below MAIN MENU to return to the CEM Main 7. CHEESE
Menu screen.
MAIN NEXT
MENU PAGE
134
Statistics
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
2. Press the applicable number for the method for which statistics are to be
Select Method
viewed and/or printed.
1. NEW METHOD
Note: Press the operation key below NEXT PAGE for additional methods, if 2. TEMP VERIFY
applicable. 3. POWER TEST
4. STD SOLUTION
5. LATEX
6. WATER BASED CHEM
7. MEAT RAW
8. CHEESE
NEXT
PAGE
4. Using the numeric keys, enter the beginning date for displaying method
STATISTICS
statistical data.
1. START DATE: XX/XX/XXXX
5. Press ENTER. 2. START TIME: XX:XX
3. END DATE: XX/XX/XXXX
6. Press 2 to enter a start time. 4. END TIME: XX:XX
MAIN PREV
MENU PAGE
135
7. Using the numeric keys, enter the time to begin displaying method statistical
STATISTICS
data.
1. START DATE: XX/XX/XXXX
8. Press ENTER. 2. START TIME: XX:XX
3. END DATE: XX/XX/XXXX
9. Press 3 and 4 and repeat steps 4 through 8 to enter the end date and end 4. END TIME: XX:XX
time.
10. Press the operation key below NEXT PAGE to access the next statistical Input time, press ENTER.
screen. Entry: XX:XX
Note: The cursor on the right side of the screen moves to select specific results.
XXXXXXXX Results
Note: The samples tagged on the previous screen are displayed with the average
XXXXXXXX Results
and deviation data.
%M %S
14. Press the operation key below PRINT DATA to print the information displayed AVERAGE: xx.xx xx.xx
on the instrument screen. STD DEV: xx.xx xx.xx
RANGE: xx.xx xx.xx
MINIMUM: xx.xx xx.xx
15. Press the operation key below PREV PAGE to return to the previous page. MAXIMUM: xx.xx xx.xx
Once the previous screen is accessed, items can be retagged for additional
data, etc.
NUMBER OF SAMPLES: XX
START: XX/XX/XXXX XX:XX
16. Press the operation key below MAIN MENU to return to the CEM Main Menu END: XX/XX/XXXX XX:XX
screen.
SELECT CLEAR PREV
ALL ALL PAGE
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
136
External Printer
The SMART Turbo supports a variety of different external printer standards
IBM
Epson
Citizen GSX-190 - Available from CEM Corporation
Canon Bubble
Epson Color 740
To install the Citizen GSX-190, follow the procedures outlined below. Refer to the manual shipped with the printer
for illustrations and additional installation procedures.
1. Press the power switch of the SMART Turbo to the off position and remove the power cord from the
electrical outlet.
2. Remove the printer and its accessories from the shipping carton. Place the printer on a vibration-free printer
stand or a solid, sturdy laboratory workbench or table. Save all packing materials.
3. Perform setup instructions as outlined in the printer manual. (For color printing, the color kit must be installed.
Refer to the printer manual for instructions.)
4. Plug one connector of the computer cable into the socket on the printer. Plug the other connector into the
parallel port of the SMART Turbo. Plug the printer power cord into a grounded AC electrical outlet.
5. Press the printer power switch located on the bottom, left side to on. Plug the SMART Turbo power cord into
the electrical outlet and press the power switch to the on position.
6. Refer to the SETUP section of this manual for instructions for selection of an external printer within the
system software.
External Balance
1. Press the power switch of the SMART Turbo to the off position.
3. Plug one connector of the cord shipped with the external balance into the socket on the balance and the other
connector into the external balance port of the SMART Turbo. Plug the balance power cord into a grounded
AC electrical outlet.
4. Based on the type of external balance used, refer to the manufacturers manual and/or CEM Corporation
instructions for specific procedures for setup and configuration of the balance and instrument.
137
Mettler:2400 Baud
Even Parity
7 Data Bits
1 Stop Pit
Sartorius:1200 Baud
Odd Parity
7 Data Bits
1 Stop Bit
Scientech:2400 Baud
Even Parity
7 Data Bits
1 Stop Bit
138
Personal Computer
Items Required:
Desktop or Notebook Computer
Windows 98 or Higher Operating System
Microsoft Word or Excel Software
Null Modem Cable (9-pin Connection Cable)
Connections
2. Connect the 9-pin connection cable to the right port on the back of the instrument labeled PC Port.
3. Connect the other end of the cable to an open serial port on the back of the computer (Com 1 or Com 2).
2. With the Main Menu displayed, press 4 to activate the Setup Menu.
4. Press 1 to toggle and select a baud rate of 9600. Press 2 to toggle and select a data bits rate of 8.
Press 3 to toggle and select a stop bits rate of 1. Press 4 to toggle and select a parity of 0.
5. Press the operation key below PREV PAGE to return to the Setup screen.
6. Press 3 to activate the Serial Options screen. Select the options to be transferred to the computer.
Computer Setup
Note: If HyperTerminal is not accessible from the Programs menu, perform steps 3 through 7.
4. From the Control Panel menu, double click the mouse to open Add/Remove Programs.
5. Select the Windows setup. From the Windows menu, double click the mouse to open Communications.
6. Using the mouse, click the box beside HyperTerminal. Using the mouse, click OK. The Windows setup
reappears. Using the mouse, click OK.
7. From the Programs menu, open Accessories. From the Accessories menu, open HyperTerminal.
9. At the name prompt, using the keyboard, type Lwterminal. Using the mouse, click OK.
10. The computer screen will read Direct to Com 1. Using the mouse, click OK.
139
11. Enter port settings as follows: Bits per second 9600, Data bits 8, Parity None, Stop bits 1, Flow
control Hardware.
1. Using the mouse, select Window on the toolbar at the top of the computer screen. Select Transfers from
the Window menu. Select Capture Text from the Transfcr menu.
2. Select a directory (default directory is Windows). Type a file name (maximum 8 characters), followed by .,
followed by a three-character extension. CEM recommends using a unique extension for the file name to
assist in file identification. Using the mouse, click OK.
3. With the Main Menu of the SMART Turbo displayed, press 3 to select and load a method for analysis.
Note: If required, press the operation key below NEXT PAGE to locate the desired method.
5. The Main Menu returns to the screen with the selected method displayed. Press READY to display the initial
screen of the selected method.
6. Follow instructions in this manual to perform the method. The method data will be electronically forwarded to
the file opened above on the computer.
7. Upon completion of sample data to be forwarded to the computer file, use the mouse to select Window on
the toolbar. Select Transfer from the Window menu. Select Capture Text from the Transfer menu. Select
Stop from the Capture Text menu.
8. Using the Program menu, open Microsoft Word or Excel. Select File on the toolbar. From the File menu,
select Open. Select the directory where the data file is stored. Select All Files to ensure the file will be
displayed. Select the applicable file. Using the mouse, click OK.
140
Cleaning Recommendations
Clean the interior of the SMART Turbo cavity with warm, soapy water applied with a soft cloth. Do not use
abrasive cleaners or solvents because they could scratch the cavity coating. Rinse and thoroughly dry all cleaned
areas.
Routine Maintenance
A monthly preventive maintenance program is recommended to ensure optimum performance of the SMART
Turbo.
1. Cover, Latch and Interlocks Carefully inspect the instrument cover, latch and interlocks to verify that they
are clean and working properly. Ensure that there is no loosening of or damage to the cover hinges or latch.
Ensure that the cover closes securely.
2. Balance Verify balance calibration using the procedure outlined in the Setup section of this manual.
Power Test Kit (907845) used to verify that microwaves are being produced.
Note: Beaker from Power Test Kit can also be used for IR Accuracy Test.
141
Troubleshooting
The most important principle in troubleshooting the SMART Turbo is to check each component of the system
separately and trace any malfunction to its source.
A qualified service technician, using standard troubleshooting techniques, should be able to identify and resolve
operational problems. If a problem persists, call the CEM Service Department or the nearest subsidiary or
distributor.
Troubleshooting Guide
Instrument Inoperative Ensure that instrument is properly connected to power outlet and that the power
switch is in the on position. Check fuses and replace if necessary.
Balance Not Operating Ensure that balance stem is installed and centered.
Results Not Sample applied unevenly to pad. Sample not homogeneous and absorbs
Reproducible microwaves unevenly.
Keep sample container closed when not extracting sample. Work quickly when
applying sample to pads and placing pads on balance pan.
Incorrect Results Verify proper sample handling, spread techniques and method parameters.
Data Results Invalid Final weight greater than initial weight. Repeat test.
displayed at End of Test Check balance calibration.
Cover Open Message Ensure that the instrument cover is properly closed.
142
Fuses Blow Check dual voltage supply and fuses (10A fuses for 60 Hz and 5A for 50 Hz) and
correct dual voltage supply and/or replace fuses, if required.
Balance Error Balance stem not installed. Turn instrument off, install balance stem and turn
instrument on.
Ensure that instrument is located on a stable work surface.
Balance cable not installed. Properly install cable.
Balance not calibrated. Perform calibration using 10g weight.
Instrument Will Not Instrument turned on before balance stem and pan were installed. Turn
Calibrate instrument off, install stem and pan, and turn instrument on.
Instrument Top Cover Gas spring installed improperly or faulty gas spring. Contact CEM Service.
Difficult to Close or
Noisy when Opened
143
Error Messages
Due to system operation and component failure, the following error messages can appear on the display screen.
COMMUNICATIONS ERROR
BALANCE ERROR
The above error messages relate to the internal balance. Ensure that the balance stem and pan are installed prior
to turning the instrument on. Ensure that the balance is properly installed and calibrated. If error message
continues after troubleshooting, replace balance.
The Balance Under Load message indicates that the weight on the balance is too small to be recognized by the
balance.
The Balance Over Load message indicates that the weight on the balance is too large to be recognized by the
balance.
STACK OVERFLOW
OP CODE ERROR
The above messages indicate component failure. If any of these error messages appear on the screen, turn the
SMART Turbo off. Do not attempt further operation. Call the CEM Service Department or the nearest subsidiary
or distributor.
THERMAL OVERLOAD
The Thermal Overload error message indicates that a door interlock switch is improperly adjusted or that the
cooling fan is not operating properly. The current method is aborted. Verify proper operation of the door interlocks
and fan. Turn the instrument off and back on. Call the CEM Service Department.
144
Note: The MONITOR Sample Kit test is for monthly checking proper operation and performance of the SMART
Turbo. It is not a calibration solution.
2. Place two (2) sample pads on the balance pan and press TARE.
3. Press START to perform a blank test. The test requires approximately 1 1.5 minutes.
6. Without removing the pads, open 1 vial of sample and pour it in the center of the pads. The sample should
form a circular puddle as it spreads across the pad.
8. Perform at least five (5) tests. After each test, record the sample test data or use the printer to print the
results.
9. Compare the results with the CEM laboratory results to determine proper instrument performance.
Note: The CEM MONITOR solution is a proprietary sample formulated so that it is minimally heat-sensitive,
requires no skilled spread technique, and is simple to run, yet effectively provides data on how the balance
system, the infrared system, and the microwave power control system are operating. It has been thoroughly
tested through several AOAC approved methods; therefore, it can be used on different moisture/solids analyzers
to check for similar results, standard deviation of test results, and the variance of sample results. The MONITOR
sample test uses a known standard to test the functionality of the SMART Turbo.
Upon installation of the SMART Turbo, the test should be performed six (6) times. Results of the tests should be
compared to the results obtained in the CEM Moisture/Solids Laboratory to determine proper operation of the
instrument.
145
The instrument is equipped with a safety interlock system which stops the generation of microwave energy when
the instrument cover is not securely closed. If the interlock system fails, a monitoring mechanism will blow the
fuse through which power is supplied to the magnetron, rendering the microwave power system inoperable.
To verify that the cover is sealing and the interlock system is working properly the SMART Turbo should be tested
for microwave leakage. To test for leakage, operate the instrument at 100% power for 5 minutes. While it is
operating, use a federally approved microwave leakage detector such as the Holaday Model HI-1500 and
measure the microwave leakage around the cavity and at the fan grill. Leakage should not exceed 5 mW/cm2. If
the instrument shows excessive microwave leakage, do not attempt further operation. Contact the CEM Service
Department or the nearest CEM subsidiary or distributor.
Microwave test meters are available from CEM Corporation. CEM does not recommend use of inexpensive
meters available in electronics stores because they lack the necessary sensitivity to properly test an instrument
for microwave leakage.
146
Intelli-Temp Calibration
Note: The SMART Turbo is completely factory calibrated. Calibration is recommended only for verification of
system operation or if a problem with calibration is suspected.
Note: Calibration of the Intelli-Temp requires a CEM SMART Turbo Intelli-Temp Calibrator (p.n. 159695). Prior to
calibration, the calibrator must be preheated.
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. SYSTEM OPTIONS
2. SYSTEM INFORMATION
3. PRINTER
4. COM PORT
5. CONTRAST
6. CLOCK
7. CALIBRATION
8. SECURITY
NEXT
PAGE
3 Plug the Intelli-Temp Calibrator into an electrical outlet. Wait until the Ready
Setup
light is illuminated.
1. COMPANY NAME
4. With the Intelli-Temp plugged in and turned on, place it into the instrument 2. DELETE METHOD
cavity, ensuring that the recess in the bottom of the calibrator is snugly fitted 3. SERIAL OPTIONS
4. UNIT SN
on the balance stem retainer so that the calibrator is flat against the cavity 5. CALIBRATE Intelli-Temp
floor.
PREV
PAGE
147
6. Lower the instrument cover until it is resting on the Intelli-Temp power cord.
CALIBRATE Intelli-Temp
Hold the cover in this position.
MAIN PREV
MENU PAGE CALIBRATE
8. Using the numeric keys, enter the calibration temperature on the calibrator
CALIBRATE Intelli-Temp
(130C).
MAIN PREV
MENU PAGE CALIBRATE
Temperature: 130.0
Scaler: x.xxxx
MAIN PREV
MENU PAGE CALIBRATE
11. Press PRINT. Retain the printout of the system information with the new
CALIBRATE Intelli-Temp
scaler value for future use during maintenance or servicing.
Calibration complete.
To record new scaler,
Press PRINT.
MAIN PREV
MENU PRINT PAGE CALIBRATE
148
Intelli-Temp Verification
The SMART Turbo Intelli-Temp temperature feedback system permits rapid temperature measurement of the
sample during the drying process in order to adjust microwave power delivery. The Intelli-Temp Verification
program is designed to verify that the system is performing properly.
CAUTION
If the SMART Turbo has not been operated for a period of one hour, preheat the instrument by
operating it empty for 5 minutes at 100% power in the Quick Test program.
Mise en garde
Lorsque le SMART Turbo nest pas en opration pour une priode de plus dune (1) heure,
rchauffer linstrument vide durant 5 minutes 100% de puissance au programme Quick Test.
1. Turn the instrument off. Lift the instrument cover. Remove the balance pan. Lift
CEM Main Menu
the balance stem straight up from the opening in the cavity. To prevent
damage to the balance assembly, do not move the balance stem from side to
1. QUICK TEST
side during removal. Turn the instrument on. 2. EDIT/CREATE METHOD
3. LOAD METHOD
2. Press 3 to access the Load Method screen. 4. SETUP
5. PRINT
6. STATISTICS
7. SMART Trac
1. TEMP VERIFY
2. POWER TEST
3. STD SOLUTION
4. LATEX
5. WATER BASED CHEM
6. MEAT RAW
7. CHEESE
8. MILK
NEXT
PAGE
4. Press READY.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
7. SMART Traac
149
8. At the end of the 5-minute period, lift the instrument cover. Using a digital
TEMP VERIFY
thermometer, stir the water. Note the temperature of the water. Remove the
thermometer.
Power: 100%
Temp (XXX): XX.X
9. Close the instrument cover. Note the temperature reading on the instrument Time: 05:00
display.
10. The reading on the display should be within 5 degrees C of the temperature
reading on the thermometer in step 8.
Press START to continue.
11. If the two temperatures ( thermometer reading from step 8 and display reading
from step 9) are not within 5C, contact the CEM Service Department or the
STOP
nearest subsidiary or distributor. TEST
12. Press the operation key below MAIN MENU to return to the CEM Main Menu.
CEM Main Menu
1. QUICK TEST
2. EDIT/CREATE METHOD
3. LOAD METHOD
4. SETUP
5. PRINT
6. STATISTICS
150
Component Replacement
WARNING
To avoid possible electrical shock or exposure to microwave energy, disconnect the instrument
from the electrical outlet prior to any disassembly procedures.
Printer Paper
1. Turn the instrument off. Using a small flat blade screwdriver, remove the printer cover. Remove the printer
paper and printer paper holder.
2. Install a new roll of printer paper on the printer paper holder. Install the printer paper holder and paper.
Position the end of the printer paper for proper feeding.
3. Install the printer cover. Turn the instrument on. Press PRINT. Press the operation key below FORM FEED to
advance the paper. If the paper does not advance, ensure that it is positioned properly to engage the form
feed.
Printer Ribbon
1. Turn the instrument off. Using a small screwdriver, remove the printer cover. Remove the printer paper and
paper holder. Remove the printer ribbon.
2. Install a new printer ribbon. Install the printer paper holder and printer paper. Install the printer cover.
Fuse(s)
1. Using a small screwdriver, pry the dual voltage supply from the power module. Remove the fuse(s) from the
fuse holder(s).
2. Based on instrument design specifications, install fuse(s) 10A (100 130V, 50 or 60 Hz - U.S and Japan)
or 5A (200 240V, 50 or 60 Hz - Europe).
3. Install the dual voltage supply cover with the proper voltage (100 120V) or (200 240V) positioned beneath
the arrow on the power module.
Install
Proper
Fuses
151
The SMART Turbo utilizes high voltage and microwave radiation. Instrument service and repair
must be undertaken only by technicians trained in the repair and maintenance of high voltage and
microwave power systems.
Mise en garde
Le SMART Turbo requiert une haute tension et produit une radiation de micro-ondes. Lentretien
et les rparations doivent tre seulement fait par un personnel form en rparation et entretien de
systmes oprant avec de haute tension et produisant de micro-ondes.
If damage to the SMART Turbo is detected, do not attempt further instrument operation. Contact the CEM Service
Department or the nearest subsidiary or distributor.
Italian Subsidiary
CEM S.r.l.
Via DellArtigianato, 6/8
24055 Cologno al Serio (Bg)
Italy
Tel: (39) 35-896224
Fax: (39) 35-891661
email: [email protected]
152
WARNING
To avoid possible electrical shock or exposure to microwave energy, disconnect the instrument
from the electrical outlet prior to any disassembly procedures.
Mise en garde
Pour viter toute possibilit dune dcharge lectrique ou une exposition aux micro-ondes,
dbrancher linstrument de la prise de courant avant toutes procdures de dsassasemblage.
It is recommended that service and repair by the user be limited to replacing components such as fuses, printed
circuit boards, interlocks, etc. The user may find it convenient to stock an assortment of replacement parts to
facilitate service procedures.
WARNING
Prior to troubleshooting or replacement of any component in the high voltage section of the
SMART Turbo, the instrument must be switched off and unplugged from the electrical outlet.
Permit the instrument to sit idle for at least two (2) minutes. Using a well insulated screwdriver,
tough the end of the screwdriver between terminals of the high voltage capacitor (illustrated in
figure 5) to discharge all residual voltage from the instrument.
Mise en garde
Avant de reparer ou remplacer une pice dans la section de haute tension, linstrument doit tre
dbranchde la prise de courant. Linstrument doit tre laiss au repos pour un minimum de deux
(2) minutes. En utilisant un tourne-vis bien isol, placer lextrmit du tourne-vis entre les
terminaux de laccumulateur de haute tension (tel quillustr la figure 5) afin de dcharger
linstrument de tout courant rsiduel.
153
Specifications
Moisture/Solids Range: 0.01% to 99.99% in liquids, solids and slurries. 0.01% resolution.
Standard Software: Constant Weight and Time, Fat, Moisture, TS, TSS, TVSS,
Dilution, and Syringe Weigh
Accessory Ports: 2 serial, RS 232, 9 pin ports for external balance, computer or
bar code reader
1 parallel port, 25 pin for external printer
Instrument Dimensions 22.0 in. (W) x 23.25 in. (D) x 14.50 in. (H)
55.9 cm (W) x 59l.1 cm (D) x 36.8 cm (H)
Weight: 55 lbs., 25 kg
154
Warranty
What Is Covered:
CEM Corporation warrants that the instrument will be free of any defect in parts or workmanship and will, at its option, replace
or repair any defective part (excluding consumables) or instrument.
Responsibilities of Purchaser:
To ensure warranty coverage, the purchaser must:
Use the instrument according to directions,
Connect the instrument properly to a power supply of proper voltage,
Replace blown fuses,
Replace consumables and
Clean the instrument as required.
Warranty Disclaimer:
CEM Corporation hereby excludes and disclaims any warranty of merchantibility or fitness for any particular
purpose. No warranty, express or implied, extends beyond the face hereof. CEM Corporation shall not be liable for
loss of use of instrument or other incidental or consequential costs, expenses or damages incurred by the purchaser
or any other user. This warranty is not transferable.
155