Heat Conduction
Heat Conduction
Heat Conduction
pressure against the heater. Electrical power was supplied to the heater by a variable AC
transformer (Powerstat, Model BP57515). The voltage across the heater was monitored
using a digital multi-meter (National Instruments, Model USB-4065). Calorimeters were
constructed using 6.35-mm-thick copper plate and copper tubing as shown in Figure 5.
Grooves were machined in the plates using a 6.35-mm ball end mill to a depth of 1.6 mm.
Copper pipe (6.35-mm-outside diameter) was soldered onto the copper plate using tinantimony solder (Alloy number 2011, Sn95/Sb5, solidus temperature 235C, liquidus
temperature 240C) in a temperature-controlled furnace. The calorimeters were
successfully pressure-checked to 1.3 atm. The calorimeters were then soldered to the
copper rod samples using tin-lead solder (Alloy number 2030, Sn62/Pb38, eutectic
temperature 183C) in the temperature-controlled furnace, as shown in Figure 6. Brass
fittings were used to place the thermocouple probes (Omega, Model EMQSS-062G-12)
in the coolant stream of the calorimeter, as shown in Figure 7. The 1.016-mm-diameter
(0.040 inch) sample thermocouple probes (Omega, Model EMQSS-040G-12) were
mounted in the sides of the rods to a depth of 19.1 mm. The mounting holes were drilled
with a precision micro drill press (Dayton, Model 2LKU8) using a 1.041 mm (0.041
inch) solid carbide drill bit, as shown in Figure 8. The sample thermocouples were held in
place using aircraft wire, as shown in Figure 9. The temperatures sensed by the
thermocouples were monitored and recorded by using a data acquisition system (DAS),
which consisted of a data acquisition board (National Instruments, Model SCC-68), four
thermocouple modules (National Instruments, Model SCC-TC01) mounted to the DAQ
Board, and a data acquisition card (National Instruments, Model PCI-6221) installed in a
PC. The assembled system is shown in Figure 10, where the samples were uninsulated.
Figure 11 shows one of the fully insulated samples, where four layers of ceramic fiber
insulation and four layers of aluminum foil were installed using aircraft wire. Both
samples were insulated in the same manner to provide a meaningful comparison.
Thermal Conductivity Calculation
The thermal conductivities of the copper rod samples were calculated using Fouriers law
of heat conduction (Incropera & DeWitt, 1990):
dT
Q=kA
dx
or
k=
Q
A ( dT /dx )
The rate of heat removed from the sample bar by the calorimeter is given by the first law
of thermodynamics (Cengel & Boles, 2006):
m
C p ( T out T in )
Q=
is the mass flow rate of water measured by the flow meter, and T in and
where m
T out are the inlet and outlet temperatures of the water measured by the calorimeter
thermocouples, respectively. The specific heat at constant pressure is evaluated at the
average of the inlet and outlet temperatures, and is given by (Lide & Kehiaian, 1994):
C p= A1 + A2 T + A 3 T 2+ A 4 T 3 + A 5 T 4
(J K-1 mol-1)
where T
is in degrees Kelvin. The numerical coefficients are as follows:
A 1=917.5 ,
A 2=10.1016 ,
A 3=0.0454134 ,
A 4 =9.07517 105 ,
A 5=6.80700 108 . The valid range for this equation is 273 T 373 K at nearatmospheric pressure. The cross-sectional area of the rod is
A=
2
D
4 s
where Ds is the diameter of the sample rod as measured by using digital Vernier
calipers. The axial temperature gradient in the rod is given by
dT T H T L
=
dx
LCC
where T H and T L are the sample temperatures measured by the thermocouples
installed in the sides of the rods. For the sample, T H =TC03 and T L =TC04 . The
center-to-center distance between the sample thermocouples was measured as follows.
Each sample was placed on a Starrett Crystal Pink precision granite surface. A precision
pin was placed into the bottom hole and then the height to the top of the pin was zeroed
using a Mitutoyo height gage with an attached Interapid indicator. This distance was then
replicated using a precision slide gage block. The height to the top of the second hole
was then measured using the same pin and that height was replicated using precision gage
blocks placed onto the slide gage block. The height was then calculated based on the
gage blocks used to zero the height of the second hole.
In terms of the eight measured quantities, the thermal conductivity of the sample rods is
given by
4m
C p ( T out T in ) LCC
Q
k=
=
2
A ( dT /dx )
Ds ( T H T L )
Measurement Uncertainty Estimates
Thermal Conductivity
The root-sum-square uncertainty for the thermal conductivity is given in terms of the
eight measured quantities as follows:
[(
2
2
k
k
k
k=
m +
Cp +
T out
m
Cp
T out
[(
)(
C p ( T out T in ) LCC
4m
D2s ( T H T L )
)(
)(
+
)(
2
2
2
k
k
k
k
T in +
LCC +
Ds +
TH
T in
LCC
Ds
TH
C p ( T out T in ) L CC
4m
D2s ( T H T L )
)(
)(
+
C p T out LCC
4m
D 2s ( T H T L )
) (
)(
+
) (
p T in LCC
4 mC
D2s ( T H T L )
)(
+
p( T
4 mC
D2s
this information was not available in the archival reference (Lide & Kehiaian, 1994), a
conservative value of 1% of the reading was taken.
Bibliography
Cengel, Y., & Boles, M. (2006). Thermodynamics: An Engineering Approach. New York:
McGraw-Hill.
Incropera, F., & DeWitt, D. (1990). Fundamentals of Heat and Mass Transfer. New York:
Wiley.
Lide, D., & Kehiaian, H. (1994). CRC Handbook of Thermophysical and
Thermochemical Data. Boca Raton: CRC Press.
Constant Head
Pressure Tank
Ball
Valve
Filter
Water-Cooled Calorimeter
Tin TL
Turbine
Flow Meter
Tout
Copper Rod Sample
TH
Electric
Heater
Digital Voltmeter
+
Variable AC Transformer
Tin
Coolant
Water In
Coolant
Water Out
LCC
Aluminum Foil Layers
TH
Figure 4: Copper heat spreader plate soldered to the sample rod using silver
solder.
T WELL95
(C)
0.002465
8
0.002270
9
0.007376
3
0.007821
9
0.007376
1
0.006225
7
0.004609
2
0.004502
4
0.004710
9
TC03 Block
Temperature
(C)
TC03
Calibration
Prediction
(C)
49.03569
48.55204
71.59958
71.84586
95.92662
96.95989
120.48850
122.31634
144.98130
147.60148
169.27022
172.67615
193.73850
197.93598
217.57960
222.54834
241.35802
247.09599
T BF
T CAL
(C)
(C)
0.1676
6
0.0551
03
0.0331
94
0.1079
2
0.1646
7
0.1024
9
0.0402
50
0.0611
89
0.1646
7
0.17443
0.06167
4
0.04487
0
0.12004
0.17635
0.11301
0.04915
9
0.06999
2
0.17368
T WELL95
(C)
0.002465
8
0.002270
9
0.007376
3
0.007821
9
0.007376
1
0.006225
7
0.004609
2
0.004502
4
0.004710
9
TC04 Block
Temperature
(C)
TC04
Calibration
Prediction
(C)
48.89668
48.54351
71.47360
71.84470
95.80870
96.96047
120.37820
122.31816
144.88528
147.61142
169.18238
172.68798
193.64406
197.93439
217.48726
222.54248
241.27156
247.08978
T BF
T CAL
(C)
(C)
0.1761
9
0.0562
60
0.0337
77
0.1097
4
0.1746
1
0.1143
2
0.0386
61
0.0670
48
0.1708
8
Calibration Uncertainty
0.176C
0.18295
0.06283
1
0.04545
3
0.12186
0.18629
0.12484
0.04757
0
0.07585
1
0.17989
TC04
0.186C
LCC (mm)
50.880 0.0254
44.958 0.0254