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TENTATIVE STANDARD 1942 OFFICIAL TEST METHOD 1946 REVISED 1971 OFFICIAL TEST METHOD 1983 REVISED 1988 STANDARD PRACTICE 1996 CORRECTED 1997 1996 TAPPI The information and data contained in this document were prepared by a technical committee of the Association. The committee and the Association assume no liability or responsibility in connection with the use of such information or data, including but not limited to any liability or responsibility under patent, copyright, or trade secret laws. The user is responsible for determining that this document is the most recent edition published.

Physical testing of pulp handsheets

1. Scope and significance

1.1 This procedure describes the testing of pulp handsheets, prepared in accordance with TAPPI T 205 Forming Handsheets for Physical Tests of Pulp, for their strength and other physical properties as well as their lightscattering coefficient. 1.2 Information derived from handsheet testing indicates pulp quality and is a measure of the potential contribution of the pulp to the strength of the finished paper product. 2. Summary

2.1 The measurements of handsheet properties to be described are as follows: mass per unit area (grammage), thickness, specific volume, apparent density, scattering coefficient, tensile strength, stretch, tensile energy absorption, bursting strength, tearing resistance, and MIT folding endurance. 2.2 Five sheets are generally enough for routine control work in a mill on a specified pulp. Ten sheets should be used wherever possible and when testing mechanical pulp in order to provide enough paper to make four tears of ten strips each. This makes it possible to use five sheets for tearing resistance and five other sheets for all other strength tests. Ten sheets cannot be made when testing pulp from TAPPI T 200 Laboratory Processing of Pulp (Beater Method) because not enough sample is available and taking a larger sample will change the amount of pulp in the beater and, therefore, change the beating time. 2.3 Results are reported in SI units and strength indexes are calculated on conditioned weight. 3. Conditioning

Inspect the sheets and discard any that are abnormal, (e.g. containing holes, uneven thickness, damaged, containing contaminants such as dirt, plastic, metal bits). Condition in an atmosphere in accordance with TAPPI T 402 Standard Conditioning and Testing Atmospheres for Paper, Board, Pulp Handsheets, and Related Products and test the sheets for each characteristic of interest according to the appropriate TAPPI test method for paper but with modifications as specified below.

Approved by the Pulp Properties Committee of the Process and Product Quality Division TAPPI

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4. Mass per unit area (grammage)

Physical testing of pulp handsheets / 2

Determine the average mass per unit area of five conditioned sheets by weighing them together on a balance sensitive to 0.001 g. The area of each sheet is approximate and is taken to be 200 cm2. The grammage is ten times the weight of the five sheets. 5. Thickness 5.1 Apparatus1

Fig. 1. Division of sheets for testing.

5.1.1 Micrometer, see TAPPI T 411 Thickness (Caliper) on Paper and Paperboard. 5.2 Procedure 5.2.1 Before cutting the test sheets, obtain their average thickness as follows: Place five sheets in a pile with their glazed surfaces in one direction. Using a motor-driven micrometer as specified in T 411, measure the thickness of the pile of sheets at ten randomly selected points recording the thickness at each point to the nearest 2
m (0.0001 in.). 5.2.2 If any reading is more than 5% above the others, make a measurement on an adjacent spot to determine if the high reading is caused by a shive, speck, foreign materials such as dirt, glass, plastic, etc. or fiber bundles resulting from a short disintegration time. If so, discard the high reading. 6. Light-scattering coefficient

6.1 Apparatus1 6.1.1 Opacimeter, see TAPPI T 425 Opacity of Paper (15/Diffuse, Illuminant A) 89% Reflectance Backing and Paper Backing. 6.1.2 Working standard of reflectance, calibrated to absolute scale as described in T 425. 6.2 Procedure 6.2.1 Place the working standard over the opening of the opacimeter and adjust the instrument reading to the value of the absolute reflectance of the working standard. 6.2.2 Obtain the reading R0 by placing each sheet in the opacimeter with its smooth side against the black body and reading the reflectivity without adjustment of the instrument. 6.2.3 Place the pile of five sheets in the opacimeter with the smooth sides toward the specimen holder and take a reading. Increase the number of sheets in the pile by inserting five more sheets of the same test or, if these are unavailable, sheets from another test that are similar in reflectance between the pile and the specimen holder. Take another reading. If there is a significant difference between the two readings, add additional sheets to the pile until no

Names of suppliers of testing equipment and materials for this method may be found on the Test Equipment Suppliers list in the bound set of TAPPI Test Methods, or may be available from the TAPPI Technical Services Department.

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significant change occurs with the addition of five more sheets. Using this pile of sheets, measure the reflectivity R
of each of the five test sheets keeping the other four test sheets immediately behind the sheet being tested. 6.2.4 Use the average values of R0 and R
to calculate light scattering coefficient as described in 13.3.4.
NOTE 1: For greater accuracy, the two measurements should be made on the same specimen area and the weight per unit area of the actual test area used. The R
value must be obtained using the opacimeter as described. A brightness reading cannot be used.

NOTE 2:

7.

Cutting the sheets for remaining physical tests

7.1 Apparatus1 7.1.1 Double-knife, 15 mm (0.59 in.) wide cutter, or a single-knife cutter equipped with a guide to give a strip 15 mm wide. 7.2 Procedure 7.2.1 Place the pile of five sheets on the cutting anvil with the diameter of the pile accurately situated along one of the anvil's edges. 7.2.2 Cut the sheets as shown in Fig. 1. By testing the folding endurance with an MIT tester at one end of a strip, with care, the longer part of the remnant is not appreciably damaged and is quite suitable for another fold test if it is inserted in the tester in such a manner that the folding test is made on the part of the strip that protruded above the top clamp. The strip should not be used for a tensile test as the tension placed on the strip in making the fold test will change the characteristics of the paper. 8. Tensile strength (stretch and tensile energy absorption)

8.1 Apparatus1 8.1.1 Tensile tester, see TAPPI T 494 Tensile Breaking Properties of Paper and Paperboard (Using Constant Rate of Elongation Apparatus). 8.2 Procedure 8.2.1 Use at least one specimen strip from each of the five test sheets, cutting each strip 15 mm wide. Set the jaws of the tensile tester 100 mm apart. 8.2.2 Determine the tensile strength, stretch, and tensile energy absorption simultaneously in accordance with T 494 except for the size of the specimen.
NOTE 3: TAPPI T 404 Tensile Breaking Strength and Elongation of Paper and Paperboard (Using Pendulum-Type Tester) may be used to determine tensile strength, but this should be noted in the report.

9.

Bursting strength

9.1 Apparatus1 9.1.1 Bursting tester, see TAPPI T 403 Bursting Strength of Paper. 9.2 Procedure 9.2.1 Determine the bursting strength by making at least ten bursts one at a time on the segments of five test sheets, the glazed side of each sheet being clamped toward the diaphragm, otherwise in accordance with T 403. 10. Tearing resistance

10.1 Apparatus1 10.1.1 Elmendorf tearing resistance tester, see TAPPI T 414 Internal Tearing Resistance of Paper. 10.2 Procedure 10.2.1 Determine the tearing resistance as described in T 414, with modifications indicated below. Clamp the sheets so that their smooth sides face the axis of the instrument and the greater part of the specimen is held in the fixed, not the moving, jaw. 10.2.2 For chemical pulps, cut sections from five test sheets in the manner shown in Fig. 2 and test the five sections (plys) together, making four tears across the width of the sections, each being through a total tearing distance

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Physical testing of pulp handsheets / 4

of 215 mm (5 x 43 mm). If the scale on the tearing resistance tester is in grams, multiply the average reading on the standard tester by 3.2 (i.e., 16/5) to obtain the force in grams required to tear a single sheet. If the specimens should be such that five sheets together give a reading above 60, reduce the number of sheets torn together to two and multiply the observed reading by 8 to give the force in grams to tear a single sheet. If the instrument scale is in millinewtons, divide the reading by the number of sheets torn. 10.2.3 For mechanical pulps, use ten sheets (plys) and multiply the average reading by 1.6 to obtain the force in grams required to tear a single sheet.
NOTE 4: Accuracy is enhanced, especially if the segments of sheets are cut somewhat narrow, if a template is used to draw a pencil line 47.0 mm from the centrally cut edges of the pack of specimens as shown in Fig. 2. When it is clamped in the jaws of the instrument, align the pack so that the scribed line coincides with the top edges of the jaws. The knife should be checked to cut 4.0 mm above these edges, to give the standard tearing distance of 43.0 mm. If an instruments digital display limits the number of available test plies (i.e., 1, 2, 4, 8, 16 plies), test the number of plies closest to the recommended number in the method and keep the total tearing distance for all test specimens for a given sample constant (i.e., 5 each, 4-ply tears for chemical pulps). Note any modifications in the report.

11.

Folding endurance 11.1 11.1.1 11.2 11.2.1 Apparatus1 MIT folding tester, see TAPPI T 511 Folding Endurance of Paper (MIT Tester). Procedure Determine the folding endurance of the 15-mm-wide strip of paper cut as shown in Fig. 1.

Fig. 2. Detail of tearing test

11.2.2 With the MIT tester, only a 10-mm portion or so of the strip needs to be clamped in the lower (moving) jaw and the exact tension of 1 kg applied, leaving the extra length of the strip projecting through the upper jaw. Because the part of the strip above the upper clamp is not appreciably affected by the test, the upper end of the strip can be used for another fold test making the fold in the part of the strip that was above the clamp. 11.2.3 For a referee test, make 20 determinations using 10 strips and making two tests on each strip.
NOTE 5: The folding test is very sensitive to moisture. Accordingly, avoid touching the vicinity of the fold line with the fingers. The fold tester should be equipped with a fan to draw room air across the head to keep it cool (see T 511).

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12. Moisture content

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12.1 Apparatus1 12.1.1 See TAPPI T 550 Determination of Equilibrium Moisture in Pulp, Paper, and Paperboard for Chemical Analysis. 12.2 Procedure 12.2.1 Determine the moisture content using the procedures described in T 550 on scrap samples of the pulp handsheets being tested. 13. Other tests

If desired, other tests, such as porosity (air pressure, applied to the glazed side of the sheets), stiffness, zero span, etc., may be made according to accepted procedures. 14. Report

14.1 Report results in terms of their derived units to three significant figures. If the direct test results are reported, i.e., the actual instrument readings, either (a) metric, (b) English, or (c) SI units may be used as is common practice, the units being stated in each case. For derived units, however, such as the various strength indexes, only the SI units are acceptable. 14.2 Calculate and report all the results on the conditioned mass per unit area of the test sheets. 14.3 The calculations of the various items reported are shown below by formulas in which: r = mass per unit area, g/m2 t = single sheet thickness, m T = single sheet thickness, 0.001 in. b = bursting strength, kPa B = bursting strength, lbf/in.2 p = tensile break load, kgf on a 15-mm strip P = tensile break load, lbf on a 0.59-in. strip e = force to tear a single sheet, g 14.3.1 14.3.2
NOTE 6:

Mass per unit area: in g/m2. Specific volume (bulk): calculated as cm /g: from t/r or 25.4 T/r.
3

The result compares the bulk of the test sheets (measured under the prescribed pressure) to water, which has a bulk of 1.0 cm3/g, about the same as a dense glassine.

14.3.3 Apparent density: calculate as g/cm3 from r/t or r/25.4 T. 14.3.4 Light scattering coefficient: obtain the value of sW from the chart in T 425 using the values obtained for R0 and R
. Scattering coefficient = sW/r. 14.3.5 Folding endurance: correct for variations in basis weight by multiplying the average folding endurance obtained by 65/r. 14.3.6 Logfold: obtain the logarithm to the base 10 for each folding endurance measurement. Average the logarithms and correct for variations in basis weight by adding (1.813-log r) to the average log. Report as the log folding endurance. 14.3.7 Bursting strength, kPa, from the formula 6.89B. 14.3.8 Tearing resistance, mN, from the formula 9.807e. 14.3.9 Tensile strength, kN/m, from the formula 0.6538 p or 0.2966 P. 14.3.10 Stretch, %. 14.3.11 Burst index, kPa m2/g, from the formula b/r or 6.89 B/r. 14.3.12 Tear index, mN m2/g from the formula 9.807 e/r. 14.3.13 Tensile index, N m/g from 653.8 p/r or 296.6 P/r. 14.3.14 Breaking length, km, calculated from the formula 200p/3r or 30.24P/r. 14.3.15 Percent moisture content on conditioned weight basis.

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NOTE 7:

Physical testing of pulp handsheets / 6

The breaking length corresponds to the length in kilometers of a uniformly wide strip of paper which, if held at one end (e.g., freely suspending a coil of that paper by its tab end), would just cause the strip to break under its own weight.

15.

Precision

A precision statement for this standard practice is not applicable as precision statements accompany each of the referenced test methods. 16. Keywords Pulp, Handsheets, Physical tests. 17. Additional Information

17.1 Effective date of issue: February 9, 1996. 17.2 This revision has been reissued as a standard practice with the inclusion of the determination and reporting of the moisture content. This revision specifies all test results will be reported on the basis of conditioned weight rather than oven dry weight, substitutes the terms burst index and tear index for the old terms of burst factor and tear factor, and introduces the use of SI units. A formula for correcting folding endurance for variations in basis weight has been introduced. Folding endurance is reported as the log fold. 17.3 Related methods: Canadian, CPPA D 12; Australian and New Zealand, APPITA P 208; German, VZUPCI.V. 10-13; Scandinavian SCAN C 28:76. References 1. 2. 3. 4. Clark, J. d'A., The Bulk of Pulp Test Sheets, Tappi 53 (7): 1340 (1970). Clark, J. d'A., Measuring Stretch Accurately with a Pendulum Tensile Tester, Tappi 53 (3): 503 (1970). Brandon, C. E., Effect of Basis Weight on Folding Endurance, Tappi 49 (6): 233 (1966). Brandon, C. E., The Precision of the TAPPI Standard Beater Test, Tappi 41 (9): 129A (1958).

Your comments and suggestions on this procedure are earnestly requested and should be sent to the TAPPI Technical  Divisions Administrator.