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    D2638 PDF

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    The document discusses density testing methods for petroleum products and lubricants. It defines density, relative density, and specific gravity. There are over a dozen ASTM test methods that measure density using instruments like hydrometers and pycnometers. One specific method, D2638, measures the real density of calcined petroleum coke. This is done by grinding a sample to a fine powder, measuring its mass and volume using a helium pycnometer, and calculating density from these values. The test is repeatable to 0.018 g/cm3 and reproducible to 0.025 g/cm3. A table compares properties, techniques, and precision of various ASTM density testing methods.

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    D2638 PDF

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    The document discusses density testing methods for petroleum products and lubricants. It defines density, relative density, and specific gravity. There are over a dozen ASTM test methods that measure density using instruments like hydrometers and pycnometers. One specific method, D2638, measures the real density of calcined petroleum coke. This is done by grinding a sample to a fine powder, measuring its mass and volume using a helium pycnometer, and calculating density from these values. The test is repeatable to 0.018 g/cm3 and reproducible to 0.025 g/cm3. A table compares properties, techniques, and precision of various ASTM density testing methods.

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    The document discusses density testing methods for petroleum products and lubricants. It defines density, relative density, and specific gravity. There are over a dozen ASTM test methods that measure density using instruments like hydrometers and pycnometers. One specific method, D2638, measures the real density of calcined petroleum coke. This is done by grinding a sample to a fine powder, measuring its mass and volume using a helium pycnometer, and calculating density from these values. The test is repeatable to 0.018 g/cm3 and reproducible to 0.025 g/cm3. A table compares properties, techniques, and precision of various ASTM density testing methods.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    224 views1 page

    D2638 PDF

    Uploaded by

    zubair195
    The document discusses density testing methods for petroleum products and lubricants. It defines density, relative density, and specific gravity. There are over a dozen ASTM test methods that measure density using instruments like hydrometers and pycnometers. One specific method, D2638, measures the real density of calcined petroleum coke. This is done by grinding a sample to a fine powder, measuring its mass and volume using a helium pycnometer, and calculating density from these values. The test is repeatable to 0.018 g/cm3 and reproducible to 0.025 g/cm3. A table compares properties, techniques, and precision of various ASTM density testing methods.

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    of 1

    94

    GUIDE

    TO

    ASTM TEST METHODS

    FOR THE

    ANALYSIS

    OF

    PETROLEUM PRODUCTS

    AND

    LUBRICANTS

    DENSITY, RELATIVE DENSITY, AND SPECIFIC GRAVITY

    GENERAL
    Density is an important property of petroleum products being part of product specications. Materials are usually bought and sold on that basis or if on volume basis then converted to mass basis via density measurements. This property is almost synonymously termed as density, relative density, gravity, and specic gravity, all terms related to each other. There are at least a dozen test method standards in D02 manuals that describe this determination (see Table 4). Usually a hydrometer, pycnometer or more modern digital density meter is used in all these standards. The plurality of the methods is because they are specically written for different products. Some basic definitions: density The mass (weight in vacuo) of liquid per unit volume at 15C. relative density The ratio of the mass of a given volume of liquid at 15C to the mass of an equal volume of pure water at the same temperature. specic gravity Same as relative density.

    REAL DENSITY OF CALCINED PETROLEUM COKE: D 2638


    Real density is obtained when the particle size of the specimen is smaller than 75 m. It directly inuences the physical and chemical properties of the manufactured carbon and graphite artifacts for which it is used.

    TEST SUMMARY
    A sample is dried and ground to pass a 75-m screen. The mass of the volume is determined directly, and the volume derived by the volume of helium displaced when the sample is introduced into a helium pycnometer. The ratio of the mass of the sample to the volume is reported as the real density.

    TEST PRECISION
    The test has a repeatability of 0.018 and reproducibility of 0.025 g/cm3. Bias of this test method is not known.

    TABLE 4Comparison of Density Methods.


    Test Method Property Matrix Technique r R Bias

    D D D D D D D D D D D D D

    71 1217 1298 1480 1481 1657 2320 2638 4052 4292 4892 5002 5004
    a

    Relative Density Density Specic Gravity Density and Relative Density Relative Density Density Density and Specic Gravity Real Density Density Bulk Density Density Specic Gravity Real Density

    Solid Pitch Liquid Fuels Liquid Fuels Viscous Liquids Viscous Liquids Light Hydrocarbons and LPG Solid Pitch Calcined Petroleum Coke Liquids Calcined Petroleum Coke Solid Pitch Crude Oil Calcined Petroleum Coke

    Gravimetry Bingham Pycnometer Hydrometer Bingham Pycnometer Lipkin Pycnometer Hydrometer Pycnometer Helium Pycnometer Digital Meter Helium Pycnometer Pycnometer Oscillating Frequency Helium Pycnometer

    0.005 0.00002 Variable 0.00005 0.00015 NA 0.011(SG) 0.007(D) 0.018 0.0001 0.014 0.02 0.00105X 0.0067

    0.007 0.00003 Variable 0.00014 0.00035 NA 0.001(SG) 0.011(D) 0.025 0.0005 0.046 0.03 0.00412X 0.0156

    NAa NA NA NA NA NA NA NA NA 0.0006 NA 0.04 NA NA

    NANot available.

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