59E Agitator Seals in Chemical-En-18.09.2008
59E Agitator Seals in Chemical-En-18.09.2008
59E Agitator Seals in Chemical-En-18.09.2008
Mechanical seals in mixing and separating processes in the chemical industry. Processes, application examples, seal designs and supply systems.
59 E
Seal selection
Seal selection for top entry arrangements. Agitators for steel, stainless steel and glass-lined vessels
Medium non-toxic, not dangerous for the environment Single seal, process leakage to the atmosphere is permitted or directed to the drain Dry running, pressure up to 6 bar, no barrier medium SeccoMix 481 SeccoMix 461 Single seal or double seal, unpressurised quench, process leakage into the buffer liquid is permitted or directed to the drain Lubricated, pressure up to 6 bar, quench medium liquid M481K.. or M481K...D M461K.. or M461K...D..
Double seal, pressurized with constant barrier pressure, no process leakage to the atmosphere Dry running, pressure up to 6 bar, barrier medium gas (N2) SeccoMix 481...D.. SeccoMix 461..D... Lubricated, pressure up to 6 bar (16 bar), barrier medium liquid M481K...D.. M461K...D.. Closed circuit TS system, open circuit SPA, SPN Contactless, pressure up to 6 bar, barrier medium gas (N2) AGSZ 481K..D. AGSZ 461K...D. Seal supply system Gas supply GSS4016/A ... Gas supply GSS4016/A ...
Quench system
Seal selection for top, side or bottom entry arrangements. Agitators, dryers, mixers, filters and special equipment.
Sterile equipment Double seal, pressurized with constant barrier pressure or with pressure adjustment Pressure up to 6 bar, barrier medium gas (N2) AGSR3-D AGSR3L-D series Pressure up to 16 bar, barrier medium liquid MR333-D MR333L-D series Pressure up to 6 bar, barrier medium gas (N2) AGSR5-D AGSR5L-D series
Double seal or multiple seal, pressurized with constant barrier pressure or with pressure adjustment Pressure up to 16 bar, barrier medium liquid MR5-D MR5L-D series Pressure up to 25 bar, barrier medium liquid HS-D, HSL-D series Pressure up to 250 bar, barrier medium liquid HSH-D, HSHL-D, HSH(V)-D, HSH(V)L-D, bottom entry HSHLU-D series Open circuit SPA SPN
Seal supply system Gas supply GSS4016/A Closed circuit TS system, sterile Gas supply GSS4016/A ... Closed circuit TS system DRU pressure booster Open circuit SPA SPN
Front page: Polymerisation reactor (Ekato) for producing ion exchanger granules at Lanxess Bitterfeld. Seals: AGS481KL-D, supply system GSS4016
Content
Seal selection Seals for mixing and separating processes Mixing processes Separating processes Mechanical seals in mixing processes Mechanical seals in mechanical and thermal separation processes EagleBurgmann agitator seals the complete range EagleBurgmann seal supply systems
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The manufacturing of chemical and pharmaceutical products puts considerable strain on the sealing technology. In addition to the process specific properties, the sealing systems must meet ever increasing requirements in terms of service life and reliability in a constantly growing global market. Optimum quality, a worldwide service network and decades of experience of application engineering have made EagleBurgmann the leading manufacturer of sealing systems in the chemical and pharmaceutical industry, biotechnology, food industry, agrochemical industry, dispersion and micro-wet milling technology, flue gas desulphurisation and many other processes. We have developed sealing solutions jointly with our customers and engineers, with due regard to the characteristics of the processes and equipment used. Today, reliable production would not be feasible without these sealing solutions.
The range of application of EagleBurgmann agitator seals is wide: Shaft diameter: 20 ... 500 mm (0.787 ... 19.685) Temperature: 80 ... +350 C (112 ... 662 F) Pressure: Vacuum ... 250 bar (3,625 PSI) Sliding velocity: ... 20 m/s (65 ft/s)
EagleBurgmann can provide technical solutions for aggressive, corrosive, adhesive, viscous, toxic, explosive, dry, environmentally hazardous or valuable media. Both modular systems and process-optimised engineered solutions are used. By combining these with mature and reliable seal supply systems, EagleBurgmann is able to offer the complete range of services through to TotalSealCare a modular service from a single supplier. Beyond this in the pharmaceutical industry, EagleBurgmann seals fulfil special requirements and directives, e.g. SIP Sterilisation in Place CIP Cleaning in Place n cGMP current Good Manufacturing Practice n EHEDG Design of Mechanical Seals for Hygienic and Aseptic Applications n FDA Food and Drug Administration n QHD Qualified Hygienic Design
n n
An Atex declaration of conformity can be issued for every EagleBurgmann mechanical seal provided that the technical design and the arrangement meet the required operating conditions and the following precise operating conditions of use are known: Area of use (zone, device group) Required temperature class n Medium (medium class) n Maximum pressure at the mechanical seal n Maximum temperature of the process medium at the mechanical seal n Rotational speed n Seal type, combination of face materials and size n Buffer/barrier medium
n n
This brochure sets out a range of solutions for different processes, machines and equipment. The selection matrix on page 2 will help you to identify the right seal for many different applications.
EagleBurgmann dual mechanical seals meet the requirements of the German Clean Air Directive (TA-Luft).
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Batch operations in process engineering For the sake of simplicity, many processes in the chemical, pharmaceutical or biotech industries can be broken down into two main areas from the viewpoint of the sealing technology: Mixing processes Agitating, mixing and kneading are basic unit operations for combining of materials. The aim is to balance out differences in concentration and to achieve greater homogeneity.
Mechanical and thermal separation processes Centrifugation, filtering, drying and evaporating are examples of unit operations for separating processes. The aim may be to obtain a high purity end product or to separate out by-products.
Top entry agitator with AGS481. Applied in sun protection products at BASF Ludwigshafen.
Mixing processes
Mixing processes are particularly important in the chemical industry. For a start, intermediate or end products are often mixtures, dispersions or emulsions, for example. And, for a chemical reaction, the reactants must be distributed as homogeneously as possible to guarantee an optimum heat and mass transfer. We distinguish between homogeneous and heterogeneous mixtures. Homogeneous mixtures consist of just one phase, e.g. salt solutions, alloys or air. Heterogeneous mixtures comprise several phases, such as emulsions or suspensions. As a rule, we use agitating for liquid phases, kneading for highviscosity, paste-like media and mixing for solid substances.
An agitator is generally used for mixing and agitating operations involving mixtures of substances consisting primarily of the liquid phase. The requirement for a successful sealing solution is a clear definition of the operating conditions. The tasks of the mixing technology can be described as follows: Homogenisation creates a uniform phase of several liquids that are soluble in one another for the purposes of balancing out differences in concentration and temperature. Intensification increases the heat exchange between the liquid phase and the heat transfer surface
Suspending is the even distribution of solids in liquids. In the starting phase, the solids at the bottom are whirled up. In the end phase, the solids are evenly distributed in the tank. Dispersing Comminuting a substance or breaking a gas down and distributing it in a liquid. The aim of dispersing is to increase the surface area between the disperse phase and the continuous phase in order to improve the mass transfer between them which increases in proportion with the size of the surface. Dispersing is also used to stabilise emulsions. A special technology has been developed for dispersing and micro wet milling. The application requirements extend from low to high viscosity products that have to be dispersed down to nanometer range. For these applications, agitated media mills are used to disperse powdered substances in liquid phases as finely as possible. This requires particularly robust seal designs to guarantee successful operation. EagleBurgmann can supply suitable seal systems for all such mixing and agitating applications.
Polymers production at BASF Ludwigshafen. Stainless steel tank with top entry agitator. Medium: Preproduct for polymers production Temperature t1: 120 C Pressure p1: 4 bar Rotational speed: 147 min-1 Seal: M451KL-D21/80-E2 with resublimation barrier with permanent flow of deionised water Supply system: TS1016/A007 Barrier medium : Glycol / water Barrier pressure p3: 6 bar
The separation of mixtures of substances is one of the most important unit operation in processes. It normally represents more than half of the investment in a chemical production plant. The majority of the raw materials and the products obtained by chemical reactions are mixtures of substances that have to be separated into the different components for further processing or end use. We distinguish between mechanical and thermal separation processes according to which physical properties are used for separation. Mechanical separation methods include e. g. centrifugation and filtering where different densities of the various components are used. Thermal separation methods such as drying and evaporating utilise the different boiling points for separation.
nologies have significantly increased over the past few years. Separators and decanters are used in the chemical, pharmaceutical and biotech industries, oil and fat recovery and starch industry and in industrial biotechnology. Filtering Filtering is the mechanical separation of a suspension into the liquid and solid phases using a filter medium. Filters perform a large number of solid/liquid separating applications. For example, modules of different designs are used in closed systems for optimised solutions that are matched to the specific application. Drying By drying, we mean the removal or reduction of the liquid content in a solid by thermal treatment. The liquid is converted into the vapour phase and removed. Drying involves a very high power consumption and must be carried out gently to prevent product deterioration, so it requires particular attention. Thermal drying always stresses the solid. It is therefore important to ensure that the process is safe as well as maintains the product quality. We distinguish between convection, contact and radiant drying according to the heat transfer method. It is also possible to distinguish by the operating conditions. For example, with
air drying, the drying is carried out with hot air at atmospheric pressure. For vacuum drying a vacuum is used. This causes the boiling point and thus the drying temperature to drop considerably, which makes the process gentler on the product. Evaporation Evaporation uses the addition of heat to evaporate and remove the solvent from a solution. This method is used to concentrate a solution, for example, to recover the pure solvent or to precipitate the dissolved solid by crystallisation.
The following separation processes are of particular importance in sealing technology. Centrifugation Separators and decanters separate solids from liquids or liquid mixtures and remove the solids at the same time. Centrifuges as stand-alone machines or integrated into complete process lines are used to implement new process technologies and make the production efficient and cost-effective. The options for using mechanical separation tech-
Gas-lubricated AGSRL-D
In closed agitator or vessels, the rotating agitator shaft must be sealed off from the cover or bottom of the vessel. This type of arrangement is known as a top or bottom entry installation. There are also horizontally arranged shaft entries and side arrangements that are not horizontal. This creates very different requirements for the mechanical seals. To meet users expectations of longer service life for low investment costs, EagleBurgmann has developed families of seals that fully cover a wide range of applications and are based on many years of experience and development. These seal designs are standardised and thus provided the most cost-effective solution for the required
application, but are still extremely reliable. Engineered solutions are still needed for special equipment. The seal design depends on the type of installation and the process-specific load. The mechanical, process-specific, physical, chemical and safety requirements must all be taken into account in the design of the mechanical seal. Seals may also have additional design features depending on the process requirements. These may include a Cooling flange for additional cooling of the seal for process temperatures in excess of 200 C. Leakage drain Leakages of media that could harm the product or environment can be drained off into an external system. Polymerisation barrier prevents polymerisation of the product in the dynamic seal area by means of a liquid reservoir on the process side or by flushing. Resublimation barrier prevents deposits in the dynamic seal area released by product resublimation by means of a liquid reservoir on the process side or by flushing.
Production of dispersions at BASF Ludwigshafen. Stainless steel vessel with top entry agitator. Medium: dispersions Temperature t1: 50 C Pressure p1: 0 ... 3 bar Rotational speed: 0 ... 30 min-1 Seal: M451KL-D20/200-E1 Supply system: SPA 2020/A40-V1 Barrier medium : Glycol Barrier pressure p3: 5 bar
Top entry installation A top entry installation is generally used to seal the gas containing headspace. It should be noted that the dynamic and stationary sealing elements on the product side can come into contact with splasher and foam from the tank. There is also a risk of polymerisation in gaps or in the dynamic sealing area. The maximum speed, temperature and system pressure to be sealed in the reactor are important factors that affect the design. The mainly overhung agitator shafts are subject to bending stresses that cause the shaft to deflect in the seal plane. The mechanical forces that act on the shaft seal and bearing also have to be analysed carefully, as well as unwanted vibrations caused by internals that affect the flow or special cases, e.g. liquid bearing missing from the agitator. Shaft deflections in the seal area of 0.1 mm to 0.3 mm are tolerated as standard, depending on the size of the drive system and agitator. Up to 2 mm is possible in special cases. EagleBurgmann seal systems have proven successfully in many different applications. Liquid-lubricated: n EagleBurgmann M481 Single or double seal with or without bearing for steel vessels n EagleBurgmann M461 Single or double seal with or without bearing for glass-lined vessels May be equipped with cooling flange, leakage drain or polymerisation barrier to meet the process requirements. Dry running, with contact of the seal faces: n EagleBurgmann SeccoMix Single seal with or without bearing n EagleBurgmann SeccoMix Double seal with or without bearing Gas-lubricated without contact of the seal faces: n EagleBurgmann AGSZ Double seal with or without bearing n EagleBurgmann AGSR Double seal with rotating seat on the product side, with or without bearing
Glass-lined polymerisation reactor (Ekato) for producing ion exchanger granules at Lanxess Bitterfeld, Energizing Chemistry. Medium: Styrene copolymer, aromatics Temperature: 20 ... 150 C Pressure: p1: 0 ... 3 bar Rotational speed: 15 ... 50 min-1 Seal: M481KL-D21/140-E1 Polymerisation barrier, ATEX zone 1 Supply system: TS2000/M226-D1 Barrier medium : White oil Barrier pressure: Plan 53
Glass-lined stirred-tank reactor (EHW Thale) with top drive for producing various intermediate products for the pharmaceutical industry, for example. Used at Chemie AG Bitterfeld-Wolfen, Multi Purpose Center. Temperature: -10 ... 200 C Pressure: p1: -1 ... 6 bar Rotational speed: 30 ... 100 min-1 Seal: M461 KL-D20/100-00 Supply system: TS 1016/A007-00, Plan 53 Barrier medium : White oil
DIN standard agitator drives DIN 28161 Requirements on agitator drives covers the most important requirements on the seal. It defines speed limits, direction of rotation, bearing, running accuracy and the stuffing box dimensions for mechanical seals. The running accuracy of the agitator is defined in relation to the shaft diameter, but does not consider dynamic loads on the agitator shaft during mixing. DIN 28161 applies to shaft diameters from 40 mm to 220 mm and a sliding velocity of up to 2 m/s, a pressure of -1 to 6 bar and a temperature from -25 C to 200 C. Within the DIN range EagleBurgmann supplies proven seal solutions tailored to different requirements, for steel or glass-lined vessels, e.g. the M4 ..., SeccoMix and AGSZ series.
Animal feed enzyme production at BASF Ludwigshafen. Stainless steel vessels with top entry agitator with sealed SeccoMix Medium: Aqueous solution Temperature t1: 5 ... 15 C Pressure p1: unpressurised Rotational speed: ... 45 min-1
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Top entry stirred-tank reactor (Chema) in the HAS system at DOMO Caproleuna. Medium: Hydroxylammonium sulphate (HAS) Temperature: max. 200 C Pressure p1: 5 bar Rotational speed: 150 min-1 Seal: M481KL-D20/180-A2 Supply system: TS1016 Barrier medium: Deionate (demineralised water) Barrier pressure: 7 bar
Bottom entry installation In contrast to top entry, it is the process medium itself which is sealed in a bottom entry installation. The rotating agitator shaft must be sealed off from the bottom of the tank and is totally immersed in the medium. It is characteristic for this installation that deposits may form in the area of the dynamic and stationary sealing elements, depending on the process medium. These can then hang up the seal. Additionally, the seal directly faces the temperature of the process medium. To cope with these tough operating conditions, mainly double seals with pressurised barrier medium are used. Other design features, such as flushing, may also be used. The materials must also be selected carefully. One decisive criterion in the choice of the barrier medium is its compatibility with the process medium. As with the top entry installation, the maximum speed and temperature, the sealed system pressure in the vessel, the chemical requirements, the bending stresses, the shaft deflection and the bearing must all be carefully analysed and evaluated. EagleBurgmann sealing systems from the liquid-lubricated MR..., MR333 and HSHLU series and process-optimised gas-lubricated seals from the AGSR series have proven successfully for bottom entry installations.
Vitamin production at BASF Ludwigshafen. Homogenisers in a vacuum dryer. Medium: Vitamin pre-product Temperature: 200 C Pressure: 1 ... 5 bar Rotational speed: 1,500 / 3,000 min-1 Seal HSMR1S24-D55/65-E1-A25
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The equipment used in separation processes are often engineered designs, so the seals must be selected and designed particularly carefully. Top, bottom and side entry installations are all used. The forces acting on the seal during operation must be considered in detail in advance and must be taken into account in the seal design in order to guarantee an optimum sealing solution. The emphasis in the seal design is placed on both the relatively high thermal loads (can be in excess of 300 C) and the product deposits in the area of the dynamic and stationary
sealing elements on the product side. They must not prevent the seal from moving as required. Process-optimised seal design with rotating seals on the product side (MR series) have proved particularly successfully. High temperatures can lead to considerable thermal expansion between the dryer drum and drive shaft. There can also be excessive relative movement, depending on whether the seal is installed on the drive side or the non-drive side. These movements must be absorbed with metal bellows or special deflector systems. Such metal
bellows are designed for a specific type of dryer and the additional forces are taken into account. EagleBurgmann seals can reliably fulfil the following process requirements: No contamination of the product Possibility of sterile operation n The mechanical seals functions are monitored by the supply system n High MTBF
n n
HSMR1AL with metal bellows for compensating for large relative movements in a paddle dryer. Radial decoupling of the vessel / flange and shaft.
Spherical dryer (Rosenmund Guedu) for manufacturing pharmaceutical powders with HSMR5L-D.
Werb.Nr. 2829
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Examples of equipment used in mechanical and thermal separation processes: Nutsche filter (pressure nutsche filter) Nutsche filters are used for the discontinuous filtration of suspensions with a relatively high solids content. They consist of a flat, cylindrical container with a horizontal filter surface. The modern types are equipped with agitators, which are generally heightadjustable. The filtration process is operated under overpressure or under
vacuum. The operating cycle for such a nutsche consists of the following steps: Filling the nutsche and filtration; the agitator distributes the suspension uniformly over the filter surface. n Washing the filter cake n Removal of the filter cake, e.g. by the agitator or by tilting the entire container
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Filter dryer (nutsche dryer) The filter dryer is a variant of the nutsche filter that brings together the filtration and the cake drying, generally under vacuum, in a single apparatus with no product transfer. The agitator, tank walls and sometimes the tank base can be heated for drying. Filter dryers are used to process sensitive materials by gentle drying conditions to a low residual humidity.
Conical dryer This type of dryer is used primarily for bulk goods that must not stick or cake too much during drying. The material is circulated gently by a mixing screw which rotates both about its own axis and along the tank wall. The conical dryer can be operated under vacuum or under overpressure. Heat is supplied via the wall heater and additionally via the heated screw. There are variants with top drive or bottom drive design which has significant effects on the operational safety and the ability to empty the apparatus. One particular challenge for the sealing technology in bottom entry installation the sealing of two coaxial agitators moving at different speeds.
Pressure nutsche filter (KHS) made of Hastelloy and steel, for drying various intermediate products at Chemie AG Bitterfeld-Wolfen, Multi-Purpose Center. Temperature: -10 ... 200 C Pressure: p1 = -1 ... 6 bar Rotational speed: 5 ... 6 min-1 Seal: HSMR35AL-D/170-E9, Supply system: Thermosiphon system, Plan 53 Barrier medium : White oil
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Paddle-dryer (Lipp Mischtechnik), frequencycontrolled, for producing and drying salicylic acid at Rhodia Syntec. Medium: Salicylic acid, various aromatics Temperature: 40 ... 220 C Pressure: -1 ... 11 bar Rotational speed: 8 ... 80 min-1 Seals: HSMR1AL-D/180-E1 Side drive, with 1 seal on drive and non-drive side Supply system: Thermosiphon system Barrier pressure: Plan 53 with circulating pump
Double cone dryer (rotary dryer) In a double cone dryer, the vessel is set in a tumbling motion by rotation. Thereby the product in the dryer is mixed and comes into contact with the heated wall. This ensures a good thermal transfer. Usually the double cone dryer is operated under a vacuum and is suitable for drying free flowing media. The internal space generally has no internals, so the apparatus is easy to empty and clean. Choppers are sometimes used to break up the product. In
this case the apparatus can sometimes be used to process paste-like media. Paddle-dryer Paddle-dryers are suitable for the discontinuous and continuous drying of pastes or free flowing media. A slowly-turning, generally heated shaft that is fitted with mixing paddles keeps the solids in movement. This intensive mixing means that even media that tend to stick together during drying can be processed. Choppers can also be used to break up the media. Smaller
apparatuses can often be opened at the end since the shaft is only mounted at one end. Large paddle-dryers can reach up to 20 m3, in which case the shaft will be mounted at both ends.
Paddle-dryers (Ldige) for drying active ingredients for the pharmaceutical industry. Operator: Berg chemical works. Medium: Active ingredients for the pharmaceutical industry Temperature: 100 C Pressure: Vacuum ... 0 bar Rotational speed: 32 min-1 Seal: HSMR5S1-D2/120-E1 Side drive, with 1 seal on drive and non-drive side Supply system: TS 1016 with 5000, plan 53 Barrier medium: White oil
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Thin-film evaporator (Chema) in the caprolactam plant at DOMO Capro Leuna. Medium: Caprolactam Temperature: 200 C Pressure: Vacuum Rotational speed: 150 min-1 Seal: M45-D90/82 Central supply system SPA 4002/A03-D1 Barrier medium: demineralised water Barrier pressure: 5 bar
Thin-film evaporators are used to increase the concentration of high-viscosity products, to recover solvents and for temperature-sensitive materials under vacuum. Rotor blades distribute the liquid uniformly, which forms a thin film on the heated wall.
Chopper Additional units in the form of cutters or rotor/stator systems can be integrated to accelerate mixing processes and to break up clumps. These choppers are generally arranged at the side, at the base of the tank. High speeds up to 3,000 min-1 are reached. The MR5 as a double seal with pumping screw and with HS grooves, if necessary, has proven particularly successfully for this application.
MR5LF-D with integrated bearing and directly attached chopper (mixing accelerator)
Glass-lined polymerisation reactor (Ekato) for producing ion exchanger granules at Lanxess Bitterfeld, Energizing Chemistry. Medium: Styrene copolymer, aromatics Temperature: 20 ... 150 C Pressure: p1: 0 ... 3 bar Rotational speed: 15 ... 50 min-1 Seal: AGS481KL-D21/140-E4-U polymerisation barrier, Atex zone 0 (in the tank), zone 1 outside Supply system: GSS4016/A003 or GSS4016/A214 Barrier medium: Air Barrier pressure: 9 bar
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EagleBurgmann
M481
EagleBurgmann SeccoMix and SeccoMix 481 Dry-running mechanical seals n FDA approved
n
Operating limits SeccoMix (cartridge units) d1 = 25 ... 220 mm (0.984 ... 8.661) p1 = vacuum ... 6 bar (87 PSI) t1 = 20 ... +150 (200) C (4 ... 302 (392) F) vg = 2 m/s (6 ft/s) Perm. axial movement: 1.5 mm Radial movement: 2 mm SeccoMix (component seals) d1 = 25 ... 160 mm (0.948 ... 6.229) p1 = vacuum ... 6 bar (87 PSI) t1 = 20 ... +150 (200) C (4 ... 302 (392) F) vg = 2 m/s (6 ft/s) Perm. axial movement: 1.5 mm Radial movement: 2 mm
Specific face material combinations allow dry-running with contact of the seal faces. The grade of carbon used in the seal face is FDA-conform. For use in pharmaceutical applications, the seal can be equipped on request with a collecting cup (CIP). The SeccoMix as a single seal does not need a supply system.
SeccoMix single seals
Werb-Nr. 2783
With a single seal, the process gas is dissipated to the atmosphere or can be diverted into drainage system. If any leakage into the atmosphere is not permitted, a SeccoMix double seal should be used. This should be pressurised with a barrier gas (preferably N2) and a barrier pressure of 0.5 to 1.0 bar above the pressure to be sealed. The hydraulic conditions ensure that the seal is closed by both the product pressure and a superimposed barrier pressure. Agitator seals from the SeccoMix series are available as components or as factory-tested cartridge units (SeccoMix 481). Connections for steel (SeccoMix 481) and glass-lined (SeccoMix 461) reactors are available to DIN standards or as required.
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Werb-Nr. 2784
EagleBurgmann M461 and M481 Liquid-lubricated mechanical seals according to DIN 28136 and DIN 28138 n for steel and glass-lined vessels n FDA approved
n n
The hydraulic conditions ensure that the seal is closed by both the product pressure and a superimposed barrier pressure. Operating limits according to DIN 28138 T2 d1 = 40 ... 220 mm (1.575 ... 8.661) vg = 2 m/s (6 ft/s) p1 = vacuum ... 6 bar (87 PSI) t1 = 25 ... +200 C (13 ... 392 F) EagleBurgmann operating limits (depends on the choice of materials and the supply system) d1 = 40 ... 220 mm (1.575 ... 8.661) vg = 5 m/s (16 ft/s) p1 = vacuum ... 16 bar (232 PSI) t1 = 80 ... +200 (+350) C (112 ... 392 (662) F)
The seals can be used for a wide range of applications, and may be used as single or multiple seals with an unpressurised liquid reservoir (quench) or pressurised with a supply system (TS1016 or TS2000). With the double seal, the operating limits are far higher than the pressures and speeds defined in the DIN standards. Agitator seals from the M461 and M481 series are supplied in the form of factory-tested cartridge units. Suitable options include cooling or heating flange, polymerisation barrier, leakage drain and cleanability for use in pharmaceutical applications. The materials used are extremely flexible, so practically all requirements can be met with the standard design variants.
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AGSZ
HS-D HSH-D
Werb.Nr. 2820
EagleBurgmann AGSZ 461 and AGSZ 481 Gas-lubricated, contact-free mechanical seals n according to DIN 28136 and DIN 28138 n for steel and glass-lined vessels
n
The AGSZ is not sensitive to radial deflection. A centrally rotating seat, stationary spring-loaded seal face and an integrated bearing, which acts at the same time as a fixed bearing for the seal and as a floating bearing for the shaft, provide effective protection against negative influences on operation. An optimum sealing gap stiffness ensures that the seal operates reliably without contact, even under tough operating conditions. Agitator seals from the AGSZ series are supplied in the form of factory-tested cartridge units.
AGSR ... for sterile applications in theWerb.Nr. pharmaceutical 2821 industry The R in AGSR standard for a rotating seat on the product side. The AGSR is particularly suitable for applications in the pharmaceutical, biotech and food industry. If certain requirements are fulfilled and with a few additional design features, the seal can also be used in direct contact with the product. Supply system for AGSZ... and AGSR... A supply system from the GSS series is needed for operation. A gas network connected upstream is sufficient to supply gas and pressure. The necessary barrier pressure must be 3 bar higher than the process pressure to be sealed. The aerostatic design ensures that the gas consumption is approximately the same across the whole operating range. Operating limits d3 = 40 ... 220 mm (1.575 ... 8.661) p1 = vacuum ... 10 bar (145 PSI) t1 = 30 (80) ... +200 (+250) C (22 (112) ... 392 (482) F) vg = 10 m/s (32 ft/s)
Mechanical seals of the HS series can be equipped with additional design feature, such as cooling and heating flange, polymerisation barrier, leakage drain and cleanability for use in pharmaceutical operations. The materials used are extremely flexible, so practically all requirements can be met. The connection sizes are matched to individual requirements. The dual seals are operated with a supply system. To run perfectly, the sliding faces are equipped with EagleBurgmann patented hydrodynamic grooves, which provide an optimum lubrication with minimal load on the sliding faces. These features ensure that the HS series is highly reliable and has a long service life. Operating limits d1 = 20 ... 500 mm (0.787 ... 19.68) p1 = vacuum ... 40 bar (580 PSI) t1 = 30 ... +200 (+350) C (22 ... 392 (662) F) vg = 5 m/s (16 ft/s)
Agitator seals of the HSH-D series are specially designed for high-pressure applications. They are engineered solutions with connection sizes matched to the specific application. The seals are operated with a supply system. Combined with hydrodynamic grooves, these seals offer minimal load on the sliding faces, optimum formation of a lubricating film, high reliability and a long service life. Operating limits d1 = 20 ... 350 mm (0.787 ... 13.78) p1 = vacuum ... 250 bar (3,625 PSI) t1 = 30 ... +200 (+350) C (22 ... 392 (662) F)
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EagleBurgmann MR Connection sizes are matched to indivi Mechanical seal for chemical and dual requirements. pharmaceutical applications The double acting seals are operated n for adhesive, paste-like and dry media with a supply system. Agitator seals of the MR series are Operating limits ideal for use with adhesive, paste-like and dry media in agitators and all types d1 = 20 ... 200 (500) mm of mixers, dryers, kneaders and reactors (0.787 ... 7.874 (19.68)) in the plastics, dyestuffs, food and p1 = vacuum ... 23 bar (333 PSI) pharmaceutical industry. p3 = 25 bar (362 PSI) p (p3 - p1) max. 10 bar (145 PSI), Building on many years practical min. 2 bar (29 PSI) experience and through the use of the t1 = 30 ... +300 C (22 ... 572 F) latest face materials, MR seals can be vg = 20 m/s (65 ft/s) found operating successfully in almost all applications. The rotating seat on the product side is an outstanding design feature.
n
Agitator seals of the HSHLU-D series are typically used for bottom entry applications such as plastics production. The seals are fully immersed in the process medium and are subject to extreme stresses. On the product side, floating throttle rings with flush prevent the intrusion of medium (e.g. polymer powder) into the seal area. The double acting seals are operated with a supply system. Operating limits d1 = 20 ... 400 mm (0.787 ... 15.748) p1 = vacuum ... 60 bar (870 PSI) t1 = 30 ... +200 C (22 ... 392 F)
The MR333 version of the seal fulfils all the criteria for sterile processes: surfaces on the product side are polished, smooth and free of gaps, CIP/ SIP compliant and conform to FDA guidelines. They can be equipped with aseptic connections, e.g. to DIN 11851.
MR-D
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Quench system Quench is the term commonly used in sealing technology for an arrangement that applies an un-pressurised external medium (liquid) to a mechanical seals sliding faces. The quench performs at least one of the following tasks: Absorption or removal of leakage by the quench medium n Monitoring of the mechanical seals leakage rate by periodic measurement of the level of the quench medium in the circulation vessel or thermosiphon vessel n Preventing of the contact between leakage and atmosphere for media which react undesirably with oxygen n Protection against dry running n Cooling n Lubrication
n
Closed circuit: Thermosiphon system / pressure booster or cooling circuit with refill unit Here, all the components are under the same pressure. They are pressurised via an external pressure source or nitrogen (TS system) via a refill system (SPN) or by the process pressure (DRU system). Before double seals start-up it is vital, to ensure a sufficient rate of circulation of the barrier liquid. The barrier liquid pressure should be 10 % or at least 1.5...2 bar above the maximum pressure to be sealed. To ensure that the sliding faces are lubricated well, the outlet temperature of the barrier medium must be regulated via the flow rate so that the boiling point of the barrier medium in the sealing gap is not exceeded at atmospheric pressure. The maximum acceptable inlet/outlet temperature differential is 15 K. The barrier liquid outlet is situated at the highest point of the seal chamber for automatic venting of any vapour. The basic operating conditions define the following functions of the supply system: Build-up pressure in the barrier interspace n Compensation of leakage n Circulation of the barrier medium n Cooling of the barrier medium n Cooling of the seal n Lubricating of the sliding faces
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Glass-lined agitated tank for producing various intermediate products. Sealed with AGS, supplied with nitrogen via GSS4016 (background) and SP25 pressure booster pump (foreground).
Depending on the type of equipment in which they are used, and on the medium, mode of operation and environmental protection requirements, etc, agitator seals may need additional design features to ensure efficient operation. As the requirements on mechanical seal increase, their design, mode of operation and ultimately their supply systems are changing. The following pages show the most commonly used and proven supply systems used in state of the art sealing technology for agitator seals. Barrier or quench systems for liquid-lubricated single and multiple mechanical seals Mechanical seals can only be guaranteed to work efficiently if the space between the product and atmosphere side of the mechanical seal is completely filled with clean medium. The liquid reservoir may be un-pressurised or pressurised.
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Supply systems Supply systems for liquid-lubricated mechanical seals can essentially be divided into two types: Open circuit: Buffer fluid system A circuit which provides both circulation and pressurisation via a supply system (e.g. EagleBurgmann SPA). The barrier medium is depressurised after it has circulated and is collected in an unpressurised tank.
SPS
PI
SPS N2
PI
N2
SPK
SPU
RP
SPU
TI TI
SPU Seal
TI
Seal
Seal
EagleBurgmann TS 1016 Thermosiphon system Pressure vessel with flat bottom and incorporated cooling coil and sight-glass for level control. Perm. operating temperature 60 ... +120 (200) C (76 ... 248 (392) F) Perm. operating pressure 18 bar (261 PSI)
EagleBurgmann TS 2000 Thermosiphon system Pressure vessel with torispherical heads and incorporated cooling coil and sight-glass for level control. Perm. operating temperature 60 ... +200 C (76 ... 392 F) Perm. operating pressure 30 bar (435 PSI) (TS 2000), 63 bar (913 PSI) (TS 2063)
EagleBurgmann DRU Pressure booster system With the DRU system it is possible to supply barrier fluid to double seals for a wide range of applications. It works similar than the TS system but, in this case, the barrier pressure is generated by the reference pressure (e.g. tank pressure) without additional superimposed nitrogen. Perm. operating temperature 60 ... +200 C (76 ... 392 F) Perm. operating pressure 63 bar (913 PSI) (DRU2063) Transmission ratio 1:1.1 or 1:1.5
Thermosiphon systems The EagleBurgmann TS system TS 1016 or TS 2000 is used to supply barrier fluid to double and tandem seal arrangement for a wide range of applications. TS vessels are equipped as standard with all the necessary connections and brackets. Additional components (e.g. circulating and refill pumps, measuring equipment, level switches and valve groups) may be installed as required. The vessel is used for storage, pressure maintenance and cooling of the quench or barrier liquid in the sealing circuit. Design, construction and production according to the EU Pressure Equipment Directive 97/23/EC. All pressure-loaded welds are butt-welded or counter butt-welded by MIG and TIG process. Sockets with recessed gasket (no contamination of the circuit by thread sealant). Cooling water connections at top (Out) and bottom (In) for venting and draining.
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Seal
TI PI PI
PCV
M LS
LG TI
Barrier pressure systems of the SPA series The basic version performs and fulfils all four tasks of a supply system essential for operating double seals: Circulation and cooling of the barrier medium, pressurisation of the barrier medium and compensation of leakage. EagleBurgmann SPA units have a high quality standard, are easy to operate and maintain, and are adaptable and rugged. Their function is based on the principle of the open circuit.
Supply systems of the SPN series with SPU These are automatic refill units with pressure switch (SPN 1000 series) or pressure control valve (3000 series) for manual barrier pressure regulation. The pressure control valve (SPN 3000 series) allows a constant barrier pressure irrespective of hysteresis-induced pressure fluctuations (hysteresis of the pressure switch). Temporary maintaining of the barrier pressure when the pump is switched off by the accumulator. Several outputs can be provided for setting different barrier pressures. The basic version of the automatic refill unit SPN only performs two of the four tasks of a barrier system, compared to an SPA: pressurisation of the barrier medium and compensation of leakage. The energy needed for pressurisation (piston pump) is supplied via a pneumatic and an electric drive, either in combination or individually. Separate components are installed in the seal barrier circuit to cool and circulate the barrier medium.
PIA
PIA
TIA
TIA
Seal
Seal
PI
FIS
FIS
PS M LS_L
LG
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SPA 4002 for supplying 12 agitator seals on thin-film evaporators at DOMO Caproleuna.
SPA 4015
GSS 4016
EagleBurgmann supply systems GSS 4016 for gas-lubricated, pressurised agitator seals. Gas-lubricated mechanical seals may only be operated if the barrier pressure is high enough. At any operating condition the barrier pressure p3 must be at least 3 bar higher than the product pressure p1 to be sealed. Gas supply systems of the GSS series are specially designed for dry running and gas-lubricated mechanical seals. Important GSS functions: Filtering of the barrier and flush gas Pressure monitoring and pressure regulation n Flow rate monitoring n Control and drainage of the leakage
n n
Key FIS LG LS LS-L M N2 PCV PI PIA PS RP TI TIA SPK SPN SPS SPU Flow switch with indicator (sight-glass) Level indicator Level switch MIN level switch Motor Nitrogen Pressure control valve Pressure gauge Contact pressure gauge Pressure switch Reference pressure Thermometer Contact thermometer EagleBurgmann components: Contact device Manual refill pump / refill unit Level switch Circulating pump
A single connection to the gas supply (or cylinder with pressure reducer) with an upstream EagleBurgmann GSS 4016 gas supply and control system is sufficient to operate the gas-lubricated agitator seals. We recommend the application of the GSS 4016 gas supply system with two flow meters (FIAH, FIAL) and a pressure monitoring unit (PIAL).
Pressure nutsche filter (Gedue) in the HAS plant at DOMO Caproleuna. Medium: HAS, catalyst Temperature: 200 C Pressure: Vacuum Rotational speed: ... 20 min-1 Seal: HSSMR35AL-D/170-E8 Supply system: TS2000 + SPU2040 Barrier medium: Deionate (demineralised water) Barrier pressure: 5 bar
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All technical specifications are based on extensive tests and our many years of experience. The diversity of possible applications means, however, that they can serve only as guide values. We must be notified of the exact conditions of application before we can provide any guarantee for a specific case. Subject to change.
Burgmann Industries GmbH & Co. KG uere Sauerlacher Str. 610 D-82515 Wolfratshausen Germany Phone +49(0)8171/23-0 Telefax +49(0)8171/23-1214 www.eagleburgmann.com