CPCL
CPCL
CPCL
(AGroupcompanyofIndianOil)
Slide1
PRESENTATION PLAN
REFINERY PROCESSES
REFINERY CONFIGURATION
PROJECT DESIGN ASPECTS
Slide2
Slide3
Examples
Separation
Breaking up a
mixture into its
components
Distillation/
fractionation
Extraction
Finishing
Conversion
- Fundamentally changing
the chemical structure
of a product by:
Breaking down
molecules
Combining
molecules
Rearranging
structure
Coking
Cracking
Alkylation (combining)
Isomerization
(rearranging)
Improving the
qualities of
products by:
Blending products
of different
qualities to get an
optimal mix
Treating products
(typically with
hydrogen) to
remove impurities
Gasoline blending
Hydro-treating
Slide4
SEPARATION PROCESS
Slide5
DISTILLATION COLUMN
Slide6
DISTILLATION PRINCIPLE
Separation of components from a liquid/vapor mixture via
distillation:
Depends on the differences in boiling points of the
individual components
Depends on the concentrations of the components
present
Hence, distillation processes depends on the vapour pressure
characteristics of liquid mixtures.
Slide7
Slide8
Reboiler
Condenser
Reflux Drum
Slide9
OPERATING VARIABLES
Temperature
Pressure
Draw off and reflux rates
Pump around
Stripping steam rate
Slide10
Inorganic salts
Acids
Desalting helps to remove these impurities
Slide11
Furnace:
Natural draft
Forced Draft
Balanced Draft
Slide12
ATMOSPHERIC DISTILLATION
Slide13
VACUUM DISTILLATION
Slide14
VACUUM DISTILLATION
Slide15
CRUDE DESALTER
Slide16
CRUDE FURNACE
Slide17
Slide18
SPINDLE
LIGHT NEUTRAL
INTERMEDIATE NEUTRAL
500 NEUTRAL
HEAVY NEUTRAL
BRIGHT STOCK
Slide19
LUBE PROPERTIES
Properties /
Components
Viscosity
Viscosity
Index
Pour Point
Paraffins
Low
High
High
Naphthenes
Medium
Medium
Medium
Aromatics
High
Low
Low
Slide20
PROCESS
Vacuum Distillation
Solvent Extraction/
PROPERTY
CONTROL
Viscosity,
Flash Point
Viscosity Index
Pour Point
Colour / Oxidation
Stability
Slide21
Furfural
Extraction
Unit
Atm.Distl
Column
Extract
Raffinate
RCO
Vacuum
Distillatn
Column
DWO
Lube
HyFi
Unit
LOBS
NMP
Extraction
Unit
Vac. Distl
DAO
Vac.
Residue
MEK
Dewax
Unit
PDA
Unit
Extract
Slack Wax
Pitch
Slide22
WAX PROCESSING
INERT GAS
NH3
REFRIGERATION
FILTERS
FEED
SOLVENT
RECOVERY
FROM WAX
HY.FI
UNIT
PRODUCT
STORAGE
CHILLING
SOLVENT
RECOVERY
FROM
FOOTS OIL
DEOILED WAX
STORAGE
FOOTS OIL
Slide23
Slide24
Conversion Process:
Thermal processes
Catalytic processes
Treating Process
Catalytic processes
Chemical treating process
Slide25
Mildthermaldecomposition(visbreaking)
Reductionofviscosity&pourpointoffeed
DesirableReaction Cracking
Somepolymerizationcondensationreactionalsooccurs
Cokeformation
Slide26
0.95 kg/cm2
160 c
GAS
96 c
9.8 kg/cm2
39
26
210 c
Stabiliser
STABNAPHTHA
GO
STEAM
130 c
426 c
25 mmhg
GAS+SLOPS
7.7 kg/cm2
LVGO
300 c
HVGO
380 c
VISBREAKER
440 c
FEED
HEATER
STEAM
SOAKER
FRACTIONATOR
300 c
VACUUM
FLASHED
CRACKED
VACUUM RESIDUE
FLASHER
Slide27
Slide28
CATALYTIC (REACTORS)
Reactor Design
Better performance and operational flexibility can be
achieved:
Choice of catalyst
Choice of feed
Operating conditions
Reactor configuration
Synergy with other units
Better internals
Slide29
REACTOR INTERNALS
Inletnozzle
Distributornozzle
Debrisbasket
Catalyst
Alumina
balls
Catalystunloading
nozzle
Outletnozzle
Screen
Slide30
REACTOR INTERNALS
Inletnozzle
Distributornozzle
Debrisbasket
Catalyst
Alumina
balls
Quench
Catalyst
Catalystunloading
nozzle
Outletnozzle
Screen
Slide31
CATALYTICREFORMING
CHEMISTRY:
Dehydrogenation
Isomerisation
Dehydro cyclization
Hydrocracking
Slide32
CATALYTICREFORMING
DEHYDROGENATION:
C7H14
Methylcyclohexane
RON:
73.8
>C7H8+3H2
Toluene
119.7
ReactionishighlyEndothermic
Promotedbylowpressureandhightemperature
Occuronmetalsite(Platinum)
FastestreactioninReforming
Slide33
CATALYTICREFORMING
ISOMERISATION:
Naphthene
Naphthene
Aromatic
+
Cyclo Hexane
RON - 110
3H2
Benzene
RON - 120
Slide34
CATALYTICREFORMING
DEHYDROCYCLISATION:
Paraffin
Aromatic
-C-C-C-C-C-C-C-
RON
n-Heptane
0.0
3H2
Toluene
119.7
Reaction is Endothermic
Promoted by low pressure and high temperature
Occur on acid and metal site
Slowest reaction in Reforming
Slide35
Naphtha
Impurities: S,N,
Metals
Risk of poisoning
CCR catalyst
Naphtha
Hydrotreating
Hydro treated
Naphtha
Impurities:
Nil or low
No Risk of
poisoning
CCR catalyst
Reformate
High Octane
Number: 102
Hydrogen
Rich gas
Low octane
number
Continuous
Catalytic
Reforming
Slide36
NHT CCR
Slide37
CCR REACTOR-REGENERATOR
Slide38
NHT ISOM
NHT Section - Main reactions
Hydrorefining reactions
removal of impurities
Desulfurization
Denitrification
Hydrogenation reactions
saturation of the olefins and diolefins
Demetallation reactions
removal of metallic impurities
Slide39
NHT ISOM
C16
LPG Product
C29
Heavy Isomerate
LPG Separator
C22
Deisohexanizer
Light Isomerate
Storage
Isom
Stabilizer
C19
C17
C13
K1A/B
Make-up H2 compressor
R3
Recycled H2
To R1
C4
NHDT Stripper
Second Isomerization
Reactor
R4
NHDT
Separator
Feed Dryer
Feed
Heater
K2 A/B
H2 Dryer
Surge Drum
C2
LPG Stripper
Feed
Naphtha
F1
HDS Reactor
C1
R2
First
Isomerization
Reactor
Diene Reactor
R1
To FCC
C5/C7+ Cut
C30
To Isomerate Storage
Slide40
HYDROCRACKER BLOCK
Reaction Chemistry
Hydro-treating Reactions
a) Demetallization
b) Desulfurization
c) Denitrification
d) Olefins Saturation
e) Aromatics Saturation
Hydrocracking Reactions
CnH2n+2
+ (x-1) H2
Catalyst (Ni3S2)
x C n/xH2n/x +2
+ Heat
Slide41
HYDROCRACKER
Recycle gas
compressor
(RGC)
Make-up H2.
VGO
feed
from HGU
Quench
H2
Recycle gas
Feed
preheating
and
filtration
Make-up H2
Amine
treating
Furnace
Gas
Make-up H2
compressor
Reactors
HP
172.5 Kg/cm2
gas separator
3780C
Liquid hydrocarbon
Off-gas to PSA
(for
H2 recovery)
LP
gas separator
Light end
recovery
section
Lighter hydrocarbons
Product
Lighter hydrocarbons
stripper
Heavier
hydrocarbons
3600C
Furnace
Kerosene / ATF
Fractionator
Diesel..
UCO (to FCCU)
Slide42
Slide43
Products to
Main Column
FLUIDCATALYTICCRACKINGUNIT
Flue
Gas
680C
Reactor
500C
Flue Gas
Slide Valve
Stripping
Steam
Regenerator
650C
Spent Catalyst
Slide Valve
Air
43000
nm3/hr
Regenerated Catalyst
Slide Valve
Catalyst circulation
10 MT/min
Raw OiL
120 m3/hr
370C
Slide44
FINISHING PROCESS
Slide45
Slide46
DHDT REACTOR
Parameters
SOR
EOR
77.7
79.6
331
375
351
388
75.0
75.0
Reactor
Dimensions
Height,m
31.3
Width,m
4.4
Slide47
Slide48
Lean amine
Tail Gas
Treating
Thermal
Converter
Acid Gas
Amine
Regn.
(ARU)
Catalytic
Converters
Sulphur
2-stage
SWS
Unit
Slide49
CPCL SRU
Slide50
PRESENTATION PLAN
1.
REFINERY PROCESSES
2.
REFINERY CONFIGURATION
3.
Slide51
Refinery Configuration
Key Considerations & Available Options
Slide52
Ref.Fuel
GasSystem
Amine
Treating
LPG
Amine
Regeneration
Amine/Merox
Treating
Atmospheric
Distillation
Naphtha(4590C)
Naphtha
Splitter
Sulphur
Recovery
H2
HexanePlant
Hydrogen
Generation
Naphtha(90130C)
MS
Hydrogen(H2)
NAPHTHA
Catalytic
Reforming
HY.NAP
ATF
PROPYLENE
PBFS/MEKFS
HEXANE
Isomerate
NHT/ISOM
LT.NAP
LPG
Reformate
ATF
ATFTreating
SK
Diesel
SK
DHDS/DHDT
Long
Residue
H2
LUBEDistillates
Extraction
Dewaxing
LUBEOIL
BASESTOCKS
Short
Residue
VGO
LCO/HCO
VBVGO/HCGO
CokerNaphtha
VBNaphtha
LPG
Treating
LPG
FO
Propylene
Recovery
FCCU
MeroxTreating
Cracked
Gasoline
ASPHALT
SULPHUR
Visbreaking
Biturox Unit
DelayedCoking
LCGO
PARAFFIN
WAX
Hydrocracker
LCGO/VBGasOil
Vacuum
Distillation
WaxDeoiling&WaxHydrofinishing
UCO
DIESEL
LubeHDT
HCGO
COKE
Slide53
Slide54
Slide55
Slide56
Projects Classification
Slide57
Slide59
Euro-III
Euro-IV
Euro-V
Sulphur, ppm
500
150
50
10
RON, min
88
91
91
95
MON, min
81
81
85
60
60
60
60
5/3
42
35
35
21
21
18
Euro-III
Euro-IV
Euro-V
500
350
50
10
Cetane Number
48
51
51
51
95% recovery, C
370
360
360
360
35
35
60
Slide61
Slide62
Slide65
Types of Refineries
Topping Refinery
Skimming Refinery
Cracking (hydro/catalytic) Refinery
Coking refinery
Integrated Refinery
Lube Refinery
Slide66
Catalytic Cracking
Hydro-cracking
Catalytic Reforming
Isomerization / Alkylation, etc
Treating Units
Hydrotreating
Slide67
Units
Capacity (MMTPA)
1.95
1.63
1.36
0.07
1.0
0.5
Isomerization Unit
0.3
6.0
2 x 180 MTPD
Slide68
Refinery Configurations
Cases Studied
S.No
SECONDARYUNITS
RESIDUNITS
VGOHDT+PetroFCC
DCU
OHCU+ConvFCC
DCU
FullConv.HCU+DHT(Integrated)
DCU
VGOHDT+PetroFCC
SDA+SlurryHCU
(50%DAO)
OHCU+PetroFCC
SDA+SlurryHCU
(50%DAO)
FullConversionHCU
SDA+SlurryHCU
(50%DAO)
ConventionalFCC
DCU
FullconversionHCU
DCU
VGOHDT+PetroFCC
SDA+SlurryHCU
(60%DAO)
10
OHCU+PetroFCC
SDA+SlurryHCU
(60%DAO)
11
FullconversionHCU
SDA+SlurryHCU
(60%DAO)
Slide69
EuroV
GASOLINE
DHT
VGO
HDT
KERO
EuroIV
GASOIL
DCU
EuroV
GASOIL
FCCPC
FCCNap.Splitter
BITUMEN
COKE
Slide70
NHT/CCR/ISOM
EuroIV
GASOLINE
CDU/
VDU
DHT
EuroV
GASOLINE
KERO
EuroIV
GASOIL
HCU
SDA
Slurry
HCU
EuroV
GASOIL
BITUMEN
COKE
Slide71
Slide73
Refinery IntegrationBenefits
Supply
Processing
Treating
Products
Distribution
Environmental
Concerns
Asset
Utilization
Slide74
Crude Oil
Associated Gas
Ethane
LPG
Naphtha
Methane
Olefins
Ethylene Propylene
Naphtha
Aromatics
C4s
PyGas
Slide75
LT. REFORMATE
NAPHTHA
HEAVY NAPHTHA
HDT
REFORMER
SPLITTER
CCR
BENZENE
340 TMT
TRANS ALKYLATION
HY. REFORMATE
Syn. Diesel/
DHDT
Naphtha
UNIT
ETHYLENE
CRACKER
UNIT
CPCL NAPHTHA
ETHYLENE
SWING UNIT
PART DIESEL
FROM DHDT
HY. NAPHTHA
FCC OFF GAS
PROPYLENE
668 TMT
1200 TMTPA
LLDPE / HDPE
362 TMT
HDPE UNIT
HDPE
400 TMT
MEG UNIT
MEG
700 TMT
DEG
135 TMT
Slide78
PROPYLENE
RECOVERY UNIT
CRACKED LPG
PROPYLENE
432 TMT
POLY
PROPYLENE UNIT
POLY
PROPYLENE
1120 TMT
PROPYLENE EXCRACKER
668 TMT
Slide79of64
Slide79
4 CH + 2 H2O + O2
(Fuel)
(Water)
(Oxygen)
Gasification Technology
4 H2
4 CO
Syngas
Slide80
Gasification MultipleSegment
Options
Fuels by F-T
Synthesis
Power
Syngas
PetCoke/
Coal
Sulphur
Slag
Hydrogen /
Power / Steam
Chemicals
SNG thru
Methanation
Slide81
Slide82
Phase-II
Project Completion
Carry out PGTR
Unit Start-up & Stabilization
Licensor Selection
Pre-Commissioning &
Commissioning stage
FLUSHING/
LEAK TEST
ORDERING/FABRICATION
P&ID
CHECK/INERTING
1ST DRYOUT
ERECTION/CONSTRUCTION
P&ID CHECK/INSPECTION
CAT. LOADING
2ND DRYOUT
FINAL INERTING
PRE-COMMISSIONING
FEED CUT-IN
Slide85
Financial Appraisal
Financing Assumptions
D/E ratio, interest rate, repayment tenor, moratorium period, etc.
Macro-economic assumptions
The net GRM for the project worked out by deducting
Operating Costs
Net incremental cash flows to the project worked out by deducting
Tax Outgo
Capital investment
Net working capital from the net benefit
Financial viability of the project established by computing posttax IRR and NPV
Net Incremental Cash Flows = [ Incremental GRM ] less [ Opex +Income Tax +
Core Capital Investment + Increase in Net Working Capital ]
Slide86
PRESENTATION PLAN
1.
REFINERY PROCESSES
2.
REFINERY CONFIGURATION
3.
Slide87
Slide88
Design Aspects
Unit/Equipment Design Philosophy (Margin & Turndown)
Battery limit philosophy for units
Vacuum Design
Instrumentation Philosophy
Metallurgy of Equipments (e.g. DSS for Water Coolers)
Piping Material Specifications
Energy efficiency / integration systems
Adherence to Standard Design & Codes
Slide89
ASME
API
ANSI
ASTM
AISI
AWWA
SSPC
MSS-SP
NACE
BS
Slide90
Slide91
Slide92
Parameter
3
4
Ambient temperature, C
Relative humidity, %
Minimum
Normal /
Average
Maximum /
Design
3.5
tmin =18
tnor = 35
@ tmin
@ tnor
tmax =45
80% @ tmax
100
450
180 km/hr (as per
IS:875 Part-III).
North East & South
West
38
29
NA
40
42
80 % at 45 o C
65 o C
Slide93
Plant Life
Default plant operating life as 15 years with 5% salvage value will
be considered for economic calculations.
The default plant equipment design life shall be taken as follows:
a) 30 years for heavy wall reactors and separators
b) 20 years for columns, vessels, heat exchanger shells and similar
services.
c) 12 years for piping, furnace tubes, High Alloy exchanger tube bundles.
d) 5 years for Carbon Steel / Low Alloy heat exchanger tube bundles.
e) 15 years for reactors removable internals
Slide94
Parameter
Minimum
Normal
Maximum
Mech Design
90
95
95
104/FV
495
505
505
505
2
Pressure, kg/cm2g
Temperature,
oC
44.8
48
54.9
58.0/FV
379
425
435
440
29.5
30.5
32.5
36.0/FV
270
280
290
300
oC
9.5
10.5
12.5
15.0/FV
200
220
240
280
5
Pressure, kg/cm2g
2.7
3.5
4.0
7.0/FV
Temperature, oC
Saturated
170
190
240
CONDENSATE RETURN
Pressure,
kg/cm2g
Temperature, oC
5.0
13
140-150
210
6.0
10.5
Amb.
65
SERVICE WATER
7
Pressure, kg/cm
2g
Temperature, oC
COOLING WATER
8
2g
4.5
8.0
2.5
8.0
oC
33
65
Return Temperature, oC
45
65
Supply Temperature,
DEMINERALISED WATER
9
Pressure,
kg/cm2g
Temperature, oC
7.0
8.0
9.0
14..0
Amb.
Amb.
Amb.
65
Slide95
Parameter
Minimum
Normal
BOILER FEED WATER (MP/HP)
Pressure, kg/cm2g
Temperature, oC
11
Maximum
Mech Design
19.0/38.0
29.0/55.0
105-110
150/150
PLANT AIR
Pressure, kg/cm2g
5.0
6.0
6.5
10.0
Temperature, oC
Amb.
Amb.
Amb.
65
12
kg/cm2g
Pressure,
Temperature, oC
13
Pressure, kg/cm2g
Temperature, oC
14
Supply Pressure, kg/cm2g
Return Pressure, kg/cm2g
Temperature, oC
15
INSTRUMENT AIR
5.0
6.0
Amb.
Amb.
FUEL GAS
2.5
3.0
40
REFINERY FUEL OIL
10.0
2.5
80
165-200
10.0
65
3.8
7.0
65
12.0
17.5
220
250
6.0
40
Pressure,
Temperature, oC
16
kg/cm2g
Pressure,
Temperature, oC
NITROGEN
5.0
Amb.
6.0
Amb.
15.0
100
7.0
Amb.
9.5
65
Slide96
WATER SYSTEMS
Backflush arrangement shall be provided for
All cooling water consumers
Only overhead condensers
Cooling water consumers with water line sizes greater than
NB.
Back flush lines to be provided with same size as main cooling water line when main line size is 6. One size lower to be provided for main
line size > 6 For much higher line sizes e.g 14 and above to be decided based on case to case basis
Slide97
Water Quality
l
Parameter
PH
Cooling Water
make up ( from
TTP of ETP)
Cooling Water
DM
Water
BFW
7.2-7.5
7.2-7.7
6.8-7.2/8.3-8.5
8.5-9.5
Turbidity, NTU
Total suspended solids,
Total dissolved solids,
Conductivity micro mho/cm
<2
< 10 mg/l
850-1050 mg/l
1200-1600 at 250C
<=30
<=30 mg/l
2500-3000 mg/l
<=5000 at 250C
Ca Hardness as CaCO3,
Total Hardness as CaCO3,
130-210 mg/l
250-360 mg/l
500-750 mg/l
850-1200 mg/l
20-25 mg/l
340-400 mg/l
100-125 mg/l
800-1000 mg/l
0.3-0.6 mg/l
<500 mg/l
3-4 mg/l
Nil
Nil mg/l
Nil ppm
<0.02 ppm
0.005 ppmv
0.01 mg/l
<=1.0 mg/l
Nil mg/l
0.01 max
120-150 mg/l
1.0-1.5 mg/l
20-25 mg/l
<10 mg/l
<30mg/l
Nil mg/l
Nil mg/l
Nil ppm
0.02 ppm
1(approx) ppm
Slide98
Water Qualitycontd
l
Parameter
PH
Turbidity, NTU
Total suspended solids,
Total dissolved solids,
Conductivity micromho/cm
Mo Alkalinity,
Ca Hardness as CaCO3,
Total Hardness as CaCO3,
Total cation/anion asCaCO3,
Total Silica as SiO2,
Colloidal Silica as SiO2, mg/l
Sodium as Na,
Potassium as K, mg/l
Chlorides as Cl,
Free chlorine,
Sulphates as SO4,
Poly phosphates as PO4,
Nitrates as NO3,
Total Iron as Fe,
Copper + Iron,
Mg , Hardness
Zinc as Zn,
Zinc Sulphate as Zn,
Boron, mg/l
Dissolved Fe, mg/ l
Oil content,
KmnO4 value at 100 oC,
Hydrazine (residual),
Morpholine (residual),
7 - 7.8
15
7-7.8
NA
NA mg/l
NA
240 (as CaCO3)mg/l
176 mg/l
350
493
2.9 (as CaCO3)mg/l
1.3 mg/l (as Ca)
608
40
NA
0.1
172 mg/l
142-220 mg/l
121 mg/l
12.5 mg/l
NA mg/l
0.3 mg/l
0.2 mg/l
NA
NA mg/l
4.5 mg/l
NA
1 mg/l
20 mg/l
NA
Slide99
Parameter
Sl
Parameter
1 Dew Point at atmospheric pressure
Plant Air
Instrument Air
water-free
(-)40oC
nil
nil
Inert Gas
Nitrogen
(-) 100oC
2
3
nil
99.99
3 (max)
1 (max)
nil
Slide100
Slide101
Fuel Systems
Burner turndown requirements have to be met at liquid fuel pressures at burner
not less than the normal anticipated return header pressure. The fuel oil system
shall be designed for a recirculation rate of 2:1.
Fuel gas liquid knockout drums and tracing for piping shall be separate for
each process unit.
In-line strainers in burner piping are recommended for each unit. These shall
be located not more than 20 meters upstream of the burner manifold and shall
be 1 on-line + 1 spare strainer with mesh sizes 100 for Fuel Oil, Fuel Gas and
atomising steam.
In-line strainers for FO, FG and atomising steam to be provided on common
header supplying to all heaters within each unit.
Hot liquid fuel temperature shall be assumed to drop by 5oC between unit
battery limits and burner manifold.
Slide102
Parameter
Case-1
Case-2
Case-3 (Note-C)
PG VR
BH
VR+VAC.DIESEL
UCO+VR
930 - 1030
4 (Note-1)
3700
978
0.84
1000 (max.)
18
5
12
<1
1.9
852-857
0.27
300
3
11
Name
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Crude stock
Density @ 15oC, kg/m3
Sulfur content, wt%
Nitrogen content, wppm
Nickel content, wppm
Vanadium content, wppm
Sodium content, wppm
Copper content, wppm
Iron content, wppm
Water content, wppm
Flash Point, oC
Pour Point, oC
Viscosity @ 50 oC, cst
Viscosity @ 100 oC, cst
Viscosity @ 200 oC , cst
Temperature, oC required for 20 cst
18
19
17 - 22
13.6
20
21
22
23
0.2
0.128
10000
-
0.12
0.124
10425
0.1
0.124
10000
200
80
traces*
66 (min)
66
7500
700
900 @ 90 oC
50 @ 120 oC
5.0 @ 80 oC
3.36
Slide103
H2O
Case A
Case B
Normal
Operation
Case C
Case D
Case E
Case F
Case G
Max FG
production
Refinery Start
up case
0.81
0.13
0.43
0.31
0.69
H2
35.35
80.1
0.0 0.86
45.49
34.48
74.96
25.63
C1
29.43
8.01
0.0
25.95
26.35
11.41
32.6
0.45
0.24
0.0
0.0
0.79
0.18
0.32
16.08
4.04
9.43
15.06
13.29
6.23
20.64
PROPYLENE
1.21
0.64
0.0
0.0
2.11
0.47
0.85
C3
7.96
2.59
44.08
6.06
8.53
3.09
9.44
IC4
1.99
0.93
9.09
1.48
3.06
0.76
2.23
1BUTENE
0.50
0.26
0.0
0.0
0.87
019
0.35
NC4
3.22
1.63
36.07
2.59
5.36
1.24
5.43
1C5
06
0.17
0.04
0.77
1.05
0.13
0.27
NC5
1.32
0.79
0.0
0.94
2.31
0.57
0.87
C6+
0.78
0.31
0.0
0.78
0.83
0.34
0.5
H2S
Note-1
Note-1
Note-1
Note-1
Note-1
Note-1
Note-1
NH3
0.00
0.00
0.00
0.00
0.01
0.00
N2
0.30
0.16
0.0
0.0
0.53
0.12
0.00
0.21
TOTAL
100.00
100.00
100.00
100.00
100.00
100.00
100.00
MW
20.004
8.2533
48.79
16.717
22.537
8.9845
22.66
KGM/HR
354.51
667.9
0.353
275.5
203
914.7
507.4
KG/HR
7091.5
5512
17.2
4605
4575
8218
11498
LHV, Cal/kg
11798
14544
10964
12184
11648
14120
11613
ETHYLENE
C2
1.29
Slide104
1
2
3
Flare system
Built- up back
pressure,
kg/cm2g
Normal flare
Acid Gas flare
High Pressure flare
0.2
0.2
Superimposed back
pressure at unit
battery limits,
kg/cm2g
default = 1.5
default = 0.5
Contingency
Low pressures
< 70 kg/cm2g
5%
(as per IBR)
20%
High pressures
> 70 kg/cm2g
5%
(as per IBR)
as per designer
1
2
Thermal relief
25%
as per designer
Operational failures
10%
as per designer
Slide106
Slide107
Slide108
Sl#
1.
2.
Stream
Operating condition
P,
kg/cm2g
6.0-16.0
4.0-6.0
Mechanical Design
T, oC
P, kg/cm2g
T, oC
40-103
70-80
27.0
27.0
141
100
Slide109
Energy integration
Improvement in overall energy efficiency shall call for unit-level and total plant-level
optimization of energy. Designer of a particular unit shall indicate the following at
the outset of design activities:
(a)The total energy consumption expressed as equivalent fuel oil (Btu/bbl or FOE
(b)The preferred temperatures for hot feeds and products from an energy
(c)integration standpoint, if these are significantly different from that stipulated in
unit BEDB.
(c)Energy shall be preferentially recovered into process streams. Steam generation
shall be considered thereafter to recover excess available energy. Steam
generation levels shall be chosen to preferably match the corresponding steam
level demand within unit.
(d) Low-level energy recoverable for external consumption, say, for Boiler Feed
Water preheat serving other units.
Slide110
Vacuum Design
Vacuum design conditions shall be stipulated for:
(a) Equipment operating normally under vacuum conditions
(b) Equipment that are subjected to vacuum conditions during start-up,
shutdown, regeneration or evacuation.
(c) Liquid full vessels that can be blocked in and cooled down
(d) Distillation columns and associated equipment that can be subjected to
vacuum conditions through loss of heat input.
(e) All steam users consuming steam during normal operation.
(f) Pressure vessels containing liquids having vapor pressure at minimum
ambient temperature less than atmospheric pressure.
Vacuum design conditions are not to be specified for the eventuality of blocking
in after equipment steam-out or operator maloperation.
Slide111
10%
10%
15%*
15% *
10%
10%
10%
10%
20%
Recycle compressors
Make-up compressors
10%
10% minimum
Pumps in general
Reflux and pumparound pumps
3-phase separators (in and out flowrate)
2-phase separators(in and out flowrate)
Crude preheat exchangers
10%
20%
10%
10%
15%
%turndown
20%
Slide112
=
=
Slide115
Slide116
FURNACE
TYPES OF FURNACE
Cylindrical furnace
Low plot space
Low cost
Higher heat flux
For clean services
Box furnace
High plot space
High cost
Even heat flux
For fouling services
Slide117
FURNACE
TYPES OF FURNACE
Natural Draft
Air for combustion enters due to pressure difference
Forced Draft
FD fan is used to supply air, usually air gets heated up in
convection zone.
Balanced Draft
FD fan is used to supply air and ID fan is used to suck the flue
gas and heat is exchanged between air and flue gas through an
external heat exchanger (APH)
Slide118
FURNACE
TYPES OF FURNACE
Single fired heater
Common pattern in heaters
For low fouling / sensitive fluid
Peak flux >80% of average flux
Double fired heater
For high fouling service
Low residence time
Fire on both side of coil
Uniform heat flux & peak flux < 20% of average flux
Slide119
Fired Heaters
Selection of fuel
Fired heaters shall be designed for continuous operation with:
100% firing on either fuel oil or fuel gas or any combination of both,
unless constrained to reject use of fuel oil from reasons of process or acid
gas dew point.
100% firing on fuel gas for heaters less than 1.5 MMKcal/hr.
Target efficiencies
Achievable fired heater efficiencies depend on service, furnace heat duty,
process temperatures and quality of fuel. Highest target efficiencies shall be
pursued by a unit designer, as found economically justified. Options such as
cast tube and glass tube air preheaters, steam generation and superheat, etc.,
shall be evaluated.
Target efficiency shall be:
92% on fuel gas fired heaters only
90% on combination firing heaters (with either fuel oil or fuel gas or dual fuel
mode)
Excess Air
Natural Draft
Forced Draft
Fuel Oil
25 %
20 %
Fuel Gas
20 %
15 %
Slide120
Fired Heaters
Heater stack
Stacks shall be individually mounted on each heater unless there are
considerations such as grade-mounted APH or combined APH system for a
group of heaters.
Minimum fired heater stack heights shall be the higher of indicated heights in
respective unit BEDB Part-A documents or as calculated from the formula
below:
H = 14 (Q)0.3
(Minimum stack height as per TNPCB / MoE&F to be provided, SOx
/ NOx nozzles to be provided)
where, H: stack height, metres
Q: total SO2 emission, kg/hr
Slide121
Convection Section
Furnace Burner
Slide122
FURNACE
OPERATION
Draft inside the furnace
Air ingression
Arch pressure slightly positive Stack damper
Combustion air control thro Air registrars
Excess air : 5-10% for gas and 10-15% for fuel oil
Monitored & controlled by Arch zone O2 analyser
Skin temperature
Stack temperature
Slide123
FURNACE
INTERLOCKS
SPECIAL OPERATION
Economiser
Steam spalling
APH interlocks
Temperature cycling
FD fan trip
ID fan trip
Coke burning
Convection water wash
Slide125
Slide126
Tube
Metallurgy
with Carbon
steel
Tube MOC
with Stainless
Steel
Slide127
Slide128
Slide129
TEMA type
> 0.0002
> 0.0002
Floating head
0.0002
> 0.0002
Floating Head
> 0.0002
0.0002
U tube bundle
0.0002
0.0002
Fixed tube
sheet/ U-tube
bundle
CS / Low Alloy
High alloy/SS/Brass
Tube Diameter
25 mm
25 mm
Tube Thickness
2.5 mm
2.0 mm
Tube Length
6.0 m
Slide130
Pitch
Pattern
Pitch
Angle
ShellSide
Fluid
Flow
Regime
Triangular
30
Clean
All
Rotated
Triangular
60
Clean
Rarelyused
Square
90
Fouling
Turbulent
Rotated
Square
45
Fouling
Laminar
Slide131
Slide132
Slide133
PUMPS
DESIGN
Selectionoftypeofpumps
Sparingofpumps
# Operating pumps
Spare pumps
Specificationofpumpseals
Specificationofdrives
Minimumflowbypass(MFB)provisions&controls
Slide134
yes
yes
yes
yes
yes
yes
no
no
no
no
no
no
Slide135
Slide136
IBR Requirements
Scope of IBR
Steam generators / steam users shall meet IBR regulations. Major IBR
requirements are summarized below:
a) Vessels: Any closed vessel exceeding 22.75 litres (five gallons) in
capacity which is used exclusively for generating steam under pressure and
include any mounting or other fittings attached to such vessels, which is
wholly or partly under pressure when steam is shut-off.
b) Piping: Any pipe through which steam passes and if:
i) Steam system mechanical design pressure exceeds 3.5 Kg/cm2 g OR
ii) Pipe size exceeds 254 mm internal diameter
c) The following are not in IBR scope:
i) Steam Tracing
ii) Heating coils
iii) Tubes of tanks
iv) Steam Jackets
d) All steam users (heat exchangers, vessels, condensate pots etc.) where
condensate is flashed to atmospheric pressure i.e. downstream is not
connected to IBR system are not under IBR and IBR specification break is done
at last isolation valve upstream of equipment.
e) All steam users where downstream piping is connected to IBR i.e.
condensate is flashed to generate IBR steam are covered under IBR
f)
Deaerator, BFW pumps are not under IBR and IBR starts from BFW
pump discharge.
Slide137
INSTRUMENTATION
InstrumentationPhilosophyforallequipments&pipelines
E.g.)PackedTowers
ForcolumndifferentialpressureindicationtwoseparatePTshallbeprovided
anddifferentialpressureshallbederivedinDCS.
Localdifferentialpressureindicationforeachbed:
Localdifferentialpressureindicationfortotalsection:
ControlRoomdifferentialpressureindicationforeachbed:
ControlRoomdifferentialpressureindicationforcriticalbeds:
ControlRoomdifferentialpressureindicationfortotalsection:
1+1Basketstrainersinlinesgoingtopackedbeds:
Singlebasketstrainersinlinesgoingtopackedbeds:
yes
yes
yes
yes
yes
yes
yes
no
no
no
no
no
no
no
Slide138
local
PI
DCS
PI
PAL/
PAH
local
TI
DCS
TI
TAL/
TAH
DCS
FI
FAL/
FAH
DCS
FQ
MP STEAM
LP STEAM
Condensate
CW supply
CW return
Instrument Air
PAL
Plant Air
Inert Gas
Fuel Gas
Fuel Oil
DM Water
Service Water
Flare
Slide139
0.75
1.5
10 12 14
0.5
Block
Bypass
0.5
0.5
0.75
Block
Bypass
0,75
0.75
0.75
0.75
Block
Bypass
1
1
1
1
1
1
1.5
Block
Bypass
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
Block
Bypass
2
2
2
2
2
2
2
2
Block
Bypass
2
2
2
2
3
3
3
3
Block
Bypass
3
3
3
3
4
3
4
4
Block
Bypass
4
4
6
4
6
6
Block
Bypass
6
6
6
6
8
6
8
8
10
Block
Bypass
8
8
8
8
10 10
8 10
12
Block
Bypass
14
Block
Bypass
12 14 14
10 12 14
16
Block
Bypass
14 16
12 14
16
Notes:
1.All sizes are nominal sizes in
inches.
2.Bypass pipe diameter shall
be same as bypass valve.
3.Bypass valve will be globe
valve upto 8" size and gate
valve above 8".
10 10 12 12
10 10 10 12
16
16
Slide140
Control Valve
Sample Datasheet
Slide141
Insulationthicknessforheatconservation,personnelprotection,electrically
tracedlines&coldinsulation
MaterialUsage
CellularGlassforprocesstemperaturesupto350C.
RockWoolforprocesstemperatureupto550C
CalciumSilicateforprocesstemperaturesfrom551 760C.
AdherencetostipulationsofOISDstandard#118formin.interequipment
spacingandinterdistancebetweenprocessunitandoffsites
Steamtracingforpipinghandlingcongealingservicesshallbe:
Steamtracingwithinunitbatterylimits,electrictracingforoffsitesupto
150C
Steamtracingwithinunitbatterylimits,electrictracingforoffsitesupto
250C
Steamtracingforbothbatterylimitsandforoffsites
LPSteamuptovacuumgasoils,MPSteamforheavyresidues
MPSteamforallcongealingservices
Slide142
Environmental Parameters
Slide143
Environ Impact
Assessment Study
144
Slide144
IsoplethsShowingMeasuredSPMConcentrations
Scale
-15000
15000
-10000
-5000
5000
10000
15000
15000
1000
2000 m
Pollutant: SPM
Unit: ug/m3
10000
10000
300
5000
5000
250
34
29
28
35
36
30
32
31
39
41
40
33
27
21
22
23
26
38
37
25
24
13
1
2
15
16
17
18
3
14
4
7
12
9
8
10
5
20
11
6
19
200
150
-5000
-5000
100
-10000
-15000
-15000
-10000
-10000
-5000
5000
10000
-15000
15000
50
Slide145
Parameter
Max
Avg
g/m3
SPM
18
287
70 234
RSPM
15
147
34 70
SO2
40
7 12
NOx
15
37
H2S
23
14
NH3
57
6 34
HC and VOC
10
14
Fugitive Emissions from the Work Zone Area of MRC Benzene < 1 ppm
(OSHA)
146
Slide146
Residential
Commercial
Industrial
Inside the
Plant Area
Noise levels
(dBA)
46 - 82
72 - 79
66 - 79
77 - 84
Standard
(dBA)
55
65
75
85
Water Environment
Surface Water
Ground Water
Bacteriological Quality
147
Slide147
37.5kW/m2
(315m)
12.5kW/m2
(591m)
4.0kW/m2
(1032m)
HeatRadiationEffectsduetoBLEVE(CDUVDU)
148
Slide148
Slide149
Slide150