Scribd Logo
Upload

Welcome to Scribd!

  • 7 views

    Lecture 4 Atmos Pressure Figure 3 - 21

    Uploaded by

    ZUL KAMARUDDIN
    Under normal pressure, the TGA curve for the dehydration of CaC2O4·H2O shows an apparent increase in mass at the beginning of the experiment due to collisions between water molecules and the sample holder during vacuum pumping. At higher pressures, the opposite effect is observed, with the TGA curve shifting to higher temperatures and having an increased reaction range. Using a lower heating rate lessens the initial mass increase effect.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PPT, PDF, TXT or read online from Scribd

    Lecture 4 Atmos Pressure Figure 3 - 21

    Uploaded by

    ZUL KAMARUDDIN
    7 views1 page
    Under normal pressure, the TGA curve for the dehydration of CaC2O4·H2O shows an apparent increase in mass at the beginning of the experiment due to collisions between water molecules and the sample holder during vacuum pumping. At higher pressures, the opposite effect is observed, with the TGA curve shifting to higher temperatures and having an increased reaction range. Using a lower heating rate lessens the initial mass increase effect.

    Original Description:

    sains note

    Original Title

    Lecture 4 Atmos Pressure Figure 3_21

    Copyright

    © Attribution Non-Commercial (BY-NC)

    Available Formats

    PPT, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Under normal pressure, the TGA curve for the dehydration of CaC2O4·H2O shows an apparent increase in mass at the beginning of the experiment due to collisions between water molecules and the sample holder during vacuum pumping. At higher pressures, the opposite effect is observed, with the TGA curve shifting to higher temperatures and having an increased reaction range. Using a lower heating rate lessens the initial mass increase effect.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    7 views1 page

    Lecture 4 Atmos Pressure Figure 3 - 21

    Uploaded by

    ZUL KAMARUDDIN
    Under normal pressure, the TGA curve for the dehydration of CaC2O4·H2O shows an apparent increase in mass at the beginning of the experiment due to collisions between water molecules and the sample holder during vacuum pumping. At higher pressures, the opposite effect is observed, with the TGA curve shifting to higher temperatures and having an increased reaction range. Using a lower heating rate lessens the initial mass increase effect.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as PPT, PDF, TXT or read online from Scribd
    Download as ppt, pdf, or txt
    of 1

    Figure 3.

    21  An apparent increase in the


    TGA curves for dehydration of sample mass at the
    CaC2O4·H2O under normal beginning of experiment
    pressure (dotted line, and under vacuum is due to
    vacuum (solid lines) collisions of water
    molecules with the sample
    holder during vacuum
    pumping process.
     At higher pressure, an
    opposite effect is observed to  This effect lessens if a lower
    the TGA curve.
    sample heating rate is used.

     Under high pressure, Ti is


    shifted towards higher
    temperature.

     Higher atmospheric pressure


    also causes an increase in the
    reaction range (Tf - Ti).

    Return to Lecture 4

    Lecture 4 S 7 Atmos Pressure figure 3.21 19-Nov-04

    You might also like