6

L Question Paper Code: 21425

B.E.lB.Tech. DEGREE EXAMINATION, MAY/JlJNE.2013.
Fifth Semester
Electronics and Instrumentation Engineering
EI 2302/EI 52/10133 EI 505 - ANALYTICAL INSTRUIvlENTS
(Common to Instrumentation and Control.Engineering)
(Regulation 2008/2010)
Time: Three hours l\1aximum': 100 marks
Answer ALL question.s.
PART A- (10 x 2 == 20 marks)
1. What is total internal reflection in spectrometry?
2. State law?
3. List the types of detectors used in gas chromatography.
4. What is HPLC?
5. Brief the principle of dust monitor.
S. What is thermal conductivity?
7. Define PH of a solution ..
8. List the demerits of glass electrode.
9, Brief the principle of scanning electron microscope.
10. \\That is mass spectrometer?
PART B - (5 x 16 == 80 marks)
11. (a) With a neat sketch, explain the instrumentation setup arid Ii ... "' .... I,.."""' ....
principle of IR spectrometer.
Or
(b) With a neat diagram, explain the instrumentation setup of Atomic
absorption spectrophotometer.
12. (a) With necessary diagrams, explain the working principle of HPLC. (High
pressure liquid chromatography)
Or
(b) With suitable diagrams, explain the various sampling t.echniques i,n Gas
Chromatography.
13. (a) With a neat sketch, explain the construction and working principle of
parametric oxygen analyzer.
Or
(b) (i) With suitable diagrams, explain the construction of smoke meter
and its working principle.
(ii) E x p l a ~ n the working principle of N02 analyzer.
14. (a) Viith neat diagram explain the working principle of dissolved oxygen
analyzer.
Or
(b) With neat diagram, explain the set up of sodium analyzer used in
industry.
15. (a) With a neat sketch, explain the NMR spectrometry and its
instrumentation set up_
Or
(b) vVith a neat sketch, explain the instrumentation set .up of Mass
spectronleter and its function.
2 21425
.., r= 4
l
.) ...
- ........,i ~
Reg. No. : [I I II I I I I I I ,
I Question Paper Code: C 1 2 6 ~ I
B.E.lB.Tech. DEGREE EXAMINATION, APRIUMAY 2010.
Sixth Semester
Electronics and Instrumentation Engineering
EI 1352 - ANALYTICAL INSTRUMENTS
(Common to Instrumentation and Control Engineering)
(Regulation 2004)
Time: 'I'hree hours Maximum: 100 marks
Answer ALL questions.
PART A - (10 x 2 = 20 nlarks)
1. State Beer-Lambert's law.
2. What is meant by attenuated total reflectance?
3. Why packing of column is done in column chromatography?
4. How is thin layer chromatography better than paper chromatography?
5. What are ion-exchangers?
6. List a few types of gas analyzers.
7. What is meant by redox potential?
8. Distinguish between glass electrode and reference electrode.
9. What is grating in spectroscopy?
10. Define mass spectroscopy_
PART B - (5 x 16 = 80 nlarks)
11. (a) Briefly, discuss the principle, working technique and application of
atomic absorption with suitable diagram.
Or
(b) With a neat instrumentation setup, describe the principle of (ill) Infra
Red, spectrophotometer and the various components involved in it.
12. (a) Explain the sample preparation, sample injection methods and
separation process in gas chromatography.
Or
(b) Explain any two types of detectors used in liquid chromatography.
13. (a) With a suitable diagram, describe the working principle of oxygen
analyzer.
Or
(b) With a neat sketch, explain the working of thermal conductivity meter ;
and using any method of calibration draw the calibration curve.
Also establish a suitable method for the compensation of the
conductivity cell.
14. (a) Explain the construction and working principle of hydrogen electrode to
measure pH. Use neat diagrams to explain.
Or
(b) With neat sketch, explain, the Ion Selective Electrode (ISE). Also explain
the general calibration procedure for any pH meter.
15. (a) Describe the working principle of Gamma camera and explain, how
signal processing is done. Also discuss about its spatial resolution.
Or
(b) Describe the working of double beam mass spectrometer and give its
application.
2 C 1268
26
Reg. No. : ll=r I I I I '-TO
: 103411
B.E.lB.Tech. DEGREE EXAMINATION, MAY/JUNE 2012.
Fifth Semester
Electronics and Instrumentation Engineering
EI 2302/EI 52 - ANALYTICAL INSTRUMENTS
(Common to Instrumentation and Control Engineering)
(Regulation 2008)
Time : Three hours Maximum: 100 marks
Answer ALL questions.
PART A - (10 x 2 = 20 marks)
1. State Beer-Lambert law.
2. What is the range covered by UV visible spectrophotometers?
3. Define partition ratio.
4. What is liquid solid chromatography?
5. What is the principle behind IR analyser?
6. What is the need for sulphur dioxide estilnation?
7. Define pH.
8. What is the purpose of biosensors?
9. What is broadband decoupling?
10. List the applications of Inass spectrometers.
7
PART B - (5 x 16::: 80 marks)
11. (a) (i) With neat diagram explain atomic absorption spectrophotometers
in detail.
(li) Explain fluorescence spectrophotometers in detail with necessary
diagrams.
Or
(b) (i) Explain single and double bearn instruments in detail.
(ii) Explain FTIR spectrophotometer in detail with necessary diagrams.
12. (a) > With neat diagram explain electron capture detector and flanle ionization
detector.
Or
(b) Explain partition chromatography in detail. Also list its application and
explain it.
13. (a) Explain the working principle of N02analyser In detail with neat
diagram.
Or
(b) (i) Explain dust and sInoke measurement in detail.
(ii) Explain thermal conductivity analyser in detail with neat diagram.
14. (a). Explain glass electrodes and ammonia electrodes in detail.
Or
(b) (i) Explain dissolved oxygen analyser in detail with neat diagrams.
(ii) Explain cyclic voltametry in detail.
15. (a) ~ x p l a i n quantum and classical description of NMR in detail.
Or
(b) (i) Explain scanning electron microscope in detail with neat diagrams.
(ii) Explain electron spin resonance spectroscopy in detail.
2 10341
Reg. No.: 1 I I. I. 1 .I II I I I 1
Question Paper Code: 55380
B.E.lB.Tech. DEGREE EXAMINATION, NOVEMBERIDECEMBER 2011.
Fifth Semester
Electronics and Instrumentation Engineering
EI 2302 - ANAL YTICAL INSTRUMENTS
(Common to Instrumentation and Control Engineering)
(Regulation 2008)
Time: Three hours Maximum: 100 marks
Answer ALL questions.
PART A - (10 x 2 = 20 marks)
1. Mention the application of Calorimeter.
2. State the Beer-Lambert Law.
3. Specify the solvents used for mobile phase in chromatography.
4. List the various detectors used in chromatography.
5. What is the need of measuring carbon monoxide in flue gas?
6. Mention the applications ofIR Gas analyzer.
7. What are the advantages of hydrogen electrode?
8. Specify the role of Buffer solution in pH measurement.
9. What is dead time in a GM Counter?
10. What is the basic principle ofNMR?
PART B - (5 x 16 = 80 marks)
11. (a) Explain in detail the construction and working principle of single focusing mass
spectrophotometer. (16)
Or
"C....,-.." / ~ . ~
(b) Explain the working principles of various radiation sources and detectors used in IR
Spectrophotometers. (16)
12. (a) Specify the role of chromatography in power plant. Also explain the method of Gas
(b)
Chromatography. (16)
Or
Give in detail the classifications of Chromatography.
chromatography.
Explain liquid
(16)
l3. (a) Explain the photometric method of measuring dust and smoke measurement in
thermal power plant. (16)
Or
(b) Why do we need temperature compensation in conductivity measurement? Describe
a method of temperature compensation. (16)
14. (a) List the types of electrodes used for pH measurement. Explain the construction
details of Digital pH meter. Also specify the need of reference electrode for pH
measurement. (16)
Or
(b) Describe a method of measuring dissolved oxygen content in the boiler feed water.
Why the dissolved oxygen content is monitored in feed water? Also specify the
cause of dissolved oxygen content in feed water. (16)
15. (a) Explain in detail about the atomic emission and absorption spectroscopy and where
they are using. (16)
Or
(b) In NMR spectroscopy, mention the advantages of using a magnet with as great a
field strength as possible. Also explain the difference between a continuous wave
and a Fourier transform NMR. (16)
2
55380
"
2011
Senlester
Ins trllil1en tati on
II 2302 ,- ANALYTICAL
to Instn:nllentati.on
Tinu: : Three h01U'S rvlaxinlUlll : 100 .......... u . .Il ... ",.,
Ansvver ALL
PAIr:r.A - 2 = 20
L State Beer- .< .. ,'-' ........ .>',_,.
2. are
5. Write nleteL
6. rvlention the uses IR analyzer.
I. are sensors?
8. Give Ineasurenlent,
9. Resonance
10. vVrite I\Iass
l
PA.RT B - x 16 = 80.'-<Uk"'U}
11, AtonJ.:ic
Or
in s tnnne:nt a U on
120 (a) the
(12)
purpose,
Or
EnUlllerate HPLCo
13, construction
Discuss the on ionization gaseso (6)
Or
(1)
anyone to
14, (a)
Or
are
Or
' ..-''-B_.'H.U.''''. the construction
Inass
11333